#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:32:10 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181063 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/43/2214353.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214353_Fobs loop_ _publ_author_name 'Liao, Bei-Ling' 'Li, Jun-Xia' 'Jiang, Yi-Min' _publ_section_title ; Bis[2-(2-pyridylmethylamino)ethanesulfonato-\k^3^N,N',O]nickel(II) ; _journal_coeditor_code NG2282 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1974 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.848 _cell_angle_gamma 90.000 _cell_length_a 9.6090 _cell_length_b 9.9270 _cell_length_c 11.4537 _exptl_crystal_F_000 508.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file ng2282Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 157.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4373.30 4431.27 38.41 o 3 0 0 550.93 579.21 6.04 o 4 0 0 2293.17 2536.07 22.88 o 5 0 0 479.02 536.26 6.39 o 6 0 0 77.18 104.98 2.53 o 7 0 0 981.10 1011.60 11.28 o 8 0 0 401.53 438.53 8.39 o 9 0 0 223.78 230.40 6.14 o 10 0 0 225.20 203.92 6.17 o 11 0 0 7.15 3.89 2.01 o 1 1 0 1537.73 1610.13 12.27 o 2 1 0 5219.21 5113.90 31.36 o 3 1 0 669.20 661.45 4.79 o 4 1 0 507.79 586.27 4.58 o 5 1 0 1211.74 1237.19 9.53 o 6 1 0 1050.72 1006.48 7.68 o 7 1 0 219.23 246.51 3.45 o 8 1 0 98.21 95.72 2.26 o 9 1 0 175.10 172.43 3.76 o 10 1 0 37.43 47.97 2.63 o 11 1 0 63.18 82.09 3.53 o 0 2 0 94.50 96.39 1.92 o 1 2 0 543.25 515.01 4.54 o 2 2 0 104.69 101.74 1.38 o 3 2 0 3231.37 3091.43 19.32 o 4 2 0 7680.99 7312.97 44.59 o 5 2 0 5288.58 5320.84 33.02 o 6 2 0 501.50 517.64 4.68 o 7 2 0 55.38 58.91 1.72 o 8 2 0 109.48 104.56 2.41 o 9 2 0 319.66 306.60 5.97 o 10 2 0 411.13 404.13 7.35 o 11 2 0 229.96 249.24 7.54 o 1 3 0 8195.09 7867.35 69.84 o 2 3 0 2.17 10.33 0.58 o 3 3 0 280.52 339.06 2.99 o 4 3 0 384.29 381.23 3.44 o 5 3 0 71.69 53.20 1.47 o 6 3 0 1209.60 1256.11 10.38 o 7 3 0 221.41 235.00 4.03 o 8 3 0 1.21 2.14 0.97 o 9 3 0 0.35 0.02 0.99 o 10 3 0 116.32 123.15 4.60 o 11 3 0 32.67 34.62 3.46 o 0 4 0 364.59 297.24 3.80 o 1 4 0 1787.61 1656.44 13.50 o 2 4 0 237.84 269.20 3.01 o 3 4 0 551.02 549.76 5.09 o 4 4 0 360.20 369.02 3.65 o 5 4 0 1078.50 1106.28 9.37 