#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214205.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214205_Fobs loop_ _publ_author_name 'Andrighetti-Fr\"ohner, Carla Regina' 'Nunes, Ricardo Jos\'e' 'da Silva, Luiz Everson' 'Sim\~oes, Cl\'audia Maria Oliveira' 'Foro, Sabine' _publ_section_title ; Pyridinium 4-[(1E)-3-oxo-3-phenylprop-1-en-1-yl]benzenesulfonate ; _journal_coeditor_code GW2010 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3156 _journal_page_last o3157 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.610 _cell_angle_gamma 90.000 _cell_length_a 17.0340 _cell_length_b 9.0682 _cell_length_c 11.8320 _exptl_crystal_F_000 768.00 _reflns_d_resolution_high 0.8378 _[local]_cod_data_source_file gw2010Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1017 (CR37) P21/C' _shelx_refln_list_code 4 _shelx_f_calc_maximum 176.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2911.38 2177.65 37.70 o 2 0 0 5972.21 4704.01 30.03 o 3 0 0 122.44 98.22 1.37 o 4 0 0 14519.69 12045.38 97.16 o 5 0 0 18206.96 15324.36 129.05 o 6 0 0 19806.86 16957.40 204.88 o 7 0 0 205.06 179.51 2.73 o 8 0 0 4780.80 4441.96 24.54 o 9 0 0 4430.87 4254.87 18.40 o 10 0 0 758.81 658.08 8.53 o 11 0 0 58.02 38.38 2.09 o 12 0 0 10.41 8.13 0.92 o 13 0 0 439.21 395.08 11.35 o 14 0 0 257.92 245.01 4.58 o 15 0 0 66.64 75.65 1.66 o 16 0 0 163.49 166.81 3.54 o 17 0 0 10.16 6.98 0.84 o 18 0 0 59.04 67.57 1.50 o 19 0 0 82.97 88.50 4.29 o 20 0 0 131.86 163.79 3.34 o 1 1 0 3959.62 4295.79 107.40 o 2 1 0 3399.96 3515.17 68.84 o 3 1 0 1149.48 908.75 15.76 o 4 1 0 92.76 102.85 1.84 o 5 1 0 215.43 202.92 3.34 o 6 1 0 30.93 13.62 0.39 o 7 1 0 1062.94 756.67 7.43 o 8 1 0 4509.59 4052.69 41.45 o 9 1 0 551.85 452.97 9.74 o 10 1 0 0.12 0.31 0.57 o 11 1 0 513.68 439.65 5.34 o 12 1 0 1628.82 1521.47 17.64 o 13 1 0 599.16 588.71 5.94 o 14 1 0 174.86 186.82 3.40 o 15 1 0 36.75 39.75 0.93 o 16 1 0 147.97 141.31 2.16 o 17 1 0 178.69 189.28 3.51 o 18 1 0 221.35 248.66 4.34 o 19 1 0 88.85 107.32 3.50 o 20 1 0 0.55 2.91 0.39 o 0 2 0 3462.58 3724.26 17.10 o 1 2 0 24170.02 30571.66 339.84 o 2 2 0 95.93 171.73 39.06 o 3 2 0 2241.51 2183.52 61.49 o 4 2 0 2103.35 1895.59 30.75 o 5 2 0 1739.58 1518.68 31.38 o 6 2 0 1306.01 1089.42 