#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/41/2214194.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214194_Fobs loop_ _publ_author_name 'How, Fiona N.-F.' 'Watkin, David J.' 'Crouse, Karen A.' 'Tahir, M. Ibrahim M.' _publ_section_title ; S-Quinolin-2-ylmethyldithiocarbazate ; _journal_coeditor_code FL2133 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3137 _journal_page_last o3138 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _audit_creation_date 07-05-01 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 113.2607(11) _cell_angle_gamma 90 _cell_length_a 11.0514(2) _cell_length_b 10.0620(2) _cell_length_c 11.2780(2) _[local]_cod_data_source_file fl2133Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 3 0 0 2034.20 2524.55 71.70 o 4 0 0 989.00 1125.08 32.50 o 5 0 0 567.40 589.97 16.10 o 6 0 0 1299.50 1284.21 38.90 o 7 0 0 69.10 64.99 2.30 o 8 0 0 754.60 756.85 20.30 o 9 0 0 1168.50 1096.86 31.90 o 10 0 0 95.80 77.81 4.60 o 11 0 0 10.10 6.63 2.30 o 12 0 0 15.10 15.48 4.10 o 13 0 0 146.00 166.62 14.60 o 3 1 0 5910.35 6137.19 245.74 o 4 1 0 162.25 122.90 5.06 o 5 1 0 570.90 578.04 15.56 o 6 1 0 99.40 81.37 3.32 o 7 1 0 1297.75 1318.25 39.21 o 8 1 0 109.10 114.71 5.57 o 9 1 0 785.75 728.48 25.06 o 10 1 0 318.20 312.88 13.07 o 11 1 0 76.95 73.47 5.45 o 12 1 0 12.85 13.37 2.63 o 13 1 0 14.40 15.63 5.63 o 2 2 0 2022.60 2093.79 73.91 o 3 2 0 532.70 562.40 15.06 o 4 2 0 1813.20 1850.07 61.37 o 5 2 0 1517.15 1271.34 43.56 o 6 2 0 0.25 1.08 0.91 o 7 2 0 61.95 61.75 2.60 o 8 2 0 628.75 594.90 21.80 o 9 2 0 20.30 24.83 2.01 o 10 2 0 -0.45 0.03 1.55 o 11 2 0 122.50 119.76 8.06 o 12 2 0 125.65 141.68 11.85 o 13 2 0 129.55 139.43 14.40 o 1 3 0 794.55 813.00 23.17 o 2 3 0 195.85 217.31 5.55 o 3 3 0 611.20 543.11 20.78 o 4 3 0 15.85 25.95 1.39 o 5 3 0 1294.10 1343.09 40.50 o 6 3 0 -0.15 4.11 1.20 o 7 3 0 22.50 15.13 1.71 o 8 3 0 9.30 6.71 1.46 o 9 3 0 54.75 65.06 3.24 o 10 3 0 406.40 403.64 19.60 o 11 3 0 394.10 358.02 22.76 o 12 3 0 86.00 86.18 9.75 o 13 3 0 4.05 4.25 4.35 o 0 4 0 177.80 188.34 7.92 o 1 4 0 235.20 248.60 7.11 o 2 4 0 90.00 85.73 3.40 o 3 4 0 671.00 598.51 18.80 o 4 4 0 296.60 271.88 12.14 o 5 4 0 17.20 7.88 1.46 o 6 4 0 39.95 45.28 2.01 o 7 4 0 46.40 40.13 2.42 o 8 4 0 2.70 1.49 1.57 o 9 4 0 45.95 52.74 3.10 o 10 4 0 12.50 18.68 3.59 o 11 4 0 46.25 48.24 