#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214211.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214211_Fobs loop_ _publ_author_name 'Chai, Wen-Li' 'Bi, Wei-Yu' 'L\"u, Xing-Qiang' 'Song, Ji-Rong' 'Ng, Seik Weng' _publ_section_title ; (S)-(+)-2,2'-Bis(2-hydroxy-3-methoxybenzylideneamino)-1,1'-binaphthyl ; _journal_coeditor_code HB2421 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3060 _journal_volume 63 _journal_year 2007 _space_group_IT_number 92 _symmetry_space_group_name_Hall 'P 4abw 2nw' _symmetry_space_group_name_H-M 'P 41 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.3285 _cell_length_b 11.3285 _cell_length_c 23.8366 _exptl_crystal_F_000 1160.00 _reflns_d_resolution_high 0.8413 _[local]_cod_data_source_file hb2421Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P41212' _shelx_refln_list_code 4 _shelx_f_calc_maximum 190.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z+3/4' '-x, -y, z+1/2' '-x+1/2, y+1/2, -z+1/4' 'y, x, -z' 'y+1/2, -x+1/2, z+3/4' '-y+1/2, x+1/2, z+1/4' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 5457.01 4467.06 52.79 o 0 2 0 3111.90 2880.61 44.48 o 1 2 0 808.97 1217.77 9.14 o 2 2 0 409.99 301.02 3.44 o 1 3 0 3530.99 3138.25 22.95 o 2 3 0 541.42 616.16 4.78 o 3 3 0 176.25 199.63 3.27 o 0 4 0 36461.20 33898.09 403.08 o 1 4 0 2955.42 2722.92 21.52 o 2 4 0 2406.05 2122.83 15.92 o 3 4 0 159.81 172.66 2.00 o 4 4 0 1966.98 1859.14 20.22 o 1 5 0 43.25 82.43 2.08 o 2 5 0 453.05 432.78 4.05 o 3 5 0 24.44 19.44 0.99 o 4 5 0 265.05 242.50 2.90 o 5 5 0 26.11 36.12 1.95 o 0 6 0 3457.78 3686.97 51.14 o 1 6 0 104.32 115.87 2.11 o 2 6 0 11.24 20.23 1.07 o 3 6 0 22.32 24.11 1.12 o 4 6 0 238.58 264.27 3.47 o 5 6 0 73.39 76.43 2.61 o 6 6 0 280.49 240.84 5.73 o 1 7 0 1.72 7.02 1.09 o 2 7 0 22.09 17.15 1.38 o 3 7 0 75.60 83.95 2.09 o 4 7 0 29.69 27.64 1.94 o 5 7 0 1.46 4.29 1.66 o 6 7 0 10.93 7.99 1.81 o 7 7 0 15.31 11.08 3.11 o 0 8 0 207.04 186.65 3.87 o 1 8 0 42.33 51.42 2.27 o 2 8 0 28.07 25.56 1.64 o 3 8 0 12.00 4.29 1.47 o 4 8 0 18.83 26.47 2.20 o 5 8 0 3.34 2.29 1.83 o 6 8 0 0.63 -1.19 1.75 o 7 8 0 1.76 -1.21 1.90 o 8 8 0 1.92 -3.88 3.30 o 1 9 0 1.03 -0.95 2.25 o 2 9 0 0.51 0.11 1.53 o 3 9 0 16.26 26.43 2.04 o 4 9 0 1.73 6.30 2.03 o 5 