#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:31:49 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181062 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/42/2214203.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214203_Fobs loop_ _publ_author_name 'Ma\/lecki, Jan Grzegorz' 'Kruszynski, Rafal' 'Kusz, Joachim' _publ_section_title ; The orthorhombic polymorph of pyrazine-2-carboxylic acid revisited ; _journal_coeditor_code GK2089 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3300 _journal_volume 63 _journal_year 2007 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.3261 _cell_length_b 6.3180 _cell_length_c 7.3389 _exptl_crystal_F_000 256.00 _reflns_d_resolution_high 0.8112 _cod_data_source_file gk2089Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ch07mg1_ in Pna2(1) converted to Pnma (by P)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 174.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 45.43 49.04 1.91 o 4 0 0 308.96 278.65 4.53 o 6 0 0 162.00 160.81 4.46 o 8 0 0 0.04 0.15 3.37 o 10 0 0 6.64 6.02 4.20 o 12 0 0 5.47 5.34 4.75 o 2 1 0 78.34 68.57 1.16 o 4 1 0 134.25 161.95 2.20 o 6 1 0 2.42 1.99 1.36 o 8 1 0 4.35 3.79 2.43 o 10 1 0 1641.95 1628.19 18.97 o 12 1 0 3.20 4.32 3.52 o 0 2 0 30491.71 28177.76 101.19 o 2 2 0 37.54 37.61 1.51 o 4 2 0 169.67 166.49 2.05 o 6 2 0 93.79 90.80 2.32 o 8 2 0 0.84 0.47 1.87 o 10 2 0 6.78 7.34 2.96 o 12 2 0 4.54 4.44 4.13 o 2 3 0 14.66 18.58 1.64 o 4 3 0 60.20 64.94 1.98 o 6 3 0 1.34 2.50 2.09 o 8 3 0 2.67 0.88 2.35 o 10 3 0 1043.96 1087.57 13.04 o 12 3 0 2.19 5.81 5.49 o 0 4 0 6591.46 6545.42 35.62 o 2 4 0 11.27 10.25 1.79 o 4 4 0 48.16 53.20 2.22 o 6 4 0 20.91 17.90 2.33 o 8 4 0 4.99 3.89 2.26 o 10 4 0 6.36 5.90 3.54 o 2 5 0 10.78 9.42 2.12 o 4 5 0 18.15 14.92 2.31 o 6 5 0 1.18 1.23 2.45 o 8 5 0 1.15 0.76 2.79 o 10 5 0 481.81 532.42 7.28 o 0 6 0 1505.17 1510.00 25.82 o 2 6 0 1.91 0.00 3.00 o 4 6 0 13.10 9.38 3.15 o 6 6 0 1.86 0.00 3.30 o 8 6 0 7.73 5.46 3.86 o 2 7 0 8.96 5.77 3.47 o 4 7 0 5.48 2.22 4.31 o 6 7 0 0.76 0.00 4.81 o 1 0 1 2104.81 1918.78 25.97 o 2 0 1 1368.39 1261.04 7.67 o 3 0 1 53.47 52.38 1.69 o 4 0 1 