#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/43/2214309.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214309_Fobs loop_ _publ_author_name 'Sonar, Vijayakumar N.' 'Venkatraj, M.' 'Parkin, Sean' 'Crooks, Peter A.' _publ_section_title ; Benzyl 2,6-dihydroxy-3-nitrobenzoate ; _journal_coeditor_code LH2412 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3226 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.582 _cell_angle_gamma 90.000 _cell_length_a 10.0050 _cell_length_b 6.1633 _cell_length_c 20.1048 _exptl_crystal_F_000 600.00 _reflns_d_resolution_high .7706 _[local]_cod_data_source_file lh2412Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' k05306 - P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 112.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2447.05 2154.97 33.88 o 2 0 0 5121.66 4550.07 72.99 o 3 0 0 86.64 64.28 1.31 o 4 0 0 5620.51 5423.82 109.93 o 5 0 0 2549.04 2510.58 48.59 o 6 0 0 1705.62 1820.29 45.98 o 7 0 0 266.03 291.76 9.59 o 8 0 0 420.09 428.16 15.58 o 9 0 0 122.21 123.22 5.56 o 10 0 0 43.06 50.44 3.16 o 11 0 0 107.23 90.10 4.25 o 12 0 0 10.56 13.29 4.25 o 2 1 0 628.09 612.39 6.23 o 3 1 0 64.62 60.62 .73 o 4 1 0 349.35 331.19 4.47 o 5 1 0 219.63 221.13 3.20 o 6 1 0 259.73 289.08 5.48 o 7 1 0 23.63 18.59 .92 o 8 1 0 169.44 172.22 4.13 o 9 1 0 250.06 270.02 6.43 o 10 1 0 .20 -1.35 2.34 o 11 1 0 47.46 46.65 2.73 o 12 1 0 4.99 2.71 3.89 o 0 2 0 525.70 408.93 6.81 o 1 2 0 424.28 410.01 4.58 o 2 2 0 316.51 309.44 3.21 o 3 2 0 346.09 366.09 5.88 o 4 2 0 387.01 420.60 4.69 o 5 2 0 451.86 475.24 5.49 o 6 2 0 538.22 497.79 7.43 o 7 2 0 574.48 608.13 13.24 o 8 2 0 1.98 1.42 1.25 o 9 2 0 356.91 381.78 9.32 o 10 2 0 13.79 14.60 2.04 o 11 2 0 6.47 5.50 3.76 o 12 2 0 1.69 -1.91 3.89 o 1 3 0 83.33 77.87 1.02 o 2 3 0 9.08 12.85 .42 o 3 3 0 324.34 370.31 4.16 o 4 3 0 1126.39 1137.60 15.07 o 5 3 0 5.63 10.65 1.31 o 6 3 0 54.80 57.12 1.47 o 7 3 0 2788.00 2969.17 58.11 o 8 3 0 8.31 7.07 1.41 o 9 3 0 232.22 238.35 6.80 o 10 3 0 2.65 3.01 2.17 o 11 3 0 167.34 150.08 6.75 o 0 4 0 8.24 11.31 1.14 o 1 4 0 .41 1.89 .46 o 2 4 0 292.07 286.36 4.39 o 3 4 0 