o 6 4 0 1122.63 1087.91 10.76 o 7 4 0 1754.96 1713.99 15.78 o 8 4 0 1106.43 1078.79 12.96 o 9 4 0 332.51 336.05 5.63 o 10 4 0 129.05 129.90 4.31 o 11 4 0 60.34 54.64 4.16 o 1 5 0 176.23 176.95 2.43 o 2 5 0 12.07 9.24 0.72 o 3 5 0 49.84 51.48 1.77 o 4 5 0 51.46 56.54 1.57 o 5 5 0 228.61 226.00 6.05 o 6 5 0 245.01 236.87 4.14 o 7 5 0 1.18 1.08 0.93 o 8 5 0 0.60 -0.72 0.97 o 9 5 0 40.23 40.86 2.23 o 10 5 0 0.71 2.12 1.45 o 11 5 0 1.13 0.59 2.13 o 0 6 0 955.29 976.63 10.38 o 1 6 0 1444.52 1509.65 11.80 o 2 6 0 1082.44 1128.50 9.42 o 3 6 0 660.91 640.95 6.23 o 4 6 0 564.76 558.94 5.79 o 5 6 0 386.63 388.56 5.51 o 6 6 0 172.85 183.09 3.76 o 7 6 0 230.73 235.56 4.54 o 8 6 0 275.12 284.51 5.22 o 9 6 0 174.46 176.70 4.29 o 10 6 0 104.65 106.79 8.76 o 1 7 0 40.81 39.52 2.07 o 2 7 0 106.19 109.07 2.30 o 3 7 0 166.44 173.42 2.93 o 4 7 0 121.80 123.19 2.98 o 5 7 0 0.10 1.40 1.17 o 6 7 0 53.70 47.93 2.17 o 7 7 0 3.10 2.85 1.20 o 8 7 0 5.90 4.28 1.32 o 9 7 0 0.60 1.07 1.47 o 10 7 0 0.09 -0.53 1.57 o 0 8 0 365.40 358.25 7.40 o 1 8 0 384.33 375.02 5.40 o 2 8 0 918.35 887.97 8.39 o 3 8 0 792.06 757.02 7.58 o 4 8 0 1173.80 1155.78 13.96 o 5 8 0 507.24 495.93 8.36 o 6 8 0 214.05 217.96 4.55 o 7 8 0 25.89 29.19 2.04 o 8 8 0 28.50 31.36 2.20 o 9 8 0 35.25 31.80 2.81 o 1 9 0 310.95 317.63 5.48 o 2 9 0 386.98 390.85 5.87 o 3 9 0 162.79 154.74 5.16 o 4 9 0 0.42 -0.75 1.16 o 5 9 0 0.24 0.56 1.12 o 6 9 0 78.00 82.02 3.07 o 7 9 0 58.06 62.26 2.86 o 8 9 0 8.65 5.18 1.60 o 0 10 0 1451.72 1405.53 20.15 o 1 10 0 820.51 831.62 9.87 o 2 10 0 130.10 131.29 6.52 o 3 10 0 90.86 81.03 3.35 o 4 10 0 50.82 50.06 2.91 o 5 10 0 6.75 7.58 2.23 o 6 10 0 212.79 223.13 5.07 o 7 10 0 394.57 425.23 10.18 o 1 11 0 21.64 20.89 1.88 o 2 11 0 75.57 78.04 3.54 o 3 11 0 78.37 83.84 3.72 o 4 11 0 5.59 7.19 1.94 o 5 11 0 168.63 183.42 5.52 o 6 11 0 137.92 149.81 5.17 o 0 12 0 2.15 2.71 2.00 o 1 12 0 14.24 8.77 1.97 o 2 12 0 132.76 137.73 7.91 o 3 12 0 478.91 502.84 9.41 o 4 12 0 375.23 387.06 10.08 o -12 1 1 131.61 138.52 4.76 o -11 1 1 178.65 170.68 4.92 o -10 1 1 391.98 406.40 6.30 o -9 1 1 445.92 429.09 6.18 o -8 1 1 404.79 408.46 5.65 o -7 1 1 183.39 197.37 3.01 o -6 1 1 253.38 227.17 2.65 o -5 1 1 2926.29 2926.05 