1022.49 947.80 4.74 o 5 0 1 980.21 997.96 5.12 o 6 0 1 4.40 5.11 1.34 o 7 0 1 9.88 7.37 1.40 o 8 0 1 634.03 628.80 6.72 o 9 0 1 339.95 324.23 5.29 o 10 0 1 28.30 30.75 3.20 o 11 0 1 0.05 0.00 3.49 o 12 0 1 0.46 3.67 4.75 o 13 0 1 42.09 44.34 4.92 o 0 1 1 176.35 165.62 2.66 o 1 1 1 1472.49 1320.17 4.10 o 2 1 1 1496.11 1310.18 3.36 o 3 1 1 271.72 268.64 1.81 o 4 1 1 201.06 204.53 1.80 o 5 1 1 1145.02 1135.33 4.47 o 6 1 1 441.23 449.83 3.18 o 7 1 1 50.48 47.14 1.80 o 8 1 1 119.25 111.21 2.18 o 9 1 1 478.46 464.13 4.64 o 10 1 1 230.57 234.16 3.85 o 11 1 1 11.88 11.09 2.46 o 12 1 1 10.13 11.16 2.66 o 13 1 1 0.37 3.03 3.91 o 1 2 1 1040.80 1025.38 3.32 o 2 2 1 724.70 682.95 3.58 o 3 2 1 33.23 28.01 0.98 o 4 2 1 579.89 557.14 2.74 o 5 2 1 606.19 609.31 3.02 o 6 2 1 2.63 3.60 1.19 o 7 2 1 5.52 3.65 1.49 o 8 2 1 470.73 489.65 5.33 o 9 2 1 261.73 257.40 3.30 o 10 2 1 20.32 19.14 2.33 o 11 2 1 0.01 0.00 2.44 o 12 2 1 0.47 1.88 2.90 o 13 2 1 33.65 36.16 3.46 o 0 3 1 64.16 60.22 1.83 o 1 3 1 403.41 404.08 2.41 o 2 3 1 449.58 428.02 2.89 o 3 3 1 92.98 93.78 1.54 o 4 3 1 67.65 71.02 1.34 o 5 3 1 471.86 475.77 2.83 o 6 3 1 199.45 211.76 2.22 o 7 3 1 21.92 22.17 1.47 o 8 3 1 52.98 49.61 2.10 o 9 3 1 296.33 308.40 3.72 o 10 3 1 138.02 143.70 3.86 o 11 3 1 10.08 10.48 2.90 o 12 3 1 8.37 6.95 3.15 o 1 4 1 286.73 304.83 2.83 o 2 4 1 184.44 182.76 2.56 o 3 4 1 6.59 6.33 1.58 o 4 4 1 169.62 170.29 2.35 o 5 4 1 192.46 198.88 2.42 o 6 4 1 0.82 1.96 1.47 o 7 4 1 0.71 0.02 1.67 o 8 4 1 227.17 243.55 3.59 o 9 4 1 134.51 139.04 3.21 o 10 4 1 8.34 7.47 2.40 o 11 4 1 0.38 1.39 2.94 o 0 5 1 8.13 8.33 1.82 o 1 5 1 105.28 107.54 2.24 o 2 5 1 100.42 102.52 2.42 o 3 5 1 19.10 18.96 1.90 o 4 5 1 14.12 15.32 1.91 o 5 5 1 129.98 133.17 2.83 o 6 5 1 59.13 61.09 2.16 o 7 5 1 5.12 3.70 1.97 o 8 5 1 12.71 12.89 2.11 o 9 5 1 136.11 144.46 3.57 o 10 5 1 57.20 56.05 3.37 o 1 6 1 93.07 94.26 3.05 o 2 6 1 43.46 43.43 2.64 o 3 6 1 0.21 0.00 3.10 o 4 6 1 46.53 41.93 2.70 o 5 6 1 49.16 50.44 2.52 o 6 6 1 0.15 0.00 2.47 o 7 6 1 0.03 0.00 3.99 o 8 6 1 87.62 90.45 3.32 o 0 7 1 0.42 0.34 3.97 o 1 7 1 34.30 27.75 3.09 o 2 7 1 24.52 19.57 3.04 o 3 7 1 3.00 1.41 