#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214269.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214269_Fobs loop_ _publ_author_name 'Gao, Shang' 'Peng, Xiao-Jun' _publ_section_title ; [\m-2-(9-Anthrylmethyl)-2-azapropane-1,3-dithiolato-\k^4^S:S']bis[tricarbonyliron(I)] ; _journal_coeditor_code HY2063 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1997 _journal_volume 63 _journal_year 2007 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.2345 _cell_length_b 11.9452 _cell_length_c 25.8399 _exptl_crystal_F_000 2336.00 _reflns_d_resolution_high 0.7745 _[local]_cod_data_source_file hy2063Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' good in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 444.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 81493.11 79399.87 1146.78 o 4 0 0 49805.73 51935.75 947.95 o 6 0 0 56302.17 55960.40 1473.29 o 8 0 0 110268.09 107994.30 2778.19 o 10 0 0 54018.95 48599.67 1375.02 o 12 0 0 1176.82 1158.06 170.77 o 14 0 0 11.77 -77.29 77.29 o 16 0 0 1621.94 1599.16 226.72 o 18 0 0 1849.71 1577.44 246.96 o 1 1 0 6.45 -9.03 9.03 o 3 1 0 64541.60 67433.75 851.59 o 5 1 0 18174.72 18984.40 315.46 o 7 1 0 916.75 897.53 57.21 o 9 1 0 1610.23 1678.67 109.03 o 11 1 0 12.99 -0.72 49.59 o 13 1 0 196.25 154.20 70.90 o 15 1 0 314.97 254.77 90.78 o 17 1 0 59.05 -23.53 76.58 o 19 1 0 237.21 156.11 106.66 o 0 2 0 122012.16 112191.86 2768.07 o 2 2 0 62877.21 64378.89 940.34 o 4 2 0 111533.76 110925.47 1393.18 o 6 2 0 9536.51 10182.90 172.19 o 8 2 0 44011.32 45709.53 735.32 o 10 2 0 9587.36 9362.04 227.05 o 12 2 0 1216.06 1168.17 139.86 o 14 2 0 324.65 474.39 94.71 o 16 2 0 328.39 336.61 109.59 o 18 2 0 117.11 120.19 96.80 o 1 3 0 191.34 207.04 17.86 o 3 3 0 21432.45 21895.31 301.12 o 5 3 0 3758.83 3995.23 85.57 o 7 3 0 233.90 190.65 27.26 o 9 3 0 4143.48 4402.03 139.36 o 11 3 0 61.02 60.15 61.81 o 13 3 0 648.76 700.82 160.10 o 15 3 0 10.73 -54.01 54.01 o 17 3 0 174.01 58.99 80.60 o 19 3 0 440.96 666.65 139.54 o 0 4 0 102749.44 101113.51 2527.92 o 2 4 0 21323.53 22310.59 428.61 o 4 4 0 38437.41 37639.75 504.16 o 6 4 0 22883.71 21075.89 311.86 o 8 4 0 3964.24 4045.06 193.37 o 10 4 0 822.86 736.07 71.50 o 12 4 0 659.41 651.00 106.73 o 14 4 0 4068.28 4089.28 172.44 o 16 4 0 625.59 589.97 273.37 o 18 4 0 32.21 -68.61 68.61 o 1 5 0 105.23 126.70 19.85 o 3 5 0 1302.89 1169.28 43.41 o 5 5 0 22197.90 22014.50 321.55 o 7 5 0 3345.40 3554.11 90.61 o 9 5 0 1971.25 1688.15 94.26 o 11 5 0 131.57 131.79 47.80 o 13 5 0 1568.33 1462.14 174.65 o 15 5 0 243.40 198.16 73.32 o 17 5 0 549.62 543.79 118.64 o 0 6 0 29126.59 29925.64 601.51 o 2 6 0 39974.17 39435.18 535.35 o 4 6 0 9166.62 8372.35 237.64 o 6 6 0 18983.94 18331.36 346.67 o 8 6 0 12281.82 11664.97 311.68 o 10 6 0 2743.26 2806.50 124.07 o 12 6 0 1579.99 1562.82 113.34 o 14 6 0 1499.34 1347.93 117.22 o 16 6 0 755.49 958.43 208.45 o 18 6 0 12.42 -36.04 87.74 o 1 7 0 4096.38 3659.71 170.96 o 3 7 0 2510.18 2475.46 71.69 o 5 7 0 9387.12 9554.09 218.35 o 7 7 0 121.32 138.64 40.63 o 9 7 0 4491.46 4440.73 155.18 o 11 7 0 19.01 55.13 61.36 o 13 7 0 1288.70 1261.88 127.82 o 15 7 0 4.75 -41.99 68.52 o 17 7 0 54.37 109.13 84.28 o 0 8 0 159.17 197.63 35.56 o 2 8 0 292.12 276.21 47.54 o 4 8 0 163.22 116.61 36.33 o 6 8 0 458.95 440.77 55.73 o 8 8 0 195.68 153.46 44.19 o 10 8 0 1.64 -27.37 51.39 o 12 8 0 37.66 9.52 45.90 o 14 8 0 49.29 67.94 57.44 o 16 8 0 42.41 5.50 68.16 o 1 9 0 22509.25 22836.95 366.36 o 3 9 0 1566.37 1533.90 88.99 o 5 9 0 1127.87 1281.93 139.37 o 7 9 0 2889.47 2907.66 127.88 o 9 9 0 4329.62 4234.25 258.96 o 11 9 0 65.02 88.83 50.71 o 13 9 0 464.32 561.52 125.68 o 15 9 0 93.90 125.70 88.73 o 0 10 0 4801.18 5095.48 194.05 o 2 10 0 13269.45 13810.44 260.39 o 4 10 0 5428.88 5338.61 273.20 o 6 10 0 1994.60 2043.32 153.18 o 8 10 0 6759.39 6762.84 205.31 o 10 10 0 1177.54 1192.32 128.61 o 12 10 0 275.42 205.82 80.82 o 14 10 0 527.79 344.83 105.67 o 1 11 0 3140.80 3500.69 118.28 o 3 11 0 21.61 -30.97 30.97 o 5 11 0 2835.65 2992.44 174.32 o 7 11 0 328.61 340.57 77.29 o 9 11 0 1822.57 1622.90 147.03 o 11 11 0 30.73 -39.30 56.74 o 13 11 0 89.04 -14.71 82.44 o 0 12 0 2222.41 2114.24 208.50 o 2 12 0 707.95 644.18 94.10 o 4 12 0 1910.18 2004.88 120.80 o 6 12 0 1086.52 1285.23 136.39 o 8 12 0 120.81 168.54 72.57 o 10 12 0 435.00 342.15 90.17 o 12 12 0 229.84 168.99 89.31 o 1 13 0 3.41 -14.78 46.20 o 3 13 0 34.08 -0.64 50.24 o 5 13 0 56.66 61.46 84.28 o 7 13 0 694.13 520.97 148.51 o 9 13 0 43.10 -84.83 84.83 o 0 14 0 1415.21 1335.45 193.96 o 2 14 0 157.52 236.58 74.44 o 4 14 0 70.64 147.77 98.27 o 6 14 0 0.44 205.55 106.92 o 8 14 0 778.86 741.43 194.51 o 1 15 0 275.62 -37.54 88.51 o 3 15 0 49.73 -84.28 84.28 o 1 1 1 49045.77 49208.95 505.24 o 2 1 1 35982.25 36663.34 382.22 o 3 1 1 14493.02 14930.75 148.53 o 4 1 1 2736.69 2928.03 49.58 o 5 1 1 16993.42 17399.27 181.23 o 6 1 1 18978.06 18425.24 209.34 o 7 1 1 6210.70 5882.17 94.24 o 8 1 1 3033.54 2862.96 70.29 o 9 1 1 14315.09 14772.61 230.95 o 10 1 1 96.34 100.26 34.44 o 11 1 1 1400.57 1372.22 83.54 o 12 1 1 43.64 73.64 40.75 o 13 1 1 0.63 -3.60 49.21 o 14 1 1 3135.43 2893.63 164.55 o 15 1 1 438.98 477.26 70.82 o 16 1 1 1817.53 1862.18 120.13 o 17 1 1 301.82 181.23 63.53 o 18 1 1 149.81 202.51 86.70 o 19 1 1 60.68 58.87 70.98 o 0 2 1 6963.57 7361.87 107.49 o 1 2 1 7420.60 7493.10 84.23 o 2 2 1 1863.24 2018.05 35.23 o 3 2 1 17394.08 18500.06 180.41 o 4 2 1 41798.97 42353.06 392.45 o 5 2 1 19515.79 19232.45 212.57 o 6 2 1 7404.01 7969.31 110.56 o 7 2 1 2084.40 2123.65 52.93 o 8 2 1 6040.78 6024.88 101.02 o 9 2 1 97.02 99.42 21.92 o 10 2 1 3895.36 4336.44 109.32 o 11 2 1 1205.66 1370.23 71.67 o 12 2 1 579.48 640.07 87.76 o 13 2 1 5951.68 6018.92 306.55 o 14 2 1 172.96 199.12 52.39 o 15 2 1 423.09 427.43 70.24 o 16 2 1 468.59 408.80 71.38 