#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:31:29 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181061 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/41/2214198.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214198_Fobs loop_ _publ_author_name 'Roth, Arne' 'Buchholz, Axel' 'G\"artner, Martin' 'G\"orls, Helmar' 'Plass, Winfried' _publ_section_title ; 3-(2-Pyridyl)-N'-salicylidenepropionohydrazide ; _journal_coeditor_code GK2074 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3073 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.6638 _cell_length_b 15.1845 _cell_length_c 15.5994 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high 0.7706 _cod_data_source_file gk2074Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 85.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7.12 1.43 2.07 o 4 0 0 225.86 240.36 17.80 o 6 0 0 0.01 -2.16 4.14 o 1 1 0 1087.66 850.72 65.28 o 2 1 0 6.89 5.54 0.85 o 3 1 0 59.61 54.80 1.99 o 4 1 0 67.76 72.20 3.82 o 5 1 0 700.51 733.73 14.76 o 6 1 0 203.21 191.26 8.58 o 7 1 0 1.88 1.92 3.62 o 0 2 0 2.85 6.11 0.72 o 1 2 0 2834.46 2551.94 87.13 o 2 2 0 11.02 9.62 1.14 o 3 2 0 7.77 6.88 1.23 o 4 2 0 4.27 2.71 1.38 o 5 2 0 1387.71 1439.61 27.50 o 6 2 0 53.35 54.95 4.63 o 7 2 0 3.06 4.75 4.26 o 1 3 0 5358.76 5186.04 94.32 o 2 3 0 649.29 643.46 11.48 o 3 3 0 135.08 137.86 3.65 o 4 3 0 96.87 92.69 3.13 o 5 3 0 149.61 137.37 4.69 o 6 3 0 121.69 139.05 7.23 o 7 3 0 4.94 0.63 3.69 o 2 4 0 216.48 212.43 9.68 o 3 4 0 5.03 3.39 1.65 o 4 4 0 194.61 190.33 5.18 o 5 4 0 59.54 63.04 3.29 o 6 4 0 331.94 356.51 16.45 o 7 4 0 1.23 9.26 4.32 o 1 5 0 4635.11 4431.99 86.46 o 2 5 0 166.03 171.67 3.87 o 3 5 0 149.63 157.66 7.16 o 4 5 0 739.22 759.20 14.69 o 5 5 0 613.69 679.41 12.53 o 6 5 0 83.08 80.23 4.52 o 7 5 0 12.75 12.23 11.60 o 0 6 0 4240.86 4089.28 93.15 o 1 6 0 85.88 112.72 2.28 o 2 6 0 36.98 45.51 1.71 o 3 6 0 126.98 116.39 2.91 o 4 6 0 1054.54 1028.48 17.81 o 5 6 0 96.57 85.50 3.36 o 6 6 0 187.33 199.79 7.21 o 7 6 0 34.40 31.53 5.14 o 1 7 0 702.73 734.68 15.73 o 2 7 0 1482.72 1513.21 23.94 o 3 7 0 38.46 47.47 2.36 o 4 7 0 4.22 4.56 1.42 o 5 7 0 0.94 -0.20 1.92 o 6 7 0 138.56 142.47 6.75 o 0 8 0 50.40 48.55 3.60 o 1 8 0 981.79 991.85 21.41 o 2 8 0 1155.91 1177.22 18.44 o 3 8 0 91.74 93.78 2.96 o 4 8 0 0.37 1.86 1.95 o 5 8 0 26.98 20.81 2.11 o 6 8 0 150.42 155.15 9.62 o 1 9 0 2177.74 2200.57 32.95 o 2 9 0 475.49 448.15 7.76 o 3 9 0 203.30 206.04 5.67 o 4 9 0 102.64 97.69 3.35 o 5 9 0 120.50 121.26 6.11 o 6 9 0 12.39 14.36 3.60 o 0 10 0 414.16 414.70 8.81 o 1 10 0 410.49 403.64 8.19 o 2 10 0 1.75 -0.12 2.75 o 3 10 0 1273.59 1311.25 21.98 o 4 10 0 635.06 697.00 11.72 o 5 10 0 146.73 135.53 14.12 o 6 10 0 2.10 -1.20 3.37 o 1 11 0 2.47 4.38 1.58 o 2 11 0 357.09 357.03 8.51 o 3 11 0 95.59 99.89 4.91 o 4 11 0 77.23 83.66 3.46 o 5 11 0 64.28 59.65 6.92 o 6 11 0 44.59 48.57 12.14 o 0 12 0 473.44 463.80 14.21 o 1 12 0 361.53 385.36 12.33 o 2 12 0 836.87 843.19 20.55 o 3 12 0 398.18 389.02 9.85 o 4 12 0 108.46 112.53 4.46 o 5 12 0 30.75 39.96 7.55 o 1 13 0 19.75 21.68 1.31 o 2 13 0 513.98 525.71 29.75 o 3 13 0 3.97 7.61 2.07 o 4 13 0 0.33 -1.42 1.55 o 5 13 0 2.38 5.78 3.17 o 0 14 0 4.79 0.72 