6.20 o 12 4 0 16.70 14.45 4.86 o 1 5 0 1493.85 1487.76 45.64 o 2 5 0 912.95 918.14 32.20 o 3 5 0 10.60 12.37 0.95 o 4 5 0 641.15 638.37 18.38 o 5 5 0 1951.70 1884.31 55.86 o 6 5 0 88.00 90.09 4.43 o 7 5 0 3.25 1.60 2.08 o 8 5 0 468.50 475.37 23.36 o 9 5 0 60.35 70.14 5.04 o 10 5 0 70.60 66.44 7.30 o 11 5 0 129.70 121.32 12.91 o 12 5 0 4.35 0.55 6.83 o 0 6 0 50.60 38.18 2.60 o 1 6 0 664.15 558.17 21.41 o 2 6 0 682.30 692.09 21.25 o 3 6 0 2210.70 2232.21 62.75 o 4 6 0 819.80 850.60 20.25 o 5 6 0 76.65 86.07 2.76 o 6 6 0 112.80 103.12 3.65 o 7 6 0 410.90 431.37 15.19 o 8 6 0 14.00 15.57 3.17 o 9 6 0 -1.90 0.17 2.74 o 10 6 0 11.55 13.35 4.88 o 11 6 0 23.95 34.34 6.33 o 1 7 0 0.40 0.36 1.41 o 2 7 0 44.10 42.41 2.08 o 3 7 0 75.15 85.30 2.96 o 4 7 0 27.10 32.65 1.88 o 5 7 0 274.10 281.36 9.32 o 6 7 0 509.90 518.91 15.06 o 7 7 0 497.95 471.95 16.50 o 8 7 0 336.70 329.69 13.95 o 9 7 0 11.95 11.89 2.83 o 10 7 0 -1.15 1.33 2.52 o 11 7 0 -2.05 0.13 3.71 o 0 8 0 589.30 613.19 23.00 o 1 8 0 453.30 461.61 10.90 o 2 8 0 478.05 469.36 14.85 o 3 8 0 225.40 215.82 7.65 o 4 8 0 672.50 641.77 22.22 o 5 8 0 15.70 15.47 1.94 o 6 8 0 890.75 835.57 37.17 o 7 8 0 21.50 21.06 2.94 o 8 8 0 171.10 164.64 8.64 o 9 8 0 263.25 256.64 13.86 o 10 8 0 40.80 42.20 6.02 o 1 9 0 46.80 53.33 2.20 o 2 9 0 513.60 518.45 12.80 o 3 9 0 7.40 9.71 1.60 o 4 9 0 1.30 0.94 1.44 o 5 9 0 327.75 315.69 12.52 o 6 9 0 43.55 40.74 3.08 o 7 9 0 226.55 229.77 14.47 o 8 9 0 149.00 156.56 9.00 o 9 9 0 42.50 37.77 4.00 o 0 10 0 8.30 10.36 1.50 o 1 10 0 38.40 41.59 1.80 o 2 10 0 345.10 333.40 11.70 o 3 10 0 235.50 206.78 7.50 o 4 10 0 56.85 56.72 3.51 o 5 10 0 0.85 4.41 0.85 o 6 10 0 31.10 28.10 3.83 o 7 10 0 9.90 11.41 2.60 o 8 10 0 17.60 21.15 3.90 o 1 11 0 25.10 24.09 1.40 o 2 11 0 263.80 253.56 9.40 o 3 11 0 92.00 95.07 4.20 o 4 11 0 308.70 300.82 10.60 o 5 11 0 98.50 99.04 5.00 o 6 11 0 -2.70 0.92 3.60 o 7 11 0 33.20 38.84 3.60 o 0 12 0 0.90 0.31 2.85 o 1 12 0 -0.40 0.46 1.77 o 2 12 0 25.00 26.46 2.40 o 3 12 0 2.70 3.95 1.70 o 4 12 0 4.90 6.45 2.10 o 5 12 0 1.60 9.18 5.30 o 1 13 0 62.60 79.77 7.20 o 2 13 0 32.50 29.64 4.70 o -13 1 1 21.35 17.80 5.68 o -12 1 1 239.50 209.37 14.66 o -11 1 1 69.10 72.06 4.07 o -10 1 1 135.05 138.11 6.65 o -9 1 1 61.00 62.26 2.93 o -8 1 1 759.50 739.91 21.38 o -7 1 1 787.45 857.73 22.19 o -6 1 1 2184.55 2333.98 