o 17 2 1 2.89 24.20 55.82 o 18 2 1 53.25 -4.69 56.46 o 19 2 1 77.56 28.60 69.60 o 1 3 1 3153.04 3291.24 49.19 o 2 3 1 3736.05 3833.66 56.41 o 3 3 1 2749.10 2825.25 65.57 o 4 3 1 11395.46 11072.03 121.49 o 5 3 1 1695.21 1690.15 42.89 o 6 3 1 5557.71 5512.04 140.11 o 7 3 1 2597.78 2827.65 62.91 o 8 3 1 7823.47 7821.43 141.15 o 9 3 1 2162.54 2371.89 91.17 o 10 3 1 4425.26 4363.93 103.18 o 11 3 1 151.22 120.94 32.19 o 12 3 1 374.56 365.38 60.83 o 13 3 1 32.62 -32.84 32.84 o 14 3 1 30.49 4.14 40.26 o 15 3 1 365.60 368.59 66.49 o 16 3 1 80.06 95.22 56.18 o 17 3 1 16.22 -5.94 49.36 o 18 3 1 7.31 34.61 60.50 o 19 3 1 14.92 35.06 67.49 o 0 4 1 3540.50 3576.81 86.52 o 1 4 1 637.86 641.52 27.09 o 2 4 1 2574.89 2797.26 49.54 o 3 4 1 12702.29 12910.41 150.77 o 4 4 1 2811.52 2818.25 50.13 o 5 4 1 575.41 629.51 24.84 o 6 4 1 4541.34 4713.45 81.46 o 7 4 1 631.13 643.33 33.77 o 8 4 1 1745.16 1713.91 53.47 o 9 4 1 558.52 494.51 41.19 o 10 4 1 446.48 517.25 38.34 o 11 4 1 3695.36 3867.81 103.12 o 12 4 1 2357.79 2400.26 121.93 o 13 4 1 1681.07 1979.88 87.44 o 14 4 1 355.82 236.42 68.71 o 15 4 1 230.31 88.68 50.49 o 16 4 1 546.70 359.71 88.45 o 17 4 1 109.48 125.38 57.65 o 18 4 1 202.34 171.33 74.16 o 1 5 1 21291.53 21452.61 232.42 o 2 5 1 12.34 -4.14 9.53 o 3 5 1 12395.48 12039.10 147.07 o 4 5 1 4003.47 3885.73 67.77 o 5 5 1 9981.55 9620.06 115.90 o 6 5 1 100.38 116.36 15.56 o 7 5 1 11729.15 11424.56 190.84 o 8 5 1 103.15 66.50 20.05 o 9 5 1 3646.88 3551.21 117.52 o 10 5 1 519.78 537.88 46.74 o 11 5 1 493.83 412.36 52.02 o 12 5 1 3486.73 3661.60 114.52 o 13 5 1 389.10 456.85 58.82 o 14 5 1 1233.28 1312.59 79.69 o 15 5 1 432.77 585.66 68.34 o 16 5 1 59.28 118.90 55.11 o 17 5 1 397.07 267.71 68.64 o 18 5 1 132.53 134.24 68.44 o 0 6 1 95.47 52.62 18.77 o 1 6 1 9681.29 9475.77 114.77 o 2 6 1 171.14 184.39 16.86 o 3 6 1 5592.15 5465.22 77.60 o 4 6 1 1691.52 1668.39 50.51 o 5 6 1 2198.40 2070.29 51.57 o 6 6 1 1078.54 1087.88 50.08 o 7 6 1 8573.47 8311.83 142.68 o 8 6 1 174.51 145.04 29.34 o 9 6 1 48.90 71.50 25.78 o 10 6 1 1.64 0.33 26.25 o 11 6 1 1163.86 1127.66 66.72 o 12 6 1 18.78 23.25 31.50 o 13 6 1 111.70 208.88 43.27 o 14 6 1 28.07 62.80 39.47 o 15 6 1 739.92 813.78 72.98 o 16 6 1 0.02 26.34 46.66 o 17 6 1 164.06 184.79 66.24 o 18 6 1 3.67 24.71 69.21 o 1 7 1 3297.69 3285.48 56.87 o 2 7 1 338.33 325.17 37.87 o 3 7 1 1756.70 1837.08 50.91 o 4 7 1 219.22 169.86 24.26 o 5 7 1 671.94 600.31 41.54 o 6 7 1 1164.22 1118.34 57.41 o 7 7 1 5370.31 5169.67 110.15 o 8 7 1 654.27 585.22 45.19 o 9 7 1 1153.64 1243.07 66.15 o 10 7 1 51.50 11.98 27.23 o 11 7 1 6.16 49.33 30.53 o 12 7 1 2203.52 2203.80 92.32 o 13 7 1 58.06 79.86 37.69 o 14 7 1 853.92 802.96 70.31 o 15 7 1 206.29 156.71 49.34 o 16 7 1 29.33 64.72 46.53 o 17 7 1 68.11 89.42 59.68 o 0 8 1 1808.12 1754.26 62.23 o 1 8 1 4975.59 4829.07 75.95 o 2 8 1 124.72 108.98 20.18 o 3 8 1 4901.86 4976.88 125.60 o 