9 0 0.03 -1.84 1.82 o 6 9 0 19.06 25.29 2.56 o 7 9 0 27.60 30.65 2.74 o 8 9 0 4.32 5.84 2.66 o 9 9 0 19.75 27.43 4.77 o 0 10 0 0.01 -4.33 3.08 o 1 10 0 22.55 30.04 2.60 o 2 10 0 7.60 6.31 2.17 o 3 10 0 2.25 1.29 2.28 o 4 10 0 3.88 1.56 2.08 o 5 10 0 32.67 32.49 3.04 o 6 10 0 32.45 32.69 2.89 o 7 10 0 0.55 0.37 2.25 o 8 10 0 0.32 -2.45 2.49 o 9 10 0 17.87 28.03 3.61 o 1 11 0 0.53 1.82 2.11 o 2 11 0 0.00 -2.93 1.95 o 3 11 0 2.30 1.37 2.58 o 4 11 0 0.12 1.76 2.48 o 5 11 0 6.36 0.29 2.66 o 6 11 0 8.03 6.14 3.29 o 7 11 0 18.79 17.28 3.06 o 0 12 0 8.09 8.83 4.09 o 1 12 0 1.10 -0.08 2.31 o 2 12 0 0.00 -3.66 2.44 o 3 12 0 5.91 3.40 2.75 o 4 12 0 6.87 5.47 3.08 o 5 12 0 1.16 0.05 2.90 o 6 12 0 3.20 6.24 3.22 o 1 13 0 0.29 -0.56 2.46 o 2 13 0 0.04 -2.70 2.79 o 3 13 0 1.25 3.08 3.07 o 0 1 1 12803.60 10682.30 89.58 o 1 1 1 544.94 541.09 4.47 o 0 2 1 30685.81 27873.01 230.72 o 1 2 1 8371.44 7506.27 42.32 o 2 2 1 86.49 151.93 1.61 o 0 3 1 21158.83 23194.55 191.40 o 1 3 1 5718.82 5311.98 29.04 o 2 3 1 358.99 314.90 1.96 o 3 3 1 2.44 4.15 0.88 o 0 4 1 13.06 2.90 2.77 o 1 4 1 1186.98 1024.29 5.91 o 2 4 1 464.66 415.75 2.68 o 3 4 1 54.72 55.66 0.87 o 4 4 1 459.81 447.07 4.22 o 0 5 1 2242.88 2135.07 17.27 o 1 5 1 1169.02 1088.38 6.58 o 2 5 1 570.57 561.33 4.02 o 3 5 1 353.96 371.01 3.49 o 4 5 1 440.15 449.92 3.00 o 5 5 1 1.83 0.73 1.08 o 0 6 1 1162.28 983.66 8.13 o 1 6 1 128.64 107.48 1.43 o 2 6 1 241.49 226.58 2.15 o 3 6 1 181.31 152.81 1.66 o 4 6 1 205.21 195.14 2.19 o 5 6 1 92.35 80.92 1.85 o 6 6 1 5.31 6.51 1.53 o 0 7 1 669.02 686.71 6.21 o 1 7 1 112.89 100.03 1.68 o 2 7 1 1.77 -0.55 0.78 o 3 7 1 29.32 33.39 1.11 o 4 7 1 142.25 136.59 1.96 o 5 7 1 35.34 41.70 1.69 o 6 7 1 21.79 22.18 1.53 o 7 7 1 0.54 -2.38 1.58 o 0 8 1 13.17 10.46 1.36 o 1 8 1 53.40 52.63 1.41 o 2 8 1 15.17 13.18 1.06 o 3 8 1 28.65 38.75 1.37 o 4 8 1 10.43 18.08 1.53 o 5 8 1 7.26 6.17 1.37 o 6 8 1 4.79 4.27 1.38 o 7 8 1 2.85 0.51 1.39 o 8 8 1 0.89 0.72 2.39 o 0 9 1 25.82 26.60 2.27 o 1 9 1 12.60 22.82 1.55 o 2 9 1 8.06 4.67 1.13 o 3 9 1 1.72 -1.04 1.16 o 4 9 1 5.83 5.45 1.37 o 5 9 1 2.25 1.54 1.38 o 6 9 1 49.35 55.83 2.16 o 7 9 1 7.34 10.32 1.66 o 8 9 1 1.50 3.68 1.84 o 9 9 1 11.69 14.61 3.44 o 0 10 1 1.47 4.92 2.42 o 1 10 1 5.09 3.23 