6.97 o 7 2 0 1163.86 1051.46 8.60 o 8 2 0 1095.88 979.59 7.53 o 9 2 0 87.34 55.69 1.13 o 10 2 0 1614.72 1462.75 16.93 o 11 2 0 84.99 71.21 1.79 o 12 2 0 173.28 165.82 6.26 o 13 2 0 107.74 96.87 3.83 o 14 2 0 250.81 251.08 5.57 o 15 2 0 199.80 188.99 7.82 o 16 2 0 1.04 4.29 0.79 o 17 2 0 16.19 15.85 1.04 o 18 2 0 75.61 70.26 3.73 o 19 2 0 75.16 90.92 4.48 o 1 3 0 98.50 95.54 1.80 o 2 3 0 12238.53 13377.37 200.11 o 3 3 0 239.81 195.95 4.92 o 4 3 0 693.15 618.26 4.94 o 5 3 0 581.76 526.25 4.88 o 6 3 0 1032.31 950.11 22.80 o 7 3 0 3489.02 3397.10 15.64 o 8 3 0 1490.26 1306.12 13.92 o 9 3 0 802.59 774.16 7.46 o 10 3 0 25.13 21.09 0.96 o 11 3 0 1399.13 1290.54 35.63 o 12 3 0 685.70 656.43 16.49 o 13 3 0 485.46 451.98 6.94 o 14 3 0 179.60 191.06 4.15 o 15 3 0 3.28 6.39 1.23 o 16 3 0 51.96 51.63 3.98 o 17 3 0 177.17 175.63 13.14 o 18 3 0 47.63 57.27 3.44 o 19 3 0 14.85 16.22 0.73 o 0 4 0 995.58 1127.07 10.23 o 1 4 0 254.84 267.45 3.42 o 2 4 0 109.51 100.88 1.91 o 3 4 0 1475.08 1486.77 26.53 o 4 4 0 1328.05 1218.53 32.01 o 5 4 0 2.96 8.46 2.44 o 6 4 0 13.71 10.26 0.56 o 7 4 0 67.93 75.59 1.58 o 8 4 0 541.96 541.69 10.55 o 9 4 0 814.42 709.70 7.71 o 10 4 0 821.16 729.98 8.97 o 11 4 0 207.97 196.07 5.80 o 12 4 0 5.45 5.68 0.84 o 13 4 0 28.12 30.32 4.30 o 14 4 0 223.42 210.39 4.39 o 15 4 0 102.23 113.05 2.43 o 16 4 0 89.38 101.96 2.21 o 17 4 0 5.03 7.18 0.76 o 18 4 0 13.62 14.28 0.81 o 1 5 0 198.78 193.85 3.41 o 2 5 0 1267.70 1312.58 23.59 o 3 5 0 4948.00 4968.85 31.07 o 4 5 0 30.45 33.82 2.11 o 5 5 0 73.34 68.64 1.44 o 6 5 0 1306.22 1288.12 11.70 o 7 5 0 627.09 612.55 7.07 o 8 5 0 1128.63 1072.20 9.88 o 9 5 0 159.48 161.46 4.89 o 10 5 0 165.79 156.61 3.36 o 11 5 0 33.11 32.00 1.11 o 12 5 0 448.79 418.04 6.86 o 13 5 0 164.66 155.04 3.29 o 14 5 0 25.82 32.53 1.22 o 15 5 0 38.85 38.53 1.18 o 16 5 0 82.80 83.30 2.46 o 17 5 0 35.21 39.62 1.03 o 0 6 0 670.74 623.55 9.81 o 1 6 0 147.79 117.25 2.64 o 2 6 0 291.24 290.68 4.70 o 3 6 0 19.44 17.64 1.40 o 4 6 0 1632.76 1583.67 14.89 o 5 6 0 1009.98 965.51 12.49 o 6 6 0 798.27 770.50 8.70 o 7 6 0 4.89 4.15 2.32 o 8 6 0 152.96 145.13 3.50 o 9 6 0 332.57 327.15 6.01 o 10 6 0 727.55 672.93 9.61 o 11 6 0 362.38 363.28 6.37 o 12 6 0 294.37 297.35 5.79 o 13 6 0 17.95 17.70 