4 8 1 161.92 90.37 25.76 o 5 8 1 6348.08 6048.47 119.82 o 6 8 1 646.37 611.34 42.13 o 7 8 1 6847.62 6682.43 135.32 o 8 8 1 125.56 173.73 34.99 o 9 8 1 24.64 29.64 26.34 o 10 8 1 57.24 43.75 30.26 o 11 8 1 85.43 64.95 34.10 o 12 8 1 126.97 92.34 37.20 o 13 8 1 80.55 5.43 37.03 o 14 8 1 7.10 -1.26 39.80 o 15 8 1 921.51 991.92 81.28 o 16 8 1 2.86 -43.25 43.36 o 1 9 1 1014.18 956.85 40.89 o 2 9 1 98.07 104.33 24.89 o 3 9 1 3884.90 3951.77 94.59 o 4 9 1 108.09 106.06 27.69 o 5 9 1 350.14 390.25 52.00 o 6 9 1 98.57 123.76 30.55 o 7 9 1 1465.53 1418.01 105.09 o 8 9 1 201.09 144.24 41.57 o 9 9 1 1026.59 1025.38 80.40 o 10 9 1 136.55 145.38 36.22 o 11 9 1 22.96 16.37 31.72 o 12 9 1 25.89 -36.28 36.28 o 13 9 1 75.18 137.47 48.56 o 14 9 1 71.55 60.61 47.52 o 15 9 1 226.60 210.85 60.87 o 0 10 1 913.14 823.08 63.44 o 1 10 1 1058.09 1139.20 50.84 o 2 10 1 858.93 936.04 44.66 o 3 10 1 960.34 1093.50 54.97 o 4 10 1 672.28 560.76 47.44 o 5 10 1 903.66 955.64 59.14 o 6 10 1 16.01 22.40 29.36 o 7 10 1 1468.30 1540.27 82.63 o 8 10 1 168.45 236.85 41.17 o 9 10 1 71.66 57.11 34.13 o 10 10 1 61.88 22.99 35.36 o 11 10 1 118.55 56.88 41.51 o 12 10 1 45.14 3.46 41.38 o 13 10 1 67.47 27.81 50.82 o 14 10 1 8.85 -60.37 60.37 o 1 11 1 3698.20 3806.53 97.55 o 2 11 1 116.39 132.73 30.21 o 3 11 1 87.88 38.94 35.43 o 4 11 1 222.79 182.80 36.91 o 5 11 1 1215.10 1254.41 76.60 o 6 11 1 678.01 637.21 61.22 o 7 11 1 3932.27 3920.49 140.43 o 8 11 1 30.72 14.27 37.21 o 9 11 1 345.77 385.04 59.08 o 10 11 1 161.86 201.39 51.80 o 11 11 1 11.28 0.53 42.78 o 12 11 1 847.04 845.25 88.88 o 13 11 1 51.08 8.63 55.31 o 0 12 1 303.37 370.96 60.67 o 1 12 1 76.18 97.63 34.17 o 2 12 1 3.36 22.74 30.61 o 3 12 1 127.06 112.00 35.83 o 4 12 1 73.54 33.53 38.66 o 5 12 1 169.88 139.72 55.98 o 6 12 1 328.03 278.32 64.88 o 7 12 1 12.94 32.85 41.06 o 8 12 1 156.23 148.64 49.24 o 9 12 1 3.01 -13.94 40.27 o 10 12 1 3.31 4.57 43.10 o 11 12 1 133.43 146.64 54.47 o 12 12 1 473.96 420.57 75.07 o 1 13 1 7.01 -20.64 33.18 o 2 13 1 240.60 194.06 47.90 o 3 13 1 79.76 109.80 50.54 o 4 13 1 249.52 312.72 62.88 o 5 13 1 13.96 65.10 99.00 o 6 13 1 0.25 -89.11 91.09 o 7 13 1 105.50 87.59 116.85 o 8 13 1 209.78 160.79 64.03 o 9 13 1 238.39 280.69 72.52 o 10 13 1 159.20 75.13 68.04 o 0 14 1 116.72 81.48 64.32 o 1 14 1 5.61 14.20 37.86 o 2 14 1 37.82 23.79 46.40 o 3 14 1 40.17 130.55 69.84 o 4 14 1 9.05 -49.30 49.30 o 5 14 1 51.49 83.86 67.66 o 6 14 1 367.96 421.20 157.52 o 7 14 1 15.90 -53.11 71.08 o 8 14 1 37.77 88.44 90.17 o 1 15 1 600.09 473.53 81.65 o 2 15 1 507.87 453.86 104.44 o 3 15 1 31.28 15.01 93.30 o 4 15 1 106.00 123.20 76.06 o 1 0 2 19998.94 20650.54 308.84 o 2 0 2 26456.62 27025.32 350.08 o 3 0 2 71752.42 71046.10 895.50 o 4 0 2 71418.99 73406.23 932.95 o 5 0 2 14378.29 14914.64 224.02 o 6 0 2 4233.59 4051.64 117.27 o 7 0 2 67783.89 66252.98 1006.36 o 8 0 2 2227.04 1965.24 104.95 o 9 0 2 21.85 