#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214330.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214330_Fobs loop_ _publ_author_name 'Beheshti, Azizolla' 'Clegg, William' 'Dale, Sophie H.' 'Hyvadi, Reza' _publ_section_title ; \m~3~-Iodido-tri-\m~3~-sulfido-tris[(triphenylphosphine)silver(I)][thioxotungsten(VI)] dichloromethane 0.45-solvate ; _journal_coeditor_code LH2438 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1990 _journal_page_last m1991 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 74.671 _cell_angle_beta 87.659 _cell_angle_gamma 63.692 _cell_length_a 12.1130 _cell_length_b 13.3231 _cell_length_c 20.0301 _exptl_crystal_F_000 1534.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file lh2438Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ab62a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 375.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 1493.60 1302.36 34.74 o 4 0 0 19865.10 18094.02 589.38 o 5 0 0 1896.08 1843.17 62.33 o 6 0 0 8818.28 7832.45 359.80 o 7 0 0 1552.38 1646.63 72.85 o 8 0 0 379.33 381.14 47.52 o 9 0 0 1479.74 1463.06 95.61 o 10 0 0 1176.40 1282.65 122.08 o 11 0 0 3636.20 3479.50 270.45 o 12 0 0 718.85 419.62 277.28 o 14 0 0 2622.84 3492.44 428.30 o -13 1 0 21.75 297.98 163.83 o -12 1 0 17.40 54.08 98.86 o -11 1 0 5174.07 4829.44 428.16 o -10 1 0 133.12 27.18 109.82 o -9 1 0 1156.98 973.62 121.04 o -8 1 0 700.83 601.52 63.17 o -7 1 0 2453.81 2344.00 95.63 o -6 1 0 17760.57 17056.45 410.74 o -5 1 0 629.81 619.74 46.22 o -4 1 0 1224.27 1171.78 35.82 o -3 1 0 36122.51 34133.46 803.19 o -2 1 0 5832.25 5323.67 174.66 o 3 1 0 17318.44 15789.96 380.55 o 4 1 0 82214.77 75283.45 1802.04 o 5 1 0 16194.89 14647.01 390.61 o 6 1 0 358.16 309.12 43.15 o 7 1 0 5323.49 5522.91 239.90 o 8 1 0 22039.39 20042.55 702.80 o 9 1 0 1493.22 1568.06 105.70 o 10 1 0 1981.08 2221.42 133.46 o 11 1 0 364.43 423.46 152.02 o 12 1 0 1055.06 1184.26 207.53 o 13 1 0 8288.47 8887.82 700.45 o 14 1 0 1010.59 1213.30 362.97 o -13 2 0 380.53 348.30 222.19 o -12 2 0 133.35 183.69 138.45 o -11 2 0 4146.75 4933.63 440.26 o -10 2 0 8398.90 8013.21 325.84 o -9 2 0 2895.78 2943.70 222.53 o -8 2 0 1406.21 1268.57 118.55 o -7 2 0 26590.91 26758.45 785.55 o -6 2 0 23129.80 21593.27 516.26 o -5 2 0 6159.14 6231.54 159.50 o -4 2 0 22858.73 22508.97 534.97 o -3 2 0 11423.53 11156.97 231.34 o -2 2 0 511.62 537.98 23.22 o 3 2 0 68106.16 64062.04 1446.90 o 4 2 0 42841.57 41730.13 914.84 o 5 2 0 82633.84 76611.41 1833.82 o 6 2 0 2027.16 2137.03 87.05 o 7 2 0 1245.58 1237.30 86.35 o 8 2 0 32595.83 32081.26 1110.65 o 9 2 0 196.62 123.54 66.42 o 10 2 0 231.48 221.87 81.22 o 11 2 0 129.55 146.05 107.52 o 12 2 0 10.29 -89.96 194.86 o 13 2 0 11966.75 12607.07 480.78 