0.98 o 14 6 0 104.86 101.57 2.21 o 15 6 0 208.43 210.84 6.30 o 16 6 0 186.85 203.76 3.84 o 1 7 0 541.43 537.45 7.13 o 2 7 0 514.21 493.81 6.94 o 3 7 0 1535.86 1531.14 12.52 o 4 7 0 1323.07 1272.88 11.49 o 5 7 0 5.91 6.60 0.86 o 6 7 0 404.42 388.95 6.48 o 7 7 0 71.36 66.58 1.55 o 8 7 0 455.81 404.78 6.71 o 9 7 0 1.59 1.20 1.19 o 10 7 0 3.52 5.08 0.84 o 11 7 0 1.64 0.36 1.59 o 12 7 0 78.26 74.63 1.58 o 13 7 0 63.03 65.76 2.83 o 14 7 0 11.81 14.44 0.81 o 15 7 0 59.73 50.09 1.88 o 0 8 0 212.92 209.60 5.97 o 1 8 0 931.54 941.33 25.99 o 2 8 0 88.92 89.07 1.98 o 3 8 0 0.15 -0.11 1.62 o 4 8 0 292.18 308.48 5.91 o 5 8 0 1128.14 1097.39 11.06 o 6 8 0 241.61 231.32 4.53 o 7 8 0 112.70 124.60 2.70 o 8 8 0 200.24 195.78 5.95 o 9 8 0 80.40 80.02 1.77 o 10 8 0 97.51 96.23 2.05 o 11 8 0 242.44 238.08 6.91 o 12 8 0 21.30 25.08 0.92 o 13 8 0 1.81 1.65 0.74 o 1 9 0 110.42 95.59 2.08 o 2 9 0 409.91 396.28 16.08 o 3 9 0 502.35 462.93 10.50 o 4 9 0 369.10 339.88 5.96 o 5 9 0 57.38 53.10 1.31 o 6 9 0 62.11 56.31 2.36 o 7 9 0 426.41 393.62 6.02 o 8 9 0 0.60 0.37 1.30 o 9 9 0 76.29 64.96 1.36 o 10 9 0 4.52 5.61 0.61 o 11 9 0 15.00 15.99 1.06 o 0 10 0 56.07 58.88 1.73 o 1 10 0 21.84 25.86 0.92 o 2 10 0 15.12 12.13 1.34 o 3 10 0 4.03 4.97 0.62 o 4 10 0 32.25 31.25 0.97 o 5 10 0 94.75 97.08 2.13 o 6 10 0 73.95 74.12 4.85 o 7 10 0 33.68 26.54 0.88 o -20 1 1 0.52 1.08 0.66 o -19 1 1 27.22 24.62 1.02 o -18 1 1 0.14 1.44 0.92 o -17 1 1 2.34 2.15 1.11 o -16 1 1 8.68 8.01 0.90 o -15 1 1 4.32 5.75 0.82 o -14 1 1 1.87 1.31 1.56 o -13 1 1 213.76 196.09 3.99 o -12 1 1 10.71 16.55 2.17 o -11 1 1 7.93 8.58 0.61 o -10 1 1 666.97 626.05 10.45 o -9 1 1 0.59 0.79 0.86 o -8 1 1 59.15 53.01 1.96 o -7 1 1 99.78 86.27 3.39 o -6 1 1 0.33 0.05 0.79 o -5 1 1 152.83 139.26 2.05 o -4 1 1 1446.19 1338.33 6.32 o -3 1 1 967.43 884.11 6.41 o -2 1 1 139.69 138.74 1.49 o -1 1 1 1009.10 928.99 67.81 o 0 1 1 10.08 12.69 3.54 o 1 1 1 173.76 188.14 28.58 o 2 1 1 187.79 188.23 15.54 o 3 1 1 1700.08 1598.86 87.01 o 4 1 1 140.43 121.94 6.06 o 5 1 1 2623.28 2211.16 31.71 o 6 1 1 578.68 515.30 23.74 o 7 1 1 548.22 556.11 19.66 o 8 1 1 84.22 66.71 1.73 o 9 1 1 118.54 116.38 2.35 o 10 1 1 197.40 186.51 3.88 o 11 1 1 549.14 510.76 10.47 o 12 1 1 60.26 54.55 