#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/41/2214188.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214188_Fobs loop_ _publ_author_name 'Watson, Amanda J.' 'Cope, Stephen K.' 'Jones, Daniel S.' 'Ogle, Craig A.' _publ_section_title ; cis-2,2-Dimethyl-1,3-diphenyl-2,3-dihydro-1H-benzo[c]silole ; _journal_coeditor_code FJ2035 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3346 _journal_volume 63 _journal_year 2007 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2n 2ac' _symmetry_space_group_name_H-M 'P c m n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.6298 _cell_length_b 14.6001 _cell_length_c 18.9843 _exptl_crystal_F_000 672.00 _reflns_d_resolution_high 0.8350 _[local]_cod_data_source_file fj20353sup2.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' = SHELXL INS file, from BOP_AW_Xtal2 least squares 2-67.5' _shelx_refln_list_code 4 _shelx_f_calc_maximum 157.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, z+1/2' 'x, -y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x, -y, -z' 'x-1/2, -y, -z-1/2' '-x, y-1/2, -z' 'x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2408.07 2660.58 11.47 o 4 0 0 817.37 1020.48 11.49 o 6 0 0 91.61 117.35 2.57 o 1 1 0 1948.83 2456.29 8.34 o 3 1 0 155.12 227.28 4.19 o 5 1 0 3.13 3.17 4.26 o 7 1 0 262.10 266.63 5.27 o 0 2 0 570.36 691.18 4.14 o 2 2 0 723.24 869.95 7.48 o 4 2 0 605.96 679.86 10.13 o 6 2 0 31.43 50.98 2.19 o 1 3 0 70.30 75.72 1.46 o 3 3 0 1167.29 1614.78 12.63 o 5 3 0 157.56 159.26 3.13 o 7 3 0 32.87 36.78 1.67 o 0 4 0 3388.67 4119.00 13.78 o 2 4 0 68.31 76.77 1.57 o 4 4 0 1630.12 2074.56 17.60 o 6 4 0 205.42 245.89 4.78 o 1 5 0 11.69 18.46 0.92 o 3 5 0 118.33 147.05 3.05 o 5 5 0 159.58 164.34 3.28 o 7 5 0 12.84 12.26 1.31 o 0 6 0 1559.59 1517.30 10.49 o 2 6 0 44.28 38.01 1.17 o 4 6 0 213.66 210.01 4.03 o 6 6 0 306.82 292.96 5.42 o 1 7 0 547.80 687.45 8.21 o 3 7 0 3.91 -2.48 3.51 o 5 7 0 214.04 203.69 4.28 o 7 7 0 0.15 0.96 2.48 o 0 8 0 127.00 83.91 1.67 o 2 8 0 1136.02 1127.76 12.09 o 4 8 0 91.71 86.17 2.02 o 6 8 0 205.20 183.18 3.53 o 1 9 0 32.60 45.47 1.48 o 3 9 0 20.85 24.47 1.50 o 5 9 0 32.57 28.04 1.61 o 0 10 0 743.76 790.42 10.91 o 2 10 0 45.47 45.11 1.63 o 4 10 0 20.78 21.28 1.57 o 6 10 0 13.64 15.95 1.11 o 1 11 0 74.14 69.63 1.86 o 3 11 0 343.87 290.74 6.04 o 5 11 0 