62.85 o -5 1 1 199.95 269.94 6.40 o -4 1 1 299.80 328.17 9.65 o -3 1 1 6424.90 7245.64 304.90 o 2 1 1 1146.40 1099.52 38.19 o 3 1 1 1655.10 1613.52 62.69 o 4 1 1 80.80 62.14 3.05 o 5 1 1 58.75 62.55 2.35 o 6 1 1 92.00 90.90 3.99 o 7 1 1 300.15 334.56 8.70 o 8 1 1 -0.10 0.15 1.19 o 9 1 1 541.95 540.17 19.08 o 10 1 1 -1.55 0.75 1.61 o 11 1 1 77.45 72.90 6.40 o 12 1 1 37.30 50.35 5.67 o -13 2 1 57.75 55.76 6.72 o -12 2 1 3.75 0.21 3.35 o -11 2 1 221.05 191.33 11.75 o -10 2 1 152.55 145.08 6.95 o -9 2 1 12.60 9.47 1.78 o -8 2 1 39.80 48.03 2.16 o -7 2 1 70.95 85.90 2.95 o -6 2 1 1342.75 1342.20 50.66 o -5 2 1 2469.10 2562.67 103.46 o -4 2 1 1221.55 1384.91 47.46 o -3 2 1 5913.60 6089.38 208.65 o -2 2 1 260.95 260.88 8.71 o 1 2 1 7.10 11.73 0.50 o 2 2 1 747.75 827.86 23.95 o 3 2 1 191.15 206.01 6.05 o 4 2 1 1824.95 1662.73 51.73 o 5 2 1 5.90 10.23 1.06 o 6 2 1 95.15 79.67 3.55 o 7 2 1 168.70 157.04 6.23 o 8 2 1 190.75 184.13 6.70 o 9 2 1 923.75 912.31 32.82 o 10 2 1 343.95 331.92 14.41 o 11 2 1 127.75 121.50 8.01 o 12 2 1 8.80 11.22 3.79 o -13 3 1 61.55 54.30 8.26 o -12 3 1 43.05 51.30 5.86 o -11 3 1 20.25 21.70 3.10 o -10 3 1 239.35 250.52 10.27 o -9 3 1 294.00 291.24 12.08 o -8 3 1 372.65 361.57 13.50 o -7 3 1 35.60 35.35 1.87 o -6 3 1 80.00 66.81 3.83 o -5 3 1 58.15 45.06 2.80 o -4 3 1 174.00 158.87 7.47 o -3 3 1 72.20 80.41 3.13 o -2 3 1 152.35 142.26 5.75 o -1 3 1 4944.60 5109.04 183.92 o 0 3 1 2583.90 2621.87 86.55 o 1 3 1 785.55 803.37 20.18 o 2 3 1 23.95 19.95 0.95 o 3 3 1 619.55 639.59 19.59 o 4 3 1 1613.70 1592.74 54.73 o 5 3 1 709.55 794.01 26.86 o 6 3 1 749.00 779.10 24.17 o 7 3 1 151.35 154.03 5.47 o 8 3 1 70.20 78.79 3.67 o 9 3 1 61.70 65.11 3.20 o 10 3 1 21.05 21.03 2.30 o 11 3 1 11.35 11.25 2.77 o 12 3 1 1.15 0.62 3.63 o -13 4 1 67.35 54.34 9.55 o -12 4 1 72.20 74.25 9.64 o -11 4 1 30.60 30.44 4.90 o -10 4 1 66.85 68.69 5.15 o -9 4 1 319.30 316.79 14.81 o -8 4 1 1282.65 1303.84 55.57 o -7 4 1 1515.90 1501.05 57.92 o -6 4 1 702.60 678.26 22.77 o -5 4 1 74.45 66.76 3.37 o -4 4 1 32.30 32.47 1.96 o -3 4 1 531.75 554.34 13.35 o -2 4 1 3292.10 3404.17 90.80 o -1 4 1 1873.20 1956.42 65.81 o 0 4 1 2363.00 2401.71 77.09 o 1 4 1 993.55 896.51 30.44 o 2 4 1 13.50 7.89 1.00 o 3 4 1 400.45 367.87 11.61 o 4 4 1 1515.55 1336.36 47.93 o 5 4 1 7.80 7.47 0.90 o 6 4 1 828.70 848.55 27.46 o 7 4 1 