1.43 o 2 10 1 33.35 24.24 1.77 o 3 10 1 29.89 33.13 2.01 o 4 10 1 58.38 62.66 2.23 o 5 10 1 12.18 11.14 1.70 o 6 10 1 7.17 7.85 1.66 o 7 10 1 9.62 8.30 1.73 o 8 10 1 16.86 14.76 1.97 o 9 10 1 15.03 14.31 2.28 o 0 11 1 9.05 15.56 2.75 o 1 11 1 1.01 -1.29 1.43 o 2 11 1 9.42 8.20 1.61 o 3 11 1 2.81 3.75 1.88 o 4 11 1 2.32 2.92 1.91 o 5 11 1 0.98 0.53 1.92 o 6 11 1 14.16 7.84 1.84 o 7 11 1 4.11 1.31 1.85 o 0 12 1 0.03 -2.30 2.16 o 1 12 1 3.94 1.74 1.64 o 2 12 1 1.15 3.45 1.90 o 3 12 1 2.09 4.50 1.98 o 4 12 1 0.30 -2.27 1.98 o 5 12 1 9.79 6.40 2.15 o 6 12 1 2.98 2.55 2.11 o 0 13 1 2.54 5.27 2.35 o 1 13 1 0.16 1.41 1.96 o 2 13 1 1.19 2.17 2.12 o 3 13 1 0.03 1.48 2.15 o 0 1 2 1112.52 1267.95 9.42 o 1 1 2 1854.52 1968.87 14.42 o 0 2 2 3748.40 3251.27 25.30 o 1 2 2 12394.39 11964.66 62.57 o 2 2 2 4959.13 4297.52 29.41 o 0 3 2 11177.30 9701.13 74.48 o 1 3 2 9805.50 9244.50 50.19 o 2 3 2 249.36 244.82 1.83 o 3 3 2 634.14 420.15 3.59 o 0 4 2 12.55 14.38 0.89 o 1 4 2 308.86 295.84 2.42 o 2 4 2 711.06 626.17 3.90 o 3 4 2 266.72 303.59 2.22 o 4 4 2 113.53 100.56 1.68 o 0 5 2 1397.66 1716.03 14.11 o 1 5 2 1003.73 1140.56 6.63 o 2 5 2 83.28 75.60 1.13 o 3 5 2 396.16 385.96 2.95 o 4 5 2 256.61 246.21 2.10 o 5 5 2 159.89 185.09 2.91 o 0 6 2 753.78 753.37 7.00 o 1 6 2 225.59 241.29 2.46 o 2 6 2 216.70 207.34 2.73 o 3 6 2 148.95 146.55 1.66 o 4 6 2 25.12 25.53 1.00 o 5 6 2 24.46 28.06 1.31 o 6 6 2 6.91 -0.77 1.57 o 0 7 2 294.46 269.33 3.48 o 1 7 2 433.14 445.81 3.50 o 2 7 2 185.84 156.90 1.80 o 3 7 2 74.20 70.40 1.49 o 4 7 2 56.00 60.31 1.60 o 5 7 2 3.78 2.48 1.11 o 6 7 2 48.13 45.53 1.79 o 7 7 2 5.40 3.58 1.69 o 0 8 2 10.61 7.83 1.33 o 1 8 2 0.82 -1.37 0.91 o 2 8 2 24.34 22.61 1.20 o 3 8 2 60.66 52.12 1.52 o 4 8 2 7.60 9.06 1.18 o 5 8 2 0.27 -0.08 1.22 o 6 8 2 0.46 -0.49 1.31 o 7 8 2 7.74 6.39 1.51 o 8 8 2 4.25 1.28 2.40 o 0 9 2 30.02 20.09 2.10 o 1 9 2 19.20 18.87 1.36 o 2 9 2 72.35 75.65 2.01 o 3 9 2 9.73 11.15 1.29 o 4 9 2 68.17 67.24 2.16 o 5 9 2 44.03 42.38 1.97 o 6 9 2 3.57 -0.12 1.44 o 7 9 2 11.03 15.16 1.99 o 8 9 2 12.48 10.64 2.00 o 9 9 2 3.65 -0.91 2.56 o 0 10 2 7.64 14.43 2.88 o 1 10 2 12.40 10.74 1.63 o 2 10 2 142.65 133.23 3.35 o 3 10 2 59.99 63.47 2.61 o 4 10 2 5.24 -0.41 1.49 o 5 10 2 22.96 28.89 