32.89 42.11 1.54 o 0 12 0 342.90 351.69 7.11 o 2 12 0 774.93 765.53 12.41 o 4 12 0 6.24 8.14 1.32 o 1 13 0 54.85 54.52 1.84 o 3 13 0 1.38 0.00 3.40 o 5 13 0 2.70 1.13 2.23 o 0 14 0 99.10 104.89 2.11 o 2 14 0 0.47 1.94 1.19 o 4 14 0 40.81 40.23 1.29 o 1 15 0 0.86 0.31 2.99 o 3 15 0 5.54 6.06 0.98 o 0 16 0 17.93 21.05 1.23 o 2 16 0 28.16 27.93 1.19 o 1 17 0 1.91 -0.71 2.07 o 1 0 1 6092.79 5679.90 27.11 o 2 0 1 818.55 853.18 6.35 o 3 0 1 1593.86 1911.19 11.98 o 4 0 1 29.91 23.55 1.32 o 5 0 1 51.97 63.63 1.96 o 6 0 1 109.49 101.90 2.59 o 7 0 1 87.54 79.18 2.21 o 1 1 1 2001.06 2127.59 7.39 o 2 1 1 488.63 573.76 5.77 o 3 1 1 810.44 884.48 8.88 o 4 1 1 72.65 91.12 1.82 o 5 1 1 11.06 13.24 1.69 o 6 1 1 17.74 20.44 2.02 o 7 1 1 90.46 103.54 2.36 o 1 2 1 2316.05 2637.32 9.43 o 2 2 1 1393.67 1688.00 9.94 o 3 2 1 49.12 47.23 1.25 o 4 2 1 150.50 173.60 3.48 o 5 2 1 225.55 236.10 4.27 o 6 2 1 0.06 -2.92 4.86 o 7 2 1 96.21 120.65 2.40 o 1 3 1 4617.01 5118.03 15.05 o 2 3 1 43.19 48.59 1.11 o 3 3 1 612.61 761.65 8.88 o 4 3 1 80.54 87.53 1.86 o 5 3 1 185.36 205.95 4.11 o 6 3 1 0.04 -0.73 1.71 o 7 3 1 122.17 125.57 2.44 o 1 4 1 273.08 273.11 4.41 o 2 4 1 309.68 386.75 5.64 o 3 4 1 482.18 544.10 7.97 o 4 4 1 127.15 138.46 2.90 o 5 4 1 60.87 65.15 2.00 o 6 4 1 44.70 50.62 2.00 o 7 4 1 109.01 106.57 2.25 o 1 5 1 1035.38 1160.92 8.83 o 2 5 1 266.20 320.90 5.60 o 3 5 1 62.22 52.97 1.42 o 4 5 1 2.91 -2.36 3.97 o 5 5 1 23.94 25.26 1.80 o 6 5 1 54.90 62.10 2.03 o 7 5 1 124.72 122.00 2.40 o 1 6 1 459.90 470.71 6.37 o 2 6 1 269.05 323.42 6.04 o 3 6 1 101.96 87.52 1.92 o 4 6 1 69.74 71.18 1.80 o 5 6 1 30.87 31.96 1.82 o 6 6 1 23.79 22.00 1.69 o 7 6 1 80.17 73.11 1.69 o 1 7 1 9.54 12.63 1.02 o 2 7 1 112.93 121.45 2.57 o 3 7 1 326.20 365.26 6.19 o 4 7 1 50.02 59.28 1.80 o 5 7 1 76.38 78.67 2.15 o 6 7 1 5.61 5.01 1.46 o 7 7 1 70.77 68.62 1.50 o 1 8 1 430.87 425.33 7.22 o 2 8 1 0.34 1.07 3.36 o 3 8 1 285.77 308.21 6.15 o 4 8 1 99.85 99.30 2.07 o 5 8 1 132.75 135.77 2.61 o 6 8 1 2.45 2.15 3.40 o 7 8 1 16.63 15.22 0.96 o 1 9 1 735.71 761.01 10.14 o 2 9 1 2.46 -0.40 3.59 o 3 9 1 92.42 98.94 2.05 o 4 9 1 17.16 11.76 1.63 o 5 9 1 52.48 47.85 1.80 o 6 9 1 0.03 0.81 1.07 o 1 10 1 69.40 55.39 1.61 o 2 10 1 6.17 -2.59 3.78 o 3 10 1 102.97 109.71 2.15 o 4 10 1 21.61 21.88 1.63 o 5 10 1 0.66 0.33 3.17 o 6 10 1 7.08 