1672.85 1668.43 57.59 o 8 4 1 748.30 729.51 31.01 o 9 4 1 101.90 110.71 5.43 o 10 4 1 63.90 74.26 4.90 o 11 4 1 10.05 14.84 3.61 o 12 4 1 54.00 58.22 7.21 o -12 5 1 4.95 1.17 5.62 o -11 5 1 169.40 167.27 14.72 o -10 5 1 545.85 542.54 29.85 o -9 5 1 374.45 343.89 16.30 o -8 5 1 121.30 123.85 6.62 o -7 5 1 47.75 38.39 3.41 o -6 5 1 79.40 79.41 3.97 o -5 5 1 79.60 100.45 3.29 o -4 5 1 4.90 4.15 0.76 o -3 5 1 3.90 1.88 1.14 o -2 5 1 11.15 7.47 1.08 o -1 5 1 470.60 497.10 17.62 o 0 5 1 95.30 136.25 3.51 o 1 5 1 2007.30 2055.32 59.74 o 2 5 1 1149.60 1271.18 38.62 o 3 5 1 341.65 377.60 10.00 o 4 5 1 1006.30 926.04 28.18 o 5 5 1 666.55 635.52 19.96 o 6 5 1 727.55 685.55 25.17 o 7 5 1 204.80 200.46 8.36 o 8 5 1 239.65 259.58 10.56 o 9 5 1 4.45 1.78 1.93 o 10 5 1 0.75 3.56 6.39 o 11 5 1 48.55 54.88 6.21 o -12 6 1 0.50 1.51 5.32 o -11 6 1 44.25 49.42 5.65 o -10 6 1 132.75 132.31 8.48 o -9 6 1 48.70 42.61 3.73 o -8 6 1 104.85 108.89 5.36 o -7 6 1 23.65 23.76 1.80 o -6 6 1 263.75 272.46 7.75 o -5 6 1 677.30 701.39 17.22 o -4 6 1 620.10 642.42 19.25 o -3 6 1 63.05 57.02 2.70 o -2 6 1 175.20 151.18 5.20 o -1 6 1 458.65 419.75 17.10 o 0 6 1 15.05 15.80 1.30 o 1 6 1 1212.65 1177.01 35.55 o 2 6 1 412.55 377.56 13.11 o 3 6 1 78.45 65.28 3.57 o 4 6 1 263.45 262.06 7.61 o 5 6 1 1292.00 1222.74 37.65 o 6 6 1 76.05 79.64 3.05 o 7 6 1 3.55 7.00 2.59 o 8 6 1 85.55 88.53 4.75 o 9 6 1 24.20 24.24 3.21 o 10 6 1 105.65 90.51 9.65 o 11 6 1 34.80 40.70 7.21 o -11 7 1 152.20 141.70 12.79 o -10 7 1 6.15 14.18 2.35 o -9 7 1 343.60 372.34 17.35 o -8 7 1 43.95 59.97 3.15 o -7 7 1 119.90 111.09 4.55 o -6 7 1 111.55 111.82 4.24 o -5 7 1 32.65 31.82 1.90 o -4 7 1 194.85 207.15 6.34 o -3 7 1 402.20 416.87 13.09 o -2 7 1 213.60 227.80 7.00 o -1 7 1 277.70 234.39 6.50 o 0 7 1 1166.25 1101.89 38.84 o 1 7 1 15.65 20.56 1.30 o 2 7 1 491.15 464.54 14.69 o 3 7 1 1443.60 1407.25 45.67 o 4 7 1 52.90 52.14 2.59 o 5 7 1 339.30 320.37 15.31 o 6 7 1 216.25 204.38 8.12 o 7 7 1 -0.30 0.02 1.55 o 8 7 1 30.30 35.98 3.30 o 9 7 1 111.15 108.15 7.70 o 10 7 1 3.50 7.41 4.40 o -10 8 1 7.30 7.87 3.55 o -9 8 1 14.45 9.85 2.95 o -8 8 1 -0.25 0.11 1.70 o -7 8 1 58.35 55.16 3.42 o -6 8 1 226.60 224.96 8.48 o -5 8 1 114.40 121.63 4.38 o -4 8 1 606.65 592.03 19.87 o -3 8 1 296.50 299.42 7.90 o -2 8 1 34.80 27.16 2.30 o -1 8 1 15.20 20.46 1.20 o 0 8 1 15.85 