1.98 o 1 14 0 0.02 -0.76 0.76 o 2 14 0 87.88 98.62 3.51 o 3 14 0 733.50 783.36 25.72 o 4 14 0 11.78 8.24 4.50 o 5 14 0 2.32 4.21 7.73 o 1 15 0 2.29 2.26 1.98 o 2 15 0 16.61 18.98 2.17 o 3 15 0 450.06 491.67 30.66 o 4 15 0 0.44 -0.52 3.51 o 0 16 0 7.66 6.11 3.78 o 1 16 0 11.93 10.53 1.22 o 2 16 0 22.95 35.84 9.98 o 3 16 0 42.86 20.81 4.12 o 4 16 0 83.37 83.42 8.54 o 1 17 0 18.62 18.92 5.13 o 2 17 0 260.22 258.43 14.21 o 3 17 0 4.08 -1.03 3.96 o 0 18 0 8.98 17.98 5.40 o 1 18 0 92.44 102.33 10.25 o 2 18 0 86.44 85.32 7.82 o 1 19 0 7.25 4.53 4.59 o 1 0 1 20.25 17.83 1.50 o 2 0 1 5.40 2.67 0.82 o 3 0 1 1.08 1.37 2.05 o 4 0 1 376.75 403.33 8.33 o 5 0 1 103.82 101.48 3.80 o 6 0 1 202.37 205.20 9.88 o 7 0 1 1.74 -5.94 6.38 o 1 1 1 99.76 87.12 1.84 o 2 1 1 404.16 393.62 5.08 o 3 1 1 494.21 496.77 6.48 o 4 1 1 84.21 78.97 2.09 o 5 1 1 174.39 182.71 3.60 o 6 1 1 224.96 242.66 7.63 o 7 1 1 5.01 0.77 2.43 o 0 2 1 1917.72 1821.78 119.73 o 1 2 1 7248.76 6604.10 206.45 o 2 2 1 53.04 48.59 1.26 o 3 2 1 217.32 227.13 3.51 o 4 2 1 380.98 397.30 8.21 o 5 2 1 755.54 787.69 11.61 o 6 2 1 205.62 204.56 6.80 o 7 2 1 4.70 5.61 2.85 o 0 3 1 5444.40 5572.56 176.06 o 1 3 1 3115.76 2939.11 33.36 o 2 3 1 547.16 553.31 6.60 o 3 3 1 237.37 254.77 4.88 o 4 3 1 262.23 245.23 3.88 o 5 3 1 420.53 451.61 6.87 o 6 3 1 49.31 47.46 3.07 o 7 3 1 3.47 9.31 2.91 o 1 4 1 864.89 841.66 15.02 o 2 4 1 281.83 284.87 3.70 o 3 4 1 9.10 7.35 0.80 o 4 4 1 459.73 455.27 6.85 o 5 4 1 360.19 379.55 6.01 o 6 4 1 292.54 295.78 9.53 o 7 4 1 16.24 12.61 3.27 o 0 5 1 722.61 734.19 14.94 o 1 5 1 662.18 633.23 8.41 o 2 5 1 1.04 3.45 0.78 o 3 5 1 11.12 10.75 0.93 o 4 5 1 20.57 17.72 1.61 o 5 5 1 57.15 62.37 2.16 o 6 5 1 24.70 21.67 2.14 o 7 5 1 139.26 134.36 6.00 o 0 6 1 305.07 323.46 7.01 o 1 6 1 2193.85 2238.51 29.97 o 2 6 1 718.68 760.22 9.02 o 3 6 1 165.38 161.45 2.72 o 4 6 1 128.46 131.22 2.70 o 5 6 1 190.46 190.54 3.87 o 6 6 1 52.25 57.10 2.88 o 0 7 1 616.11 646.76 11.57 o 1 7 1 1998.04 2002.56 25.64 o 2 7 1 1069.58 1165.49 15.34 o 3 7 1 133.73 137.84 4.49 o 4 7 1 592.39 611.27 8.67 o 5 7 1 70.26 68.38 2.18 o 6 7 1 3.76 8.01 2.06 o 0 8 1 717.98 737.36 11.36 o 1 8 1 441.34 437.23 5.57 o 2 8 1 702.65 754.10 8.65 o 3 8 1 498.29 505.38 6.06 o 4 8 1 762.59 778.97 10.25 o 5 8 1 103.10 101.86 3.00 o 6 8 1 18.61 17.60 2.32 o 0 9 1 0.80 1.46 0.51 o 1 9 1 430.43 449.59 5.79 o 2 9 1 89.27 82.97 1.67 o 3 9 1 77.02 70.16 2.46 o 4 9 1 3.43 5.08 1.33 o 5 9 1 21.05 22.89 1.76 o 6 9 1 45.68 49.21 3.04 o 0 10 1 72.09 62.15 2.88 o 1 10 1 18.66 22.61 1.17 o 2 10 1 618.19 654.57 7.96 o 3 10 1 76.43 81.22 2.07 o 4 10 1 1.32 -0.46 0.93 o 5 10 1 78.85 73.84 2.35 o 6 10 1 7.31 6.26 2.71 o 0 11 1 329.00 350.23 7.56 o 1 11 1 159.89 162.35 3.05 o 2 11 1 115.32 114.48 2.77 o 3 11 1 519.25 533.73 11.43 o 4 11 1 66.52 66.74 2.40 o 5 11 1 10.27 4.43 1.59 o 6 11 1 7.51 7.05 5.18 o 0 12 1 20.09 19.23 1.84 o 1 12 1 447.35 467.53 7.75 o 2 12 1 1035.56 1082.87 14.69 o 3 12 1 72.48 76.12 2.04 o 4 12 1 28.30 23.68 1.56 o 5 12 1 2.54 2.65 2.20 o 0 13 1 276.57 278.47 6.61 o 1 13 1 171.23 166.90 2.87 o 2 13 1 81.17 84.59 2.97 o 3 13 1 22.49 25.13 1.59 o 4 13 1 79.34 79.82 5.09 o 5 13 1 7.83 7.31 3.65 o 0 14 1 102.84 110.33 11.78 o 1 