17.65 29.02 o 10 0 2 2737.89 2587.11 138.12 o 11 0 2 977.67 1060.71 108.20 o 12 0 2 802.61 842.82 105.91 o 13 0 2 1317.59 1444.11 134.74 o 14 0 2 1.55 -6.32 65.44 o 15 0 2 5275.29 5403.67 289.28 o 16 0 2 0.10 11.26 72.85 o 17 0 2 261.76 315.75 102.02 o 18 0 2 77.77 3.32 86.92 o 19 0 2 164.30 158.92 104.36 o 1 1 2 16837.81 16868.35 200.56 o 2 1 2 124.69 124.56 8.98 o 3 1 2 21050.02 21438.59 220.27 o 4 1 2 17834.03 18389.77 194.77 o 5 1 2 28516.87 28800.83 300.29 o 6 1 2 1158.69 1186.79 45.63 o 7 1 2 8655.22 9121.48 126.37 o 8 1 2 478.60 533.64 36.22 o 9 1 2 759.18 775.67 44.39 o 10 1 2 34.02 76.67 37.79 o 11 1 2 105.54 59.59 36.38 o 12 1 2 1933.00 2015.56 115.42 o 13 1 2 171.03 206.69 58.83 o 14 1 2 452.99 501.44 69.74 o 15 1 2 95.06 208.87 57.98 o 16 1 2 6.22 43.95 52.64 o 17 1 2 53.09 63.62 56.31 o 18 1 2 73.19 80.60 60.87 o 19 1 2 0.05 -15.73 67.78 o 0 2 2 17892.22 18562.08 219.91 o 1 2 2 36863.89 37356.84 361.40 o 2 2 2 1908.72 1896.38 34.73 o 3 2 2 24219.82 25113.45 240.68 o 4 2 2 10496.75 10834.46 120.90 o 5 2 2 6889.15 6869.83 89.50 o 6 2 2 1993.33 2240.74 50.97 o 7 2 2 20486.11 20241.09 234.17 o 8 2 2 1162.74 1314.16 47.09 o 9 2 2 4357.00 4431.50 94.88 o 10 2 2 506.23 537.49 42.98 o 11 2 2 1746.02 1714.72 78.34 o 12 2 2 1200.22 1258.54 138.01 o 13 2 2 486.95 455.31 63.69 o 14 2 2 662.98 613.29 71.85 o 15 2 2 1048.52 1140.25 95.37 o 16 2 2 324.35 207.70 59.80 o 17 2 2 431.62 373.36 72.20 o 18 2 2 360.93 345.73 74.61 o 19 2 2 20.83 -20.89 64.01 o 1 3 2 1356.73 1328.48 37.34 o 2 3 2 1923.86 2149.56 65.00 o 3 3 2 3678.40 3777.51 59.22 o 4 3 2 3859.90 3897.35 63.61 o 5 3 2 1113.64 1060.94 34.53 o 6 3 2 8362.21 8119.48 114.41 o 7 3 2 2980.01 3007.73 64.96 o 8 3 2 5.77 -1.27 15.96 o 9 3 2 155.29 191.03 28.10 o 10 3 2 1664.08 1587.67 58.44 o 11 3 2 884.02 870.13 65.78 o 12 3 2 7263.89 7293.42 222.61 o 13 3 2 2.99 -21.31 34.89 o 14 3 2 1483.18 1863.86 116.60 o 15 3 2 211.79 92.01 51.74 o 16 3 2 51.53 132.76 54.21 o 17 3 2 26.19 35.95 54.79 o 18 3 2 37.71 46.23 60.79 o 19 3 2 42.70 14.11 65.57 o 0 4 2 667.84 768.60 32.49 o 1 4 2 165.67 176.98 15.03 o 2 4 2 49.28 33.22 10.62 o 3 4 2 4212.82 4025.53 64.72 o 4 4 2 12879.23 12835.97 154.03 o 5 4 2 2355.08 2267.37 57.92 o 6 4 2 11904.54 11593.94 161.50 o 7 4 2 65.36 65.08 17.71 o 8 4 2 1360.56 1276.93 48.38 o 9 4 2 9.72 -1.10 18.16 o 10 4 2 459.06 545.52 43.44 o 11 4 2 197.81 195.60 31.70 o 12 4 2 401.49 503.91 49.68 o 13 4 2 2761.25 2908.33 102.83 o 14 4 2 204.65 192.76 48.86 o 15 4 2 670.90 605.31 69.42 o 16 4 2 204.35 218.72 59.85 o 17 4 2 81.70 87.07 56.75 o 18 4 2 16.23 -49.84 53.77 o 1 5 2 30.21 27.45 11.13 o 2 5 2 823.42 794.76 30.36 o 3 5 2 1185.07 1172.52 46.18 o 4 5 2 55.15 14.55 12.97 o 5 5 2 770.26 754.91 33.22 o 6 5 2 13.63 18.96 15.43 o 7 5 2 2632.57 2812.36 64.65 o 8 5 2 642.53 605.61 36.74 o 9 5 2 1333.50 1261.07 81.01 o 10 5 2 341.00 282.76 37.40 o 11 5 2 0.31 -22.26 25.95 