2.97 o 4 7 1 2.80 2.07 3.04 o 5 7 1 33.38 31.19 3.31 o 0 0 2 24.87 17.46 1.50 o 1 0 2 229.94 234.11 4.44 o 2 0 2 318.74 321.96 2.78 o 3 0 2 367.76 358.20 4.40 o 4 0 2 266.68 299.55 3.30 o 5 0 2 184.14 209.46 3.07 o 6 0 2 393.96 437.96 4.35 o 7 0 2 59.63 68.17 2.48 o 8 0 2 45.52 42.87 2.34 o 9 0 2 265.19 237.73 5.94 o 10 0 2 42.34 41.74 3.80 o 11 0 2 7.46 4.11 3.64 o 12 0 2 69.27 64.48 4.77 o 13 0 2 103.16 120.44 5.86 o 1 1 2 20.72 19.11 1.21 o 2 1 2 318.08 317.24 2.21 o 3 1 2 1879.42 1857.35 5.04 o 4 1 2 637.45 671.46 3.22 o 5 1 2 0.38 0.39 1.16 o 6 1 2 60.83 57.61 1.52 o 7 1 2 0.39 1.81 1.33 o 8 1 2 3.75 1.64 1.40 o 9 1 2 4.87 4.86 1.78 o 10 1 2 20.11 19.49 2.47 o 11 1 2 64.51 66.32 3.18 o 12 1 2 41.81 48.97 3.26 o 13 1 2 40.66 36.77 3.44 o 0 2 2 8.05 5.39 1.56 o 1 2 2 139.08 141.15 1.89 o 2 2 2 188.13 186.94 1.77 o 3 2 2 226.90 226.09 1.78 o 4 2 2 163.46 179.49 1.76 o 5 2 2 125.56 141.94 1.90 o 6 2 2 263.56 284.41 2.69 o 7 2 2 38.84 42.21 1.63 o 8 2 2 35.45 33.28 2.00 o 9 2 2 212.91 203.83 3.48 o 10 2 2 37.18 37.32 2.71 o 11 2 2 5.40 3.04 2.64 o 12 2 2 53.13 54.47 3.35 o 13 2 2 82.81 92.42 4.00 o 1 3 2 8.88 11.47 1.26 o 2 3 2 113.25 109.38 1.65 o 3 3 2 684.52 657.69 3.55 o 4 3 2 270.13 286.02 2.32 o 5 3 2 1.47 2.99 1.17 o 6 3 2 32.73 33.88 1.58 o 7 3 2 0.06 0.12 1.50 o 8 3 2 4.86 1.66 1.86 o 9 3 2 3.91 4.60 2.13 o 10 3 2 13.32 14.24 2.70 o 11 3 2 37.06 38.51 3.15 o 12 3 2 26.02 31.34 3.39 o 0 4 2 0.41 0.00 1.91 o 1 4 2 41.72 41.74 1.64 o 2 4 2 44.63 45.34 1.68 o 3 4 2 74.72 76.04 1.94 o 4 4 2 48.53 48.89 1.97 o 5 4 2 62.18 61.67 1.84 o 6 4 2 103.01 105.18 2.28 o 7 4 2 12.35 12.17 1.89 o 8 4 2 19.28 17.87 2.32 o 9 4 2 120.56 120.74 3.55 o 10 4 2 25.50 18.94 2.97 o 11 4 2 2.15 2.34 3.60 o 1 5 2 8.19 7.49 1.54 o 2 5 2 23.60 21.46 2.00 o 3 5 2 154.38 153.86 3.05 o 4 5 2 87.82 90.19 2.67 o 5 5 2 4.34 4.43 1.93 o 6 5 2 13.43 15.96 2.03 o 7 5 2 0.01 0.00 2.20 o 8 5 2 4.89 2.35 2.60 o 9 5 2 2.53 2.26 2.82 o 10 5 2 6.72 3.05 3.43 o 0 6 2 0.01 3.23 3.40 o 1 6 2 9.95 7.87 2.49 o 2 6 2 5.80 6.13 2.50 o 3 6 2 21.07 19.33 2.63 o 4 6 2 10.97 6.46 2.32 o 5 6 2 30.42 26.58 2.57 o 6 6 2 34.02 30.83 2.69 o 7 6 2 2.22 