7.08 1.04 o 1 11 1 346.76 335.79 6.77 o 2 11 1 58.04 68.28 1.88 o 3 11 1 66.88 58.97 1.94 o 4 11 1 6.27 9.83 1.40 o 5 11 1 0.93 -3.20 3.20 o 6 11 1 2.62 3.20 0.84 o 1 12 1 311.24 314.38 5.96 o 2 12 1 9.43 11.19 1.67 o 3 12 1 53.69 42.08 1.75 o 4 12 1 35.41 37.14 1.57 o 5 12 1 20.87 18.02 1.15 o 1 13 1 15.71 16.47 1.54 o 2 13 1 4.56 4.89 3.63 o 3 13 1 14.01 13.95 1.38 o 4 13 1 8.07 5.10 1.17 o 5 13 1 17.90 15.41 0.98 o 1 14 1 0.26 2.03 3.28 o 2 14 1 1.03 2.76 3.03 o 3 14 1 13.35 10.88 1.19 o 4 14 1 0.01 -2.34 2.34 o 1 15 1 31.33 31.84 1.48 o 2 15 1 3.81 6.35 1.09 o 3 15 1 25.41 26.28 1.17 o 4 15 1 2.77 2.61 2.13 o 1 16 1 13.38 10.82 1.07 o 2 16 1 0.68 2.03 2.42 o 3 16 1 3.57 3.76 0.79 o 1 17 1 14.79 13.70 0.92 o 0 0 2 3535.00 3429.71 16.86 o 1 0 2 13434.95 14129.77 47.59 o 2 0 2 2607.77 2644.55 10.97 o 3 0 2 0.75 2.46 2.42 o 4 0 2 1.57 1.19 2.97 o 5 0 2 1.28 0.15 4.11 o 6 0 2 352.87 348.02 6.65 o 7 0 2 115.82 125.60 2.38 o 0 1 2 8688.97 8144.12 29.85 o 1 1 2 3134.29 2846.24 8.82 o 2 1 2 29.04 23.36 0.86 o 3 1 2 167.63 182.57 3.63 o 4 1 2 667.43 658.87 9.34 o 5 1 2 96.26 102.66 2.19 o 6 1 2 32.21 39.88 2.07 o 7 1 2 59.47 61.41 1.94 o 0 2 2 4034.85 3809.73 23.52 o 1 2 2 2671.18 2810.65 9.75 o 2 2 2 316.99 331.14 4.70 o 3 2 2 549.74 640.75 7.74 o 4 2 2 172.99 212.07 4.34 o 5 2 2 3.59 4.32 4.32 o 6 2 2 162.79 176.18 3.28 o 7 2 2 4.94 3.67 4.03 o 0 3 2 8143.58 7854.05 40.93 o 1 3 2 887.07 853.25 6.30 o 2 3 2 643.54 659.02 6.73 o 3 3 2 1128.26 1347.98 11.45 o 4 3 2 1311.03 1399.68 14.25 o 5 3 2 58.22 47.28 1.98 o 6 3 2 278.39 289.92 5.76 o 7 3 2 0.29 2.71 3.61 o 0 4 2 1246.02 1226.05 7.78 o 1 4 2 229.59 231.77 4.19 o 2 4 2 7.86 14.93 0.94 o 3 4 2 637.90 797.25 9.56 o 4 4 2 66.36 86.31 1.90 o 5 4 2 96.79 90.93 2.15 o 6 4 2 0.01 1.38 3.93 o 7 4 2 29.60 29.46 1.55 o 0 5 2 3073.80 3014.40 13.65 o 1 5 2 141.59 161.63 3.29 o 2 5 2 2.14 5.47 0.94 o 3 5 2 543.12 612.01 8.72 o 4 5 2 295.32 294.58 6.17 o 5 5 2 0.65 2.80 4.28 o 6 5 2 148.33 158.51 3.07 o 7 5 2 13.58 11.88 1.27 o 0 6 2 3911.52 4334.62 17.97 o 1 6 2 54.37 61.93 1.27 o 2 6 2 127.91 165.68 3.34 o 3 6 2 24.54 33.57 1.40 o 4 6 2 0.11 1.90 4.05 o 5 6 2 104.40 108.48 2.32 o 6 6 2 11.53 12.69 1.52 o 7 6 2 11.79 9.62 1.25 o 0 7 2 6.77 12.80 1.04 o 1 7 2 145.69 201.43 4.13 o 2 7 2 300.46 358.66 6.77 o 3 7 2 3.22 5.20 3.68 o 4 7 2 