o 12 5 2 718.14 855.61 62.46 o 13 5 2 204.68 361.57 49.64 o 14 5 2 674.87 643.69 66.27 o 15 5 2 24.84 54.68 46.56 o 16 5 2 367.38 490.88 70.28 o 17 5 2 82.76 -6.95 55.28 o 18 5 2 161.82 112.89 69.14 o 0 6 2 267.75 234.32 27.50 o 1 6 2 782.29 877.30 31.60 o 2 6 2 458.82 444.90 22.39 o 3 6 2 301.98 406.61 31.69 o 4 6 2 3710.75 3674.37 70.00 o 5 6 2 5476.09 5333.19 90.05 o 6 6 2 3509.79 3649.98 73.71 o 7 6 2 3220.29 3087.99 79.96 o 8 6 2 0.93 0.27 22.20 o 9 6 2 353.49 365.79 38.81 o 10 6 2 0.54 -5.28 24.54 o 11 6 2 1207.73 1198.45 68.24 o 12 6 2 0.75 4.77 31.84 o 13 6 2 3617.63 4084.26 120.64 o 14 6 2 721.79 680.76 64.25 o 15 6 2 516.45 599.28 65.47 o 16 6 2 86.20 57.71 49.04 o 17 6 2 213.47 132.94 58.49 o 18 6 2 2.65 -59.85 60.03 o 1 7 2 1910.09 1856.20 40.12 o 2 7 2 6151.42 5751.15 91.83 o 3 7 2 311.41 362.89 55.22 o 4 7 2 52.93 43.19 17.36 o 5 7 2 3404.69 3560.63 84.87 o 6 7 2 8939.58 8676.76 147.67 o 7 7 2 479.40 473.19 40.23 o 8 7 2 2566.52 2610.20 81.67 o 9 7 2 1171.03 1079.98 60.11 o 10 7 2 145.57 100.46 31.96 o 11 7 2 420.13 449.35 47.86 o 12 7 2 86.00 76.86 36.04 o 13 7 2 162.04 207.79 44.91 o 14 7 2 650.84 971.14 74.24 o 15 7 2 300.67 251.09 52.36 o 16 7 2 669.93 959.11 81.85 o 17 7 2 12.35 43.24 58.10 o 0 8 2 591.93 620.38 42.36 o 1 8 2 23.66 11.46 14.88 o 2 8 2 72.02 76.90 18.66 o 3 8 2 542.77 561.00 50.37 o 4 8 2 2.38 -3.16 22.66 o 5 8 2 18.57 -4.15 20.23 o 6 8 2 427.08 451.25 40.02 o 7 8 2 58.69 46.54 26.25 o 8 8 2 248.24 248.97 35.75 o 9 8 2 250.50 222.20 37.54 o 10 8 2 692.57 721.31 56.82 o 11 8 2 1014.33 1011.42 92.08 o 12 8 2 60.40 64.94 38.02 o 13 8 2 20.79 -33.49 33.49 o 14 8 2 0.26 -34.91 34.91 o 15 8 2 29.03 17.57 46.68 o 16 8 2 4.07 -45.15 48.87 o 1 9 2 2154.86 2264.49 56.97 o 2 9 2 4048.69 4187.36 82.32 o 3 9 2 670.21 612.94 41.01 o 4 9 2 834.94 802.82 50.48 o 5 9 2 345.38 404.19 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1428.77 99.28 o 5 10 20 56.02 25.54 51.90 o 6 10 20 588.59 507.54 84.78 o 7 10 20 25.80 9.07 51.98 o 8 10 20 44.87 -11.40 57.26 o 9 10 20 16.48 -54.26 54.26 o 1 11 20 2.86 10.36 48.58 o 2 11 20 688.09 719.49 76.86 o 3 11 20 0.57 15.05 57.28 o 4 11 20 31.52 51.89 58.87 o 5 11 20 28.58 -35.03 54.35 o 6 11 20 233.44 260.96 97.14 o 7 11 20 2.07 18.56 74.14 o 0 12 20 30.88 169.20 91.33 o 1 12 20 43.74 63.23 69.80 o 2 12 20 292.50 204.77 72.99 o 3 12 20 39.11 39.35 64.54 o 1 1 21 8950.13 9187.88 162.78 o 2 1 21 1924.52 2018.48 76.61 o 3 1 21 961.08 951.88 76.71 o 4 1 21 245.45 245.94 36.43 o 5 1 21 145.82 185.35 35.17 o 6 1 21 76.94 38.72 28.59 o 7 1 21 17.79 6.34 31.74 o 8 1 21 4.85 29.15 29.24 o 9 1 21 2015.71 2211.77 99.90 o 10 1 21 1842.55 1933.10 114.80 o 11 1 21 2753.22 2679.25 129.71 o 12 1 21 647.59 693.61 72.85 o 13 1 21 27.58 19.86 44.09 o 14 1 21 10.22 15.59 45.77 o 15 1 21 252.93 295.08 94.56 o 0 2 21 4292.26 3983.16 224.37 o 1 2 21 6.14 -4.81 25.82 o 2 2 21 364.63 355.64 