1.97 3.38 o 8 6 2 8.45 8.36 3.30 o 1 7 2 6.09 2.31 2.93 o 2 7 2 3.84 2.22 3.24 o 3 7 2 30.63 32.40 3.20 o 4 7 2 28.25 24.76 3.22 o 5 7 2 4.24 3.29 3.65 o 1 0 3 5.75 3.93 1.37 o 2 0 3 27.04 26.40 1.51 o 3 0 3 137.23 144.59 2.66 o 4 0 3 119.62 118.10 2.34 o 5 0 3 6.10 11.80 1.53 o 6 0 3 98.57 107.46 2.88 o 7 0 3 257.59 253.66 3.36 o 8 0 3 0.05 0.40 2.16 o 9 0 3 136.83 130.25 3.54 o 10 0 3 205.19 175.07 5.43 o 11 0 3 76.73 77.94 4.70 o 12 0 3 21.83 23.17 4.28 o 13 0 3 150.31 187.19 6.83 o 0 1 3 2342.01 2396.87 11.88 o 1 1 3 1.06 1.28 1.12 o 2 1 3 206.38 201.95 2.07 o 3 1 3 0.44 0.54 0.92 o 4 1 3 505.42 520.29 3.06 o 5 1 3 10.93 12.92 1.30 o 6 1 3 80.13 84.28 1.86 o 7 1 3 1.09 1.61 1.24 o 8 1 3 0.47 0.63 1.59 o 9 1 3 21.76 18.03 2.04 o 10 1 3 21.23 19.98 2.57 o 11 1 3 10.05 6.11 2.65 o 12 1 3 3.18 2.56 2.98 o 13 1 3 5.74 3.73 3.44 o 1 2 3 2.24 1.88 1.01 o 2 2 3 14.40 12.47 0.98 o 3 2 3 78.58 80.79 1.78 o 4 2 3 82.72 83.60 1.86 o 5 2 3 6.16 8.38 1.24 o 6 2 3 66.47 71.11 1.86 o 7 2 3 172.01 174.93 2.52 o 8 2 3 0.03 0.00 1.81 o 9 2 3 104.56 100.68 2.57 o 10 2 3 167.99 160.98 3.45 o 11 2 3 60.57 58.82 2.91 o 12 2 3 17.23 18.52 3.21 o 0 3 3 953.55 1003.36 6.59 o 1 3 3 0.44 0.00 1.30 o 2 3 3 85.05 81.89 1.57 o 3 3 3 0.14 0.14 1.19 o 4 3 3 222.36 229.25 2.43 o 5 3 3 3.00 2.04 1.17 o 6 3 3 46.74 48.99 1.75 o 7 3 3 0.08 0.00 1.67 o 8 3 3 0.00 0.57 1.92 o 9 3 3 11.83 7.08 2.78 o 10 3 3 12.65 15.40 2.82 o 11 3 3 8.00 1.99 3.38 o 12 3 3 1.50 1.77 4.28 o 1 4 3 0.08 1.22 1.49 o 2 4 3 0.59 0.24 1.47 o 3 4 3 15.98 16.62 1.56 o 4 4 3 39.00 39.30 1.81 o 5 4 3 6.96 8.07 1.74 o 6 4 3 23.56 24.34 2.22 o 7 4 3 57.76 56.30 2.95 o 8 4 3 0.01 0.00 2.80 o 9 4 3 51.03 51.34 3.45 o 10 4 3 96.86 91.34 4.08 o 11 4 3 31.87 27.95 3.89 o 0 5 3 303.96 317.75 5.85 o 1 5 3 0.25 0.09 1.67 o 2 5 3 24.41 25.60 1.87 o 3 5 3 2.76 2.09 1.99 o 4 5 3 62.80 62.32 2.33 o 5 5 3 0.08 0.46 2.21 o 6 5 3 20.39 21.44 2.34 o 7 5 3 0.16 2.60 2.55 o 8 5 3 0.24 0.00 2.70 o 9 5 3 4.05 0.00 2.96 o 1 6 3 1.42 1.02 2.51 o 2 6 3 1.02 0.07 2.54 o 3 6 3 1.02 0.93 2.35 o 4 6 3 16.53 14.63 2.77 o 5 6 3 6.25 1.57 2.63 o 6 6 3 5.69 5.51 2.80 o 7 6 3 12.37 8.99 3.25 o 0 7 3 