#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/42/2214248.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214248_Fobs loop_ _publ_author_name 'Sabounchei, Seyyed Javad' 'Dadras, Alireza' 'Jafarzadeh, Mojtaba' 'Khavasi, Hamid Reza' _publ_section_title ; 4-Bromobenzoylmethylene--triphenylphosphorane ylide ; _journal_coeditor_code HK2238 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3160 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.983 _cell_angle_gamma 90.000 _cell_length_a 16.6819 _cell_length_b 10.9590 _cell_length_c 23.7178 _exptl_crystal_F_000 1872.00 _reflns_d_resolution_high 0.7883 _[local]_cod_data_source_file hk2238Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' KH71 SABOUNCHEI/BU ALI UNI/21.05.85' _shelx_refln_list_code 4 _shelx_f_calc_maximum 404.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 30636.72 29261.96 244.94 o 4 0 0 20960.82 20305.19 160.52 o 6 0 0 39445.14 38117.89 170.74 o 8 0 0 460.07 287.71 64.74 o 10 0 0 57553.07 60531.43 174.71 o 12 0 0 14799.72 14609.18 99.30 o 14 0 0 329.88 365.02 65.08 o 16 0 0 4118.20 4194.45 180.72 o 18 0 0 3845.86 3673.58 258.21 o 20 0 0 2020.65 2104.16 73.95 o 1 1 0 834.27 909.70 56.88 o 3 1 0 1004.28 1011.08 57.30 o 5 1 0 76129.73 74804.46 409.70 o 7 1 0 99.67 200.69 46.55 o 9 1 0 6300.64 5841.47 75.64 o 11 1 0 11294.97 10751.41 62.07 o 13 1 0 11.48 86.46 44.75 o 15 1 0 25256.06 25015.15 158.25 o 17 1 0 13912.56 14063.89 220.49 o 19 1 0 5017.84 5123.79 56.70 o 0 2 0 98325.33 97727.25 837.96 o 2 2 0 28143.56 29008.89 205.34 o 4 2 0 1267.42 1386.06 47.18 o 6 2 0 7554.48 7171.72 59.59 o 8 2 0 647.81 644.15 37.02 o 10 2 0 11539.92 10791.40 111.15 o 12 2 0 7887.16 7897.72 93.18 o 14 2 0 1345.61 1264.73 46.21 o 16 2 0 3650.32 3525.72 63.35 o 18 2 0 26.04 131.74 36.97 o 20 2 0 719.95 788.78 43.13 o 1 3 0 24587.09 24932.92 237.27 o 3 3 0 1056.71 1066.40 50.02 o 5 3 0 28903.13 29481.76 249.98 o 7 3 0 2654.24 2384.70 51.50 o 9 3 0 5385.71 5299.75 69.71 o 11 3 0 16043.15 15569.94 115.81 o 13 3 0 2510.10 2411.87 43.80 o 15 3 0 465.27 608.06 57.91 o 17 3 0 1367.60 1389.58 50.14 o 19 3 0 576.88 530.13 42.39 o 0 4 0 19.25 -15.76 79.39 o 2 4 0 2.63 24.88 33.27 o 4 4 0 369.88 333.30 49.14 o 6 4 0 2626.39 2674.11 48.20 o 8 4 0 370.70 362.96 34.71 o 10 4 0 361.46 472.44 43.37 o 12 4 0 1615.76 1566.76 46.36 o 14 4 0 1374.64 1346.75 59.10 o 16 4 0 648.57 734.08 41.06 o 18 