#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:32:10 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181063 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/43/2214369.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214369_Fobs loop_ _publ_author_name 'Hong, Zhe' _publ_section_title ; Bis[N-ethyl-N'-(pyridin-2-ylmethylene)ethane-1,2-diamine]nickel(II) bis(perchlorate) ; _journal_coeditor_code OM2138 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2026 _journal_volume 63 _journal_year 2007 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yc' _symmetry_space_group_name_H-M 'P 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.531 _cell_angle_gamma 90.000 _cell_length_a 21.1172 _cell_length_b 16.8787 _cell_length_c 12.0819 _exptl_crystal_F_000 1908.00 _reflns_d_resolution_high 0.7706 _cod_data_source_file om2138Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in P2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 345.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 84179.83 79608.01 1288.40 o 4 0 0 18507.39 24211.01 218.60 o 5 0 0 35003.92 40413.54 371.91 o 6 0 0 30620.84 36094.07 324.81 o 7 0 0 503.34 384.73 33.82 o 8 0 0 8956.47 8134.27 98.76 o 9 0 0 17978.19 17329.47 181.07 o 10 0 0 28854.05 28147.58 275.77 o 12 0 0 287.23 409.89 44.12 o 13 0 0 5809.90 5462.28 162.06 o 14 0 0 84.88 85.64 31.79 o 15 0 0 1205.55 1278.47 82.52 o 16 0 0 2184.51 2079.71 105.75 o 17 0 0 292.11 232.91 48.66 o 18 0 0 5.20 -10.12 29.45 o 19 0 0 1345.43 1544.21 102.51 o 20 0 0 1186.39 1131.20 97.06 o 21 0 0 2.44 -25.56 37.24 o 22 0 0 680.41 732.98 87.20 o 23 0 0 107.59 64.10 49.44 o 24 0 0 71.73 58.13 53.33 o 25 0 0 106.56 60.85 56.57 o 26 0 0 65.77 -10.25 46.71 o 3 1 0 28503.38 26782.43 183.39 o 5 1 0 7139.62 8376.28 70.36 o 6 1 0 304.47 239.19 10.31 o 7 1 0 21504.94 19751.53 150.26 o 9 1 0 4778.48 4768.64 55.56 o 11 1 0 2225.17 2448.92 46.42 o 12 1 0 415.93 317.00 23.08 o 13 1 0 980.62 818.99 35.00 o 14 1 0 456.29 402.39 35.50 o 15 1 0 1.00 3.60 18.57 o 16 1 0 164.17 169.22 32.05 o 17 1 0 2023.66 1973.21 75.79 o 18 1 0 257.61 265.45 38.12 o 19 1 0 143.47 83.22 30.93 o 20 1 0 45.72 53.60 29.98 o 21 1 0 64.26 34.07 29.60 o 22 1 0 2.93 26.67 32.44 o 23 1 0 234.71 300.77 47.80 o 24 1 0 5.16 -14.05 64.49 o 25 1 0 0.00 -2.58 34.69 o 26 1 0 7.45 -28.67 35.99 o 0 2 0 40376.11 34686.78 519.93 o 3 2 0 37275.62 42669.32 321.19 o 4 2 0 3652.16 2819.62 30.23 o 5 2 0 1465.19 1500.71 22.24 o 6 2 0 2465.63 2659.00 33.37 o 7 2 0 10744.41 11450.34 96.59 o 8 2 0 9884.97 10662.90 94.04 o 9 2 0 258.12 217.11 13.25 o 10 2 0 8440.50 