14 1 1.04 3.31 0.91 o 2 14 1 96.16 90.75 3.33 o 3 14 1 116.14 114.68 3.78 o 4 14 1 52.35 52.96 3.14 o 5 14 1 4.05 7.15 3.04 o 0 15 1 95.37 97.12 4.12 o 1 15 1 44.85 43.41 1.63 o 2 15 1 22.03 28.23 4.53 o 3 15 1 256.28 260.58 9.23 o 4 15 1 13.82 8.97 2.47 o 0 16 1 4.65 6.48 2.25 o 1 16 1 43.67 39.28 2.00 o 2 16 1 318.65 318.81 9.07 o 3 16 1 138.87 132.90 13.45 o 4 16 1 52.25 52.50 3.93 o 0 17 1 18.53 14.80 1.71 o 1 17 1 37.20 23.64 4.05 o 2 17 1 65.20 49.13 3.55 o 3 17 1 41.72 39.90 3.79 o 0 18 1 8.43 12.28 3.92 o 1 18 1 20.79 23.55 5.27 o 2 18 1 27.09 21.35 3.50 o 0 19 1 42.28 41.59 5.61 o 1 19 1 60.26 48.37 4.44 o 0 0 2 642.51 506.42 16.19 o 1 0 2 4521.92 4077.23 90.92 o 2 0 2 557.85 495.66 7.85 o 3 0 2 256.99 267.91 4.99 o 4 0 2 44.04 43.04 2.03 o 5 0 2 0.33 -1.61 1.89 o 6 0 2 161.76 176.13 6.65 o 7 0 2 0.01 -7.10 7.28 o 0 1 2 166.59 152.26 2.82 o 1 1 2 4058.59 3706.85 47.79 o 2 1 2 268.19 250.89 3.05 o 3 1 2 848.06 840.10 9.40 o 4 1 2 90.10 105.50 2.43 o 5 1 2 0.86 2.49 1.10 o 6 1 2 12.67 12.41 2.34 o 7 1 2 51.28 49.15 3.75 o 0 2 2 559.00 522.90 10.41 o 1 2 2 1840.13 1693.77 15.87 o 2 2 2 712.91 691.12 7.64 o 3 2 2 270.70 302.34 4.03 o 4 2 2 321.36 325.25 5.07 o 5 2 2 46.60 49.70 2.11 o 6 2 2 0.03 1.78 1.73 o 7 2 2 15.03 11.29 3.47 o 0 3 2 0.08 3.11 1.25 o 1 3 2 944.87 889.19 8.65 o 2 3 2 937.12 915.46 9.95 o 3 3 2 93.37 107.32 2.23 o 4 3 2 121.72 120.06 2.39 o 5 3 2 238.09 243.69 4.20 o 6 3 2 15.08 12.09 3.21 o 7 3 2 6.62 8.23 3.07 o 0 4 2 262.39 298.68 6.35 o 1 4 2 1741.32 1659.60 22.79 o 2 4 2 679.42 699.59 7.75 o 3 4 2 120.18 117.69 2.16 o 4 4 2 55.41 55.92 2.21 o 5 4 2 60.89 62.45 2.19 o 6 4 2 54.81 49.39 3.46 o 7 4 2 42.74 44.06 4.15 o 0 5 2 87.45 92.40 5.63 o 1 5 2 412.04 397.20 4.14 o 2 5 2 227.07 222.75 3.39 o 3 5 2 21.97 22.32 1.01 o 4 5 2 78.62 79.82 2.08 o 5 5 2 48.06 40.70 2.10 o 6 5 2 47.18 54.54 3.65 o 7 5 2 17.34 15.68 3.48 o 0 6 2 274.64 256.61 23.02 o 1 6 2 615.13 617.41 9.70 o 2 6 2 373.75 381.23 5.51 o 3 6 2 38.72 45.33 1.69 o 4 6 2 34.55 30.09 1.56 o 5 6 2 13.14 13.84 1.55 o 6 6 2 27.33 27.28 3.13 o 0 7 2 637.33 664.62 12.77 o 1 7 2 121.26 128.62 1.94 o 2 7 2 172.89 176.39 2.59 o 3 7 2 44.64 52.27 1.41 o 4 7 2 53.12 51.00 1.79 o 5 7 2 3.39 1.81 1.61 o 6 7 2 34.61 38.21 3.97 o 0 8 2 1.49 -0.41 0.72 o 1 8 2 306.94 327.58 5.03 o 2 8 2 643.03 677.87 7.91 o 3 8 2 141.66 151.78 2.52 o 4 8 2 320.88 314.56 4.86 o 5 8 2 49.98 51.72 2.37 o 6 8 2 15.15 14.10 2.06 o 0 9 2 7.42 7.27 0.79 o 1 9 2 126.30 127.27 2.13 o 2 9 2 54.20 62.08 1.38 o 3 9 2 2.90 1.64 0.87 o 4 9 2 274.35 267.69 4.08 o 5 9 2 5.11 7.49 1.54 o 6 9 2 19.38 13.37 2.03 o 0 10 2 75.46 81.19 2.59 o 1 10 2 117.17 117.23 1.98 o 2 10 2 351.98 366.19 4.54 o 3 10 2 249.70 251.22 3.75 o 4 10 2 68.28 69.95 2.44 o 5 10 2 14.31 12.00 3.08 o 6 10 2 2.28 3.34 3.27 o 0 11 2 79.21 89.46 3.15 o 1 11 2 105.54 98.81 2.61 o 2 11 2 4.14 5.69 2.46 o 3 11 2 181.46 185.12 3.06 o 4 11 2 122.92 119.40 3.47 o 5 11 2 25.27 20.88 2.00 o 6 11 2 0.58 -1.13 2.74 o 0 12 2 7.75 6.01 1.80 o 1 12 2 375.81 384.97 5.33 o 2 12 2 70.73 61.29 3.58 o 3 12 2 199.71 203.13 4.43 o 4 12 2 46.46 48.07 1.95 o 5 12 2 25.57 27.10 3.56 o 0 13 2 485.59 530.18 11.44 o 1 13 2 27.71 29.54 1.23 o 2 13 2 76.12 