96.12 93.53 5.79 o 1 7 3 0.10 1.04 3.09 o 2 7 3 6.12 4.87 3.48 o 3 7 3 3.45 3.27 3.60 o 4 7 3 15.03 10.28 3.80 o 0 0 4 96.37 88.64 3.74 o 1 0 4 74.71 96.37 2.32 o 2 0 4 442.61 455.12 7.66 o 3 0 4 30.20 27.63 1.54 o 4 0 4 21.48 18.41 1.63 o 5 0 4 487.21 473.95 4.41 o 6 0 4 15.77 15.33 1.77 o 7 0 4 9.35 6.48 1.97 o 8 0 4 0.00 0.35 2.34 o 9 0 4 131.42 117.15 4.44 o 10 0 4 4.40 2.81 3.50 o 11 0 4 57.93 47.54 4.44 o 12 0 4 29.14 32.02 4.55 o 1 1 4 991.03 1087.30 4.72 o 2 1 4 39.89 39.58 1.49 o 3 1 4 20.00 23.80 1.47 o 4 1 4 127.21 125.53 2.28 o 5 1 4 10.25 9.55 1.37 o 6 1 4 168.46 165.76 2.39 o 7 1 4 107.46 112.22 2.13 o 8 1 4 146.18 136.38 2.43 o 9 1 4 0.17 0.37 1.83 o 10 1 4 9.08 3.81 2.89 o 11 1 4 38.86 33.94 3.44 o 12 1 4 1.16 1.94 3.63 o 0 2 4 63.03 61.89 3.08 o 1 2 4 53.97 69.28 1.90 o 2 2 4 288.62 305.11 2.87 o 3 2 4 18.40 17.37 1.56 o 4 2 4 17.99 16.95 1.63 o 5 2 4 361.11 360.68 3.47 o 6 2 4 12.48 12.05 1.82 o 7 2 4 7.79 5.09 1.81 o 8 2 4 0.02 0.00 2.39 o 9 2 4 100.62 94.82 2.93 o 10 2 4 3.50 4.12 3.02 o 11 2 4 46.10 40.67 3.62 o 12 2 4 25.69 24.67 3.87 o 1 3 4 437.44 463.02 3.07 o 2 3 4 22.31 23.84 1.76 o 3 3 4 6.72 6.87 1.62 o 4 3 4 70.38 70.80 2.15 o 5 3 4 9.66 9.79 1.76 o 6 3 4 92.69 94.26 2.44 o 7 3 4 49.35 49.79 2.45 o 8 3 4 94.74 94.17 3.53 o 9 3 4 0.99 0.00 2.92 o 10 3 4 5.94 5.59 2.89 o 11 3 4 27.31 22.64 3.64 o 0 4 4 22.48 24.33 2.47 o 1 4 4 30.71 31.58 1.82 o 2 4 4 103.12 103.84 2.11 o 3 4 4 4.50 3.67 1.69 o 4 4 4 12.86 12.97 1.93 o 5 4 4 174.54 180.61 3.41 o 6 4 4 7.00 5.58 2.21 o 7 4 4 4.85 2.47 2.56 o 8 4 4 0.16 1.75 3.05 o 9 4 4 48.76 49.05 3.63 o 10 4 4 1.97 1.81 3.62 o 1 5 4 123.47 128.57 2.69 o 2 5 4 10.44 8.05 2.09 o 3 5 4 0.82 0.31 2.15 o 4 5 4 30.65 26.76 2.67 o 5 5 4 7.89 4.63 2.38 o 6 5 4 34.39 34.86 2.52 o 7 5 4 11.68 11.70 2.79 o 8 5 4 44.39 46.45 3.21 o 0 6 4 6.50 6.27 10.25 o 1 6 4 16.67 11.55 3.11 o 2 6 4 29.86 25.19 3.29 o 3 6 4 0.34 0.50 3.37 o 4 6 4 7.80 3.66 2.89 o 5 6 4 69.00 70.84 3.51 o 6 6 4 3.24 1.66 3.62 o 1 0 5 307.33 322.40 5.85 o 2 0 5 0.32 0.20 1.59 o 3 0 5 126.58 117.89 3.89 o 4 0 5 759.62 718.45 8.55 o 5 0 5 459.30 445.88 11.43 o 6 0 5 268.62 280.89 4.08 o 7 