#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/42/2214278.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214278_Fobs loop_ _publ_author_name 'Cai, Chang-Quan' 'Luo, Hong' 'He, Ping' 'Yang, Zhen-Zhen' _publ_section_title ; 3-(4-Fluorophenyl)-2-morpholinoquinazolin-4(3H)-one ; _journal_coeditor_code IS2172 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3196 _journal_volume 63 _journal_year 2007 _space_group_IT_number 88 _symmetry_space_group_name_Hall '-I 4ad' _symmetry_space_group_name_H-M 'I 41/a :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 22.9526 _cell_length_b 22.9526 _cell_length_c 12.7318 _exptl_crystal_F_000 2720.00 _reflns_d_resolution_high 0.7835 _[local]_cod_data_source_file is2172Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070512cm in I4(1)/a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 449.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-y+3/4, x+1/4, z+1/4' 'y+3/4, -x+3/4, z+3/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-y+5/4, x+3/4, z+3/4' 'y+5/4, -x+5/4, z+5/4' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'y-3/4, -x-1/4, -z-1/4' '-y-3/4, x-3/4, -z-3/4' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'y-1/4, -x+1/4, -z+1/4' '-y-1/4, x-1/4, -z-1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 112604.41 109454.66 2887.54 o 2 2 0 139472.80 137188.61 1577.48 o -2 4 0 34922.01 35041.32 1161.54 o 0 4 0 12544.97 12107.08 80.64 o 2 4 0 47.60 30.05 56.26 o 4 4 0 55425.14 56206.26 889.43 o -4 6 0 7.23 1.31 35.28 o -2 6 0 29610.07 29904.49 633.50 o 0 6 0 12217.48 10810.65 40.32 o 2 6 0 71517.83 73492.16 513.81 o 4 6 0 1866.18 1612.77 21.64 o 6 6 0 500.75 550.31 40.22 o -6 8 0 1840.31 1741.22 95.25 o -4 8 0 8137.10 8291.84 89.54 o -2 8 0 24968.95 25369.95 254.21 o 0 8 0 5898.41 6822.28 47.11 o 2 8 0 69435.99 66785.38 858.38 o 4 8 0 12136.40 13086.49 156.71 o 6 8 0 0.58 12.67 10.50 o 8 8 0 1427.82 1493.07 42.26 o -8 10 0 4682.80 5180.66 61.11 o -6 10 0 152.21 196.14 10.58 o -4 10 0 6215.82 6743.43 76.84 o -2 10 0 64.23 126.38 11.25 o 0 10 0 23.38 12.36 7.98 o 2 10 0 2087.71 2308.63 48.98 o 4 10 0 13686.34 15770.09 146.67 o 6 10 0 42859.50 48043.27 356.60 o 8 10 0 15016.95 16812.92 191.11 o 10 10 0 3203.15 3363.58 61.64 o -10 12 0 6144.47 5803.73 74.67 o -8 12 0 2842.20 2987.83 70.06 o -6 12 0 9922.35 10591.48 108.11 o -4 12 0 5282.34 5630.33 69.10 o -2 12 0 3877.39 4674.96 54.81 o 0 12 0 2626.15 2654.14 47.11 o 2 12 0 6355.90 6896.68 79.83 o 4 12 0 9102.23 9978.97 138.67 o 6 12 0 26768.77 28932.66 206.10 o 8 12 0 1676.40 1946.76 59.90 o 10 12 0 339.00 424.64 37.00 o 12 12 0 87.55 