1.26 o 13 1 1 29.11 28.56 1.07 o 14 1 1 10.66 9.12 0.87 o 15 1 1 5.66 4.37 0.82 o 16 1 1 65.89 65.41 1.55 o 17 1 1 7.30 8.10 0.87 o 18 1 1 0.00 0.37 0.88 o 19 1 1 12.20 15.41 1.19 o -19 2 1 4.41 8.83 1.04 o -18 2 1 0.80 0.50 1.00 o -17 2 1 56.57 62.26 2.11 o -16 2 1 9.74 9.71 1.23 o -15 2 1 118.01 117.93 3.39 o -14 2 1 352.10 371.50 9.04 o -13 2 1 71.84 80.43 2.27 o -12 2 1 108.77 95.42 2.92 o -11 2 1 77.11 74.71 2.31 o -10 2 1 671.60 673.39 9.90 o -9 2 1 2.14 10.33 0.81 o -8 2 1 546.04 503.04 7.40 o -7 2 1 1220.98 1201.85 11.11 o -6 2 1 4.87 7.60 0.58 o -5 2 1 656.51 642.91 6.83 o -4 2 1 50.55 43.70 1.42 o -3 2 1 143.40 135.00 2.74 o -2 2 1 6133.28 6691.01 28.29 o -1 2 1 18580.65 24035.39 158.17 o 0 2 1 1834.19 1917.97 10.77 o 1 2 1 9268.10 10800.08 91.56 o 2 2 1 3643.90 3995.30 18.96 o 3 2 1 196.58 211.40 3.41 o 4 2 1 282.31 250.15 3.96 o 5 2 1 290.85 273.09 4.50 o 6 2 1 135.34 148.40 3.58 o 7 2 1 552.55 559.71 7.52 o 8 2 1 0.03 -0.19 1.38 o 9 2 1 0.30 1.11 1.46 o 10 2 1 384.96 379.71 7.63 o 11 2 1 2.36 0.65 1.77 o 12 2 1 102.29 94.06 2.85 o 13 2 1 6.19 8.60 1.15 o 14 2 1 45.66 46.65 1.88 o 15 2 1 11.84 9.68 1.27 o 16 2 1 67.52 63.35 2.23 o 17 2 1 0.39 0.38 1.84 o 18 2 1 0.00 -0.61 0.92 o 19 2 1 5.24 3.72 0.96 o -19 3 1 4.63 3.19 0.92 o -18 3 1 12.66 13.40 1.19 o -17 3 1 0.05 1.42 2.11 o -16 3 1 0.62 -1.19 2.15 o -15 3 1 85.42 102.13 3.31 o -14 3 1 4.99 5.95 1.04 o -13 3 1 167.11 167.38 4.74 o -12 3 1 270.12 262.39 7.29 o -11 3 1 8.08 9.56 1.15 o -10 3 1 51.32 54.57 1.61 o -9 3 1 292.60 288.37 6.41 o -8 3 1 22.08 22.01 1.04 o -7 3 1 96.58 90.94 2.85 o -6 3 1 36.88 34.01 0.96 o -5 3 1 54.95 68.91 2.04 o -4 3 1 1200.51 1162.70 10.03 o -3 3 1 15.09 13.79 0.69 o -2 3 1 3812.26 4016.45 20.81 o -1 3 1 5000.10 5554.71 26.11 o 0 3 1 1026.83 1023.78 8.40 o 1 3 1 78.05 68.91 1.96 o 2 3 1 492.83 488.43 5.82 o 3 3 1 153.33 131.68 3.13 o 4 3 1 780.84 812.10 8.25 o 5 3 1 529.95 561.71 7.17 o 6 3 1 591.49 595.31 7.88 o 7 3 1 565.91 625.68 8.49 o 8 3 1 49.16 58.77 1.81 o 9 3 1 24.47 20.13 1.08 o 10 3 1 87.03 86.30 2.73 o 11 3 1 192.44 193.81 5.28 o 12 3 1 49.47 53.15 1.88 o 13 3 1 76.56 69.86 2.19 o 14 3 1 17.86 20.39 1.46 o 15 3 1 2.81 1.61 2.03 o 16 3 1 28.47 28.69 1.69 o 17 3 1 33.66 32.15 1.50 o 18 3 1 