235.02 232.71 4.67 o 5 7 2 0.46 -4.13 4.13 o 6 7 2 201.89 209.08 4.07 o 7 7 2 10.55 7.83 1.04 o 0 8 2 205.29 247.43 4.71 o 1 8 2 680.71 763.74 9.50 o 2 8 2 0.67 -2.67 3.30 o 3 8 2 2.17 -3.09 3.61 o 4 8 2 0.86 0.88 3.80 o 5 8 2 98.50 93.46 2.21 o 6 8 2 0.71 -0.77 3.34 o 7 8 2 1.78 0.77 2.13 o 0 9 2 1220.51 1121.40 12.02 o 1 9 2 43.77 38.01 1.42 o 2 9 2 527.88 503.48 9.05 o 3 9 2 53.55 50.04 1.71 o 4 9 2 259.55 277.94 5.26 o 5 9 2 0.10 -3.68 3.68 o 6 9 2 43.15 37.12 1.38 o 0 10 2 57.84 63.29 1.63 o 1 10 2 101.70 102.59 1.94 o 2 10 2 106.63 95.10 1.90 o 3 10 2 34.31 37.79 1.75 o 4 10 2 81.07 79.08 2.09 o 5 10 2 1.30 2.61 1.25 o 6 10 2 0.65 -2.46 2.61 o 0 11 2 1009.57 988.03 13.06 o 1 11 2 14.26 15.93 1.44 o 2 11 2 313.58 276.95 5.67 o 3 11 2 37.27 22.27 1.65 o 4 11 2 6.74 8.02 1.36 o 5 11 2 3.98 3.67 1.13 o 6 11 2 22.82 23.30 1.04 o 0 12 2 5.88 7.18 1.48 o 1 12 2 100.51 91.93 2.21 o 2 12 2 0.90 2.99 3.91 o 3 12 2 12.20 10.69 1.52 o 4 12 2 1.49 0.33 3.32 o 5 12 2 35.86 30.10 1.25 o 0 13 2 0.20 3.51 3.51 o 1 13 2 3.57 0.35 3.76 o 2 13 2 42.56 44.32 1.69 o 3 13 2 2.74 -2.63 3.44 o 4 13 2 53.69 53.75 1.54 o 5 13 2 0.02 3.13 2.11 o 0 14 2 122.95 96.15 2.05 o 1 14 2 15.85 16.60 1.44 o 2 14 2 0.99 0.48 3.26 o 3 14 2 7.40 7.43 1.17 o 4 14 2 0.04 -0.98 2.34 o 0 15 2 83.93 79.21 1.82 o 1 15 2 0.54 0.90 2.96 o 2 15 2 31.58 32.76 1.34 o 3 15 2 2.16 -2.71 2.71 o 4 15 2 27.08 26.41 0.96 o 0 16 2 0.29 -1.25 2.59 o 1 16 2 4.31 3.44 1.02 o 2 16 2 2.65 1.69 2.34 o 3 16 2 0.04 -0.73 1.90 o 0 17 2 19.84 20.19 1.02 o 1 17 2 2.16 1.80 1.96 o 1 0 3 24671.12 25162.58 72.43 o 2 0 3 188.51 173.64 3.46 o 3 0 3 2086.06 2046.14 12.52 o 4 0 3 0.06 -1.09 3.11 o 5 0 3 9.91 6.12 4.15 o 6 0 3 37.04 36.81 1.94 o 7 0 3 89.51 65.70 1.88 o 1 1 3 3350.12 3201.07 10.07 o 2 1 3 130.11 143.84 2.75 o 3 1 3 789.66 740.73 7.93 o 4 1 3 123.12 127.27 2.44 o 5 1 3 14.16 12.86 1.57 o 6 1 3 58.05 56.76 2.07 o 7 1 3 0.10 1.27 3.67 o 1 2 3 1745.95 1701.00 8.00 o 2 2 3 128.87 133.95 2.46 o 3 2 3 253.72 230.21 4.09 o 4 2 3 1.54 1.21 3.28 o 5 2 3 152.11 149.05 3.11 o 6 2 3 16.64 15.55 1.78 o 7 2 3 70.93 84.28 2.00 o 1 3 3 200.63 206.76 3.62 o 2 3 3 8.54 8.96 0.84 o 3 3 3 1050.48 1177.07 10.70 o 4 3 3 552.05 598.04 9.66 o 5 3 3 326.32 348.47 7.50 o 6 3 3 5.16 4.57 1.69 o 7 3 3 16.41 19.46 1.52 o 1 4 3 1.92 1.44 2.25 o 2 4 3 713.63 