133.61 28.88 o -12 14 0 945.64 966.71 46.04 o -10 14 0 2524.07 2499.15 67.07 o -8 14 0 2286.14 2229.30 47.21 o -6 14 0 2018.27 2105.16 45.94 o -4 14 0 1808.38 1759.71 41.56 o -2 14 0 2228.68 2711.54 42.67 o 0 14 0 7086.77 7053.08 84.76 o 2 14 0 1153.89 884.75 51.48 o 4 14 0 532.33 518.47 43.83 o 6 14 0 3679.21 3870.01 69.76 o 8 14 0 1723.81 1668.84 67.67 o 10 14 0 2.38 15.56 15.62 o 12 14 0 18.96 33.18 17.73 o 14 14 0 2041.74 1772.98 68.65 o -14 16 0 91.85 116.25 24.56 o -12 16 0 30.70 29.32 26.57 o -10 16 0 2931.90 2775.84 93.26 o -8 16 0 4497.76 4551.28 80.54 o -6 16 0 10175.20 9906.28 124.30 o -4 16 0 3016.65 2909.51 73.69 o -2 16 0 0.29 21.41 20.31 o 0 16 0 311.98 404.98 50.26 o 2 16 0 243.65 176.35 43.92 o 4 16 0 10993.94 10840.80 177.73 o 6 16 0 333.28 391.54 53.65 o 8 16 0 2395.14 2376.35 73.49 o 10 16 0 1114.54 1331.41 61.64 o 12 16 0 34.18 41.18 23.19 o 14 16 0 29.54 37.38 22.52 o 16 16 0 364.88 434.07 54.23 o -16 18 0 3414.06 3147.35 131.59 o -14 18 0 18.43 26.23 27.00 o -12 18 0 3152.73 2889.76 112.67 o -10 18 0 3243.53 3095.29 93.87 o -8 18 0 581.12 604.20 56.12 o -6 18 0 169.65 244.29 29.34 o -4 18 0 6249.92 3625.03 1484.81 o -2 18 0 1225.44 1165.49 57.81 o 0 18 0 675.13 683.87 46.47 o 2 18 0 341.52 380.86 31.85 o 4 18 0 1633.13 1635.36 63.21 o 6 18 0 1355.06 1225.55 63.89 o 8 18 0 2606.37 2653.88 109.67 o 10 18 0 5643.28 5276.51 134.00 o 12 18 0 1312.64 1209.18 70.36 o 14 18 0 1548.20 1312.26 72.49 o 16 18 0 768.85 721.57 74.63 o 18 18 0 172.23 196.37 47.06 o -18 20 0 2254.19 2292.40 112.44 o -16 20 0 748.38 642.63 109.88 o -14 20 0 3.61 75.46 44.46 o -12 20 0 78.62 107.78 37.70 o -10 20 0 47.95 42.39 29.62 o -8 20 0 77.69 109.29 26.01 o -6 20 0 9202.33 8283.49 163.62 o -4 20 0 1112.07 952.43 108.26 o -2 20 0 14101.22 13718.31 205.36 o 0 20 0 3171.70 2786.87 97.76 o 2 20 0 4997.07 4529.46 117.37 o 4 20 0 2177.79 2135.23 81.94 o 6 20 0 901.82 836.77 62.64 o 8 20 0 2006.49 1622.62 90.15 o 10 20 0 2071.34 1719.78 78.61 o 12 20 0 31.57 41.91 29.65 o 14 20 0 37.13 68.89 30.51 o 16 20 0 6.78 16.11 30.98 o 18 20 0 49.24 44.93 34.62 o 20 20 0 47.28 102.16 44.56 o -18 22 0 903.78 875.98 127.54 o -16 22 0 1225.19 1224.49 143.56 o -14 22 0 195.07 96.09 69.80 o -12 22 0 1030.97 971.66 97.39 o -10 22 0 585.61 702.69 97.84 o -8 22 0 41.40 45.41 25.85 o -6 22 0 1730.63 1688.12 78.66 o -4 22 0 506.77 555.94 56.11 o -2 22 0 14031.70 12844.17 212.04 o 0 22 0 4456.76 3972.15 119.23 o 2 22 0 4429.17 3895.68 119.87 o 4 22 0 1500.78 1316.00 76.91 o 6 22 0 1520.94 1513.64 79.02 o 8 22 0 261.11 244.93 49.76 o 10 22 0 7.64 19.40 25.39 o 12 22 0 501.74 398.91 56.10 o 