1.90 o 6 10 2 33.73 34.03 2.03 o 7 10 2 5.32 8.95 1.91 o 8 10 2 0.77 -2.55 1.70 o 0 11 2 0.05 -1.53 2.43 o 1 11 2 32.15 36.31 1.98 o 2 11 2 0.97 1.30 1.69 o 3 11 2 2.05 -0.14 1.82 o 4 11 2 9.19 2.63 2.00 o 5 11 2 2.42 0.91 1.81 o 6 11 2 2.32 0.65 1.80 o 7 11 2 1.82 -2.65 1.77 o 0 12 2 1.00 0.15 2.28 o 1 12 2 5.14 4.25 1.72 o 2 12 2 0.65 -1.37 1.72 o 3 12 2 1.79 -2.30 1.90 o 4 12 2 5.45 1.65 1.99 o 5 12 2 1.22 1.78 2.55 o 6 12 2 0.43 -1.83 2.10 o 0 13 2 0.64 -1.28 2.26 o 1 13 2 1.39 1.01 1.96 o 2 13 2 1.06 -1.11 2.06 o 3 13 2 0.90 -3.06 2.04 o 0 1 3 4292.14 4561.89 31.23 o 1 1 3 571.29 576.51 4.25 o 0 2 3 18.75 18.18 0.96 o 1 2 3 8251.09 8620.52 46.79 o 2 2 3 3225.83 2560.09 17.76 o 0 3 3 10384.45 9899.42 76.00 o 1 3 3 4289.77 4046.05 23.10 o 2 3 3 227.03 319.02 2.17 o 3 3 3 20.63 29.38 1.09 o 0 4 3 2017.09 1803.05 17.35 o 1 4 3 250.06 264.72 1.97 o 2 4 3 1205.42 1093.96 6.59 o 3 4 3 43.32 41.11 0.85 o 4 4 3 96.80 90.21 1.75 o 0 5 3 1272.27 1152.02 9.85 o 1 5 3 1783.02 1704.08 9.57 o 2 5 3 313.59 330.38 2.49 o 3 5 3 1123.91 1043.72 6.52 o 4 5 3 5.97 12.86 0.78 o 5 5 3 7.08 4.66 1.16 o 0 6 3 115.24 63.45 2.08 o 1 6 3 93.30 111.32 1.42 o 2 6 3 1339.51 1295.09 8.52 o 3 6 3 329.88 291.91 2.57 o 4 6 3 212.72 213.06 2.20 o 5 6 3 1.57 3.19 0.98 o 6 6 3 8.38 17.82 1.77 o 0 7 3 2.62 1.15 1.00 o 1 7 3 300.12 297.22 2.56 o 2 7 3 55.27 50.87 1.53 o 3 7 3 57.98 61.63 1.45 o 4 7 3 87.98 84.24 1.77 o 5 7 3 72.82 74.91 1.83 o 6 7 3 11.72 10.95 1.43 o 7 7 3 0.08 0.57 1.84 o 0 8 3 160.69 154.62 3.57 o 1 8 3 65.52 78.96 1.65 o 2 8 3 97.22 90.77 1.75 o 3 8 3 4.63 5.32 1.04 o 4 8 3 13.47 15.04 1.27 o 5 8 3 0.44 -0.55 1.20 o 6 8 3 11.41 9.99 1.50 o 7 8 3 0.33 -1.99 1.39 o 8 8 3 0.52 1.91 2.26 o 0 9 3 69.71 88.20 3.20 o 1 9 3 14.00 14.99 1.35 o 2 9 3 15.40 16.54 1.38 o 3 9 3 61.17 62.60 1.96 o 4 9 3 14.80 11.31 1.52 o 5 9 3 13.90 18.20 1.68 o 6 9 3 7.38 9.35 1.58 o 7 9 3 20.19 20.01 1.81 o 8 9 3 4.71 4.72 1.92 o 9 9 3 1.83 -3.94 2.62 o 0 10 3 1.27 4.40 2.61 o 1 10 3 210.26 207.44 3.27 o 2 10 3 35.42 35.02 1.85 o 3 10 3 125.72 131.36 2.96 o 4 10 3 1.92 2.82 1.64 o 5 10 3 58.44 69.67 2.40 o 6 10 3 10.98 11.80 1.72 o 7 10 3 10.68 9.73 1.84 o 8 10 3 0.56 -2.06 1.69 o 0 11 3 10.16 5.19 2.31 o 1 11 3 9.27 14.02 1.73 o 