835.08 8.14 o 3 4 3 1532.42 1703.73 13.62 o 4 4 3 265.30 278.82 5.17 o 5 4 3 118.13 137.93 2.75 o 6 4 3 15.69 14.49 1.71 o 7 4 3 86.71 90.07 1.92 o 1 5 3 41.01 63.10 1.21 o 2 5 3 58.54 68.44 1.38 o 3 5 3 179.88 163.83 3.32 o 4 5 3 75.91 74.53 1.86 o 5 5 3 39.86 52.00 2.02 o 6 5 3 3.25 3.42 4.09 o 7 5 3 49.34 46.15 1.52 o 1 6 3 1396.58 1331.76 10.72 o 2 6 3 4.29 4.64 1.02 o 3 6 3 319.37 284.98 5.59 o 4 6 3 10.59 12.67 1.52 o 5 6 3 104.83 110.15 2.42 o 6 6 3 2.39 -0.71 3.95 o 7 6 3 88.49 80.66 1.67 o 1 7 3 23.52 29.81 1.15 o 2 7 3 132.05 179.98 3.76 o 3 7 3 119.89 112.09 2.25 o 4 7 3 32.45 30.69 1.61 o 5 7 3 141.21 139.48 2.82 o 6 7 3 1.04 -2.17 3.65 o 7 7 3 21.68 21.38 1.13 o 1 8 3 406.61 362.62 7.00 o 2 8 3 300.23 371.83 6.15 o 3 8 3 94.35 82.94 1.86 o 4 8 3 63.27 60.64 1.98 o 5 8 3 97.97 93.35 2.15 o 6 8 3 1.51 -1.34 3.22 o 1 9 3 146.87 130.10 2.48 o 2 9 3 56.15 59.95 1.63 o 3 9 3 252.92 260.69 5.26 o 4 9 3 50.51 57.28 2.03 o 5 9 3 25.54 24.30 1.57 o 6 9 3 4.87 4.30 2.90 o 1 10 3 24.99 27.54 1.46 o 2 10 3 84.83 73.99 1.84 o 3 10 3 142.47 142.51 2.86 o 4 10 3 60.04 61.08 1.92 o 5 10 3 1.59 -0.33 3.57 o 6 10 3 1.10 -0.21 2.38 o 1 11 3 226.11 218.29 4.51 o 2 11 3 24.63 20.34 1.57 o 3 11 3 53.37 56.67 1.92 o 4 11 3 0.91 2.94 3.97 o 5 11 3 0.80 -3.05 3.05 o 6 11 3 7.77 8.60 0.90 o 1 12 3 248.30 258.62 4.98 o 2 12 3 0.80 0.88 4.15 o 3 12 3 46.06 55.76 1.80 o 4 12 3 1.38 3.93 3.26 o 5 12 3 43.33 41.17 1.32 o 1 13 3 0.82 2.65 3.80 o 2 13 3 3.19 4.66 1.36 o 3 13 3 17.54 16.97 1.34 o 4 13 3 9.58 11.57 1.17 o 5 13 3 14.27 14.64 0.92 o 1 14 3 32.67 31.40 1.63 o 2 14 3 9.88 9.63 1.32 o 3 14 3 32.20 34.22 1.42 o 4 14 3 0.48 -1.06 2.36 o 1 15 3 6.76 4.87 3.30 o 2 15 3 2.60 -1.61 2.80 o 3 15 3 18.84 20.65 1.13 o 1 16 3 22.71 28.92 1.23 o 2 16 3 2.57 3.28 0.90 o 3 16 3 6.46 6.10 0.81 o 1 17 3 0.61 2.82 1.96 o 0 0 4 12312.89 12313.34 47.02 o 1 0 4 325.61 270.14 3.55 o 2 0 4 1790.61 1812.93 9.86 o 3 0 4 256.79 302.67 5.40 o 4 0 4 986.18 949.29 10.90 o 5 0 4 375.58 307.63 6.54 o 6 0 4 327.42 308.42 6.07 o 7 0 4 5.50 2.34 3.63 o 0 1 4 957.02 925.95 5.37 o 1 1 4 1415.34 1441.48 7.42 o 2 1 4 277.13 248.01 4.17 o 3 1 4 127.77 158.58 3.05 o 4 1 4 13.15 0.12 3.38 o 5 1 4 7.39 -2.86 4.24 o 6 1 4 153.24 159.77 3.13 o 7 1 4 6.37 4.28 1.40 o 0 2 4 10458.31 10326.26 47.23 o 1 2 4 7005.90 6547.71 40.45 