18.74 o -4 1 1 3406.62 3380.91 21.13 o -3 1 1 1449.41 1496.62 11.16 o -2 1 1 105.18 111.12 2.24 o -1 1 1 5309.05 5115.25 78.26 o 0 1 1 9231.41 7524.37 241.28 o 1 1 1 28.76 34.84 0.74 o 2 1 1 2118.01 2193.58 15.06 o 3 1 1 2285.93 2229.13 14.22 o 4 1 1 5987.77 6092.37 37.31 o 5 1 1 764.51 709.71 5.70 o 6 1 1 679.08 706.75 5.93 o 7 1 1 112.92 104.64 2.01 o 8 1 1 9.35 13.08 1.48 o 9 1 1 447.76 434.18 6.25 o 10 1 1 156.82 143.23 5.29 o 11 1 1 65.88 68.57 6.27 o -12 2 1 14.82 14.34 2.25 o -11 2 1 15.40 18.79 2.80 o -10 2 1 2.19 2.93 1.39 o -9 2 1 1.85 3.73 1.29 o -8 2 1 0.08 -0.35 0.70 o -7 2 1 55.00 60.85 1.75 o -6 2 1 574.11 587.45 5.72 o -5 2 1 170.34 202.76 2.30 o -4 2 1 18.40 26.43 0.89 o -3 2 1 355.28 378.07 3.54 o -2 2 1 0.19 -0.56 0.37 o -1 2 1 19337.37 15823.00 528.26 o 0 2 1 1021.50 1005.53 6.62 o 1 2 1 791.43 803.08 6.04 o 2 2 1 1716.65 1751.29 12.16 o 3 2 1 227.80 269.88 2.55 o 4 2 1 110.84 113.96 1.83 o 5 2 1 5.54 9.92 0.66 o 6 2 1 343.97 346.52 3.67 o 7 2 1 12.52 14.76 1.07 o 8 2 1 3.64 3.28 0.87 o 9 2 1 1.19 -1.16 1.09 o 10 2 1 129.26 135.98 5.43 o 11 2 1 5.83 8.70 3.74 o -11 3 1 26.55 25.22 3.44 o -10 3 1 149.50 153.72 6.27 o -9 3 1 228.35 255.88 5.52 o -8 3 1 1204.97 1241.00 13.59 o -7 3 1 1145.36 1161.79 12.97 o -6 3 1 1832.28 1791.24 13.86 o -5 3 1 1195.78 1243.72 8.87 o -4 3 1 1006.28 1069.82 7.59 o -3 3 1 355.53 366.80 4.92 o -2 3 1 144.75 140.79 1.82 o -1 3 1 11176.70 10395.92 190.82 o 0 3 1 6645.49 6375.60 39.09 o 1 3 1 1826.58 1811.43 14.39 o 2 3 1 14.43 34.26 1.03 o 3 3 1 663.43 671.78 4.93 o 4 3 1 88.70 85.73 1.30 o 5 3 1 27.36 29.69 1.03 o 6 3 1 600.93 611.33 6.09 o 7 3 1 1901.23 1916.74 17.07 o 8 3 1 1452.32 1464.15 14.13 o 9 3 1 733.85 760.05 9.94 o 10 3 1 326.17 333.70 8.57 o 11 3 1 32.98 28.94 4.90 o -11 4 1 1.40 1.86 1.64 o -10 4 1 75.57 83.80 3.57 o -9 4 1 118.94 120.62 3.32 o -8 4 1 192.42 186.23 3.89 o -7 4 1 2.88 2.93 0.99 o -6 4 1 1018.04 1005.08 10.10 o -5 4 1 714.48 706.03 7.54 o -4 4 1 138.49 144.36 2.92 o -3 4 1 32.74 40.93 1.27 o -2 4 1 130.50 188.67 2.39 o -1 4 1 373.18 458.57 3.29 o 0 4 1 21.94 16.76 1.41 o 1 4 1 1541.57 1557.41 11.52 o 2 4 1 1021.30 1046.25 8.32 o 3 4 1 534.59 551.75 5.17 o 4 4 1 92.56 107.07 1.70 o 5 4 1 885.96 