o 14 2 0 1162.92 1285.29 133.26 o -12 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3946.35 131.31 o -5 4 0 1803.85 1664.95 79.28 o -4 4 0 6305.44 6093.29 172.57 o -3 4 0 10033.48 9907.76 445.95 o -2 4 0 17663.68 18149.04 423.24 o -1 4 0 104763.16 102641.48 1846.38 o 0 4 0 19493.99 20488.54 387.43 o 1 4 0 29526.77 28383.20 518.28 o 2 4 0 68.77 86.24 9.74 o 3 4 0 9205.64 8735.35 206.48 o 4 4 0 1826.97 1943.65 55.11 o 5 4 0 76923.79 74577.86 1529.35 o 6 4 0 2465.86 2652.87 77.12 o 7 4 0 22153.81 22082.09 592.59 o 8 4 0 311.86 408.79 33.41 o 9 4 0 12120.68 12187.76 444.89 o 10 4 0 10480.33 10635.20 400.76 o 11 4 0 560.14 714.81 134.72 o 12 4 0 19331.86 21299.11 1461.54 o 13 4 0 2155.77 2109.04 279.13 o 14 4 0 1443.86 1473.61 146.17 o -11 5 0 135.20 143.20 181.98 o -10 5 0 1313.33 874.25 197.99 o -9 5 0 4491.70 4834.93 293.66 o -8 5 0 2448.19 2340.79 183.62 o -7 5 0 877.56 894.94 70.28 o -6 5 0 98.95 125.26 46.27 o -5 5 0 902.59 828.21 49.33 o -4 5 0 18482.01 18838.79 793.40 o -3 5 0 25041.45 24741.12 840.09 o -2 5 0 14248.21 14898.04 308.65 o -1 5 0 59627.77 59682.83 1378.71 o 0 5 0 61.86 83.92 14.30 o 1 5 0 91703.87 88769.30 1835.17 o 2 5 0 657.65 645.29 26.98 o 3 5 0 48102.32 47587.32 1035.11 o 4 5 0 3039.42 3087.88 80.18 o 5 5 0 4388.71 5070.05 155.59 o 6 5 0 1903.79 1948.08 54.73 o 7 5 0 5229.43 5186.10 135.15 o 8 5 0 3109.43 3131.29 100.73 o 9 5 0 13129.95 12862.93 354.46 o 10 5 0 19543.37 19724.73 698.31 o 11 5 0 975.62 820.53 108.26 o 12 5 0 11483.66 12584.66 894.32 o 13 5 0 2315.61 2561.11 286.10 o -10 6 0 91.17 29.67 264.61 o -9 6 0 726.08 480.25 181.63 o -8 6 0 4132.43 3730.43 316.85 o -7 6 0 1895.10 1994.82 130.34 o -6 6 0 763.10 816.63 93.73 o -5 6 0 1359.47 1480.80 100.48 o -4 6 0 3251.22 2977.50 137.56 o -3 6 0 4673.04 4493.87 207.48 o -2 6 0 35264.46 35889.45 1252.25 o -1 6 0 16615.91 17577.38 361.60 o 0 6 0 7937.71 7549.16 153.07 o 1 6 0 62164.01 61332.58 1351.52 o 2 6 0 4008.18 4004.87 88.61 o 3 6 0 29947.97 29385.28 594.49 o 4 6 0 74706.91 74259.96 1924.42 o 5 6 0 37330.41 37598.88 947.21 o 6 6 0 9684.93 9270.84 244.48 o 7 6 0 10002.43 9985.54 249.42 o 8 6 0 4566.07 4501.60 137.36 o 9 6 0 58.84 36.35 34.53 o 10 6 0 5092.10 5363.10 179.47 o 11 6 0 1059.03 1052.48 102.55 o 12 6 0 2368.22 2185.52 135.17 o -9 7 0 963.06 251.37 270.45 o -8 7 0 6609.39 6908.34 362.87 o -7 7 0 2415.24 2399.38 178.25 o -6 7 0 687.78 698.89 110.04 o -5 7 0 533.24 615.79 75.49 o -4 7 0 125.69 94.01 48.63 o -3 7 0 68.24 73.65 37.09 o -2 7 0 26915.73 24954.60 647.40 o -1 7 0 2434.74 2484.19 90.31 o 0 7 0 8530.36 8579.06 181.32 o 1 7 0 34.20 96.10 18.56 o 2 7 0 9931.99 9400.05 200.04 o 3 7 0 11205.75 10671.57 241.83 o 4 7 0 109170.87 103258.14 2408.61 o 5 7 0 35070.75 34217.98 794.71 