41.76 o 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6 2 28 36.19 115.78 68.46 o 7 2 28 1141.95 1132.50 122.41 o 8 2 28 14.72 -1.61 63.16 o 9 2 28 157.76 235.07 82.02 o 10 2 28 15.27 42.39 70.85 o 1 3 28 685.30 698.16 83.36 o 2 3 28 183.86 134.44 66.02 o 3 3 28 1.02 -19.67 55.86 o 4 3 28 150.33 75.26 62.51 o 5 3 28 21.46 39.36 53.93 o 6 3 28 2.36 -30.50 55.43 o 7 3 28 903.29 917.73 120.06 o 8 3 28 23.94 0.33 64.76 o 9 3 28 220.00 159.18 124.36 o 0 4 28 33.37 -57.05 83.91 o 1 4 28 28.37 32.45 57.42 o 2 4 28 92.64 64.44 59.55 o 3 4 28 436.74 497.73 72.25 o 4 4 28 382.06 341.12 67.74 o 5 4 28 246.39 333.21 98.06 o 6 4 28 4.73 -45.90 45.90 o 7 4 28 28.87 49.62 52.11 o 8 4 28 5.15 8.56 56.28 o 9 4 28 4.90 -43.57 57.39 o 1 5 28 5.68 22.92 48.93 o 2 5 28 879.37 874.72 87.26 o 3 5 28 233.14 141.87 50.88 o 4 5 28 241.02 142.29 59.60 o 5 5 28 10.59 -12.67 51.79 o 6 5 28 101.93 12.26 56.36 o 7 5 28 29.02 3.51 55.86 o 8 5 28 127.99 252.29 71.99 o 0 6 28 16.76 -2.64 74.90 o 1 6 28 36.56 34.00 46.69 o 2 6 28 123.76 175.55 56.16 o 3 6 28 312.27 326.97 66.87 o 4 6 28 692.12 767.04 88.98 o 5 6 28 142.27 119.96 53.62 o 6 6 28 141.81 81.61 56.71 o 7 6 28 1.33 3.68 51.29 o 1 7 28 82.32 47.84 55.28 o 2 7 28 700.80 700.72 102.82 o 3 7 28 8.44 -7.60 52.83 o 4 7 28 166.43 173.19 64.47 o 5 7 28 142.18 22.73 57.00 o 0 8 28 303.28 371.09 104.68 o 1 8 28 136.27 103.43 61.56 o 2 8 28 8.51 -25.49 54.42 o 3 8 28 38.92 -50.78 75.65 o 1 1 29 1458.08 1648.52 117.87 o 2 1 29 11.42 22.64 54.15 o 3 1 29 946.48 880.86 95.14 o 4 1 29 2.78 -26.54 51.56 o 5 1 29 1056.47 1259.72 109.08 o 6 1 29 135.09 205.34 76.16 o 7 1 29 164.22 228.43 80.85 o 8 1 29 401.96 372.35 90.92 o 9 1 29 683.24 715.49 109.22 o 0 2 29 2995.03 2925.73 205.69 o 1 2 29 51.91 8.30 53.30 o 2 2 29 2309.30 2172.62 130.06 o 3 2 29 3.74 20.24 53.18 o 4 2 29 1558.08 2041.12 152.02 o 5 2 29 0.47 57.26 67.27 o 6 2 29 1768.19 2108.60 158.07 o 7 2 29 16.85 -34.32 62.29 o 8 2 29 1138.58 1136.38 141.41 o 9 2 29 128.03 182.44 81.98 o 1 3 29 389.70 481.66 75.48 o 2 3 29 9.30 59.64 62.34 o 3 3 29 11.34 5.94 61.34 o 4 3 29 11.66 -38.55 57.76 o 5 3 29 214.03 286.06 74.06 o 6 3 29 70.82 -43.50 60.39 o 7 3 29 21.71 3.52 66.27 o 8 3 29 9.22 -21.28 71.95 o 0 4 29 947.73 794.24 186.97 o 1 4 29 265.51 246.39 76.15 o 2 4 29 553.35 498.88 90.71 o 3 4 29 247.84 260.12 112.67 o 4 4 29 1017.81 1085.91 119.44 o 5 4 29 27.13 -50.87 61.79 o 6 4 29 1390.04 1277.05 139.35 o 7 4 29 15.25 39.61 71.07 o 8 4 29 413.26 374.54 115.30 o 1 5 29 1.28 -4.78 68.44 o 2 5 29 71.11 -6.66 56.31 o 3 5 29 71.67 -9.77 55.12 o 4 5 29 27.82 -3.17 52.26 o 5 5 29 4.46 -21.99 56.04 o 6 5 29 0.57 62.03 60.39 o 7 5 29 136.65 25.58 61.42 o 0 6 29 1214.08 1352.25 279.99 o 1 6 29 79.45 67.22 51.66 o 2 6 29 372.57 217.25 65.06 o 3 6 29 68.70 43.36 55.00 o 4 6 29 9.31 -51.55 51.55 o 5 6 29 159.62 244.86 79.74 o 1 7 29 153.69 186.72 64.00 o 2 7 29 1.87 -53.72 53.72 o 3 7 29 37.58 46.18 56.89 o 0 0 30 2453.34 2314.64 273.83 o 1 0 30 585.49 569.89 114.02 o 2 0 30 177.85 109.93 113.63 o 3 0 30 125.08 200.89 92.32 o 4 0 30 167.40 192.81 91.39 o 5 0 30 404.10 323.14 126.88 o 6 0 30 1.39 79.83 81.59 o 7 0 30 325.74 316.15 172.25 o 8 0 30 796.48 533.67 178.32 o 1 1 30 600.89 585.47 103.99 o 2 1 30 7.71 -22.49 51.44 o 3 1 30 665.78 603.90 135.83 o 4 1 30 1.08 9.63 55.40 o 5 1 30 576.92 639.73 102.70 o 6 1 30 26.98 -7.03 69.86 o 7 1 30 447.11 465.13 94.88 o 8 1 30 52.46 58.29 77.68 o 0 2 30 1152.34 1578.72 211.35 o 1 2 30 109.46 95.76 60.16 o 2 2 30 99.32 116.31 60.22 o 3 2 30 488.99 384.99 88.10 o 4 2 30 307.27 231.68 77.20 o 5 2 30 48.49 4.21 68.86 o 6 2 30 10.47 120.51 74.13 o 7 2 30 375.98 412.99 95.17 o 8 2 30 252.83 137.19 80.37 o 1 3 30 979.18 753.24 103.54 o 2 3 30 49.07 47.64 71.05 o 3 3 30 1829.07 1994.07 153.32 o 4 3 30 164.53 115.06 75.06 o 5 3 30 1214.70 1305.24 131.23 o 6 3 30 3.17 24.48 69.12 o 7 3 30 959.40 1045.93 128.71 o 0 4 30 26.15 -18.95 109.49 o 1 4 30 114.59 142.14 89.47 o 2 4 30 36.60 80.07 72.65 o 3 4 30 168.16 189.17 71.38 o 4 4 30 224.35 182.53 75.35 o 5 4 30 15.71 14.75 69.48 o 6 4 30 93.12 105.23 78.35 o 1 5 30 0.92 -83.82 99.65 o 2 5 30 118.91 67.13 84.20 o 3 5 30 163.54 253.14 106.64 o 4 5 30 6.93 -67.73 67.73 o 5 5 30 628.18 616.25 106.19 o 0 6 30 76.68 51.41 79.47 o 1 6 30 30.33 -8.83 81.85 o 2 6 30 366.31 301.68 83.62 o 3 6 30 0.35 -58.93 58.93 o 1 1 31 1.23 -0.74 58.15 o 2 1 31 1071.87 968.64 102.76 o 3 1 31 218.30 151.65 65.51 o 4 1 31 5.19 -56.44 56.44 o 5 1 31 349.30 459.67 95.67 o 6 1 31 1109.94 1094.47 132.11 o 7 1 31 63.34 105.52 102.40 o 0 2 31 54.30 -54.78 75.90 o 1 2 31 89.75 111.54 62.69 o 2 2 31 70.62 68.51 63.11 o 3 2 31 26.15 23.08 69.72 o 4 2 31 137.33 42.71 71.36 o 5 2 31 43.71 1.08 72.67 o 6 2 31 37.42 11.00 73.06 o 1 3 31 188.48 193.11 76.84 o 2 3 31 196.38 65.49 75.96 o 3 3 31 0.05 4.84 67.57 o 4 3 31 153.99 158.40 83.64 o 5 3 31 16.13 55.98 72.81 o 6 3 31 231.30 137.77 101.55 o 0 4 31 10.24 -26.13 128.26 o 1 4 31 7.48 39.58 87.10 o 2 4 31 5.42 -31.20 71.89 o 3 4 31 128.26 246.92 83.29 o 4 4 31 0.93 -55.96 67.97 o 1 5 31 150.42 -46.45 80.37 o 2 5 31 8.87 42.70 86.23 o 3 5 31 12.31 14.91 85.72 o 0 0 32 1849.25 1805.45 267.57 o 1 0 32 107.21 135.18 148.87 o 2 0 32 71.42 35.52 87.29 o 3 0 32 30.93 -29.06 86.15 o 4 0 32 658.74 505.80 123.33 o 5 0 32 199.61 101.74 143.91 o 1 1 32 249.88 283.04 77.00 o 2 1 32 0.47 20.31 63.46 o 3 1 32 169.45 182.44 83.30 o 4 1 32 0.08 -4.98 73.03 o 5 1 32 56.93 24.00 76.59 o 0 2 32 627.36 742.63 140.98 o 1 2 32 13.34 0.79 61.29 o 2 2 32 48.78 20.29 72.05 o 3 2 32 28.86 -52.41 71.07 o 4 2 32 201.47 163.88 87.23 o 1 3 32 600.84 556.67 102.96 o 2 3 32 57.67 16.47 74.81 o 3 3 32 410.45 318.74 95.41 o 0 4 32 4.48 47.11 126.79 o 1 4 32 19.48 142.16 101.45 o 1 1 33 679.90 846.07 107.67 o 2 1 33 166.34 145.97 73.95 o