4.82 2.84 0.96 o 19 3 1 4.21 6.18 0.81 o -18 4 1 33.84 30.97 1.38 o -17 4 1 0.30 0.92 1.88 o -16 4 1 11.79 14.63 1.27 o -15 4 1 14.96 17.20 1.38 o -14 4 1 0.04 0.81 1.84 o -13 4 1 16.36 16.71 1.42 o -12 4 1 113.55 110.38 3.31 o -11 4 1 246.19 218.10 5.86 o -10 4 1 193.87 180.29 5.20 o -9 4 1 3.10 6.03 0.92 o -8 4 1 217.32 171.80 5.05 o -7 4 1 14.58 12.29 0.84 o -6 4 1 226.26 222.82 5.13 o -5 4 1 0.38 0.81 1.23 o -4 4 1 897.82 936.79 10.02 o -3 4 1 36.39 43.85 1.31 o -2 4 1 2015.14 2079.71 15.07 o -1 4 1 120.06 121.93 3.27 o 0 4 1 283.30 318.38 5.19 o 1 4 1 468.09 541.82 7.04 o 2 4 1 181.48 194.89 4.28 o 3 4 1 62.29 58.41 1.69 o 4 4 1 32.96 35.89 1.15 o 5 4 1 477.24 471.29 7.38 o 6 4 1 25.25 31.50 1.15 o 7 4 1 16.45 14.67 1.04 o 8 4 1 152.99 146.63 4.24 o 9 4 1 55.55 47.16 1.58 o 10 4 1 15.75 13.94 1.19 o 11 4 1 27.80 26.93 1.50 o 12 4 1 1.35 1.80 2.19 o 13 4 1 55.10 54.73 2.08 o 14 4 1 56.48 49.12 1.84 o 15 4 1 142.25 133.96 3.89 o 16 4 1 21.86 23.08 1.38 o 17 4 1 0.01 1.04 1.88 o 18 4 1 0.14 1.15 1.38 o -18 5 1 20.81 27.35 1.23 o -17 5 1 29.23 29.27 1.38 o -16 5 1 2.39 0.61 1.07 o -15 5 1 1.39 1.96 1.07 o -14 5 1 3.55 4.68 1.15 o -13 5 1 8.64 10.14 1.23 o -12 5 1 157.73 155.75 4.66 o -11 5 1 27.87 21.24 1.38 o -10 5 1 761.55 739.71 12.31 o -9 5 1 121.25 129.03 4.04 o -8 5 1 136.02 125.50 3.89 o -7 5 1 161.79 151.35 4.35 o -6 5 1 47.97 41.01 1.38 o -5 5 1 9.06 10.18 0.88 o -4 5 1 60.79 79.96 2.31 o -3 5 1 918.49 899.52 10.78 o -2 5 1 92.46 71.83 2.00 o -1 5 1 1143.22 1308.82 12.78 o 0 5 1 6.32 62.82 1.84 o 1 5 1 264.13 277.16 5.80 o 2 5 1 252.07 264.04 5.75 o 3 5 1 949.27 985.95 11.45 o 4 5 1 16.70 20.85 1.11 o 5 5 1 3.68 6.18 0.92 o 6 5 1 543.08 509.21 8.89 o 7 5 1 163.53 161.48 4.62 o 8 5 1 7.23 7.95 1.00 o 9 5 1 117.48 115.24 3.39 o 10 5 1 229.32 205.60 5.75 o 11 5 1 112.41 100.45 3.19 o 12 5 1 1.15 1.42 1.00 o 13 5 1 0.12 0.81 2.00 o 14 5 1 5.66 7.03 1.15 o 15 5 1 36.63 39.61 1.73 o 16 5 1 35.86 32.23 1.46 o 17 5 1 37.28 47.53 1.50 o -16 6 1 16.15 15.44 1.19 o -15 6 1 53.89 60.15 1.92 o -14 6 1 69.86 72.47 2.23 o -13 6 1 24.04 23.01 1.50 o -12 6 1 13.70 12.75 1.38 o -11 6 1 1.49 1.84 2.23 o -10 6 1 22.98 21.35 1.42 o -9 6 1 894.25 840.27 13.55 o -8 6 1 29.13 23.66 1.50 o -7 6 1 6.35 6.60 