o 2 2 4 204.16 202.16 4.00 o 3 2 4 189.19 227.89 4.13 o 4 2 4 469.39 384.39 6.25 o 5 2 4 493.82 490.26 8.18 o 6 2 4 393.02 405.52 8.08 o 7 2 4 0.27 -3.30 3.76 o 0 3 4 10224.69 9785.81 50.60 o 1 3 4 3409.75 3312.60 12.85 o 2 3 4 389.62 416.27 5.64 o 3 3 4 0.85 -2.76 2.84 o 4 3 4 44.37 44.65 1.61 o 5 3 4 78.55 74.93 2.05 o 6 3 4 17.73 16.52 1.71 o 7 3 4 0.15 0.00 3.19 o 0 4 4 2362.67 2111.43 10.69 o 1 4 4 84.81 62.03 1.27 o 2 4 4 726.20 710.69 7.68 o 3 4 4 149.43 159.29 3.13 o 4 4 4 535.60 497.58 9.39 o 5 4 4 2.14 0.73 4.55 o 6 4 4 109.34 112.56 2.40 o 7 4 4 0.98 0.42 3.09 o 0 5 4 1095.11 1051.60 8.52 o 1 5 4 228.66 247.42 4.71 o 2 5 4 273.89 281.82 5.61 o 3 5 4 60.32 70.49 1.55 o 4 5 4 15.26 15.16 1.50 o 5 5 4 7.11 10.00 1.69 o 6 5 4 3.96 1.13 4.03 o 7 5 4 45.27 44.40 1.54 o 0 6 4 3482.02 3550.13 17.13 o 1 6 4 143.33 120.16 2.42 o 2 6 4 624.13 612.69 8.42 o 3 6 4 10.38 12.44 1.32 o 4 6 4 263.50 242.72 4.80 o 5 6 4 0.02 -0.13 1.54 o 6 6 4 49.22 51.23 1.77 o 7 6 4 5.18 1.69 2.92 o 0 7 4 363.14 518.48 7.46 o 1 7 4 366.80 357.99 6.75 o 2 7 4 2.44 3.38 3.11 o 3 7 4 2.79 3.70 3.74 o 4 7 4 20.03 17.52 1.55 o 5 7 4 14.25 18.02 1.65 o 6 7 4 0.86 0.65 3.15 o 7 7 4 10.47 9.40 1.00 o 0 8 4 331.83 294.78 5.25 o 1 8 4 73.58 71.92 1.54 o 2 8 4 445.23 416.17 8.16 o 3 8 4 79.94 78.98 1.90 o 4 8 4 543.76 564.82 11.08 o 5 8 4 0.70 3.88 3.90 o 6 8 4 49.17 46.86 1.57 o 0 9 4 168.21 190.13 3.82 o 1 9 4 4.44 7.16 1.23 o 2 9 4 27.82 26.58 1.44 o 3 9 4 149.26 160.42 3.28 o 4 9 4 57.51 61.33 2.02 o 5 9 4 2.78 3.99 3.63 o 6 9 4 1.18 2.90 2.82 o 0 10 4 288.85 268.81 5.04 o 1 10 4 16.26 9.54 1.38 o 2 10 4 1.42 -1.46 4.05 o 3 10 4 257.69 259.40 5.02 o 4 10 4 182.14 183.61 3.76 o 5 10 4 0.27 -3.32 3.32 o 6 10 4 8.69 10.69 1.02 o 0 11 4 37.81 43.01 1.65 o 1 11 4 16.38 20.25 1.57 o 2 11 4 25.19 19.37 1.67 o 3 11 4 1.64 -4.05 4.05 o 4 11 4 14.39 12.69 1.46 o 5 11 4 0.56 0.54 2.76 o 6 11 4 10.54 8.83 0.84 o 0 12 4 255.74 235.02 4.71 o 1 12 4 22.54 23.09 1.65 o 2 12 4 257.84 250.21 4.52 o 3 12 4 0.00 1.23 3.40 o 4 12 4 99.25 88.61 1.88 o 5 12 4 4.22 3.36 2.59 o 0 13 4 9.92 6.24 1.48 o 1 13 4 36.61 33.15 1.63 o 2 13 4 0.06 0.17 3.32 o 3 13 4 20.78 12.99 1.36 o 4 13 4 8.52 4.55 3.03 o 5 13 4 0.05 -0.92 2.05 o 0 14 4 22.92 15.60 1.48 o 1 14 4 60.20 55.78 1.79 o 2 14 4 1.76 3.61 3.24 o 3 14 4 0.00 0.40 2.84 