0 5 14.26 18.78 2.24 o 8 0 5 5.59 5.73 2.69 o 9 0 5 161.35 162.71 5.36 o 10 0 5 16.21 9.78 5.27 o 11 0 5 15.29 10.77 5.69 o 0 1 5 17.39 17.28 3.07 o 1 1 5 283.43 306.70 3.49 o 2 1 5 31.71 30.50 1.61 o 3 1 5 4.74 4.28 1.55 o 4 1 5 70.49 71.34 2.17 o 5 1 5 82.87 82.74 2.69 o 6 1 5 461.66 471.55 4.97 o 7 1 5 55.49 58.27 2.45 o 8 1 5 28.37 21.06 2.29 o 9 1 5 69.16 59.88 2.68 o 10 1 5 7.24 9.19 3.12 o 11 1 5 9.36 9.33 3.52 o 1 2 5 209.20 220.22 3.73 o 2 2 5 0.29 0.38 1.46 o 3 2 5 100.03 93.31 2.22 o 4 2 5 588.52 594.48 6.11 o 5 2 5 349.85 357.39 5.20 o 6 2 5 208.24 219.56 3.36 o 7 2 5 9.48 10.70 2.27 o 8 2 5 4.34 3.31 2.65 o 9 2 5 126.83 130.15 3.36 o 10 2 5 13.52 9.17 3.02 o 11 2 5 13.13 13.51 3.77 o 0 3 5 10.31 8.28 2.10 o 1 3 5 144.87 156.91 2.86 o 2 3 5 14.27 15.08 2.19 o 3 3 5 2.94 2.52 1.96 o 4 3 5 34.82 35.59 2.02 o 5 3 5 56.96 55.79 2.26 o 6 3 5 296.32 317.30 3.85 o 7 3 5 38.97 42.70 2.76 o 8 3 5 18.69 16.49 2.99 o 9 3 5 42.54 41.30 3.94 o 10 3 5 3.82 4.48 3.66 o 1 4 5 76.89 81.83 2.39 o 2 4 5 0.33 1.12 2.04 o 3 4 5 56.01 58.79 2.58 o 4 4 5 312.10 334.48 6.89 o 5 4 5 174.23 183.97 4.71 o 6 4 5 107.52 115.38 3.62 o 7 4 5 2.99 2.96 2.74 o 8 4 5 2.21 3.23 3.31 o 9 4 5 65.18 64.83 3.96 o 0 5 5 4.57 0.54 3.62 o 1 5 5 50.03 52.14 2.93 o 2 5 5 3.71 3.11 2.35 o 3 5 5 1.40 1.85 2.36 o 4 5 5 10.75 11.12 2.74 o 5 5 5 30.24 27.75 2.95 o 6 5 5 140.03 143.19 4.16 o 7 5 5 20.38 23.20 3.39 o 1 6 5 19.66 23.32 4.06 o 2 6 5 0.47 0.00 5.39 o 3 6 5 25.08 20.27 3.52 o 4 6 5 133.48 137.56 4.25 o 0 0 6 203.81 177.25 9.41 o 1 0 6 1.75 3.47 2.73 o 2 0 6 151.76 162.58 5.06 o 3 0 6 185.02 187.86 8.41 o 4 0 6 822.50 828.56 9.27 o 5 0 6 113.01 114.05 4.43 o 6 0 6 133.53 135.63 4.25 o 7 0 6 17.42 18.00 3.07 o 8 0 6 2.51 3.32 3.75 o 9 0 6 1.69 2.03 4.01 o 10 0 6 17.07 21.83 5.77 o 1 1 6 0.04 1.33 1.93 o 2 1 6 0.43 1.61 2.66 o 3 1 6 4.98 5.33 2.08 o 4 1 6 283.32 279.74 4.16 o 5 1 6 163.08 164.35 3.57 o 6 1 6 261.98 268.93 4.03 o 7 1 6 59.87 58.96 2.72 o 8 1 6 0.00 1.39 2.68 o 9 1 6 6.88 6.22 2.96 o 10 1 6 46.05 51.04 4.51 o 0 2 6 156.14 148.91 4.70 o 1 2 6 1.27 0.33 2.03 o 2 2 6 113.45 121.55 3.12 o 3 2 6 151.93 155.25 3.10 o 4 2 6 