14.33 1.80 o 1 8 1 0.65 4.73 1.32 o 2 8 1 43.70 38.79 2.33 o 3 8 1 194.80 186.66 7.24 o 4 8 1 43.10 45.68 3.07 o 5 8 1 1.50 1.40 1.96 o 6 8 1 4.70 2.05 2.06 o 7 8 1 -0.15 0.46 1.49 o 8 8 1 102.85 116.43 5.85 o 9 8 1 0.15 0.08 3.06 o 10 8 1 27.85 31.05 5.14 o -10 9 1 9.90 11.02 3.50 o -9 9 1 24.30 24.87 3.20 o -8 9 1 4.50 0.54 2.80 o -7 9 1 99.60 100.46 5.26 o -6 9 1 3.05 3.73 1.15 o -5 9 1 938.45 880.62 41.54 o -4 9 1 1089.00 1065.92 30.80 o -3 9 1 -0.80 1.17 2.15 o -2 9 1 25.60 27.80 2.00 o -1 9 1 81.30 79.13 3.00 o 0 9 1 70.00 71.67 2.30 o 1 9 1 5.75 6.99 1.75 o 2 9 1 318.25 308.85 13.79 o 3 9 1 278.65 274.25 11.08 o 4 9 1 458.75 459.60 21.12 o 5 9 1 349.55 346.42 16.43 o 6 9 1 315.50 300.92 18.21 o 7 9 1 14.00 16.09 2.47 o 8 9 1 175.40 166.89 12.10 o 9 9 1 92.60 88.19 8.78 o -9 10 1 0.50 5.73 4.81 o -8 10 1 79.00 75.82 6.10 o -7 10 1 0.70 1.22 3.35 o -6 10 1 12.40 17.52 1.60 o -5 10 1 199.00 194.92 7.20 o -4 10 1 465.70 440.74 15.80 o -3 10 1 2.70 1.49 1.60 o -2 10 1 2.20 1.18 1.80 o -1 10 1 13.10 14.32 1.10 o 0 10 1 36.30 41.87 1.60 o 1 10 1 483.00 480.85 12.70 o 2 10 1 114.20 116.63 6.53 o 3 10 1 509.85 477.74 19.16 o 4 10 1 37.35 37.04 3.07 o 5 10 1 82.25 87.28 5.69 o 6 10 1 9.60 12.67 2.67 o 7 10 1 27.80 28.86 4.30 o 8 10 1 1.30 4.06 3.00 o -7 11 1 12.00 7.09 2.90 o -6 11 1 1.70 1.04 5.10 o -5 11 1 26.20 26.83 2.40 o -4 11 1 4.50 4.14 2.10 o -3 11 1 3.20 6.05 1.60 o -2 11 1 0.10 1.30 1.08 o -1 11 1 80.50 78.04 4.10 o 0 11 1 351.60 332.21 8.40 o 1 11 1 41.40 37.88 2.40 o 2 11 1 279.00 277.69 8.90 o 3 11 1 39.75 39.17 3.61 o 4 11 1 91.80 105.95 4.80 o 5 11 1 20.70 25.93 3.50 o 6 11 1 15.20 11.17 4.60 o -5 12 1 -0.80 0.12 6.08 o -4 12 1 0.90 0.44 5.50 o -3 12 1 83.90 85.51 4.60 o -2 12 1 635.80 652.33 22.10 o -1 12 1 106.00 103.30 4.70 o 0 12 1 6.50 10.94 1.40 o 1 12 1 133.50 151.13 5.70 o 2 12 1 55.00 57.31 3.30 o 3 12 1 0.50 2.63 2.69 o 4 12 1 25.40 30.65 3.10 o 5 12 1 4.80 0.15 4.70 o -2 13 1 31.00 33.77 3.50 o -1 13 1 20.00 18.23 3.50 o 0 13 1 210.30 203.41 16.00 o 1 13 1 79.90 88.17 9.30 o 2 13 1 3.40 4.93 5.60 o -14 0 2 141.50 148.12 16.50 o -13 0 2 49.10 53.25 6.80 o -12 0 2 -0.20 4.06 3.94 o -11 0 2 109.40 122.25 4.90 o -10 0 2 162.30 181.62 7.50 o -9 0 2 5195.80 5253.51 199.60 o -8 0 2 37.70 53.87 2.50 o -7 0 2 91.70 102.39 3.30 o -6 0 2 344.00 362.45 10.40 o -5 0 2 1381.60 