o 4 14 4 56.53 56.29 1.34 o 0 15 4 18.79 18.60 1.36 o 1 15 4 0.50 -2.17 3.13 o 2 15 4 6.64 7.83 1.11 o 3 15 4 6.63 6.49 1.04 o 0 16 4 24.30 21.19 1.17 o 1 16 4 2.78 3.28 0.94 o 2 16 4 24.88 21.40 1.11 o 0 17 4 14.11 14.24 0.88 o 1 17 4 1.14 -0.56 2.02 o 1 0 5 17043.81 17514.73 68.91 o 2 0 5 52.57 38.21 0.94 o 3 0 5 773.50 738.09 8.22 o 4 0 5 22.02 25.03 1.32 o 5 0 5 28.79 25.03 1.65 o 6 0 5 0.14 2.65 3.91 o 7 0 5 19.75 20.46 1.44 o 1 1 5 1937.57 1972.79 9.36 o 2 1 5 840.82 908.17 7.59 o 3 1 5 751.15 741.54 8.31 o 4 1 5 96.82 95.60 1.88 o 5 1 5 254.66 243.67 5.40 o 6 1 5 9.77 9.52 1.65 o 7 1 5 189.69 188.47 3.71 o 1 2 5 369.23 360.29 4.55 o 2 2 5 13.90 18.79 0.90 o 3 2 5 201.78 202.90 3.96 o 4 2 5 114.60 97.18 1.84 o 5 2 5 61.79 66.82 1.98 o 6 2 5 25.47 22.03 1.73 o 7 2 5 0.35 -3.36 3.36 o 1 3 5 1977.38 1775.09 9.98 o 2 3 5 2069.31 2102.70 12.39 o 3 3 5 938.55 841.14 9.44 o 4 3 5 166.06 172.70 3.23 o 5 3 5 303.21 293.88 5.98 o 6 3 5 8.87 4.47 4.05 o 7 3 5 93.93 87.80 1.84 o 1 4 5 210.18 223.76 4.29 o 2 4 5 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6 7 7 2.60 5.83 1.19 o 1 8 7 125.48 128.13 2.34 o 2 8 7 147.58 153.70 3.11 o 3 8 7 214.24 222.48 4.73 o 4 8 7 24.55 28.23 1.80 o 5 8 7 108.20 121.60 2.53 o 6 8 7 3.65 2.90 2.88 o 1 9 7 7.27 1.71 3.70 o 2 9 7 64.45 62.49 1.86 o 3 9 7 88.28 80.58 2.13 o 4 9 7 44.88 50.52 1.96 o 5 9 7 3.03 3.86 3.45 o 6 9 7 1.32 -1.27 2.36 o 1 10 7 3.42 3.38 4.05 o 2 10 7 130.85 144.98 2.77 o 3 10 7 200.72 207.92 4.30 o 4 10 7 9.84 13.99 1.50 o 5 10 7 64.96 61.95 1.63 o 6 10 7 0.06 -0.65 2.03 o 1 11 7 47.33 37.85 1.75 o 2 11 7 73.06 66.19 2.00 o 3 11 7 2.13 0.54 3.72 o 4 11 7 31.16 25.57 1.52 o 5 11 7 1.23 2.09 1.00 o 1 12 7 39.15 36.83 1.75 o 2 12 7 8.24 6.79 1.44 o 3 12 7 81.32 88.01 1.98 o 4 12 7 0.47 -1.23 2.97 o 5 12 7 64.17 58.50 1.29 o 1 13 7 0.46 2.88 1.32 o 2 13 7 5.73 4.11 3.59 o 3 13 7 1.46 0.58 3.11 o 4 13 7 7.77 9.44 1.04 o 1 14 7 47.52 46.30 1.61 o 2 14 7 5.99 6.01 1.19 o 3 14 7 38.39 41.25 1.31 o 4 14 7 0.50 -1.77 2.05 o 1 15 7 12.94 13.30 1.13 o 2 15 7 0.15 -2.21 2.69 o 3 15 7 2.32 2.30 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157.65 152.57 3.19 o 1 10 8 129.62 125.28 2.75 o 2 10 8 26.68 24.18 1.67 o 3 10 8 55.89 47.03 1.88 o 4 10 8 17.10 14.95 1.48 o 5 10 8 20.99 18.06 1.27 o 0 11 8 11.58 7.81 1.57 o 1 11 8 