14 22 0 329.74 335.72 48.39 o 16 22 0 53.39 112.94 40.90 o 18 22 0 120.84 233.73 53.66 o -16 24 0 688.44 701.06 122.20 o -14 24 0 169.95 202.62 58.79 o -12 24 0 205.95 188.20 55.04 o -10 24 0 3.59 37.51 39.29 o -8 24 0 1515.60 1310.22 111.87 o -6 24 0 0.30 36.48 27.10 o -4 24 0 1454.68 1329.55 82.50 o -2 24 0 274.78 252.66 43.00 o 0 24 0 1799.87 1616.43 84.33 o 2 24 0 151.60 140.51 35.66 o 4 24 0 32.56 30.01 25.32 o 6 24 0 503.97 485.26 56.16 o 8 24 0 671.71 740.26 80.14 o 10 24 0 0.82 42.98 29.82 o 12 24 0 254.40 290.09 47.99 o 14 24 0 66.23 150.33 38.54 o 16 24 0 24.20 93.77 43.42 o -12 26 0 450.62 613.85 88.46 o -10 26 0 7.29 36.00 39.11 o -8 26 0 136.53 232.73 55.95 o -6 26 0 126.80 93.96 35.86 o -4 26 0 3088.04 2785.07 109.87 o -2 26 0 505.64 475.69 61.79 o 0 26 0 1180.66 1349.67 89.74 o 2 26 0 93.34 98.62 36.18 o 4 26 0 123.90 109.14 38.44 o 6 26 0 1.79 25.55 31.19 o 8 26 0 284.40 282.42 50.02 o 10 26 0 12.22 35.52 31.11 o 12 26 0 22.20 50.52 34.67 o -8 28 0 261.74 242.87 66.96 o -6 28 0 56.48 98.71 50.68 o -4 28 0 35.75 33.20 32.86 o -2 28 0 561.03 512.48 66.14 o 0 28 0 0.21 54.03 34.99 o 2 28 0 301.21 291.28 48.16 o 4 28 0 33.01 53.85 35.66 o 6 28 0 66.32 78.14 36.39 o 8 28 0 456.97 544.41 65.34 o 0 1 1 597.66 547.10 54.00 o -1 2 1 9746.79 9944.38 303.50 o 1 2 1 37691.17 38187.18 196.58 o -2 3 1 5532.85 6880.40 174.17 o 0 3 1 9527.49 7985.24 374.27 o 2 3 1 887.67 1233.55 39.48 o -3 4 1 36893.05 36919.44 403.47 o -1 4 1 62515.42 4774.39 12163.62 o 1 4 1 1368.24 2064.59 40.59 o 3 4 1 88276.88 92018.43 1254.34 o -4 5 1 784.94 539.52 21.32 o -2 5 1 17161.89 19213.27 265.98 o 0 5 1 6286.27 7524.57 116.74 o 2 5 1 102861.05 97034.38 2733.58 o 4 5 1 36428.86 39486.05 567.76 o -5 6 1 19701.09 20303.57 99.64 o -3 6 1 9691.98 10931.04 111.56 o -1 6 1 4622.74 5956.76 76.21 o 1 6 1 14368.39 16519.97 188.59 o 3 6 1 31579.12 33424.09 341.53 o 5 6 1 4065.77 3713.48 71.55 o -6 7 1 7119.04 7861.57 70.38 o -4 7 1 308.51 363.24 13.49 o -2 7 1 20027.02 19710.94 534.16 o 0 7 1 48842.42 50882.07 509.03 o 2 7 1 500.17 534.75 15.13 o 4 7 1 2581.32 2977.22 33.88 o 6 7 1 20656.00 22896.19 147.58 o -7 8 1 10755.61 12180.22 113.15 o -5 8 1 15453.31 16895.23 143.11 o -3 8 1 499.97 504.70 23.37 o -1 8 1 13672.78 14094.48 109.39 o 1 8 1 1595.61 1768.89 14.95 o 3 8 1 3071.28 2914.93 28.35 o 5 8 1 6652.98 6943.21 78.48 o 7 8 1 6351.20 6617.64 80.14 o -8 9 1 12930.32 14525.62 136.38 o -6 9 1 132.77 152.69 11.70 o -4 9 1 352.89 441.49 13.90 o -2 9 1 2311.23 2022.71 135.51 o 0 9 1 1963.23 1968.21 27.98 o 2 9 1 8398.35 8725.47 76.90 o 4 9 1 1437.78 1643.17 25.75 o 6 9 1 767.79 711.87 