870.04 7.74 o 6 4 1 1335.20 1335.51 15.01 o 7 4 1 657.66 639.42 7.67 o 8 4 1 7.55 5.80 1.27 o 9 4 1 75.93 67.76 3.10 o 10 4 1 7.32 8.91 3.82 o 11 4 1 34.25 37.36 5.82 o -11 5 1 266.26 262.71 8.28 o -10 5 1 175.01 161.12 4.88 o -9 5 1 208.50 205.30 4.41 o -8 5 1 63.55 58.04 2.36 o -7 5 1 27.96 28.87 1.70 o -6 5 1 480.85 488.27 6.33 o -5 5 1 3139.43 3018.33 24.80 o -4 5 1 2365.72 2275.51 16.83 o -3 5 1 1228.20 1161.32 9.40 o -2 5 1 3762.54 3675.60 25.59 o -1 5 1 1366.51 1390.32 8.61 o 0 5 1 614.54 677.35 5.31 o 1 5 1 11.28 9.07 0.55 o 2 5 1 1834.42 1875.41 14.04 o 3 5 1 3751.95 3797.30 26.63 o 4 5 1 2668.69 2662.36 19.52 o 5 5 1 2881.23 2869.10 23.83 o 6 5 1 621.31 616.48 7.43 o 7 5 1 28.51 27.50 2.50 o 8 5 1 33.88 31.27 2.29 o 9 5 1 21.09 19.95 2.16 o 10 5 1 103.08 107.86 4.16 o -10 6 1 57.96 65.98 2.92 o -9 6 1 100.11 92.23 3.13 o -8 6 1 92.82 87.16 2.89 o -7 6 1 39.26 40.39 2.00 o -6 6 1 141.89 139.74 3.27 o -5 6 1 1077.02 1071.90 12.56 o -4 6 1 214.12 211.35 3.72 o -3 6 1 370.75 382.13 4.34 o -2 6 1 590.03 582.13 5.70 o -1 6 1 118.45 92.56 2.31 o 0 6 1 320.16 387.70 3.67 o 1 6 1 1830.57 1894.69 14.34 o 2 6 1 445.54 448.61 4.83 o 3 6 1 41.96 46.61 1.53 o 4 6 1 1.01 3.28 1.10 o 5 6 1 373.54 369.31 5.38 o 6 6 1 1267.41 1253.64 12.64 o 7 6 1 474.02 457.64 6.61 o 8 6 1 26.61 22.72 2.14 o 9 6 1 40.94 46.16 4.37 o 10 6 1 67.60 69.23 3.60 o -10 7 1 13.54 9.85 1.81 o -9 7 1 187.73 189.11 7.31 o -8 7 1 275.61 269.74 5.27 o -7 7 1 567.92 569.14 7.79 o -6 7 1 82.52 81.41 2.74 o -5 7 1 10.63 13.45 1.37 o -4 7 1 61.13 63.99 2.23 o -3 7 1 38.55 35.18 1.42 o -2 7 1 718.48 706.59 6.83 o -1 7 1 2713.39 2729.26 20.09 o 0 7 1 6374.94 6278.07 48.06 o 1 7 1 4302.94 4278.93 30.15 o 2 7 1 2559.50 2499.55 18.78 o 3 7 1 771.14 718.78 7.10 o 4 7 1 113.78 112.17 3.48 o 5 7 1 18.87 22.64 1.62 o 6 7 1 174.11 184.73 4.09 o 7 7 1 528.84 536.39 7.57 o 8 7 1 420.36 417.09 7.94 o 9 7 1 99.73 102.77 5.05 o -9 8 1 77.78 77.79 3.23 o -8 8 1 79.46 91.59 3.26 o -7 8 1 8.52 7.15 1.38 o -6 8 1 482.98 470.31 6.91 o -5 8 1 80.32 87.14 2.80 o -4 8 1 126.40 127.78 3.71 o -3 8 1 91.70 87.93 4.17 o -2 8 1 236.95 238.67 4.16 o -1 8 1 988.54 1016.08 10.51 o 0 8 1 385.41 382.73 5.45 o 1 8 1 187.59 200.02 3.80 o 2 8 1 