73.92 2.43 o 3 13 2 99.20 96.44 2.75 o 4 13 2 9.18 8.30 1.46 o 5 13 2 22.38 28.08 3.45 o 0 14 2 7.10 5.40 1.03 o 1 14 2 68.72 59.96 3.35 o 2 14 2 248.41 232.87 6.80 o 3 14 2 74.21 69.87 4.70 o 4 14 2 6.93 7.85 2.27 o 5 14 2 0.95 3.11 2.69 o 0 15 2 120.23 125.08 3.63 o 1 15 2 76.55 77.10 1.97 o 2 15 2 35.18 35.08 1.98 o 3 15 2 57.51 48.09 4.83 o 4 15 2 30.66 42.93 3.63 o 0 16 2 3.57 3.19 3.04 o 1 16 2 13.39 12.99 1.01 o 2 16 2 28.01 20.52 5.47 o 3 16 2 24.65 26.59 4.74 o 4 16 2 0.38 -1.56 2.39 o 0 17 2 28.71 31.94 4.76 o 1 17 2 42.18 38.09 3.21 o 2 17 2 32.55 44.59 5.55 o 3 17 2 12.16 16.74 3.06 o 0 18 2 14.53 11.80 3.84 o 1 18 2 35.45 40.38 3.70 o 2 18 2 7.49 6.19 2.36 o 0 19 2 0.10 0.77 3.24 o 1 19 2 55.92 55.42 4.31 o 1 0 3 468.13 441.73 6.20 o 2 0 3 1355.61 1378.55 20.68 o 3 0 3 2204.86 2444.80 36.28 o 4 0 3 659.69 701.24 13.89 o 5 0 3 9.44 6.17 1.67 o 6 0 3 0.64 -2.31 2.31 o 7 0 3 15.68 18.24 5.22 o 1 1 3 5852.81 5051.71 71.20 o 2 1 3 2493.31 2444.34 26.16 o 3 1 3 71.24 75.31 1.67 o 4 1 3 32.71 30.05 1.25 o 5 1 3 53.55 54.80 1.83 o 6 1 3 21.52 20.81 2.21 o 7 1 3 51.62 55.79 4.03 o 0 2 3 1387.68 1237.65 15.47 o 1 2 3 997.77 898.91 8.38 o 2 2 3 68.26 62.99 1.23 o 3 2 3 430.85 440.83 5.46 o 4 2 3 39.43 42.02 1.88 o 5 2 3 42.36 44.64 1.73 o 6 2 3 8.48 5.05 1.86 o 7 2 3 3.46 0.56 2.77 o 0 3 3 119.05 101.08 1.76 o 1 3 3 197.91 180.02 2.29 o 2 3 3 329.14 330.76 3.99 o 3 3 3 1285.37 1329.68 14.52 o 4 3 3 94.03 85.31 1.98 o 5 3 3 52.69 53.31 1.80 o 6 3 3 17.91 18.36 2.35 o 7 3 3 3.13 1.63 2.58 o 0 4 3 195.80 182.41 4.14 o 1 4 3 598.70 597.79 6.08 o 2 4 3 672.77 703.68 7.81 o 3 4 3 953.46 998.09 12.39 o 4 4 3 226.12 242.78 3.72 o 5 4 3 240.80 260.43 4.39 o 6 4 3 49.63 47.01 3.95 o 7 4 3 4.28 7.47 2.86 o 0 5 3 1503.94 1403.28 17.62 o 1 5 3 1061.03 1061.59 11.34 o 2 5 3 1259.47 1374.46 15.25 o 3 5 3 429.38 419.17 5.33 o 4 5 3 130.05 142.65 2.70 o 5 5 3 14.97 16.33 1.56 o 6 5 3 100.25 97.34 4.21 o 7 5 3 14.12 17.82 3.92 o 0 6 3 30.88 37.93 1.06 o 1 6 3 876.54 869.98 9.11 o 2 6 3 1156.77 1246.95 15.55 o 3 6 3 39.30 47.57 1.95 o 4 6 3 437.55 449.53 6.37 o 5 6 3 17.32 20.03 1.57 o 6 6 3 15.73 17.75 3.11 o 0 7 3 354.67 354.46 5.42 o 1 7 3 1075.69 1060.09 10.12 o 2 7 3 7.61 4.26 0.71 o 3 7 3 59.02 58.56 1.53 o 4 7 3 54.00 53.99 2.10 o 5 7 3 53.68 54.33 2.19 o 6 7 3 9.81 17.11 4.02 o 0 8 3 4.87 1.26 0.64 o 1 8 3 587.24 620.95 6.85 o 2 8 3 292.17 320.08 3.88 o 3 8 3 134.93 135.75 2.27 o 4 8 3 84.49 86.09 3.05 o 5 8 3 161.00 172.51 4.02 o 6 8 3 3.16 1.86 2.46 o 0 9 3 162.03 161.75 3.81 o 1 9 3 452.72 459.71 5.27 o 2 9 3 15.76 18.41 1.38 o 3 9 3 45.86 44.60 1.72 o 4 9 3 99.45 102.75 2.21 o 5 9 3 165.78 177.64 7.14 o 6 9 3 14.11 12.99 2.58 o 0 10 3 129.90 157.36 8.54 o 1 10 3 302.21 316.22 3.79 o 2 10 3 101.38 90.87 2.38 o 3 10 3 183.51 186.32 4.01 o 4 10 3 116.95 113.00 2.77 o 5 10 3 53.25 58.14 3.18 o 6 10 3 83.33 89.73 5.74 o 0 11 3 9.92 13.37 0.95 o 1 11 3 153.86 150.25 2.75 o 2 11 3 183.62 193.04 3.12 o 3 11 3 25.61 26.08 1.10 o 4 11 3 2.96 3.58 1.60 o 5 11 3 92.37 84.33 4.82 o 6 11 3 74.45 93.40 7.19 o 0 12 3 107.35 106.45 2.15 o 1 12 3 61.71 59.77 1.56 o 2 12 3 62.21 70.74 2.01 o 3 12 3 33.67 27.25 1.67 o 4 12 3 50.53 51.31 1.96 o 5 12 3 56.30 53.99 