627.77 651.26 6.15 o 5 2 6 91.88 90.80 3.10 o 6 2 6 114.60 118.39 3.39 o 7 2 6 13.94 11.33 2.97 o 8 2 6 2.35 5.35 3.13 o 9 2 6 1.33 1.99 3.12 o 1 3 6 0.01 0.06 2.23 o 2 3 6 0.90 2.36 2.10 o 3 3 6 2.36 1.50 2.28 o 4 3 6 189.04 187.80 3.60 o 5 3 6 106.41 105.88 3.48 o 6 3 6 164.11 169.82 5.60 o 7 3 6 40.13 34.70 4.68 o 8 3 6 0.01 0.00 4.47 o 0 4 6 79.33 84.71 4.72 o 1 4 6 0.52 0.00 2.50 o 2 4 6 53.50 57.73 3.09 o 3 4 6 90.77 91.16 3.45 o 4 4 6 305.64 334.02 4.99 o 5 4 6 53.11 54.76 3.25 o 6 4 6 74.25 68.59 3.45 o 7 4 6 7.61 5.67 4.09 o 1 5 6 0.15 2.36 3.17 o 2 5 6 1.13 0.00 3.26 o 3 5 6 0.61 0.61 3.32 o 4 5 6 93.80 86.14 4.18 o 5 5 6 50.85 44.48 4.24 o 1 0 7 31.90 24.01 4.16 o 2 0 7 28.65 28.01 4.17 o 3 0 7 206.97 203.88 6.10 o 4 0 7 0.05 0.14 3.03 o 5 0 7 5.40 4.28 3.20 o 6 0 7 44.53 43.26 3.68 o 7 0 7 6.83 9.42 3.57 o 8 0 7 11.95 12.73 4.58 o 0 1 7 12.73 6.90 4.84 o 1 1 7 133.97 119.70 4.50 o 2 1 7 194.42 184.54 5.16 o 3 1 7 6.44 4.08 2.79 o 4 1 7 0.07 0.39 2.85 o 5 1 7 0.72 1.39 2.68 o 6 1 7 36.67 37.89 3.06 o 7 1 7 19.03 16.13 3.00 o 8 1 7 8.20 8.19 3.24 o 1 2 7 28.66 27.43 2.77 o 2 2 7 24.01 23.76 3.02 o 3 2 7 165.73 167.68 5.07 o 4 2 7 0.11 0.06 2.97 o 5 2 7 4.50 2.54 3.00 o 6 2 7 35.20 39.48 3.47 o 7 2 7 5.57 5.30 3.89 o 8 2 7 9.84 11.13 3.76 o 0 3 7 6.61 8.61 3.63 o 1 3 7 83.66 82.99 3.08 o 2 3 7 123.52 120.17 3.79 o 3 3 7 3.80 1.95 3.07 o 4 3 7 0.79 1.72 3.10 o 5 3 7 0.42 0.00 3.70 o 6 3 7 20.47 16.04 3.90 o 7 3 7 13.38 4.80 4.83 o 1 4 7 20.92 19.53 3.00 o 2 4 7 14.74 12.38 3.26 o 3 4 7 90.73 92.90 5.50 o 4 4 7 0.29 0.00 3.54 o 5 4 7 2.72 0.58 5.76 o 0 0 8 14.14 10.65 5.52 o 1 0 8 10.36 3.50 4.24 o 2 0 8 36.15 31.35 4.76 o 3 0 8 10.99 8.59 4.36 o 4 0 8 11.35 11.11 4.45 o 5 0 8 29.27 31.32 4.81 o 6 0 8 1.93 6.32 4.78 o 1 1 8 12.91 17.43 3.52 o 2 1 8 67.35 65.10 4.47 o 3 1 8 30.58 29.42 3.60 o 4 1 8 8.05 10.59 3.48 o 5 1 8 7.75 9.23 3.62 o 6 1 8 12.62 12.41 3.15 o 0 2 8 13.79 8.65 4.46 o 1 2 8 9.06 4.85 3.36 o 2 2 8 26.89 20.02 3.57 o 3 2 8 9.10 3.96 3.82 o 4 2 8 8.81 7.28 3.95 o 5 2 8 24.20 25.77 3.81 o 1 3 8 6.29 6.87 3.54 o 2 3 8 45.64 48.86 3.94 o 3 3 8 22.76 23.50 3.41 o 1 0 9 0.07 0.89 4.92 o