2 11 3 16.20 14.37 1.85 o 3 11 3 12.37 10.05 1.84 o 4 11 3 24.54 24.96 2.25 o 5 11 3 1.86 0.76 1.81 o 6 11 3 1.89 -0.78 1.81 o 7 11 3 5.32 5.03 1.86 o 0 12 3 3.32 6.72 2.44 o 1 12 3 5.92 3.40 1.70 o 2 12 3 1.27 5.46 2.03 o 3 12 3 8.27 6.56 2.44 o 4 12 3 0.21 -1.35 1.98 o 5 12 3 1.64 0.54 2.09 o 0 13 3 0.71 1.02 2.34 o 1 13 3 3.47 2.67 1.95 o 2 13 3 0.09 -0.97 2.08 o 3 13 3 1.66 1.90 2.22 o 0 0 4 14415.24 14070.96 202.09 o 0 1 4 111.04 92.70 1.09 o 1 1 4 4032.43 3793.32 27.54 o 0 2 4 2568.64 2498.32 19.62 o 1 2 4 702.30 743.91 4.30 o 2 2 4 145.61 135.80 1.67 o 0 3 4 872.87 1109.78 9.21 o 1 3 4 1390.02 1271.58 7.66 o 2 3 4 153.64 163.69 1.46 o 3 3 4 10.82 5.30 0.62 o 0 4 4 230.28 225.79 2.66 o 1 4 4 1374.21 1281.20 7.56 o 2 4 4 190.01 208.40 1.90 o 3 4 4 46.91 64.58 1.02 o 4 4 4 292.94 279.86 2.89 o 0 5 4 18.58 14.38 1.05 o 1 5 4 143.47 136.61 1.40 o 2 5 4 382.23 418.51 3.35 o 3 5 4 67.35 72.29 1.42 o 4 5 4 30.47 34.34 0.98 o 5 5 4 65.45 63.77 1.79 o 0 6 4 4833.17 4547.44 35.85 o 1 6 4 413.19 445.21 3.18 o 2 6 4 297.99 308.65 2.61 o 3 6 4 7.55 3.43 0.76 o 4 6 4 312.77 315.42 2.94 o 5 6 4 84.97 89.96 1.67 o 6 6 4 60.47 65.53 2.50 o 0 7 4 71.47 74.25 1.76 o 1 7 4 130.11 115.77 1.68 o 2 7 4 2.21 1.61 0.80 o 3 7 4 1.75 -0.42 0.81 o 4 7 4 10.33 8.95 1.10 o 5 7 4 12.99 21.98 1.33 o 6 7 4 24.24 23.39 1.57 o 7 7 4 3.60 0.78 1.82 o 0 8 4 6.30 0.45 1.40 o 1 8 4 252.99 255.40 3.01 o 2 8 4 92.30 92.89 1.79 o 3 8 4 18.80 17.96 1.24 o 4 8 4 49.15 53.07 1.71 o 5 8 4 17.88 21.01 1.49 o 6 8 4 4.26 2.49 1.39 o 7 8 4 0.09 -0.85 1.38 o 8 8 4 5.02 0.88 2.49 o 0 9 4 247.08 228.99 5.98 o 1 9 4 34.90 45.04 1.72 o 2 9 4 130.09 135.11 2.31 o 3 9 4 82.15 93.66 2.11 o 4 9 4 61.99 53.16 1.93 o 5 9 4 51.77 44.92 1.99 o 6 9 4 41.38 46.94 2.22 o 7 9 4 0.78 -0.70 1.54 o 8 9 4 1.01 0.84 1.87 o 9 9 4 6.24 1.31 2.82 o 0 10 4 132.80 125.03 5.57 o 1 10 4 40.35 35.02 1.92 o 2 10 4 147.21 135.78 2.62 o 3 10 4 79.35 73.61 2.68 o 4 10 4 55.96 66.52 3.36 o 5 10 4 7.99 7.06 1.64 o 6 10 4 34.37 39.34 2.43 o 7 10 4 13.32 10.36 1.82 o 8 10 4 0.94 -1.73 1.76 o 0 11 4 10.27 11.85 2.47 o 1 11 4 60.52 61.57 2.35 o 2 11 4 21.99 23.44 2.03 o 3 11 4 0.25 0.49 1.76 o 4 11 4 2.83 1.33 1.89 o 5 11 4 15.88 25.69 2.15 o 6 11 4 3.20 -1.17 1.81 o 7 11 