4.15 o 0 13 3 15.89 15.08 2.08 o 1 13 3 104.96 103.93 2.67 o 2 13 3 22.72 22.59 1.47 o 3 13 3 90.09 85.15 3.87 o 4 13 3 7.01 4.23 1.94 o 5 13 3 25.64 30.24 6.81 o 0 14 3 135.87 150.16 3.22 o 1 14 3 15.44 10.62 2.36 o 2 14 3 9.24 12.32 1.51 o 3 14 3 82.21 86.98 3.22 o 4 14 3 50.53 54.96 3.58 o 5 14 3 3.98 0.70 2.70 o 0 15 3 14.78 13.83 4.40 o 1 15 3 208.40 209.23 5.27 o 2 15 3 76.11 69.82 2.65 o 3 15 3 5.09 7.71 1.84 o 4 15 3 48.61 45.81 3.59 o 0 16 3 17.95 19.23 2.00 o 1 16 3 8.01 7.17 1.08 o 2 16 3 18.75 13.36 2.26 o 3 16 3 13.67 11.80 2.28 o 4 16 3 2.06 2.68 2.21 o 0 17 3 4.15 8.63 4.14 o 1 17 3 25.92 25.35 2.84 o 2 17 3 13.16 10.66 3.56 o 3 17 3 37.15 34.28 3.79 o 0 18 3 49.86 49.61 12.68 o 1 18 3 4.89 4.87 2.43 o 2 18 3 80.51 66.70 4.18 o 0 19 3 47.24 41.14 5.78 o 1 19 3 10.03 9.59 2.91 o 0 0 4 3027.34 2718.39 88.48 o 1 0 4 1910.48 1773.13 22.95 o 2 0 4 0.91 1.76 1.29 o 3 0 4 263.81 279.28 5.32 o 4 0 4 60.16 55.04 2.15 o 5 0 4 3.95 4.71 1.52 o 6 0 4 41.07 34.88 3.35 o 7 0 4 14.54 13.62 4.00 o 0 1 4 156.90 160.09 2.66 o 1 1 4 1849.73 1727.53 15.64 o 2 1 4 242.26 248.37 2.82 o 3 1 4 521.96 557.93 6.66 o 4 1 4 75.66 81.01 2.41 o 5 1 4 165.30 172.14 3.35 o 6 1 4 62.76 62.61 2.81 o 7 1 4 11.59 19.93 3.51 o 0 2 4 5080.47 4800.17 150.70 o 1 2 4 2382.68 2243.25 20.73 o 2 2 4 1931.98 2003.66 19.99 o 3 2 4 557.54 595.21 7.00 o 4 2 4 20.80 19.84 1.38 o 5 2 4 58.76 51.98 1.90 o 6 2 4 65.70 61.08 4.05 o 7 2 4 11.20 7.18 2.90 o 0 3 4 1250.21 1154.07 24.76 o 1 3 4 22.74 16.69 0.54 o 2 3 4 562.12 621.79 6.74 o 3 3 4 106.30 127.97 2.09 o 4 3 4 61.71 65.97 3.10 o 5 3 4 3.76 4.16 1.25 o 6 3 4 107.68 115.57 3.84 o 7 3 4 103.31 110.44 9.73 o 0 4 4 863.36 856.37 10.37 o 1 4 4 65.77 62.05 1.17 o 2 4 4 813.00 811.79 8.27 o 3 4 4 324.06 329.82 5.39 o 4 4 4 194.84 200.29 3.33 o 5 4 4 3.68 2.85 1.18 o 6 4 4 46.98 47.77 3.05 o 7 4 4 42.31 59.46 4.18 o 0 5 4 406.61 445.17 6.09 o 1 5 4 33.12 31.05 0.79 o 2 5 4 71.97 70.25 1.54 o 3 5 4 24.93 24.09 1.19 o 4 5 4 2.06 0.15 0.87 o 5 5 4 66.78 61.72 2.05 o 6 5 4 1.27 3.56 2.12 o 0 6 4 37.30 43.60 1.21 o 1 6 4 864.50 897.20 8.05 o 2 6 4 120.28 147.35 2.13 o 3 6 4 216.82 225.07 3.41 o 4 6 4 271.37 271.82 4.37 o 5 6 4 32.32 32.78 1.86 o 6 6 4 19.32 23.86 2.85 o 0 7 4 92.99 90.09 4.20 o 1 7 4 854.43 892.95 9.36 o 2 7 4 339.74 362.82 5.67 o 3 7 4 72.51 69.40 1.77 o 4 7 4 198.49 196.19 3.44 o 5 7 4 111.61 105.86 2.76 o 6 7 4 35.78 28.41 4.05 o 0 8 4 1216.99 1270.95 41.85 o 1 8 4 309.81 323.47 3.88 o 2 8 4 329.51 356.23 4.10 o 3 8 4 23.29 20.12 1.12 o 4 8 4 59.66 63.76 1.78 o 5 8 4 15.97 15.24 1.83 o 6 8 4 13.02 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35.37 31.38 2.05 o 4 10 9 0.03 -1.08 1.08 o 5 10 9 9.15 17.00 4.00 o 0 11 9 18.02 18.44 1.33 o 1 11 9 137.10 134.55 2.16 o 2 11 9 130.16 123.94 2.43 o 3 11 9 37.40 35.92 1.96 o 4 11 9 7.20 10.88 1.65 o 5 11 9 4.34 4.86 3.06 o 0 12 9 1.61 0.72 1.53 o 1 12 9 55.15 49.40 1.38 o 2 12 9 74.78 80.71 3.35 o 3 12 9 56.90 56.56 2.32 o 4 12 9 38.56 36.24 2.53 o 0 13 9 55.03 62.12 3.96 o 1 13 9 111.82 102.92 3.29 o 2 13 9 40.70 36.16 1.90 o 3 13 9 49.83 48.70 2.29 o 4 13 9 8.22 3.32 2.80 o 0 14 9 30.54 27.63 2.86 o 1 14 9 101.07 105.70 3.10 o 2 14 9 6.84 7.34 0.98 o 3 14 9 