4 0 85.73 125.07 39.23 o 1 5 0 120.52 71.38 64.62 o 3 5 0 401.47 414.16 37.83 o 5 5 0 29.02 66.33 33.69 o 7 5 0 26.36 70.53 36.29 o 9 5 0 2003.46 1770.78 40.53 o 11 5 0 4329.21 4114.42 107.12 o 13 5 0 39.01 11.32 42.88 o 15 5 0 2563.81 2526.08 104.22 o 17 5 0 488.03 467.38 40.51 o 19 5 0 916.64 921.67 42.38 o 0 6 0 43805.15 44200.89 130.36 o 2 6 0 7284.07 7314.70 56.30 o 4 6 0 3259.27 3287.73 43.48 o 6 6 0 10219.32 10312.49 106.68 o 8 6 0 36.97 65.06 41.32 o 10 6 0 1587.68 1615.51 34.74 o 12 6 0 11.87 97.12 38.51 o 14 6 0 1107.57 1123.41 40.45 o 16 6 0 318.28 406.50 44.58 o 18 6 0 5.79 82.38 93.13 o 1 7 0 72.65 113.08 35.54 o 3 7 0 2930.92 2919.81 36.39 o 5 7 0 1711.59 1607.98 43.24 o 7 7 0 148.10 155.63 42.52 o 9 7 0 4641.26 4559.16 157.37 o 11 7 0 7327.65 6632.77 64.91 o 13 7 0 1527.91 1555.47 109.64 o 15 7 0 4592.68 4506.54 114.81 o 17 7 0 1212.63 1248.71 105.24 o 0 8 0 24861.30 24246.61 137.43 o 2 8 0 10316.12 9947.71 113.02 o 4 8 0 2673.65 2619.00 36.11 o 6 8 0 17322.70 17586.11 228.95 o 8 8 0 191.03 250.55 28.65 o 10 8 0 4446.34 4412.00 75.09 o 12 8 0 4251.04 4178.80 45.24 o 14 8 0 145.03 241.24 77.60 o 16 8 0 4351.12 4431.81 81.64 o 1 9 0 8179.62 8297.70 185.21 o 3 9 0 541.04 639.14 37.18 o 5 9 0 5315.86 5470.97 108.12 o 7 9 0 1181.78 1249.04 80.18 o 9 9 0 2104.74 2297.19 123.77 o 11 9 0 4603.93 4579.46 46.27 o 13 9 0 357.83 305.34 55.16 o 15 9 0 2954.49 2892.36 94.88 o 0 10 0 864.91 1034.94 81.71 o 2 10 0 323.57 264.88 40.69 o 4 10 0 157.55 230.98 64.31 o 6 10 0 1306.51 1337.51 57.21 o 8 10 0 70.44 136.75 63.93 o 10 10 0 1297.79 1313.93 34.26 o 12 10 0 1295.80 1219.77 45.30 o 14 10 0 605.98 686.01 41.48 o 1 11 0 5866.54 5942.71 95.81 o 3 11 0 3082.03 3271.82 43.05 o 5 11 0 10557.05 10406.04 133.81 o 7 11 0 7234.97 6900.02 56.56 o 9 11 0 259.74 297.78 35.11 o 11 11 0 1819.24 1916.05 92.58 o 0 12 0 280.27 293.47 127.41 o 2 12 0 558.69 586.61 61.80 o 4 12 0 1014.73 987.25 43.88 o 6 12 0 470.07 552.06 65.73 o 8 12 0 1554.16 1591.03 64.35 o 10 12 0 2608.24 2541.66 82.41 o 1 13 0 999.13 916.83 56.51 o 3 13 0 307.75 352.18 61.13 o 5 13 0 38.93 -7.10 38.72 o 7 13 0 331.33 394.79 101.64 o -19 1 1 18.26 -12.07 42.12 o -17 1 1 703.45 697.22 48.19 o -15 1 1 1484.44 1518.12 48.75 o -13 1 1 1287.76 1404.43 47.34 o -11 1 1 7910.13 7723.31 59.19 o -9 1 1 1313.78 1851.27 48.82 o -7 1 1 1917.81 2024.80 47.25 o -5 1 1 23027.57 22832.46 127.55 o -3 1 