o 6 7 0 27121.97 26372.74 745.04 o 7 7 0 6404.98 5823.03 182.42 o 8 7 0 4035.17 3880.44 146.29 o 9 7 0 1542.11 1485.10 53.96 o 10 7 0 166.19 187.80 48.71 o 11 7 0 7996.85 8424.01 326.26 o -8 8 0 4984.80 4752.57 355.42 o -7 8 0 5713.09 5138.17 362.68 o -6 8 0 662.97 737.85 149.88 o -5 8 0 111.01 232.21 87.62 o -4 8 0 4164.61 4226.09 265.54 o -3 8 0 1198.22 1305.03 161.76 o -2 8 0 1305.28 1321.80 64.66 o -1 8 0 2597.25 2649.81 80.20 o 0 8 0 3816.35 3861.93 104.61 o 1 8 0 17812.40 18247.65 446.16 o 2 8 0 5652.07 5723.15 152.75 o 3 8 0 12917.41 13300.07 321.33 o 4 8 0 20577.89 20507.25 487.84 o 5 8 0 1382.97 1410.16 87.90 o 6 8 0 36164.97 36214.24 1015.32 o 7 8 0 598.01 543.21 51.54 o 8 8 0 25370.14 25683.17 771.44 o 9 8 0 9.77 -103.81 90.87 o 10 8 0 3486.45 3762.38 163.75 o 11 8 0 16763.25 16905.79 718.48 o 12 8 0 9244.33 9346.90 437.46 o 13 8 0 92.24 6.27 114.87 o 14 8 0 1363.08 1671.94 178.39 o -8 9 0 789.47 395.30 384.60 o -7 9 0 3810.43 4157.45 323.25 o -6 9 0 5819.28 5221.26 515.77 o -5 9 0 96.40 -37.28 93.77 o -4 9 0 3361.22 3092.43 153.34 o -3 9 0 15411.05 14826.29 533.93 o -2 9 0 1018.35 976.69 68.42 o -1 9 0 2781.42 2564.89 107.83 o 0 9 0 24583.57 24630.69 650.67 o 1 9 0 10854.35 11112.95 368.21 o 2 9 0 7338.96 7118.71 180.14 o 3 9 0 2814.33 2710.86 78.66 o 4 9 0 6225.46 6084.44 156.64 o 5 9 0 1841.45 1849.27 67.52 o 6 9 0 20814.18 20486.30 528.10 o 7 9 0 77.97 64.25 44.59 o 8 9 0 21484.23 21718.50 685.07 o 9 9 0 5609.81 5526.29 212.90 o 10 9 0 6176.00 5988.20 230.62 o 11 9 0 12590.47 12568.61 438.69 o -7 10 0 26.77 -72.54 273.79 o -6 10 0 3726.26 4068.06 311.30 o -5 10 0 1011.51 889.48 140.77 o -4 10 0 2334.50 2835.40 327.88 o -3 10 0 14300.01 14891.57 1051.79 o -2 10 0 209.12 329.49 67.55 o -1 10 0 170.00 205.63 70.07 o 0 10 0 14015.68 14122.53 436.27 o 1 10 0 3267.22 3193.40 145.66 o 2 10 0 3440.64 3408.29 129.84 o 3 10 0 2531.71 2507.18 77.16 o 4 10 0 24965.57 24359.01 581.45 o 5 10 0 643.16 694.98 39.02 o 6 10 0 4566.39 4414.10 135.64 o 7 10 0 4446.89 4516.59 157.06 o 8 10 0 3914.95 3861.12 150.72 o 9 10 0 14216.24 13961.26 420.97 o 10 10 0 8007.91 7871.13 256.61 o 11 10 0 9538.84 9454.10 429.52 o 13 10 0 274.55 200.27 176.50 o 14 10 0 60.70 -68.85 132.63 o 15 10 0 1387.17 1508.09 199.10 o -5 11 0 112.06 442.25 359.12 o -4 11 0 4466.63 4191.04 286.81 o -3 11 0 4461.89 4285.86 328.05 o -2 11 0 20.51 69.79 70.45 o -1 11 0 1406.91 1250.56 85.38 o 0 11 0 665.21 627.35 64.15 o 1 11 0 20010.38 19973.17 709.23 o 2 11 0 2952.66 2954.08 133.61 o 3 11 0 10519.50 10963.90 428.44 o 4 11 0 21151.60 21031.17 630.98 o 5 11 0 18469.00 17484.31 919.28 o 6 11 0 263.84 236.98 62.13 o 7 11 0 3969.86 4061.46 149.09 o 8 11 0 486.65 567.70 66.88 o 9 11 0 3145.58 3296.14 140.36 o 10 11 0 