24.84 23.89 2.26 o 4 14 9 1.75 -2.32 2.88 o 0 15 9 90.28 97.78 11.73 o 1 15 9 44.75 46.12 2.03 o 2 15 9 27.88 27.81 2.32 o 3 15 9 36.52 30.13 3.68 o 0 16 9 96.40 104.27 4.99 o 1 16 9 0.55 0.50 2.40 o 2 16 9 16.66 14.48 2.80 o 0 17 9 9.11 -2.79 3.97 o 1 17 9 4.87 7.34 2.69 o 0 0 10 108.17 108.95 5.13 o 1 0 10 30.48 30.90 1.98 o 2 0 10 143.06 124.54 2.67 o 3 0 10 89.87 92.37 2.88 o 4 0 10 37.06 31.57 1.72 o 5 0 10 0.17 0.85 2.32 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2.28 o 2 6 10 93.87 91.65 1.77 o 3 6 10 305.37 320.04 6.24 o 4 6 10 204.32 217.41 3.90 o 5 6 10 84.61 92.29 3.16 o 0 7 10 448.44 466.56 7.57 o 1 7 10 259.12 250.36 3.20 o 2 7 10 188.21 190.48 2.65 o 3 7 10 308.70 311.17 4.76 o 4 7 10 63.40 64.65 1.94 o 5 7 10 18.28 16.41 1.98 o 0 8 10 608.98 652.67 10.42 o 1 8 10 129.16 124.93 1.94 o 2 8 10 244.10 252.57 3.31 o 3 8 10 78.75 71.91 2.68 o 4 8 10 3.15 3.90 1.53 o 5 8 10 39.39 42.26 2.70 o 0 9 10 64.63 67.81 3.69 o 1 9 10 170.66 166.78 2.51 o 2 9 10 192.04 198.26 2.85 o 3 9 10 17.12 13.23 1.84 o 4 9 10 8.30 6.51 1.34 o 5 9 10 67.77 79.31 4.19 o 0 10 10 108.87 115.20 8.81 o 1 10 10 32.58 27.18 1.47 o 2 10 10 68.47 72.37 1.85 o 3 10 10 29.22 28.27 1.93 o 4 10 10 36.13 37.05 3.38 o 5 10 10 120.06 131.08 6.72 o 0 11 10 413.25 432.42 7.76 o 1 11 10 39.94 36.51 1.47 o 2 11 10 60.39 60.66 1.91 o 3 11 10 53.65 53.03 2.00 o 4 11 10 95.08 88.77 7.40 o 0 12 10 376.13 426.85 8.20 o 1 12 10 113.72 121.14 2.68 o 2 12 10 65.39 65.76 1.85 o 3 12 10 8.74 8.36 1.18 o 4 12 10 24.29 24.21 3.27 o 0 13 10 56.33 59.71 3.24 o 1 13 10 100.94 107.89 4.62 o 2 13 10 46.96 44.34 2.19 o 3 13 10 31.59 28.50 2.01 o 4 13 10 3.37 5.30 2.45 o 0 14 10 40.84 35.25 2.35 o 1 14 10 6.45 5.17 0.95 o 2 14 10 24.89 22.76 2.79 o 3 14 10 46.02 50.04 3.13 o 0 15 10 96.22 102.72 7.47 o 1 15 10 16.96 13.05 1.54 o 2 15 10 29.34 28.24 2.12 o 3 15 10 19.52 15.86 3.14 o 0 16 10 51.77 49.45 4.20 o 1 16 10 140.65 136.06 4.97 o 2 16 10 16.90 12.06 2.22 o 0 17 10 192.56 201.67 10.59 o 1 0 11 197.36 205.65 5.03 o 2 0 11 973.19 960.99 17.86 o 3 0 11 668.33 677.17 11.89 o 4 0 11 46.19 39.79 1.85 o 5 0 11 0.07 1.56 3.02 o 6 0 11 4.48 3.47 3.23 o 0 1 11 62.45 70.77 1.71 o 1 1 11 181.32 193.70 3.27 o 2 1 11 1483.31 1520.52 17.90 o 3 1 11 1016.35 1043.29 10.60 o 4 1 11 20.17 22.15 2.16 o 5 1 11 3.33 6.02 1.33 o 6 1 11 2.72 0.33 2.02 o 0 2 11 35.99 38.85 1.23 o 1 2 11 10.18 8.57 0.83 o 2 2 11 275.99 272.93 3.91 o 3 2 11 530.55 540.21 5.90 o 4 2 11 43.53 42.15 1.85 o 5 2 11 40.17 41.04 1.97 o 6 2 11 22.99 26.19 2.67 o 0 3 11 43.67 48.88 1.86 o 1 3 11 83.48 80.74 1.42 o 2 3 11 16.42 13.41 1.42 o 3 3 11 635.63 673.70 7.72 o 4 3 11 216.33 227.72 4.46 o 5 3 11 2.38 1.54 1.20 o 6 3 11 6.16 3.24 3.35 o 0 4 11 1.19 1.35 0.72 o 1 4 11 90.95 86.92 1.68 o 2 4 11 907.50 921.31 9.73 o 3 4 11 116.00 121.96 2.61 o 4 4 11 49.64 49.45 1.54 o 5 4 11 11.50 11.70 1.93 o 0 5 11 88.47 97.31 2.15 o 1 5 11 586.69 578.93 6.19 o 2 5 11 1440.34 1507.24 15.57 o 3 5 11 485.64 504.23 6.02 o 4 5 11 40.82 42.77 1.53 o 5 5 11 0.05 3.85 1.47 o 0 6 11 190.12 192.50 3.61 o 1 6 11 26.10 24.14 0.75 o 2 6 11 92.62 96.35 1.72 o 3 6 11 89.39 90.17 1.99 o 4 6 11 141.11 137.25 2.84 o 5 6 11 15.30 10.81 2.05 o 0 7 11 8.85 