1 758.82 846.48 62.78 o -1 1 1 523.61 599.77 51.70 o 1 1 1 3976.08 4063.06 76.58 o 3 1 1 21872.03 22054.62 109.93 o 5 1 1 8304.68 8513.54 107.29 o 7 1 1 811.35 765.58 43.47 o 9 1 1 291.99 180.64 39.21 o 11 1 1 146.04 135.21 37.68 o 13 1 1 31.02 53.08 39.47 o 15 1 1 4448.62 4482.81 54.37 o 17 1 1 1172.11 1142.23 48.47 o 19 1 1 1530.04 1596.95 51.31 o -20 2 1 1321.46 1406.83 51.94 o -18 2 1 12.87 -23.94 45.63 o -16 2 1 616.00 778.69 46.08 o -14 2 1 108.80 121.80 39.59 o -12 2 1 1389.44 1272.90 41.50 o -10 2 1 3771.99 3878.73 51.62 o -8 2 1 3904.00 3931.81 49.07 o -6 2 1 43612.36 44545.52 146.33 o -4 2 1 30747.48 31638.53 156.82 o -2 2 1 34874.65 34905.93 282.22 o 0 2 1 51138.18 51333.18 176.92 o 2 2 1 50230.18 51718.39 489.70 o 4 2 1 85953.54 88100.42 614.10 o 6 2 1 4539.98 4210.79 46.24 o 8 2 1 549.02 655.47 43.51 o 10 2 1 10738.50 10778.70 69.98 o 12 2 1 10673.84 10176.89 57.50 o 14 2 1 706.19 783.99 101.35 o 16 2 1 2191.07 2247.40 54.27 o 18 2 1 481.43 513.62 63.74 o 20 2 1 299.57 350.03 41.93 o -19 3 1 1090.73 1091.51 42.78 o -17 3 1 11487.01 11138.89 102.43 o -15 3 1 5454.24 5455.49 109.94 o -13 3 1 7918.28 7714.63 61.56 o -11 3 1 33182.85 32098.45 207.58 o -9 3 1 2369.18 2312.41 39.90 o -7 3 1 7684.55 9821.38 78.20 o -5 3 1 9702.68 8694.85 135.66 o -3 3 1 89.96 54.68 42.50 o -1 3 1 32984.57 33026.77 113.18 o 1 3 1 11714.24 11633.34 90.91 o 3 3 1 1267.90 1129.94 43.18 o 5 3 1 9075.96 8620.56 59.60 o 7 3 1 90.34 127.45 34.98 o 9 3 1 16231.17 15929.03 155.63 o 11 3 1 1208.67 1307.07 48.50 o 13 3 1 5513.48 5241.04 52.50 o 15 3 1 10242.17 10342.61 57.49 o 17 3 1 882.24 889.12 45.99 o 19 3 1 5460.68 5290.58 51.21 o -20 4 1 296.58 402.52 65.72 o -18 4 1 67.27 78.10 52.19 o -16 4 1 3455.51 3426.65 58.03 o -14 4 1 322.46 472.27 44.20 o -12 4 1 4906.13 4806.49 68.33 o -10 4 1 1152.96 1110.99 44.38 o -8 4 1 5661.72 5523.55 84.79 o -6 4 1 30025.26 29885.12 419.44 o -4 4 1 2513.04 2702.32 44.00 o -2 4 1 33689.74 33658.28 108.33 o 0 4 1 27317.97 26958.43 139.50 o 2 4 1 5674.92 6547.70 52.02 o 4 4 1 106273.15 110144.29 1148.36 o 6 4 1 28697.55 28857.69 178.49 o 8 4 1 1074.86 1406.90 40.18 o 10 4 1 12090.86 12094.89 58.84 o 12 4 1 7216.26 7187.89 51.90 o 14 4 1 5323.62 5428.95 69.95 o 16 4 1 4839.29 4763.35 135.55 o 18 4 1 384.45 426.56 53.89 o -19 5 1 118.83 131.86 40.16 o -17 5 1 4961.14 5159.58 53.05 o -15 5 1 10333.66 10294.12 99.97 o -13 5 1 2683.98 