572.47 609.79 9.44 o 3 8 1 239.90 246.88 3.82 o 4 8 1 75.44 66.26 2.46 o 5 8 1 80.41 78.71 2.78 o 6 8 1 120.34 120.26 4.27 o 7 8 1 17.57 15.17 1.72 o 8 8 1 13.41 13.43 2.10 o 9 8 1 11.75 13.53 3.15 o -8 9 1 123.91 125.86 4.03 o -7 9 1 95.95 85.88 4.41 o -6 9 1 118.37 112.22 3.46 o -5 9 1 594.18 574.64 8.03 o -4 9 1 1347.18 1372.84 14.01 o -3 9 1 941.13 923.33 12.19 o -2 9 1 492.12 484.32 6.67 o -1 9 1 26.23 26.55 1.72 o 0 9 1 6.13 7.22 1.21 o 1 9 1 15.88 14.22 1.41 o 2 9 1 31.11 36.19 1.95 o 3 9 1 232.76 239.45 5.36 o 4 9 1 334.72 360.52 7.18 o 5 9 1 378.52 406.58 7.21 o 6 9 1 194.82 184.56 4.41 o 7 9 1 30.06 31.97 2.74 o 8 9 1 21.97 21.88 2.62 o -7 10 1 8.95 6.07 1.63 o -6 10 1 26.84 28.31 2.18 o -5 10 1 42.64 44.92 2.88 o -4 10 1 165.25 163.19 4.77 o -3 10 1 18.76 15.45 2.20 o -2 10 1 214.02 208.95 5.22 o -1 10 1 218.68 217.02 4.45 o 0 10 1 3.34 4.78 1.37 o 1 10 1 7.55 10.24 1.50 o 2 10 1 23.73 25.25 2.68 o 3 10 1 25.23 24.08 3.49 o 4 10 1 8.42 6.98 1.70 o 5 10 1 0.21 1.11 1.50 o 6 10 1 11.58 13.37 1.88 o 7 10 1 14.12 19.11 2.54 o -6 11 1 229.19 240.92 8.07 o -5 11 1 101.00 116.92 4.52 o -4 11 1 257.98 247.60 10.28 o -3 11 1 186.83 186.99 5.33 o -2 11 1 53.90 55.57 3.08 o -1 11 1 109.19 118.02 3.56 o 0 11 1 281.19 269.71 6.59 o 1 11 1 267.02 273.56 5.37 o 2 11 1 113.33 112.15 4.09 o 3 11 1 169.55 165.65 4.95 o 4 11 1 57.88 55.94 3.20 o 5 11 1 90.69 101.83 4.29 o -4 12 1 26.66 32.08 2.95 o -3 12 1 10.02 11.72 2.19 o -2 12 1 62.69 59.49 4.79 o -1 12 1 50.61 48.77 3.10 o 0 12 1 0.34 1.19 1.32 o 1 12 1 13.39 10.94 2.00 o 2 12 1 0.08 -0.64 1.58 o 3 12 1 0.30 2.39 1.77 o 4 12 1 12.11 14.60 2.42 o -12 0 2 48.21 39.95 4.96 o -11 0 2 149.29 151.83 5.65 o -10 0 2 184.32 187.04 5.86 o -9 0 2 405.83 435.43 8.78 o -8 0 2 203.22 237.35 5.87 o -7 0 2 2182.20 2201.66 26.97 o -6 0 2 109.79 83.75 3.57 o -5 0 2 781.51 932.73 13.72 o -4 0 2 2605.23 2723.23 37.95 o -3 0 2 670.45 689.87 12.05 o -2 0 2 3551.09 3813.30 33.15 o -1 0 2 8083.86 7210.08 94.24 o 0 0 2 17483.82 14151.76 152.25 o 1 0 2 24754.42 19462.63 163.57 o 2 0 2 6146.64 6144.34 65.03 o 3 0 2 8772.74 8687.05 128.43 o 4 0 2 3230.19 3433.63 30.75 o 5 0 2 567.37 517.75 6.48 o 6 0 2 1462.71 1414.85 15.05 o 7 0 2 1453.92 1438.90 