142.73 149.38 2.72 o 4 4 0 28.36 29.27 .97 o 5 4 0 96.48 93.70 1.99 o 6 4 0 196.74 202.50 4.01 o 7 4 0 1.37 1.74 1.42 o 8 4 0 44.97 46.72 3.16 o 9 4 0 67.44 65.26 3.32 o 10 4 0 240.15 273.85 9.76 o 11 4 0 459.47 408.19 21.31 o 1 5 0 93.06 97.43 2.89 o 2 5 0 166.00 160.25 2.74 o 3 5 0 89.25 82.58 2.35 o 4 5 0 27.19 24.65 3.05 o 5 5 0 7.03 4.79 1.91 o 6 5 0 182.33 173.45 4.06 o 7 5 0 135.28 146.06 4.35 o 8 5 0 53.70 45.36 4.52 o 9 5 0 123.53 121.31 8.99 o 10 5 0 4.95 11.72 4.68 o 0 6 0 45.94 48.63 3.08 o 1 6 0 287.62 299.81 8.50 o 2 6 0 234.14 270.53 5.41 o 3 6 0 322.17 346.24 11.11 o 4 6 0 458.46 528.72 11.56 o 5 6 0 23.83 21.75 1.89 o 6 6 0 75.34 76.39 3.04 o 7 6 0 .87 2.45 2.88 o 8 6 0 136.74 123.67 6.06 o 1 7 0 5.97 7.63 4.41 o 2 7 0 78.47 75.59 3.35 o 3 7 0 6.13 7.70 3.00 o 4 7 0 328.23 333.94 12.64 o 5 7 0 227.16 255.58 8.35 o 6 7 0 41.40 29.73 3.89 o -12 1 1 20.01 26.29 3.76 o -11 1 1 1.84 4.33 2.61 o -10 1 1 12.23 11.18 2.45 o -9 1 1 18.66 18.13 1.69 o -8 1 1 214.99 208.08 5.07 o -7 1 1 124.61 130.22 4.79 o -6 1 1 632.19 659.73 10.90 o -5 1 1 4.12 7.76 .50 o -4 1 1 .69 .48 .93 o -3 1 1 124.40 108.07 1.19 o -2 1 1 5400.95 5016.80 55.73 o -1 1 1 516.10 479.82 5.17 o 0 1 1 2414.08 2120.43 25.84 o 1 1 1 428.93 379.26 4.20 o 2 1 1 68.11 78.89 1.20 o 3 1 1 21.69 30.55 .50 o 4 1 1 495.08 529.32 6.50 o 5 1 1 .71 3.52 .82 o 6 1 1 331.56 320.18 6.04 o 7 1 1 7.79 7.73 1.31 o 8 1 1 .92 .20 1.69 o 9 1 1 41.53 36.81 2.29 o 10 1 1 17.86 14.46 2.12 o 11 1 1 69.72 61.96 3.32 o 12 1 1 41.05 37.26 9.04 o -12 2 1 .40 .92 3.51 o -11 2 1 9.49 6.48 4.47 o -10 2 1 35.16 33.60 2.42 o -9 2 1 446.89 485.01 11.86 o -8 2 1 30.06 34.24 1.69 o -7 2 1 277.28 290.34 6.19 o -6 2 1 91.41 95.56 1.81 o -5 2 1 145.89 142.98 1.96 o -4 2 1 179.69 201.81 2.22 o -3 2 1 2285.92 2272.43 23.43 o -2 2 1 3534.10 3337.32 34.99 o -1 2 1 687.26 649.21 6.82 o 0 2 1 102.07 90.92 1.16 o 1 2 1 3189.87 3072.91 32.86 o 2 2 1 526.84 456.77 4.79 o 3 2 1 713.64 692.23 7.25 o 4 2 1 .29 3.30 .82 o 5 2 1 189.71 205.36 3.00 o 6 2 1 45.05 42.65 2.29 o 7 2 1 1208.96 1260.04 22.64 o 8 2 1 12.73 11.41 1.38 o 9 2 1 144.65 151.51 7.95 o 10 2 1 1.02 .31 1.78 o 11 2 1 22.11 21.62 2.48 o 12 2 1 4.50 6.12 9.37 o -11 3 1 666.75 689.49 26.99 o -10 3 1 119.32 117.88 4.30 o -9 3 1 19.15 17.34 1.80 o -8 3 1 121.87 118.59 5.28 o -7 3 1 1778.77 1864.83 34.61 o -6 3 1 1443.33 1515.78 25.76 o -5 3 1 14.01 14.84 .87 o -4 3 1 24.98 27.81 1.09 o -3 3 1 6.55 10.19 1.91 o -2 3 1 2604.81 2800.03 30.84 o -1 3 1 1685.02 1669.98 17.96 o 0 3 1 726.77 773.46 9.10 o 1 3 1 231.31 221.31 2.61 o 2 3 1 462.31 468.98 5.27 o 3 3 1 103.56 86.88 1.80 o 4 3 1 1715.88 1744.06 21.77 o 5 3 1 149.50 151.38 5.39 o 6 3 1 3.66 1.08 .87 o 7 3 1 1362.08 1425.02 33.66 o 8 3 1 3.16 3.87 1.59 o 9 3 1 .05 -1.65 1.65 o 10 3 1 12.41 8.52 2.26 o 11 3 1 347.03 367.60 14.44 o -11 4 1 512.08 516.65 43.80 o -10 4 1 8.49 12.41 3.92 o -9 4 1 160.76 175.96 5.60 o -8 4 1 98.62 105.64 3.32 o -7 4 1 324.24 345.75 7.11 o -6 4 1 .19 -.15 .99 o -5 4 1 27.00 31.81 1.36 o -4 4 1 238.99 224.07 3.50 o -3 4 1 37.68 45.94 1.36 o -2 4 1 137.97 126.71 1.77 o -1 4 1 216.62 229.76 3.00 o 0 4 1 511.06 569.45 8.00 o 1 4 1 33.57 44.28 1.42 o 2 4 1 161.95 167.55 2.70 o 3 4 1 124.08 122.83 1.93 o 4 4 1 20.89 15.65 .73 o 5 4 1 17.64 16.53 1.31 o 6 4 1 230.74 233.50 4.39 o 7 4 1 50.45 48.46 1.86 o 8 4 1 55.42 56.13 4.03 o 9 4 1 238.24 245.10 7.35 o 10 4 1 1.49 2.02 2.53 o 11 4 1 .87 -2.94 5.34 o -10 5 1 53.96 41.47 5.83 o -9 5 1 32.30 38.53 4.11 o -8 5 1 59.29 52.55 3.33 o -7 5 1 81.48 80.18 3.21 o -6 5 1 2.89 1.98 1.74 o -5 5 1 1.25 .83 1.15 o -4 5 1 44.77 38.59 1.60 o -3 5 1 51.31 57.30 1.67 o -2 5 1 232.85 211.09 3.47 o -1 5 1 13.52 11.92 .99 o 0 5 1 20.86 18.93 1.42 o 1 5 1 .20 1.63 .65 o 2 5 1 118.51 127.93 3.05 o 3 5 1 .01 -1.17 1.31 o 4 5 1 1.17 1.23 1.85 o 5 5 1 1.92 -.42 2.45 o 6 5 1 13.55 14.79 1.57 o 7 5 1 .02 -.74 1.74 o 8 5 1 159.56 172.14 5.83 o 9 5 1 8.86 9.49 2.93 o -8 6 1 43.07 45.62 3.41 o -7 6 1 1.93 2.20 4.85 o -6 6 1 7.70 11.53 1.99 o -5 6 1 30.54 23.42 2.04 o -4 6 1 914.01 959.51 17.68 o -3 6 1 314.79 311.15 6.43 o -2 6 1 37.77 39.63 4.63 o -1 6 1 11.82 9.47 1.53 o 0 6 1 1.40 -.84 3.05 o 1 6 1 69.59 61.30 2.94 o 2 6 1 235.78 244.70 5.18 o 3 6 1 8.73 6.43 1.54 o 4 6 1 678.92 710.59 15.81 