4 0.22 -1.09 2.07 o 0 12 4 17.14 15.95 2.51 o 1 12 4 1.94 0.54 1.78 o 2 12 4 2.43 5.88 1.88 o 3 12 4 2.29 4.20 2.07 o 4 12 4 12.43 16.50 2.54 o 5 12 4 3.27 0.55 2.08 o 0 13 4 2.16 3.23 2.57 o 1 13 4 3.73 6.60 1.93 o 2 13 4 0.59 1.11 2.09 o 0 1 5 1529.04 1382.22 10.40 o 1 1 5 1097.73 1216.22 8.22 o 0 2 5 91.34 56.78 1.03 o 1 2 5 109.79 97.72 1.03 o 2 2 5 331.29 316.00 2.79 o 0 3 5 1420.48 1311.61 10.79 o 1 3 5 963.72 983.66 5.67 o 2 3 5 223.64 277.73 2.41 o 3 3 5 30.85 33.71 0.94 o 0 4 5 43.24 62.58 1.41 o 1 4 5 66.41 61.55 1.10 o 2 4 5 215.00 195.86 2.14 o 3 4 5 158.27 166.95 1.60 o 4 4 5 322.41 294.84 3.00 o 0 5 5 713.19 784.51 7.15 o 1 5 5 278.32 287.80 2.34 o 2 5 5 166.66 203.21 1.97 o 3 5 5 240.48 253.13 2.36 o 4 5 5 107.15 113.88 1.49 o 5 5 5 87.40 86.00 1.96 o 0 6 5 55.36 61.03 2.89 o 1 6 5 841.81 812.58 4.95 o 2 6 5 100.53 104.63 1.54 o 3 6 5 222.17 207.49 2.17 o 4 6 5 169.39 189.16 2.22 o 5 6 5 125.86 146.72 2.14 o 6 6 5 148.31 155.54 3.34 o 0 7 5 39.62 45.65 1.70 o 1 7 5 113.87 125.74 2.55 o 2 7 5 168.50 199.86 2.28 o 3 7 5 20.09 18.28 1.06 o 4 7 5 30.30 35.32 1.40 o 5 7 5 72.59 65.68 1.75 o 6 7 5 5.49 2.12 1.21 o 7 7 5 32.10 37.35 2.56 o 0 8 5 3.20 3.25 1.50 o 1 8 5 64.69 61.19 1.59 o 2 8 5 11.70 11.49 1.13 o 3 8 5 35.32 40.79 1.52 o 4 8 5 11.87 10.57 1.28 o 5 8 5 36.99 36.92 1.75 o 6 8 5 42.14 50.74 1.90 o 7 8 5 10.14 10.36 1.56 o 8 8 5 5.17 2.03 2.58 o 0 9 5 1130.54 1088.35 12.61 o 1 9 5 228.92 219.60 2.99 o 2 9 5 300.51 317.72 3.47 o 3 9 5 39.53 47.85 1.94 o 4 9 5 246.88 263.68 3.44 o 5 9 5 22.90 25.35 1.83 o 6 9 5 30.19 35.95 2.03 o 7 9 5 6.92 3.15 1.59 o 8 9 5 6.15 0.57 1.83 o 9 9 5 5.14 7.61 2.98 o 0 10 5 264.99 272.65 7.22 o 1 10 5 9.74 7.21 1.63 o 2 10 5 57.13 60.87 2.25 o 3 10 5 42.96 50.44 2.12 o 4 10 5 42.75 40.13 2.19 o 5 10 5 2.80 1.29 1.70 o 6 10 5 26.60 35.10 2.08 o 7 10 5 6.90 6.23 1.74 o 8 10 5 2.04 -1.49 1.92 o 0 11 5 164.43 152.78 4.41 o 1 11 5 3.76 5.73 1.80 o 2 11 5 57.62 74.50 2.52 o 3 11 5 1.29 -0.90 1.60 o 4 11 5 25.26 28.19 2.18 o 5 11 5 0.35 -2.54 1.78 o 6 11 5 2.32 0.81 1.83 o 7 11 5 1.57 -1.39 1.89 o 0 12 5 0.28 -1.98 2.55 o 1 12 5 0.50 4.49 1.86 o 2 12 5 1.42 -2.13 1.79 o 3 12 5 3.99 3.98 2.09 o 4 12 5 0.61 -3.38 2.25 o 5 12 5 1.01 -2.34 2.08 o 0 13 5 