2494.22 55.37 o -11 5 1 25767.24 25809.44 175.68 o -9 5 1 4162.92 4332.90 74.92 o -7 5 1 7760.14 7310.41 59.13 o -5 5 1 32044.54 31959.02 124.08 o -3 5 1 251.13 371.62 34.28 o -1 5 1 14573.20 14466.01 63.32 o 1 5 1 26719.52 27149.70 288.31 o 3 5 1 278.24 266.81 34.39 o 5 5 1 11762.92 11416.61 98.09 o 7 5 1 1647.33 1677.23 37.13 o 9 5 1 3273.38 3108.95 67.06 o 11 5 1 8599.67 8127.46 58.07 o 13 5 1 4507.04 4435.86 92.58 o 15 5 1 11424.17 11289.82 60.15 o 17 5 1 3479.74 3501.56 50.11 o 19 5 1 905.16 841.94 41.39 o -18 6 1 215.03 308.56 51.87 o -16 6 1 6209.67 5843.52 106.57 o -14 6 1 388.59 361.97 52.09 o -12 6 1 10332.77 10018.37 78.66 o -10 6 1 10072.00 10074.04 118.20 o -8 6 1 52.27 117.09 46.97 o -6 6 1 18789.21 18788.00 163.73 o -4 6 1 8256.88 8434.68 74.54 o -2 6 1 6573.11 6684.68 61.38 o 0 6 1 23231.65 22682.35 75.29 o 2 6 1 1218.47 1275.86 39.60 o 4 6 1 16080.88 15971.87 68.71 o 6 6 1 9525.91 8764.77 129.82 o 8 6 1 14.12 8.56 46.60 o 10 6 1 12803.03 12601.60 184.60 o 12 6 1 7107.27 7185.17 203.21 o 14 6 1 1143.92 1164.29 67.27 o 16 6 1 3570.21 3507.68 41.56 o 18 6 1 176.74 67.28 47.92 o -17 7 1 65.02 23.59 68.30 o -15 7 1 1021.70 896.01 37.32 o -13 7 1 1520.39 1485.10 83.33 o -11 7 1 574.97 600.34 35.94 o -9 7 1 1073.29 1105.89 34.46 o -7 7 1 3916.39 4045.07 38.66 o -5 7 1 12775.63 12853.48 102.91 o -3 7 1 3085.67 3175.32 78.70 o -1 7 1 8399.17 7979.24 115.32 o 1 7 1 6675.13 6753.01 105.15 o 3 7 1 6041.08 5842.84 41.34 o 5 7 1 24315.76 24040.18 212.86 o 7 7 1 137.72 232.58 33.19 o 9 7 1 1848.63 2022.93 33.40 o 11 7 1 14132.42 13405.91 98.11 o 13 7 1 66.97 124.76 44.67 o 15 7 1 989.35 1248.53 72.60 o 17 7 1 952.65 934.78 44.65 o -16 8 1 3444.68 3505.73 71.24 o -14 8 1 1097.63 907.17 50.76 o -12 8 1 870.85 926.13 47.18 o -10 8 1 68.17 135.05 107.30 o -8 8 1 416.60 400.12 37.96 o -6 8 1 195.76 242.70 50.83 o -4 8 1 3832.63 3634.31 81.21 o -2 8 1 6390.50 6429.84 54.82 o 0 8 1 1199.46 1170.07 34.56 o 2 8 1 297.51 433.71 30.91 o 4 8 1 1368.33 1447.12 86.56 o 6 8 1 166.42 183.36 51.41 o 8 8 1 42.73 81.99 56.96 o 10 8 1 2703.82 2504.06 42.59 o 12 8 1 32.99 84.14 57.28 o 14 8 1 2552.09 2268.69 52.38 o 16 8 1 863.21 985.73 53.13 o -15 9 1 83.14 209.16 44.81 o -13 9 1 1162.73 1117.11 40.23 o -11 9 1 548.16 573.84 60.34 o -9 9 1 2.79 67.32 52.58 o -7 9 1 139.81 318.00 40.74 o -5 9 1 1183.06 1413.87 38.29 o -3 9 1 1037.79 1049.60 59.70 o -1 9 1 