16.45 o 8 9 1 545.96 849.78 24.18 o -9 10 1 772.18 1051.11 19.42 o -7 10 1 1281.18 1478.32 32.69 o -5 10 1 110.03 176.36 16.94 o -3 10 1 2704.09 2885.30 29.90 o -1 10 1 308.36 429.99 9.92 o 1 10 1 1092.89 970.13 20.30 o 3 10 1 783.49 876.92 17.92 o 5 10 1 2871.73 3174.89 37.84 o 7 10 1 938.53 1052.11 21.05 o 9 10 1 113.89 132.54 11.60 o -10 11 1 9226.15 9519.61 78.23 o -8 11 1 8005.61 8644.51 64.15 o -6 11 1 132.52 153.37 13.96 o -4 11 1 3642.02 3898.74 35.80 o -2 11 1 4756.11 4742.53 106.71 o 0 11 1 1251.93 1276.91 24.22 o 2 11 1 11028.71 11942.78 91.37 o 4 11 1 10736.08 12181.19 171.09 o 6 11 1 6367.72 7560.29 128.09 o 8 11 1 694.38 963.80 30.63 o 10 11 1 6.53 3.39 7.78 o -11 12 1 972.56 1015.35 32.44 o -9 12 1 1308.14 1157.09 32.12 o -7 12 1 594.01 561.59 24.62 o -5 12 1 1356.46 1453.53 30.90 o -3 12 1 223.57 170.20 23.59 o -1 12 1 4113.43 4089.60 37.70 o 1 12 1 4078.71 4385.21 47.36 o 3 12 1 4110.50 4807.43 47.66 o 5 12 1 27392.61 30168.16 291.46 o 7 12 1 655.10 590.12 21.34 o 9 12 1 3095.61 2994.96 54.48 o 11 12 1 47.64 66.70 13.54 o -12 13 1 3269.85 3034.35 54.75 o -10 13 1 3322.23 3365.67 46.27 o -8 13 1 36.71 61.86 9.46 o -6 13 1 866.65 924.87 25.18 o -4 13 1 38.19 57.81 13.25 o -2 13 1 206.27 255.83 18.49 o 0 13 1 6137.75 6277.05 38.04 o 2 13 1 8370.71 8818.66 86.43 o 4 13 1 20.61 16.62 15.66 o 6 13 1 1532.77 1668.59 42.44 o 8 13 1 583.60 555.00 28.63 o 10 13 1 2595.19 2465.10 51.89 o 12 13 1 342.19 328.82 26.37 o -13 14 1 22.26 18.37 14.12 o -11 14 1 292.94 243.66 18.50 o -9 14 1 434.81 464.50 16.85 o -7 14 1 2836.29 2949.78 37.36 o -5 14 1 99.69 114.03 14.67 o -3 14 1 151.94 221.33 19.77 o -1 14 1 1088.58 1160.52 22.69 o 1 14 1 334.88 342.41 14.31 o 3 14 1 327.14 434.14 25.72 o 5 14 1 14452.08 14522.85 102.63 o 7 14 1 1768.46 1647.02 56.35 o 9 14 1 3640.79 3949.54 65.81 o 11 14 1 2409.69 2252.29 48.93 o 13 14 1 3.15 12.87 11.79 o -14 15 1 432.83 460.98 31.94 o -12 15 1 7.09 34.23 12.85 o -10 15 1 4816.91 4737.22 66.04 o -8 15 1 1762.82 1841.93 36.95 o -6 15 1 2027.20 1970.13 35.17 o -4 15 1 6670.35 6614.37 69.99 o -2 15 1 1654.20 1721.59 41.23 o 0 15 1 1453.11 1406.77 31.02 o 2 15 1 1901.77 1838.22 51.57 o 4 15 1 1816.05 1863.90 36.90 o 6 15 1 337.89 412.25 32.45 o 8 15 1 321.99 426.09 35.80 o 10 15 1 847.89 891.36 38.44 o 12 15 1 159.76 136.45 17.52 o 14 15 1 101.68 94.46 16.14 o -15 16 1 1.14 23.98 16.42 o -13 16 1 667.43 624.46 32.11 o -11 16 1 50.75 93.20 13.76 o -9 16 1 1.98 15.41 12.45 o -7 16 1 681.18 674.70 28.79 o -5 16 1 885.58 779.83 27.29 o -3 16 1 15.32 11.30 11.25 o -1 16 1 32.52 43.08 13.39 o 1 16 1 160.79 165.77 15.25 o 3 16 1 253.96 