15.28 o 8 0 2 924.08 957.21 11.55 o 9 0 2 926.53 916.37 21.41 o 10 0 2 43.79 59.44 5.45 o 11 0 2 1.30 0.10 2.90 o -12 1 2 51.96 48.91 3.50 o -11 1 2 0.83 0.75 1.45 o -10 1 2 6.06 10.52 1.49 o -9 1 2 140.41 150.63 4.17 o -8 1 2 243.71 242.50 4.15 o -7 1 2 37.62 32.79 2.20 o -6 1 2 342.11 359.20 3.49 o -5 1 2 521.14 519.41 6.74 o -4 1 2 141.37 180.02 2.25 o -3 1 2 105.21 98.61 2.02 o -2 1 2 1858.25 1885.87 13.11 o -1 1 2 950.88 1076.80 7.74 o 0 1 2 498.56 647.85 5.48 o 1 1 2 3705.49 3649.57 22.07 o 2 1 2 980.19 954.12 5.96 o 3 1 2 706.52 685.27 5.57 o 4 1 2 106.04 113.74 1.67 o 5 1 2 52.75 47.99 2.85 o 6 1 2 1184.40 1175.09 8.92 o 7 1 2 651.59 641.24 5.89 o 8 1 2 14.06 11.22 1.29 o 9 1 2 49.02 43.79 5.42 o 10 1 2 56.41 65.75 5.90 o 11 1 2 59.57 62.12 6.21 o -12 2 2 114.25 116.86 4.53 o -11 2 2 364.85 369.69 9.13 o -10 2 2 452.90 435.12 7.76 o -9 2 2 719.36 682.75 9.76 o -8 2 2 176.94 173.48 3.06 o -7 2 2 5.76 5.59 0.82 o -6 2 2 1139.58 1142.45 9.47 o -5 2 2 4035.80 4099.39 30.06 o -4 2 2 4900.07 4895.13 38.99 o -3 2 2 2488.14 2422.14 21.44 o -2 2 2 7335.57 6940.81 51.79 o -1 2 2 4221.40 4505.97 29.82 o 0 2 2 1671.98 1755.06 11.00 o 1 2 2 55.93 52.11 0.93 o 2 2 2 699.36 730.41 5.31 o 3 2 2 2762.00 2817.05 16.31 o 4 2 2 1637.94 1548.88 11.65 o 5 2 2 2629.43 2640.12 17.42 o 6 2 2 1110.26 1105.03 8.56 o 7 2 2 3.23 5.43 1.20 o 8 2 2 20.09 17.07 1.47 o 9 2 2 164.29 155.34 6.84 o 10 2 2 115.07 127.58 7.90 o 11 2 2 128.47 130.03 8.46 o -11 3 2 12.42 18.14 2.28 o -10 3 2 34.25 35.26 3.22 o -9 3 2 94.13 103.47 3.54 o -8 3 2 266.64 272.53 4.56 o -7 3 2 40.28 34.70 2.32 o -6 3 2 732.26 725.50 6.77 o -5 3 2 223.00 209.65 2.81 o -4 3 2 119.19 94.37 1.66 o -3 3 2 871.51 916.83 6.50 o -2 3 2 15.48 26.80 0.71 o -1 3 2 1024.64 1024.06 7.04 o 0 3 2 326.92 400.58 2.99 o 1 3 2 2303.65 2473.62 15.72 o 2 3 2 1417.95 1454.10 9.81 o 3 3 2 32.21 23.67 0.83 o 4 3 2 479.72 533.09 4.16 o 5 3 2 176.21 182.91 2.21 o 6 3 2 452.21 432.72 3.98 o 7 3 2 139.99 157.33 3.42 o 8 3 2 118.38 109.64 3.60 o 9 3 2 2.07 1.32 1.31 o 10 3 2 37.39 36.24 5.17 o 11 3 2 46.20 52.90 6.39 o -11 4 2 5.09 4.37 1.68 o -10 4 2 86.27 100.10 3.84 o -9 4 2 131.60 142.88 3.53 o -8 4 2 501.02 496.80 6.70 o -7 4 2 569.98 569.08 7.01 o -6 4 2 4143.14 4011.47 32.03 o -5 4 2 2057.25 1996.36 17.09 o -4 4 2 1646.98 1674.39 11.34 o -3 4 2 304.73 300.70 4.98 o -2 4 2 5863.43 5898.14 56.77 o -1 4 2 3790.96 3970.82 28.00 o 0 4 2 2291.01 2244.88 13.20 o 1 4 2 785.81 724.64 7.07 o 2 4 2 585.45 546.92 4.52 o 3 4 2 246.25 240.40 2.66 o 4 4 2 8.66 8.48 0.68 o 5 4 2 5.18 8.68 1.07 o 6 4 2 131.14 140.15 3.25 o 7 4 2 513.30 523.32 7.26 o 8 4 2 1136.21 1098.01 18.98 o 9 4 2 350.37 341.63 6.84 o 10 4 2 235.53 239.11 7.42 o -11 5 2 0.16 0.38 1.66 o -10 5 2 81.13 76.46 3.57 o -9 5 2 59.35 58.24 2.51 o -8 5 2 190.81 190.28 4.05 o -7 5 2 49.12 43.69 2.64 o -6 5 2 94.14 93.36 2.60 o -5 5 2 72.40 73.29 2.23 o -4 5 2 96.95 89.29 2.25 o -3 5 2 7.33 13.85 0.84 o -2 5 2 1004.17 1059.60 17.78 o -1 5 2 307.98 297.84 5.09 o 0 5 2 0.87 0.42 0.44 o 1 5 2 0.32 0.47 0.40 o 2 5 2 317.26 364.03 3.49 o 3 5 2 118.31 125.91 3.31 o 4 5 2 15.40 17.50 1.28 o 5 5 2 0.16 0.06 0.67 o 6 5 2 87.24 89.98 2.63 o 7 5 2 3.66 4.82 1.36 o 8 5 2 2.64 2.62 1.40 o 9 5 2 4.87 1.90 1.43 o 10 5 2 0.42 2.03 2.09 o -10 6 2 226.69 226.47 5.93 o -9 6 2 282.71 287.78 5.44 o -8 6 2 169.35 171.15 4.01 o -7 6 2 83.23 78.71 2.66 o -6 6 2 543.76 519.47 6.82 o -5 6 2 1262.38 1254.95 12.28 o -4 6 2 219.97 208.94 3.72 o -3 6 2 606.67 575.37 9.19 o -2 6 2 2625.29 2617.00 19.12 o -1 6 2 1604.56 1608.25 12.47 o 0 6 2 732.76 723.78 5.30 o 1 6 2 641.62 649.61 6.19 o 2 6 2 1569.54 1630.37 12.85 o 3 6 2 364.31 372.90 4.46 o 4 6 2 595.14 596.13 6.23 o 5 6 2 447.04 454.71 6.16 o 6 6 2 177.71 184.18 3.84 o 7 6 2 246.11 246.89 5.57 o 8 6 2 284.20 283.18 6.31 o 9 6 2 120.53 125.28 4.42 o -10 7 2 4.14 4.11 1.55 o -9 7 2 2.53 5.43 1.48 o -8 7 2 20.80 16.77 1.75 o -7 7 2 86.16 84.15 2.89 o -6 7 2 157.14 153.15 3.61 o -5 7 2 125.64 126.46 3.15 o -4 7 2 201.28 205.69 3.87 o -3 7 2 13.96 15.98 1.28 o -2 7 2 128.16 138.93 3.93 o -1 7 2 442.31 455.39 5.00 o 0 7 2 85.10 91.29 2.44 o 1 7 2 72.60 80.65 2.00 o 2 7 2 232.69 254.94 3.90 o 3 7 2 50.65 53.55 1.77 o 4 7 2 1.76 1.65 0.82 o 5 7 2 7.13 7.40 1.23 o 6 7 2 5.75 3.97 1.43 o 7 7 2 31.27 33.01 2.48 o 8 7 2 11.70 12.75 2.46 o 9 7 2 0.74 0.19 1.49 o -9 8 2 295.39 290.49 5.91 o -8 8 2 146.93 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