7.94 0.90 o 1 7 11 126.62 127.00 1.94 o 2 7 11 24.87 26.12 1.13 o 3 7 11 39.18 40.66 1.37 o 4 7 11 361.58 382.09 6.99 o 5 7 11 12.46 9.53 1.92 o 0 8 11 8.38 9.69 0.99 o 1 8 11 349.47 362.27 4.76 o 2 8 11 17.72 15.42 0.80 o 3 8 11 164.08 168.48 3.06 o 4 8 11 140.61 148.79 6.94 o 5 8 11 49.02 46.92 3.17 o 0 9 11 196.23 216.26 5.48 o 1 9 11 608.48 640.55 8.04 o 2 9 11 13.97 9.87 0.93 o 3 9 11 129.99 122.73 3.63 o 4 9 11 164.08 155.02 8.08 o 5 9 11 72.42 79.70 6.18 o 0 10 11 26.01 24.70 1.33 o 1 10 11 371.80 388.88 6.42 o 2 10 11 88.31 87.96 1.88 o 3 10 11 50.11 47.40 1.58 o 4 10 11 7.20 3.87 3.03 o 0 11 11 88.76 87.30 4.05 o 1 11 11 11.87 11.52 2.16 o 2 11 11 123.97 115.77 2.54 o 3 11 11 0.01 -0.42 1.02 o 4 11 11 48.24 40.55 3.79 o 0 12 11 108.33 116.35 3.31 o 1 12 11 110.01 111.72 4.35 o 2 12 11 15.69 16.50 1.32 o 3 12 11 16.19 14.89 1.63 o 4 12 11 100.07 105.47 6.59 o 0 13 11 819.66 896.39 14.35 o 1 13 11 56.17 63.77 1.81 o 2 13 11 25.19 22.12 2.16 o 3 13 11 0.32 3.62 1.86 o 0 14 11 91.85 88.27 6.07 o 1 14 11 110.66 108.36 4.04 o 2 14 11 56.90 53.78 3.26 o 3 14 11 6.36 6.62 2.53 o 0 15 11 5.40 7.35 2.02 o 1 15 11 48.31 45.90 2.39 o 2 15 11 5.63 6.17 3.21 o 0 16 11 52.82 50.47 5.14 o 1 16 11 59.57 50.99 3.54 o 0 0 12 1012.52 1032.65 28.77 o 1 0 12 11.33 16.80 1.17 o 2 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4 6 12 94.69 92.60 2.21 o 5 6 12 16.81 19.82 3.02 o 0 7 12 68.10 70.10 2.10 o 1 7 12 780.30 823.52 9.08 o 2 7 12 412.04 425.08 5.15 o 3 7 12 29.82 29.62 2.28 o 4 7 12 101.40 102.79 4.50 o 5 7 12 0.91 0.64 3.97 o 0 8 12 35.71 35.13 1.51 o 1 8 12 127.90 135.45 3.09 o 2 8 12 95.95 93.35 1.91 o 3 8 12 2.95 1.18 1.23 o 4 8 12 40.16 44.14 2.09 o 5 8 12 15.10 14.96 2.71 o 0 9 12 16.38 18.90 1.98 o 1 9 12 23.44 24.12 1.04 o 2 9 12 5.56 6.49 0.79 o 3 9 12 14.78 14.09 1.07 o 4 9 12 77.96 78.49 5.71 o 0 10 12 226.37 243.59 5.40 o 1 10 12 69.47 71.94 1.73 o 2 10 12 30.32 30.40 1.84 o 3 10 12 32.23 28.23 1.33 o 4 10 12 114.57 112.40 4.42 o 0 11 12 319.77 357.03 6.92 o 1 11 12 188.31 202.11 3.49 o 2 11 12 7.09 7.12 1.07 o 3 11 12 38.96 41.44 2.28 o 4 11 12 25.01 29.82 2.69 o 0 12 12 53.47 56.47 2.22 o 1 12 12 84.72 85.25 3.40 o 2 12 12 12.53 13.96 1.80 o 3 12 12 23.00 26.37 2.84 o 0 13 12 44.80 46.95 3.13 o 1 13 12 113.10 110.82 2.50 o 2 13 12 12.45 13.12 2.34 o 3 13 12 11.41 8.84 1.97 o 0 14 12 182.22 198.87 5.90 o 1 14 12 85.23 77.97 3.30 o 2 14 12 13.27 11.38 2.01 o 0 15 12 27.69 32.36 5.80 o 1 15 12 117.98 115.95 4.07 o 1 0 13 35.72 34.91 1.59 o 2 0 13 7.36 8.99 2.92 o 3 0 13 92.39 94.05 3.57 o 4 0 13 1.79 -0.03 0.96 o 5 0 13 26.36 24.38 5.13 o 0 1 13 37.42 43.42 2.31 o 1 1 13 28.81 30.91 1.61 o 2 1 13 29.31 27.18 1.44 o 3 1 13 160.97 149.46 2.71 o 4 1 13 18.72 17.19 1.30 o 5 1 13 3.85 2.39 2.34 o 0 2 13 0.00 -0.90 1.27 o 1 2 13 41.57 43.55 1.47 o 2 2 13 62.14 63.03 1.98 o 3 2 13 101.30 100.46 2.00 o 4 2 13 29.99 29.36 1.81 o 5 2 13 27.90 30.13 3.10 o 0 3 13 15.51 16.21 1.91 o 1 3 13 19.03 19.96 1.10 o 2 3 13 51.91 49.12 1.59 o 3 3 13 106.54 104.30 3.13 o 4 3 13 0.64 1.44 0.98 o 5 3 13 14.12 20.06 3.11 o 0 4 13 297.58 302.08 9.59 o 1 4 13 66.76 67.17 1.38 o 2 4 13 99.32 100.97 2.07 o 3 4 13 3.70 2.03 0.89 o 4 4 13 73.29 70.58 2.09 