o 5 6 1 5.59 5.28 1.77 o 6 6 1 9.19 4.16 2.27 o 7 6 1 23.97 24.33 3.00 o 8 6 1 6.09 7.54 3.16 o -6 7 1 110.12 109.87 8.55 o -5 7 1 488.39 511.66 18.36 o -4 7 1 275.53 304.82 14.16 o -3 7 1 150.76 173.05 5.55 o -2 7 1 117.69 120.67 7.14 o -1 7 1 40.50 44.08 7.35 o 0 7 1 233.38 239.01 10.24 o 1 7 1 93.88 89.43 3.65 o 2 7 1 18.10 17.84 6.10 o 3 7 1 1.16 .80 2.30 o 4 7 1 35.52 33.40 2.77 o 5 7 1 233.98 224.64 7.38 o 6 7 1 11.12 11.85 3.82 o -12 0 2 128.13 136.95 9.26 o -11 0 2 10.51 14.49 4.14 o -10 0 2 33.16 34.65 2.61 o -9 0 2 63.92 61.88 3.38 o -8 0 2 538.75 568.81 17.32 o -7 0 2 1377.19 1533.10 44.89 o -6 0 2 739.18 757.95 15.91 o -5 0 2 49.91 45.00 1.20 o -4 0 2 437.43 437.31 6.43 o -3 0 2 1984.62 1810.81 28.11 o -2 0 2 1235.88 1175.87 16.56 o -1 0 2 1.17 2.29 .22 o 1 0 2 1308.07 1167.70 26.47 o 2 0 2 1654.06 1590.30 35.30 o 3 0 2 178.27 158.19 3.05 o 4 0 2 247.29 273.68 5.34 o 6 0 2 1095.99 1113.00 31.27 o 7 0 2 112.73 140.00 4.58 o 8 0 2 30.32 31.38 1.85 o 9 0 2 18.57 21.79 2.18 o 10 0 2 43.27 46.30 3.05 o 11 0 2 945.30 925.18 43.03 o -12 1 2 7.36 9.39 3.49 o -11 1 2 1.09 -.57 2.27 o -10 1 2 96.84 102.86 5.99 o -9 1 2 26.06 20.25 1.47 o -8 1 2 124.89 128.04 3.44 o -7 1 2 1080.19 1127.74 22.12 o -6 1 2 36.16 49.09 1.42 o -5 1 2 377.61 379.44 4.48 o -4 1 2 1151.56 1108.68 12.21 o -3 1 2 102.01 98.19 1.07 o -2 1 2 473.81 423.51 4.35 o -1 1 2 228.96 208.73 2.15 o 0 1 2 75.53 80.19 .85 o 1 1 2 3029.76 2706.35 27.33 o 2 1 2 1002.62 931.43 9.74 o 3 1 2 710.98 613.85 6.95 o 4 1 2 760.94 830.33 10.62 o 5 1 2 874.98 955.60 13.23 o 6 1 2 53.21 55.98 1.53 o 7 1 2 11.30 10.44 2.29 o 8 1 2 22.11 17.95 2.56 o 9 1 2 .11 .37 1.33 o 10 1 2 142.13 136.22 4.54 o 11 1 2 20.25 15.13 2.22 o 12 1 2 42.71 39.98 7.41 o -12 2 2 31.33 22.97 3.95 o -11 2 2 45.63 44.96 3.58 o -10 2 2 84.79 93.74 4.79 o -9 2 2 .74 4.84 2.34 o -8 2 2 693.53 725.92 17.10 o -7 2 2 90.42 88.83 2.28 o -6 2 2 54.84 57.13 2.89 o -5 2 2 437.61 444.10 5.94 o -4 2 2 963.66 1026.32 11.18 o -3 2 2 48.07 60.36 .76 o -2 2 2 1230.83 1366.90 15.09 o -1 2 2 856.39 788.33 8.48 o 0 2 2 142.20 108.46 1.58 o 1 2 2 822.96 757.69 8.33 o 2 2 2 627.59 