301.96 27.25 o 5 16 1 4228.34 4037.11 76.10 o 7 16 1 137.17 188.67 19.06 o 9 16 1 409.90 392.89 34.26 o 11 16 1 47.09 34.85 13.55 o 13 16 1 222.64 179.02 21.78 o 15 16 1 657.67 701.10 41.89 o -16 17 1 460.50 585.70 43.79 o -14 17 1 0.75 31.19 16.48 o -12 17 1 4.53 27.20 15.32 o -10 17 1 1596.43 1387.05 68.00 o -8 17 1 2933.22 2863.53 50.14 o -6 17 1 400.56 518.34 29.34 o -4 17 1 348.95 215.50 48.41 o -2 17 1 20.71 36.88 16.35 o 0 17 1 1987.09 1909.73 45.04 o 2 17 1 522.96 579.23 27.74 o 4 17 1 73.68 85.86 13.06 o 6 17 1 996.49 1004.27 44.03 o 8 17 1 2011.52 1922.04 61.06 o 10 17 1 96.90 68.89 18.11 o 12 17 1 2202.16 1797.75 53.97 o 14 17 1 1607.15 1507.08 52.14 o 16 17 1 1364.97 1327.04 57.28 o -17 18 1 77.36 84.67 24.56 o -15 18 1 54.52 34.54 20.73 o -13 18 1 32.01 44.75 14.94 o -11 18 1 467.35 398.22 43.56 o -9 18 1 2090.77 2064.77 52.55 o -7 18 1 616.28 659.18 33.04 o -5 18 1 5924.99 5587.18 91.50 o -3 18 1 66.41 102.85 17.06 o -1 18 1 20.83 39.65 14.53 o 1 18 1 504.88 499.05 35.66 o 3 18 1 760.96 826.55 38.77 o 5 18 1 1.98 4.31 12.72 o 7 18 1 1615.59 1430.68 47.41 o 9 18 1 16.55 32.94 15.98 o 11 18 1 1.56 20.13 15.28 o 13 18 1 1.23 24.95 16.79 o 15 18 1 5.15 22.86 17.74 o 17 18 1 64.03 97.87 26.24 o -18 19 1 79.33 116.26 29.57 o -16 19 1 161.54 169.99 28.51 o -14 19 1 2303.10 2188.48 65.68 o -12 19 1 1072.79 1046.14 58.33 o -10 19 1 227.57 198.53 32.26 o -8 19 1 1607.96 1512.28 48.90 o -6 19 1 1609.59 1618.49 50.08 o -4 19 1 232.44 138.15 28.36 o -2 19 1 858.98 974.77 44.94 o 0 19 1 606.82 675.26 36.92 o 2 19 1 12.52 24.36 16.12 o 4 19 1 1756.32 1600.82 53.52 o 6 19 1 800.34 900.67 46.70 o 8 19 1 3387.17 3005.65 94.86 o 10 19 1 637.89 516.40 51.76 o 12 19 1 1.66 35.21 17.14 o 14 19 1 35.34 33.26 18.31 o 16 19 1 5.76 24.85 20.46 o 18 19 1 412.72 451.94 45.02 o -19 20 1 170.44 224.70 37.55 o -17 20 1 32.74 41.85 28.33 o -15 20 1 1.35 14.99 23.52 o -13 20 1 236.70 249.42 39.30 o -11 20 1 393.97 421.25 47.69 o -9 20 1 601.70 491.54 37.68 o -7 20 1 1008.12 904.30 46.53 o -5 20 1 1538.68 1318.24 82.88 o -3 20 1 4.96 28.00 15.73 o -1 20 1 19.50 46.11 16.77 o 1 20 1 1922.10 1739.59 55.38 o 3 20 1 8.75 30.81 16.77 o 5 20 1 104.16 138.52 22.64 o 7 20 1 19.31 20.26 15.91 o 9 20 1 399.54 339.18 39.10 o 11 20 1 324.84 310.04 33.44 o 13 20 1 31.35 65.72 19.83 o 15 20 1 66.54 30.49 21.48 o 17 20 1 80.10 93.80 27.60 o 19 20 1 115.34 117.16 32.05 o -20 21 1 1403.62 1412.77 110.14 o -18 21 1 107.81 255.41 52.84 o -16 21 1 225.21 273.43 45.85 o -14 21 1 587.95 722.37 60.49 o -12 21 1 258.57 261.41 38.53 o -10 21 1 474.23 462.52 49.73 o -8 21 1 606.97 717.17 42.03 o -6 