10557.86 10739.10 194.56 o 1 9 1 1169.99 1241.99 51.64 o 3 9 1 17.76 49.24 30.94 o 5 9 1 5414.38 5276.13 164.61 o 7 9 1 117.94 242.66 59.67 o 9 9 1 138.42 218.01 42.58 o 11 9 1 4973.53 4480.73 58.17 o 13 9 1 2855.88 2947.32 87.27 o 15 9 1 89.93 87.41 39.74 o -14 10 1 306.45 336.59 53.05 o -12 10 1 111.93 67.25 39.18 o -10 10 1 170.40 304.35 65.78 o -8 10 1 1467.17 1585.13 72.91 o -6 10 1 575.86 538.85 68.28 o -4 10 1 492.87 522.11 29.69 o -2 10 1 1331.94 1275.05 38.40 o 0 10 1 748.64 944.36 68.49 o 2 10 1 1.04 77.41 32.26 o 4 10 1 3369.44 3317.21 38.88 o 6 10 1 2498.55 2424.98 34.77 o 8 10 1 207.41 337.37 40.96 o 10 10 1 366.17 333.50 53.06 o 12 10 1 277.46 172.17 36.26 o 14 10 1 4.85 70.72 63.07 o -11 11 1 2429.00 2346.90 42.77 o -9 11 1 1883.20 1778.53 38.64 o -7 11 1 63.49 132.89 36.85 o -5 11 1 4860.01 4794.32 71.18 o -3 11 1 5.69 8.20 33.12 o -1 11 1 125.47 297.04 102.21 o 1 11 1 11297.22 11253.29 138.88 o 3 11 1 63.88 160.81 44.08 o 5 11 1 580.33 442.50 33.92 o 7 11 1 134.79 84.68 40.94 o 9 11 1 1902.40 1765.88 129.10 o 11 11 1 239.22 306.71 39.59 o -10 12 1 1269.44 1270.87 73.42 o -8 12 1 64.94 93.20 40.75 o -6 12 1 537.45 575.03 75.79 o -4 12 1 1771.66 1876.47 75.63 o -2 12 1 637.65 676.29 41.44 o 0 12 1 903.55 951.21 39.22 o 2 12 1 6.15 15.19 66.95 o 4 12 1 2309.46 2300.44 207.12 o 6 12 1 3778.89 3797.47 56.90 o 8 12 1 224.99 355.90 56.81 o 10 12 1 640.77 791.55 77.03 o -7 13 1 24.67 16.11 63.98 o -5 13 1 1847.38 1916.28 74.28 o -3 13 1 3085.81 3029.94 99.16 o -1 13 1 922.95 1157.64 60.77 o 1 13 1 2177.94 2358.31 41.93 o 3 13 1 2585.92 2592.05 96.93 o 5 13 1 1495.75 1652.66 42.12 o 7 13 1 313.62 406.19 32.26 o -20 0 2 4670.80 4416.97 143.47 o -18 0 2 725.32 780.28 84.94 o -16 0 2 10277.12 10088.20 91.41 o -14 0 2 1773.35 1792.72 116.15 o -12 0 2 9663.26 9804.31 91.49 o -10 0 2 4309.84 4270.13 76.43 o -8 0 2 5394.58 5358.03 86.64 o -6 0 2 31997.27 30967.90 172.17 o 0 0 2 3921.06 3740.84 130.47 o 2 0 2 26785.15 26715.35 195.84 o 4 0 2 32483.83 31062.01 241.90 o 6 0 2 61048.55 60422.10 590.10 o 8 0 2 2924.83 2320.72 59.37 o 10 0 2 44590.79 42818.09 142.75 o 12 0 2 3027.18 2837.61 191.15 o 14 0 2 8282.36 8398.88 75.00 o 16 0 2 22636.59 23745.93 424.94 o 18 0 2 441.13 349.48 57.83 o 20 0 2 508.33 555.11 135.19 o -19 1 2 4999.17 5061.05 55.18 o -17 1 2 14842.37 15127.87 103.62 o -15 1 2 420.73 434.68 45.49 o -13 1 2 14107.69 13893.32 