8.21 1.13 2.60 o 1 13 5 2.63 -1.68 1.83 o 2 13 5 1.03 3.19 2.17 o 0 1 6 10.62 30.85 0.90 o 1 1 6 764.80 839.79 5.62 o 0 2 6 833.04 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o 0 4 21 190.79 183.10 4.18 o 1 4 21 40.27 58.11 2.13 o 2 4 21 39.00 41.77 1.96 o 3 4 21 7.08 6.33 1.78 o 4 4 21 3.99 4.66 2.29 o 0 5 21 5.57 7.80 2.66 o 1 5 21 44.93 49.33 2.15 o 2 5 21 14.61 17.79 1.76 o 3 5 21 73.56 85.10 2.62 o 4 5 21 4.21 4.34 1.57 o 5 5 21 1.85 0.33 2.27 o 0 6 21 2.14 -3.22 2.48 o 1 6 21 33.28 36.90 2.16 o 2 6 21 4.95 1.48 1.67 o 3 6 21 8.22 5.68 1.78 o 4 6 21 1.84 0.90 1.63 o 5 6 21 0.46 -1.75 1.65 o 6 6 21 4.63 1.11 2.48 o 0 7 21 3.53 2.58 2.58 o 1 7 21 36.52 42.58 2.72 o 2 7 21 0.42 -2.61 1.74 o 3 7 21 12.69 10.88 2.09 o 4 7 21 1.28 3.22 1.85 o 5 7 21 0.57 -1.15 1.87 o 0 8 21 50.96 83.23 8.11 o 1 8 21 0.21 3.14 2.18 o 2 8 21 2.51 -2.55 1.90 o 3 8 21 5.66 9.52 2.31 o 4 8 21 4.94 3.24 2.18 o 0 9 21 0.14 -1.19 3.40 o 0 1 22 54.99 64.51 2.44 o 1 1 22 88.28 90.88 2.90 o 0 2 22 0.34 -1.31 1.69 o 1 2 22 65.68 64.53 1.93 o 2 2 22 0.01 -3.11 2.40 o 0 3 22 5.82 3.84 1.74 o 1 3 22 4.23 2.32 1.29 o 2 3 22 3.99 4.91 1.41 o 3 3 22 173.32 165.39 4.44 o 0 4 22 0.00 1.81 1.98 o 1 4 22 108.53 117.26 2.62 o 2 4 22 101.03 101.28 2.52 o 3 4 22 20.75 23.01 1.88 o 4 4 22 2.88 3.74 2.35 o 0 5 22 31.87 30.83 3.17 o 1 5 22 9.65 11.77 1.73 o 2 5 22 7.73 9.56 1.74 o 3 5 22 8.53 10.29 1.77 o 4 5 22 3.18 1.44 1.61 o 5 5 22 2.45 -0.09 2.40 o 0 6 22 8.68 5.28 2.71 o 1 6 22 10.29 7.88 2.09 o 2 6 22 10.38 14.72 1.95 o 3 6 22 6.19 4.08 1.79 o 4 6 22 17.61 17.35 1.90 o 5 6 22 4.16 2.17 1.70 o 6 6 22 0.36 -3.70 2.47 o 0 7 22 0.77 4.94 2.80 o 1 7 22 2.53 1.80 2.05 o 2 7 22 3.30 1.89 1.93 o 3 7 22 0.81 2.54 1.99 o 4 7 22 2.30 1.59 1.91 o 0 8 22 3.21 1.97 3.43 o 1 8 22 11.25 13.94 2.49 o 2 8 22 6.96 9.09 2.39 o 0 1 23 42.48 43.43 2.40 o 1 1 23 4.37 -1.15 1.71 o 0 2 23 55.95 55.35 2.58 o 1 2 23 22.68 23.14 1.56 o 2 2 23 6.30 4.72 2.08 o 0 3 23 13.28 11.63 2.21 o 1 3 23 5.19 7.40 1.41 o 2 3 23 14.57 12.62 1.63 o 3 3 23 37.45 43.54 3.12 o 0 4 23 65.81 81.94 3.63 o 1 4 23 25.53 24.18 1.79 o 2 4 23 27.67 27.50 1.95 o 3 4 23 0.68 0.29 1.53 o 4 4 23 19.60 16.13 2.59 o 0 5 23 2.89 4.37 2.69 o 1 5 23 22.38 23.58 2.01 o 2 5 23 16.96 