21 1 117.21 107.05 20.40 o -4 21 1 81.39 93.31 19.94 o -2 21 1 815.78 775.92 44.52 o 0 21 1 331.22 378.88 34.20 o 2 21 1 1192.54 1138.58 51.73 o 4 21 1 859.24 869.82 47.74 o 6 21 1 927.37 897.10 48.25 o 8 21 1 112.86 81.89 21.32 o 10 21 1 804.66 696.50 43.41 o 12 21 1 2206.12 1845.48 67.18 o 14 21 1 341.22 312.27 32.70 o 16 21 1 153.29 207.79 34.91 o 18 21 1 307.40 301.72 42.02 o 20 21 1 28.99 81.68 29.48 o -19 22 1 35.07 131.71 45.81 o -17 22 1 117.44 146.92 44.47 o -15 22 1 89.29 62.75 30.54 o -13 22 1 541.19 425.71 79.93 o -11 22 1 5.91 26.26 24.37 o -9 22 1 119.03 133.49 29.62 o -7 22 1 739.61 731.78 42.67 o -5 22 1 3149.26 1987.84 310.46 o -3 22 1 4664.53 4252.72 86.32 o -1 22 1 1218.30 1203.22 53.22 o 1 22 1 232.50 258.33 30.02 o 3 22 1 1020.89 1039.26 52.12 o 5 22 1 792.38 712.18 45.79 o 7 22 1 74.22 55.53 20.07 o 9 22 1 43.65 40.44 18.86 o 11 22 1 444.70 300.69 30.58 o 13 22 1 6.50 27.37 18.50 o 15 22 1 246.77 210.32 33.42 o 17 22 1 713.40 831.66 61.93 o 19 22 1 130.27 201.06 36.23 o -18 23 1 150.94 191.93 52.96 o -16 23 1 0.08 8.37 28.90 o -14 23 1 170.98 140.44 33.09 o -12 23 1 39.14 57.96 28.06 o -10 23 1 180.39 205.56 39.18 o -8 23 1 490.69 569.41 51.72 o -6 23 1 512.87 527.78 40.66 o -4 23 1 575.82 621.51 43.69 o -2 23 1 551.80 625.37 43.73 o 0 23 1 1910.94 1780.42 58.84 o 2 23 1 535.04 541.23 42.74 o 4 23 1 354.05 359.99 35.18 o 6 23 1 34.59 38.86 19.66 o 8 23 1 3.37 19.80 19.07 o 10 23 1 155.40 161.09 27.37 o 12 23 1 42.30 64.77 22.81 o 14 23 1 91.67 108.02 25.15 o 16 23 1 426.15 544.26 49.14 o 18 23 1 37.83 64.97 30.24 o -15 24 1 32.35 28.63 32.96 o -13 24 1 7.25 33.36 27.21 o -11 24 1 443.10 535.04 59.08 o -9 24 1 13.97 42.27 24.65 o -7 24 1 58.10 109.17 23.27 o -5 24 1 204.97 128.49 39.90 o -3 24 1 637.41 582.85 43.93 o -1 24 1 2205.46 2009.91 65.26 o 1 24 1 3712.96 3418.07 84.10 o 3 24 1 23.16 21.22 18.36 o 5 24 1 35.46 32.85 20.74 o 7 24 1 2.62 22.70 18.82 o 9 24 1 0.05 24.40 19.67 o 11 24 1 25.61 42.04 22.22 o 13 24 1 153.84 183.32 28.28 o 15 24 1 15.11 56.56 26.70 o -14 25 1 0.70 25.80 28.90 o -12 25 1 28.37 28.25 28.90 o -10 25 1 6.27 18.16 25.98 o -8 25 1 238.64 272.83 40.13 o -6 25 1 2465.29 2231.52 71.14 o -4 25 1 3565.01 3249.56 81.31 o -2 25 1 0.50 10.16 17.98 o 0 25 1 74.88 81.32 23.12 o 2 25 1 348.70 387.90 37.05 o 4 25 1 375.91 342.27 36.92 o 6 25 1 10.75 28.06 20.05 o 8 25 1 264.41 365.28 37.68 o 10 25 1 185.13 205.24 30.69 o 12 25 1 29.13 70.89 24.71 o 14 25 1 88.23 109.30 27.12 o -13 26 1 99.02 65.65 33.02 o -11 26 1 333.48 355.47 48.06 o -9 26 1 1.42 15.02 25.33 o -7 26 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