1346.96 43.20 o -4 0 2 1028.30 992.20 31.90 o -3 0 2 386.70 375.99 8.50 o 2 0 2 2563.00 2732.24 63.30 o 3 0 2 512.30 462.03 17.60 o 4 0 2 5470.80 5544.46 170.70 o 5 0 2 1832.50 2109.87 52.20 o 6 0 2 2421.10 2466.61 64.80 o 7 0 2 1770.50 1761.09 50.10 o 8 0 2 1.40 3.38 1.50 o 9 0 2 69.90 79.02 4.30 o 10 0 2 2.30 1.84 1.80 o 11 0 2 102.70 105.24 7.70 o 12 0 2 535.40 421.37 47.50 o -13 1 2 7.70 6.83 3.85 o -12 1 2 29.10 27.68 3.07 o -11 1 2 11.85 17.02 1.91 o -10 1 2 44.10 43.61 2.86 o -9 1 2 5.15 1.10 1.55 o -8 1 2 20.20 17.43 1.85 o -7 1 2 68.60 85.12 2.90 o -6 1 2 330.55 320.27 11.15 o -5 1 2 1434.65 1473.57 49.50 o -4 1 2 1085.55 1170.12 33.32 o -3 1 2 5362.30 5506.40 203.57 o 1 1 2 302.70 328.98 10.20 o 2 1 2 729.10 839.68 21.54 o 3 1 2 695.05 742.86 22.60 o 4 1 2 1984.75 1964.47 72.03 o 5 1 2 149.15 133.87 4.42 o 6 1 2 50.00 44.05 2.85 o 7 1 2 2121.65 2050.97 57.71 o 8 1 2 24.75 25.68 2.25 o 9 1 2 62.65 63.36 3.95 o 10 1 2 34.40 43.79 3.35 o 11 1 2 117.40 117.22 10.64 o 12 1 2 19.90 25.27 4.53 o -13 2 2 471.60 445.54 41.93 o -12 2 2 276.30 267.10 19.21 o -11 2 2 161.95 159.07 8.56 o -10 2 2 4.75 4.08 1.61 o -9 2 2 70.10 78.61 3.41 o -8 2 2 13.15 15.93 1.30 o -7 2 2 900.85 868.00 28.65 o -6 2 2 2092.85 2186.24 65.37 o -5 2 2 4429.15 4329.07 140.38 o -4 2 2 892.00 852.77 26.50 o -3 2 2 481.55 530.22 12.78 o -2 2 2 3385.15 3366.32 129.01 o -1 2 2 6962.40 6809.34 302.90 o 0 2 2 4924.60 4992.00 129.72 o 1 2 2 0.85 2.19 0.59 o 2 2 2 391.05 477.93 16.67 o 3 2 2 709.85 867.24 23.05 o 4 2 2 970.10 984.94 29.09 o 5 2 2 117.70 114.33 4.12 o 6 2 2 174.65 158.32 5.71 o 7 2 2 20.90 26.37 1.80 o 8 2 2 1333.70 1241.81 41.68 o 9 2 2 222.05 213.51 10.16 o 10 2 2 53.60 53.19 4.20 o 11 2 2 3.75 3.40 2.45 o 12 2 2 30.60 33.02 6.10 o -13 3 2 72.85 71.38 11.26 o -12 3 2 28.30 34.30 5.25 o -11 3 2 315.55 305.82 20.27 o -10 3 2 373.95 374.19 17.05 o -9 3 2 7.10 9.55 2.29 o -8 3 2 729.20 710.21 28.20 o -7 3 2 961.85 913.79 33.30 o -6 3 2 374.90 331.34 13.77 o -5 3 2 62.15 86.98 2.75 o -4 3 2 3901.60 3887.15 123.83 o -3 3 2 975.30 975.08 36.41 o -2 3 2 45.00 46.38 2.22 o -1 3 2 1.20 0.25 1.40 o 0 3 2 48.45 40.89 2.25 o 1 3 2 1368.25 1349.75 32.65 o 2 3 2 3376.60 3247.51 92.41 o 3 3 2 826.30 787.84 24.54 o 4 3 2 491.95 594.13 14.50 o 5 3 2 72.80 87.37 2.46 o 6 3 2 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