8302.55 95.74 o 11 2 0 829.11 1151.63 38.59 o 12 2 0 51.37 32.82 13.45 o 13 2 0 1113.44 1198.80 52.39 o 14 2 0 884.41 973.99 40.64 o 15 2 0 381.18 410.20 33.29 o 16 2 0 175.45 176.92 38.41 o 17 2 0 357.95 363.75 40.86 o 18 2 0 294.21 305.44 44.64 o 19 2 0 1629.59 1750.49 77.29 o 20 2 0 53.33 44.40 33.67 o 21 2 0 276.23 232.96 45.54 o 22 2 0 599.62 586.19 65.72 o 23 2 0 9.19 47.76 49.05 o 24 2 0 1.35 -10.50 35.75 o 25 2 0 257.49 260.61 52.36 o 26 2 0 12.51 -7.50 35.43 o 2 3 0 33382.46 34553.09 263.28 o 3 3 0 6791.46 7744.02 72.80 o 4 3 0 18169.17 18274.47 152.01 o 5 3 0 1337.29 1027.86 36.92 o 6 3 0 926.09 850.38 17.74 o 7 3 0 561.50 468.04 14.77 o 8 3 0 16195.99 15687.38 146.56 o 10 3 0 104.85 112.67 14.39 o 11 3 0 3673.11 2752.26 60.01 o 12 3 0 1256.98 1207.00 41.32 o 13 3 0 23.66 14.86 13.73 o 14 3 0 4240.56 4097.33 142.01 o 15 3 0 785.84 798.99 39.38 o 16 3 0 0.11 -14.47 14.47 o 17 3 0 2248.93 2359.16 68.57 o 18 3 0 370.55 325.80 65.79 o 19 3 0 26.96 -13.98 23.57 o 20 3 0 59.34 41.48 28.75 o 21 3 0 601.50 640.84 57.16 o 22 3 0 34.63 3.52 55.15 o 23 3 0 1.05 16.00 30.74 o 24 3 0 135.87 155.23 42.97 o 25 3 0 27.52 56.82 38.61 o 26 3 0 30.79 78.76 42.10 o 0 4 0 27456.90 28851.13 315.38 o 1 4 0 19632.94 19364.65 155.37 o 2 4 0 1728.70 2085.52 29.54 o 3 4 0 5339.22 6301.24 64.69 o 4 4 0 6447.31 6209.44 66.05 o 6 4 0 2000.23 1976.43 50.19 o 7 4 0 1000.28 1302.98 30.10 o 8 4 0 4050.31 4320.15 60.79 o 9 4 0 4134.76 3820.88 58.45 o 10 4 0 354.67 385.53 23.60 o 11 4 0 5778.28 4423.02 79.16 o 12 4 0 3.32 0.45 11.37 o 13 4 0 919.65 986.19 39.88 o 14 4 0 1059.30 921.16 40.84 o 15 4 0 36.78 15.73 16.08 o 17 4 0 29.45 -10.19 18.13 o 18 4 0 1.21 -17.20 17.20 o 19 4 0 656.20 681.38 54.72 o 20 4 0 197.27 222.92 78.05 o 21 4 0 16.53 25.30 31.51 o 22 4 0 335.83 374.99 52.20 o 23 4 0 0.78 38.23 48.92 o 24 4 0 11.00 47.23 35.31 o 25 4 0 14.72 -32.78 32.78 o 1 5 0 3663.84 3712.94 43.11 o 3 5 0 9027.29 7842.05 122.86 o 4 5 0 1566.13 1648.42 30.11 o 5 5 0 9729.24 11337.43 109.49 o 6 5 0 204.31 358.73 16.54 o 8 5 0 3304.73 2954.79 49.64 o 9 5 0 2.24 -5.03 9.21 o 10 5 0 127.37 141.25 26.84 o 11 5 0 2098.84 2402.16 57.94 o 12 5 0 12.89 14.91 13.10 o 13 5 0 2072.77 1924.52 55.30 o 14 5 0 1687.86 1586.24 65.64 o 15 5 0 1204.24 1308.88 50.16 o 16 5 0 56.57 21.84 18.14 o 17 5 0 52.35 42.36 21.32 o 18 5 0 411.95 411.13 36.82 o 19 5 0 197.62 224.44 31.77 o 20 5 0 502.49 510.52 52.14 o 21 5 0 502.28 515.11 54.04 o 22 5 0 117.83 82.98 35.65 o 23 5 0 45.73 22.57 33.99 o 24 5 0 283.95 345.04 53.07 o 25 5 0 5.12 80.89 42.61 o 0 6 0 14579.91 18372.57 239.72 o 1 6 0 1953.81 