559.22 5.42 o 3 2 2 688.73 659.17 6.72 o 4 2 2 163.03 163.45 2.01 o 5 2 2 126.84 130.97 2.78 o 6 2 2 16.69 14.78 .97 o 7 2 2 4.34 2.77 .94 o 8 2 2 287.27 295.90 6.84 o 9 2 2 .14 1.48 1.85 o 10 2 2 291.44 322.31 8.59 o 11 2 2 20.26 14.38 2.56 o 12 2 2 6.10 2.83 5.77 o -12 3 2 125.18 135.37 7.03 o -11 3 2 .94 4.68 2.96 o -10 3 2 50.83 49.59 2.73 o -9 3 2 142.23 138.94 4.11 o -8 3 2 51.35 50.65 2.07 o -7 3 2 484.41 506.37 8.54 o -6 3 2 47.13 44.28 2.07 o -5 3 2 46.55 41.38 1.02 o -4 3 2 24.07 30.16 .82 o -3 3 2 60.64 58.31 .94 o -2 3 2 2394.53 2748.55 32.18 o -1 3 2 101.89 109.70 1.27 o 0 3 2 1490.24 1621.10 18.94 o 1 3 2 338.59 341.41 4.14 o 2 3 2 696.71 809.37 8.98 o 3 3 2 21.48 20.34 1.58 o 4 3 2 2546.52 2799.18 36.57 o 5 3 2 76.16 70.10 4.14 o 6 3 2 243.38 222.97 4.19 o 7 3 2 11.95 12.27 1.63 o 8 3 2 220.86 238.76 5.99 o 9 3 2 619.70 689.58 18.88 o 10 3 2 140.26 139.72 5.10 o 11 3 2 13.55 4.51 3.92 o -11 4 2 55.77 42.47 5.39 o -10 4 2 45.05 48.18 3.70 o -9 4 2 31.81 30.02 2.14 o -8 4 2 2.98 .81 2.12 o -7 4 2 43.62 43.44 3.98 o -6 4 2 676.66 731.47 14.82 o -5 4 2 228.81 242.10 4.39 o -4 4 2 175.67 155.10 2.72 o -3 4 2 17.98 17.14 1.20 o -2 4 2 307.51 327.11 4.39 o -1 4 2 1114.25 1121.36 15.55 o 0 4 2 1503.51 1565.10 23.11 o 1 4 2 101.70 104.72 1.75 o 2 4 2 25.32 20.81 1.69 o 3 4 2 71.69 68.14 1.50 o 4 4 2 649.40 661.53 10.00 o 5 4 2 339.95 339.90 6.42 o 6 4 2 46.18 45.45 1.57 o 7 4 2 39.65 31.43 1.59 o 8 4 2 20.22 17.01 1.75 o 9 4 2 63.39 58.61 3.30 o 10 4 2 51.78 51.17 4.03 o -10 5 2 9.59 6.83 4.68 o -9 5 2 113.62 136.09 6.37 o -8 5 2 10.72 10.46 3.05 o -7 5 2 12.60 12.10 2.26 o -6 5 2 19.04 12.54 1.43 o -5 5 2 124.66 113.60 3.10 o -4 5 2 2.26 3.39 1.42 o -3 5 2 4.44 .89 .98 o -2 5 2 51.15 48.11 1.69 o -1 5 2 123.61 116.40 5.99 o 0 5 2 281.60 287.52 4.96 o 1 5 2 11.40 9.45 2.18 o 2 5 2 512.37 521.95 8.90 o 3 5 2 2.21 .44 1.00 o 4 5 2 57.34 67.39 1.99 o 5 5 2 48.12 47.33 1.70 o 6 5 2 36.98 41.23 1.94 o 7 5 2 33.59 31.96 2.83 o 8 5 2 28.22 30.72 2.56 o 9 5 2 16.04 10.59 2.93 o -8 6 2 .32 3.57 2.73 o -7 6 2 1.15 -.78 2.83 o -6 6 2 103.28 98.09 3.49 o -5 6 2 .45 2.09 3.05 o -4 6 2 61.53 