10.60 1.89 o 3 5 23 9.91 6.80 1.72 o 4 5 23 9.01 8.04 1.83 o 5 5 23 5.49 7.84 2.58 o 0 6 23 7.99 5.34 2.74 o 1 6 23 11.64 11.94 2.24 o 2 6 23 1.13 -1.23 1.77 o 3 6 23 7.90 5.24 1.88 o 4 6 23 2.05 0.56 1.86 o 5 6 23 4.48 2.44 1.82 o 0 7 23 12.33 18.14 3.13 o 1 7 23 4.55 5.88 2.23 o 2 7 23 4.43 3.25 2.25 o 3 7 23 6.85 3.07 2.02 o 0 0 24 3.46 -4.62 3.08 o 0 1 24 40.59 57.85 2.64 o 1 1 24 13.23 15.57 2.27 o 0 2 24 0.35 -0.64 1.94 o 1 2 24 34.17 36.88 1.76 o 2 2 24 0.40 -0.81 1.93 o 0 3 24 0.58 1.04 2.00 o 1 3 24 46.34 50.01 1.95 o 2 3 24 21.58 21.47 1.78 o 3 3 24 0.56 -1.78 3.03 o 0 4 24 0.06 0.64 2.29 o 1 4 24 22.03 14.51 1.82 o 2 4 24 7.11 3.67 1.66 o 3 4 24 24.76 26.26 2.03 o 4 4 24 0.14 -2.22 2.28 o 0 5 24 3.43 3.01 2.67 o 1 5 24 24.03 30.02 2.19 o 2 5 24 0.26 0.01 1.81 o 3 5 24 11.33 10.99 1.86 o 4 5 24 2.30 0.51 1.80 o 5 5 24 21.22 28.88 3.16 o 0 6 24 2.92 3.12 2.81 o 1 6 24 5.06 5.80 2.70 o 2 6 24 17.34 21.55 2.36 o 3 6 24 1.44 3.76 1.95 o 0 7 24 22.26 28.43 4.20 o 1 7 24 21.20 22.66 2.58 o 0 1 25 3.83 4.43 2.08 o 1 1 25 21.55 13.01 2.32 o 0 2 25 13.78 15.18 2.46 o 1 2 25 12.89 14.36 1.65 o 2 2 25 0.80 -3.16 2.11 o 0 3 25 5.47 4.63 2.19 o 1 3 25 21.04 16.17 1.78 o 2 3 25 7.36 4.75 1.71 o 3 3 25 2.99 2.96 2.36 o 0 4 25 1.61 2.16 2.37 o 1 4 25 21.01 24.53 2.02 o 2 4 25 2.19 -1.78 1.65 o 3 4 25 0.17 -1.95 1.67 o 4 4 25 7.74 8.13 2.58 o 0 5 25 19.76 8.89 2.97 o 1 5 25 5.19 7.21 2.01 o 2 5 25 8.51 5.73 2.10 o 3 5 25 11.40 9.77 1.97 o 0 6 25 24.25 40.62 3.78 o 1 6 25 23.93 27.19 2.65 o 2 6 25 3.56 0.47 2.27 o 0 1 26 16.71 17.35 2.39 o 1 1 26 5.55 4.42 2.20 o 0 2 26 3.19 6.42 2.32 o 1 2 26 0.13 -0.09 1.62 o 2 2 26 9.21 6.10 2.36 o 0 3 26 24.51 22.26 3.08 o 1 3 26 4.61 7.21 1.77 o 2 3 26 13.58 17.11 1.99 o 3 3 26 4.20 4.80 2.62 o 0 4 26 0.84 -1.75 2.51 o 1 4 26 0.05 0.61 1.83 o 2 4 26 1.72 1.84 1.77 o 3 4 26 1.64 -1.20 1.82 o 0 5 26 1.49 0.92 2.81 o 1 5 26 27.73 28.87 2.50 o 0 1 27 3.63 3.37 2.51 o 1 1 27 3.17 1.79 2.50 o 0 2 27 0.01 -2.40 2.18 o 1 2 27 11.69 8.37 1.97 o 2 2 27 0.73 0.81 2.50 o 0 3 27 23.28 29.20 2.83 o 1 3 27 29.09 35.53 2.26 o 2 3 27 3.85 5.28 1.81 o 0 4 27 0.65 -3.28 2.52 o 0 0 28 108.81 134.17 10.39 o 0 1 28 0.14 4.93 2.92 o 1 1 28 11.97 12.85 2.95 o 0 2 28 1.50 3.18 2.77 o