68.33 o -11 1 2 12324.82 11659.19 66.68 o -9 1 2 6847.59 7053.59 61.54 o -7 1 2 28406.51 27722.24 157.66 o -5 1 2 24340.34 23787.56 165.38 o -3 1 2 9871.92 10350.85 100.65 o -1 1 2 44566.56 44797.83 338.08 o 1 1 2 6653.94 7158.56 81.55 o 3 1 2 152.46 160.90 60.10 o 5 1 2 44065.09 44146.98 151.60 o 7 1 2 663.34 644.99 36.16 o 9 1 2 4560.77 4338.82 50.72 o 11 1 2 12911.88 12804.15 101.90 o 13 1 2 455.96 563.91 38.61 o 15 1 2 7639.73 7745.18 121.14 o 17 1 2 2413.51 2374.56 61.52 o 19 1 2 3731.82 3905.26 54.00 o -20 2 2 949.59 927.27 66.53 o -18 2 2 43.30 158.61 45.66 o -16 2 2 4010.53 4171.61 58.41 o -14 2 2 179.51 272.55 38.35 o -12 2 2 2295.18 2171.48 47.59 o -10 2 2 69.28 73.89 42.20 o -8 2 2 10976.35 11306.90 67.22 o -6 2 2 3646.82 3209.20 50.71 o -4 2 2 416.14 358.09 49.92 o -2 2 2 163407.41 165572.36 489.93 o 0 2 2 5006.10 4970.07 62.92 o 2 2 2 28665.23 28988.35 109.69 o 4 2 2 11502.06 11432.33 72.77 o 6 2 2 6774.60 6408.97 58.68 o 8 2 2 4645.78 4496.19 51.92 o 10 2 2 29862.94 30204.41 187.96 o 12 2 2 2279.65 2242.86 70.62 o 14 2 2 3230.28 3323.73 155.67 o 16 2 2 16468.10 16386.04 71.45 o 18 2 2 326.97 301.98 38.95 o 20 2 2 700.68 765.36 49.55 o -19 3 2 624.46 661.07 46.41 o -17 3 2 3810.45 3936.33 53.74 o -15 3 2 2058.49 2047.83 68.76 o -13 3 2 152.30 238.00 45.02 o -11 3 2 4474.73 4500.22 48.36 o -9 3 2 1231.63 1645.12 43.30 o -7 3 2 34921.31 36965.55 192.45 o -5 3 2 17844.14 18945.78 197.62 o -3 3 2 9987.04 10680.99 68.78 o -1 3 2 25519.26 26115.55 176.62 o 1 3 2 14753.74 14963.82 131.70 o 3 3 2 13904.21 14095.05 74.21 o 5 3 2 9694.69 9372.35 105.56 o 7 3 2 78.52 140.67 32.38 o 9 3 2 2133.09 2070.46 39.69 o 11 3 2 2474.84 2384.91 43.11 o 13 3 2 796.79 824.52 61.38 o 15 3 2 2194.62 2084.79 51.07 o 17 3 2 411.92 475.12 46.05 o 19 3 2 76.97 98.85 46.37 o -20 4 2 37.30 9.61 47.20 o -18 4 2 303.92 376.09 50.28 o -16 4 2 3436.32 3401.38 50.55 o -14 4 2 4194.21 4001.86 48.44 o -12 4 2 4639.70 4646.94 51.51 o -10 4 2 2403.90 2408.26 44.40 o -8 4 2 48.42 34.07 37.41 o -6 4 2 1150.49 1023.74 40.41 o -4 4 2 8882.77 8958.77 118.48 o -2 4 2 1491.19 1658.03 43.90 o 0 4 2 14745.29 14898.21 113.28 o 2 4 2 10163.14 11720.99 81.55 o 4 4 2 1099.74 1223.45 38.28 o 6 4 2 7.97 48.39 41.68 o 8 4 2 2.38 32.85 57.38 o 10 4 2 2348.80 2365.03 43.25 o 12 4 2 855.58 938.58 50.95 o 14 4 2 19.66 87.70 38.60 o 16 4 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