53.69 2.46 o -3 6 2 586.99 576.04 12.17 o -2 6 2 89.76 80.48 2.67 o -1 6 2 .19 .82 2.45 o 0 6 2 30.22 26.00 1.95 o 1 6 2 .16 1.47 1.67 o 2 6 2 327.49 339.03 6.86 o 3 6 2 181.49 164.85 4.00 o 4 6 2 27.73 24.86 1.99 o 5 6 2 6.22 7.32 1.84 o 6 6 2 1.21 -.73 2.34 o 7 6 2 173.22 200.98 8.54 o 8 6 2 31.59 30.49 8.23 o -6 7 2 .01 3.92 4.16 o -5 7 2 21.46 27.77 6.70 o -4 7 2 182.17 201.28 6.74 o -3 7 2 .12 1.24 5.23 o -2 7 2 9.94 7.19 2.23 o -1 7 2 1.44 1.48 2.17 o 0 7 2 51.48 51.53 2.70 o 1 7 2 327.39 328.59 9.48 o 2 7 2 .87 -1.55 3.98 o 3 7 2 27.45 28.28 2.77 o 4 7 2 28.72 24.28 2.77 o 5 7 2 6.94 2.98 3.43 o 6 7 2 31.79 36.72 6.62 o -12 1 3 60.14 60.83 5.44 o -11 1 3 13.68 12.45 3.35 o -10 1 3 18.87 18.35 1.91 o -9 1 3 493.20 548.24 11.39 o -8 1 3 156.54 162.67 3.50 o -7 1 3 1400.95 1442.21 23.54 o -6 1 3 87.81 90.76 1.69 o -5 1 3 235.67 229.36 2.69 o -4 1 3 230.51 216.43 2.33 o -3 1 3 6530.14 6283.17 79.90 o -1 1 3 1559.29 1461.32 15.81 o 0 1 3 93.21 105.11 1.12 o 1 1 3 383.62 347.84 3.66 o 2 1 3 893.41 828.35 8.91 o 3 1 3 516.63 529.16 5.93 o 4 1 3 24.98 24.08 .52 o 5 1 3 55.91 93.16 1.58 o 6 1 3 716.81 766.20 14.63 o 7 1 3 .37 .30 .78 o 8 1 3 1.37 2.84 .94 o 9 1 3 12.94 14.52 2.78 o 10 1 3 17.08 16.65 1.91 o 11 1 3 300.06 291.05 10.89 o 12 1 3 54.84 47.28 6.32 o -12 2 3 .00 1.38 4.55 o -11 2 3 19.98 16.18 2.88 o -10 2 3 33.85 32.86 2.49 o -9 2 3 674.85 754.84 18.91 o -8 2 3 53.03 57.10 2.61 o -7 2 3 33.24 30.36 1.13 o -6 2 3 8.11 8.79 .78 o -5 2 3 115.35 121.80 2.29 o -4 2 3 1162.77 1323.20 13.87 o -3 2 3 1203.17 1234.01 13.35 o -2 2 3 697.09 752.49 7.38 o -1 2 3 2423.52 2339.85 23.46 o 0 2 3 76.26 74.53 .87 o 1 2 3 8.11 5.56 .31 o 2 2 3 152.68 127.47 1.50 o 3 2 3 8.93 9.21 .39 o 4 2 3 61.41 78.07 1.18 o 5 2 3 107.65 104.46 1.88 o 6 2 3 468.13 456.59 9.25 o 7 2 3 47.76 49.25 2.89 o 8 2 3 14.07 11.19 1.26 o 9 2 3 379.37 397.76 9.02 o 10 2 3 .40 -.62 2.00 o 11 2 3 24.02 23.19 2.85 o 12 2 3 22.32 16.08 11.33 o -12 3 3 7.03 6.98 3.64 o -11 3 3 .95 6.53 3.12 o -10 3 3 30.40 33.15 3.54 o -9 3 3 7.98 4.58 1.58 o -8 3 3 46.32 47.68 1.71 o -7 3 3 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