1.20 0.73 3.78 o 2 11 8 35.27 36.32 1.69 o 3 11 8 6.52 10.25 1.48 o 4 11 8 19.62 16.83 1.38 o 5 11 8 2.08 -0.65 2.67 o 0 12 8 156.79 139.80 2.61 o 1 12 8 86.45 80.25 2.05 o 2 12 8 59.54 64.23 1.86 o 3 12 8 4.37 3.68 3.40 o 4 12 8 56.49 58.66 1.54 o 5 12 8 4.70 2.21 2.05 o 0 13 8 0.30 4.45 3.20 o 1 13 8 4.38 6.54 1.32 o 2 13 8 33.05 28.48 1.46 o 3 13 8 1.90 2.78 1.07 o 4 13 8 5.67 0.90 2.51 o 0 14 8 0.12 1.36 3.01 o 1 14 8 4.33 3.95 1.21 o 2 14 8 27.20 32.03 1.34 o 3 14 8 0.00 -0.54 2.36 o 0 15 8 20.51 20.75 1.19 o 1 15 8 6.44 7.71 1.06 o 2 15 8 4.22 2.65 0.98 o 0 16 8 48.04 54.88 1.27 o 1 16 8 7.25 4.87 0.86 o 1 0 9 288.01 262.89 5.06 o 2 0 9 1180.98 1308.01 11.33 o 3 0 9 10.12 14.18 1.29 o 4 0 9 339.13 368.77 6.84 o 5 0 9 77.27 76.85 2.07 o 6 0 9 50.13 44.80 1.73 o 7 0 9 11.55 10.00 1.13 o 1 1 9 592.01 507.34 6.67 o 2 1 9 9.33 9.19 1.00 o 3 1 9 713.98 663.34 9.40 o 4 1 9 22.20 17.75 1.55 o 5 1 9 169.07 168.09 3.40 o 6 1 9 26.13 24.32 1.54 o 7 1 9 88.93 82.72 1.59 o 1 2 9 271.47 279.48 5.33 o 2 2 9 116.60 105.59 2.07 o 3 2 9 10.63 9.27 1.27 o 4 2 9 253.92 245.13 5.09 o 5 2 9 56.15 66.26 2.00 o 6 2 9 38.69 37.62 1.65 o 7 2 9 11.54 10.98 1.09 o 1 3 9 2795.72 2674.52 15.66 o 2 3 9 129.76 123.20 2.44 o 3 3 9 628.60 621.51 9.59 o 4 3 9 13.09 10.77 1.48 o 5 3 9 110.74 101.07 2.21 o 6 3 9 13.06 17.60 1.48 o 7 3 9 34.24 34.67 1.25 o 1 4 9 1531.25 1495.51 12.40 o 2 4 9 250.73 237.94 4.96 o 3 4 9 9.33 9.06 1.31 o 4 4 9 2.46 0.17 4.09 o 5 4 9 2.46 0.00 4.03 o 6 4 9 2.35 0.00 3.47 o 7 4 9 0.51 -0.10 2.38 o 1 5 9 440.36 408.01 7.23 o 2 5 9 453.28 492.65 8.54 o 3 5 9 626.84 554.38 9.90 o 4 5 9 110.97 87.60 2.19 o 5 5 9 10.05 11.30 1.57 o 6 5 9 39.78 34.51 1.54 o 1 6 9 197.04 173.39 3.55 o 2 6 9 34.97 35.51 1.57 o 3 6 9 13.72 12.74 1.52 o 4 6 9 0.07 5.72 3.91 o 5 6 9 28.91 25.89 1.65 o 6 6 9 0.73 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21 0.02 -0.98 2.59 o 1 3 21 89.12 90.97 1.80 o 2 3 21 1.57 2.21 0.98 o 1 4 21 32.85 35.24 1.36 o 2 4 21 6.94 6.47 1.00 o 1 5 21 4.65 5.64 1.06 o 2 5 21 2.38 1.17 0.90 o 1 6 21 19.66 15.78 1.07 o 0 0 22 67.84 73.28 1.56 o 1 0 22 24.55 22.80 1.15 o 2 0 22 15.85 18.27 1.06 o 0 1 22 0.40 0.63 2.61 o 1 1 22 4.23 4.64 1.00 o 0 2 22 34.67 37.39 1.31 o 1 2 22 30.33 37.31 1.27 o 0 3 22 20.29 15.62 1.09 o 1 3 22 8.43 7.81 1.04 o 0 4 22 12.67 15.07 1.02 o