o 5 4 13 9.78 12.47 3.07 o 0 5 13 23.10 22.84 1.06 o 1 5 13 78.77 71.12 1.85 o 2 5 13 25.09 26.35 1.13 o 3 5 13 67.35 66.15 1.35 o 4 5 13 71.55 65.98 3.48 o 5 5 13 9.49 8.60 3.03 o 0 6 13 34.15 34.94 4.17 o 1 6 13 40.97 37.93 1.55 o 2 6 13 11.65 12.71 0.94 o 3 6 13 35.34 36.64 1.94 o 4 6 13 19.70 17.56 1.77 o 5 6 13 16.74 13.30 5.21 o 0 7 13 90.05 94.68 7.10 o 1 7 13 42.70 44.42 1.45 o 2 7 13 79.62 86.05 3.14 o 3 7 13 69.59 68.15 2.63 o 4 7 13 19.25 18.89 2.09 o 0 8 13 0.02 0.10 1.17 o 1 8 13 167.61 175.72 3.26 o 2 8 13 56.34 54.08 1.40 o 3 8 13 70.46 74.46 3.08 o 4 8 13 8.65 4.60 2.06 o 0 9 13 215.99 225.99 5.66 o 1 9 13 29.60 27.85 1.45 o 2 9 13 46.48 43.02 1.85 o 3 9 13 0.68 0.14 2.05 o 4 9 13 10.62 14.78 2.59 o 0 10 13 24.92 21.56 1.59 o 1 10 13 6.04 5.99 0.86 o 2 10 13 51.58 49.91 1.86 o 3 10 13 5.10 5.03 1.26 o 4 10 13 17.10 19.26 2.15 o 0 11 13 193.84 208.74 8.54 o 1 11 13 15.78 13.63 0.96 o 2 11 13 8.76 6.71 1.36 o 3 11 13 9.83 9.31 1.63 o 0 12 13 15.05 14.55 1.54 o 1 12 13 12.24 10.99 1.17 o 2 12 13 29.84 29.80 1.68 o 3 12 13 3.88 6.05 1.67 o 0 13 13 42.56 36.93 4.44 o 1 13 13 57.27 59.19 2.04 o 2 13 13 10.52 10.23 2.39 o 0 14 13 1.39 2.29 2.30 o 1 14 13 50.11 43.48 2.75 o 2 14 13 16.30 21.90 2.71 o 0 15 13 70.77 69.99 7.72 o 0 0 14 293.15 273.64 13.85 o 1 0 14 9.79 4.71 2.20 o 2 0 14 9.48 10.14 1.92 o 3 0 14 262.61 271.42 16.25 o 4 0 14 164.53 162.90 5.85 o 5 0 14 0.44 3.98 3.43 o 0 1 14 19.14 17.21 1.93 o 1 1 14 136.52 133.34 2.51 o 2 1 14 118.75 133.55 4.63 o 3 1 14 45.90 46.91 3.35 o 4 1 14 1.37 0.92 1.63 o 5 1 14 51.51 47.60 4.60 o 0 2 14 65.35 58.63 1.67 o 1 2 14 222.72 216.20 4.85 o 2 2 14 82.22 81.78 2.41 o 3 2 14 112.65 117.37 3.18 o 4 2 14 54.37 54.61 3.09 o 5 2 14 0.33 -1.48 2.45 o 0 3 14 51.99 43.88 2.93 o 1 3 14 12.11 8.94 0.76 o 2 3 14 68.26 71.54 2.41 o 3 3 14 23.18 22.34 1.03 o 4 3 14 21.54 23.69 2.80 o 5 3 14 36.98 43.92 4.49 o 0 4 14 0.16 0.45 1.59 o 1 4 14 56.42 51.56 1.94 o 2 4 14 81.30 77.98 1.99 o 3 4 14 46.92 48.52 1.71 o 4 4 14 55.60 57.92 2.91 o 5 4 14 19.06 29.99 3.80 o 0 5 14 1.18 0.43 0.86 o 1 5 14 275.25 276.92 4.45 o 2 5 14 133.31 128.15 2.47 o 3 5 14 29.38 27.98 1.47 o 4 5 14 34.69 37.50 3.69 o 0 6 14 85.40 80.74 2.54 o 1 6 14 38.14 40.79 1.40 o 2 6 14 3.61 4.51 0.91 o 3 6 14 204.26 215.20 4.12 o 4 6 14 14.20 13.90 2.41 o 0 7 14 34.58 34.58 3.38 o 1 7 14 120.30 110.25 2.25 o 2 7 14 99.60 97.47 2.29 o 3 7 14 11.19 11.95 1.18 o 4 7 14 13.90 19.97 3.14 o 0 8 14 67.84 65.44 5.84 o 1 8 14 1.08 -0.02 0.54 o 2 8 14 6.08 7.00 0.79 o 3 8 14 33.07 35.73 2.75 o 4 8 14 25.16 28.55 3.17 o 0 9 14 30.90 29.45 2.45 o 1 9 14 36.04 36.81 1.16 o 2 9 14 0.59 0.42 1.26 o 3 9 14 17.32 18.67 1.73 o 4 9 14 74.04 75.59 4.46 o 0 10 14 64.93 71.41 4.33 o 1 10 14 6.12 5.29 0.89 o 2 10 14 48.52 47.24 1.96 o 3 10 14 11.25 8.45 1.74 o 0 11 14 15.08 15.53 1.70 o 1 11 14 27.45 28.67 1.36 o 2 11 14 31.11 32.65 2.56 o 3 11 14 8.74 7.13 2.28 o 0 12 14 5.10 6.31 1.55 o 1 12 14 23.92 22.23 1.85 o 2 12 14 1.38 3.23 2.79 o 0 13 14 1.63 2.88 2.35 o 1 13 14 23.41 24.28 1.97 o 2 13 14 36.90 34.53 4.07 o 0 14 14 11.54 11.99 3.02 o 1 0 15 2.03 2.14 0.86 o 2 0 15 7.62 6.63 1.43 o 3 0 15 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