9767.24 9780.71 333.96 o 11 11 0 5980.44 5924.65 213.10 o 12 11 0 19.03 -62.08 225.39 o 13 11 0 319.33 431.25 185.12 o 14 11 0 165.36 315.71 223.76 o 15 11 0 3173.83 3438.64 457.05 o -3 12 0 1804.86 2048.63 281.62 o -2 12 0 16.68 119.14 261.34 o -1 12 0 25.27 68.75 269.16 o 0 12 0 1097.48 1044.87 83.06 o 1 12 0 25990.39 25681.84 901.00 o 2 12 0 3566.56 3663.95 169.60 o 3 12 0 29.38 107.31 61.63 o 4 12 0 7154.55 7187.30 239.40 o 5 12 0 26259.33 26195.08 1079.67 o 6 12 0 1748.12 1593.63 112.90 o 7 12 0 2369.06 2507.19 127.54 o 8 12 0 721.03 821.81 109.12 o 9 12 0 2874.48 2814.83 154.53 o 10 12 0 4699.49 4691.12 211.99 o 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14 0 187.73 88.59 161.53 o 12 14 0 499.76 393.13 146.37 o 13 14 0 987.34 557.12 381.61 o 2 15 0 300.45 515.41 302.90 o 3 15 0 4776.37 4374.95 372.50 o 4 15 0 1456.08 1587.80 275.14 o 5 15 0 1788.77 2378.49 258.35 o 6 15 0 3276.37 2600.68 323.82 o 7 15 0 218.92 296.05 99.44 o 8 15 0 81.75 -100.95 106.41 o 9 15 0 6642.87 6635.07 280.12 o 10 15 0 9964.59 9794.14 472.72 o 11 15 0 16.45 -221.34 147.56 o 12 15 0 743.90 564.27 212.07 o 4 16 0 5685.73 5593.80 457.34 o 5 16 0 2127.39 1939.66 323.11 o 6 16 0 1701.81 2211.96 346.60 o 7 16 0 53.18 -54.66 268.03 o 8 16 0 5506.15 5285.06 466.45 o 9 16 0 109.09 -96.37 224.40 o 10 16 0 3535.64 3527.24 228.38 o -10 -16 1 1257.21 1321.48 146.73 o -9 -16 1 453.39 419.14 159.13 o -8 -16 1 943.81 1003.78 312.86 o -7 -16 1 3786.55 3835.91 363.68 o -6 -16 1 75.65 -82.98 197.00 o -5 -16 1 2459.62 2201.42 339.19 o -12 -15 1 901.77 752.41 148.38 o -11 -15 1 1854.56 1737.69 165.06 o -10 -15 1 8780.44 8660.87 425.03 o -9 -15 1 1027.95 829.89 149.42 o -8 -15 1 15.39 33.43 125.95 o -7 -15 1 1705.87 1934.21 223.47 o -6 -15 1 100.31 198.89 107.60 o -5 -15 1 216.02 759.52 234.29 o -4 -15 1 9384.19 8798.29 596.54 o -13 -14 1 715.90 745.24 203.39 o -12 -14 1 3251.06 3425.08 242.79 o -11 -14 1 2883.64 2696.14 205.05 o -10 -14 1 20085.74 19405.01 836.35 o -9 -14 1 1626.80 1400.35 148.25 o -8 -14 1 8558.56 8665.49 408.47 o -7 -14 1 1743.31 1977.15 224.61 o -6 -14 1 1662.53 1514.15 136.43 o -5 -14 1 179.12 170.42 185.61 o -4 -14 1 1293.93 1322.67 113.13 o -3 -14 1 110.58 -67.73 300.91 o -2 -14 1 771.16 589.29 153.87 o 1 -14 1 1653.80 2457.92 416.63 o -14 -13 1 235.53 -51.64 187.11 o -13 -13 1 2021.99 2016.52 409.08 o -12 -13 1 1355.18 1347.18 227.46 o -11 -13 1 4053.36 3983.34 199.50 o -10 -13 1 13225.02 13001.66 516.75 o -9 -13 1 46.84 -92.31 151.16 o -8 -13 1 20304.99 20544.63 869.92 o -7 -13 1 955.18 808.46 101.20 o -6 -13 1 9878.93 10105.88 449.17 o -5 -13 1 76.52 69.81 234.29 o -4 -13 1 3770.78 3843.27 193.44 o -3 -13 1 1577.61 1738.19 103.53 o 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