1.08 o -6 6 1 1.37 -1.88 2.23 o -5 6 1 73.03 71.82 2.11 o -4 6 1 379.85 398.31 8.09 o -3 6 1 347.58 331.08 7.35 o -2 6 1 54.97 56.81 1.88 o -1 6 1 188.57 261.72 6.28 o 0 6 1 30.80 34.92 1.42 o 1 6 1 73.21 62.60 1.85 o 2 6 1 29.46 32.84 1.31 o 3 6 1 17.26 25.88 1.34 o 4 6 1 11.96 10.98 1.11 o 5 6 1 0.12 0.15 1.00 o 6 6 1 66.08 69.54 2.08 o 7 6 1 211.44 202.11 5.47 o 8 6 1 231.90 226.51 6.13 o 9 6 1 125.34 121.06 3.77 o 10 6 1 11.36 9.10 1.23 o 11 6 1 63.21 57.35 2.04 o 12 6 1 21.63 20.24 1.38 o 13 6 1 25.57 21.82 1.46 o 14 6 1 1.06 2.30 1.00 o 15 6 1 10.16 9.06 1.11 o 16 6 1 0.75 2.11 0.88 o -15 7 1 13.86 11.37 1.08 o -14 7 1 3.85 4.88 0.92 o -13 7 1 5.24 5.57 1.08 o -12 7 1 0.28 -1.04 1.73 o -11 7 1 60.02 57.96 1.88 o -10 7 1 3.14 -2.34 2.53 o -9 7 1 822.16 827.76 13.41 o -8 7 1 93.53 88.61 2.81 o -7 7 1 6.62 7.53 1.19 o -6 7 1 13.68 14.75 1.34 o -5 7 1 106.74 109.02 3.62 o -4 7 1 317.15 306.56 7.80 o -3 7 1 43.79 50.22 1.81 o -2 7 1 8.02 7.83 1.08 o -1 7 1 26.49 25.43 1.42 o 0 7 1 8.91 13.90 1.23 o 1 7 1 0.83 1.42 2.11 o 2 7 1 14.04 12.37 1.27 o 3 7 1 64.24 70.80 2.19 o 4 7 1 32.74 33.19 1.50 o 5 7 1 57.13 61.22 2.11 o 6 7 1 74.59 72.47 2.15 o 7 7 1 106.92 108.98 3.39 o 8 7 1 36.76 37.92 1.81 o 9 7 1 18.57 15.75 1.38 o 10 7 1 3.36 1.54 1.15 o 11 7 1 21.38 15.21 1.27 o 12 7 1 7.09 6.53 1.00 o 13 7 1 1.06 1.92 1.04 o 14 7 1 0.35 -1.34 1.73 o 15 7 1 9.19 9.60 0.96 o -13 8 1 0.63 -1.31 1.54 o -12 8 1 22.39 20.01 1.19 o -11 8 1 5.63 3.92 1.04 o -10 8 1 0.03 1.65 2.00 o -9 8 1 9.85 14.90 1.42 o -8 8 1 0.24 0.96 1.15 o -7 8 1 12.84 11.71 1.38 o -6 8 1 1.56 0.00 2.57 o -5 8 1 71.55 57.74 2.00 o -4 8 1 0.03 0.61 2.19 o -3 8 1 9.47 5.99 1.19 o -2 8 1 0.53 0.61 1.00 o -1 8 1 4.47 9.56 1.19 o 0 8 1 15.77 17.93 1.38 o 1 8 1 1.52 1.80 1.19 o 2 8 1 3.55 3.19 1.19 o 3 8 1 36.58 40.88 1.81 o 4 8 1 3.91 3.61 1.19 o 5 8 1 19.99 22.77 1.61 o 6 8 1 10.10 10.67 1.38 o 7 8 1 156.39 152.09 4.66 o 8 8 1 1.41 1.31 2.42 o 9 8 1 20.43 15.29 1.23 o 10 8 1 0.81 1.31 1.61 o 11 8 1 5.78 5.91 1.00 o 12 8 1 27.96 21.44 1.23 o 13 8 1 13.43 16.59 1.00 o -11 9 1 1.56 1.38 1.38 o -10 9 1 0.20 0.23 1.50 o -9 9 1 2.56 1.08 0.92 o -8 9 1 8.19 11.37 1.19 o -7 9 1 4.70 0.00 2.07 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