1865.07 29.89 o 3 6 0 1.89 41.27 12.51 o 4 6 0 2361.18 2159.62 54.60 o 5 6 0 1316.30 1925.15 41.21 o 6 6 0 404.68 372.77 21.71 o 7 6 0 5080.56 5352.96 88.03 o 8 6 0 5914.85 5599.83 85.79 o 9 6 0 422.58 378.86 24.01 o 10 6 0 36.21 47.98 13.76 o 11 6 0 3219.20 3075.70 66.75 o 12 6 0 368.66 398.58 28.53 o 13 6 0 44.71 37.53 16.50 o 14 6 0 95.04 45.72 30.11 o 15 6 0 221.26 183.05 25.90 o 16 6 0 311.34 405.71 43.65 o 17 6 0 1672.42 1553.65 58.68 o 18 6 0 18.04 50.55 26.53 o 19 6 0 9.84 2.73 22.31 o 20 6 0 30.07 45.75 25.39 o 21 6 0 68.32 62.69 31.93 o 22 6 0 2.87 10.05 31.15 o 23 6 0 137.31 203.77 43.82 o 24 6 0 34.60 -7.58 66.95 o 25 6 0 25.30 27.46 43.66 o 0 7 0 16112.62 14659.68 186.72 o 1 7 0 731.32 923.09 22.10 o 2 7 0 12610.57 13642.89 124.52 o 3 7 0 63.65 85.96 11.47 o 4 7 0 120.61 65.16 11.71 o 5 7 0 1485.87 1588.24 39.02 o 7 7 0 1896.84 2058.79 47.88 o 8 7 0 34.05 40.47 19.91 o 9 7 0 1305.33 1325.27 59.95 o 10 7 0 56.64 33.88 14.46 o 11 7 0 8465.63 8195.26 122.10 o 12 7 0 140.67 105.83 19.33 o 13 7 0 0.73 15.61 15.83 o 14 7 0 671.88 795.92 46.39 o 15 7 0 70.62 69.03 21.59 o 16 7 0 197.70 134.19 26.61 o 17 7 0 2945.08 3216.25 98.02 o 18 7 0 54.21 11.72 30.39 o 19 7 0 35.57 37.81 23.36 o 20 7 0 303.13 298.12 36.44 o 21 7 0 141.05 157.60 46.84 o 22 7 0 130.94 112.39 38.35 o 23 7 0 144.56 111.49 40.47 o 24 7 0 4.87 74.45 40.04 o 25 7 0 62.69 92.39 42.43 o 0 8 0 2679.80 3300.27 66.63 o 2 8 0 863.44 683.29 21.14 o 3 8 0 1334.03 1485.06 41.75 o 4 8 0 2150.80 2431.83 82.32 o 5 8 0 1868.14 2152.30 51.30 o 6 8 0 1762.34 1961.71 47.02 o 7 8 0 48.80 14.46 11.11 o 8 8 0 220.98 267.11 31.09 o 9 8 0 109.18 76.83 15.95 o 10 8 0 2109.45 2097.55 55.34 o 11 8 0 171.58 112.11 19.39 o 12 8 0 4.39 -15.42 15.90 o 13 8 0 755.86 976.14 74.81 o 14 8 0 3404.31 3323.69 80.32 o 15 8 0 567.72 497.78 57.29 o 16 8 0 561.49 454.70 44.42 o 17 8 0 321.27 253.02 33.40 o 18 8 0 105.25 141.55 29.51 o 19 8 0 16.76 33.59 23.53 o 20 8 0 751.32 788.68 51.13 o 21 8 0 1.61 -12.29 27.70 o 22 8 0 77.17 71.33 27.89 o 23 8 0 93.88 65.54 36.79 o 24 8 0 2.29 18.93 35.96 o 0 9 0 4487.93 4592.59 85.72 o 1 9 0 1206.93 1068.20 35.79 o 2 9 0 7300.40 6616.06 88.83 o 3 9 0 7812.29 8252.74 91.07 o 5 9 0 2567.53 2228.83 61.02 o 6 9 0 3656.09 3726.05 83.27 o 7 9 0 2012.14 2292.34 58.21 o 8 9 0 11175.90 10841.69 220.49 o 9 9 0 1677.14 1857.11 65.16 o 10 9 0 385.17 419.95 29.04 o 11 9 0 4187.14 3868.75 81.21 o 12 9 0 2155.19 2199.77 62.47 o 13 9 0 1160.79 1225.35 49.76 o 14 9 0 3086.49 3014.75 77.57 o 15 9 0 127.03 117.15 32.23 o 16 9 0 337.99 260.87 32.28 o 17 9 0 970.77 1159.51 63.73 o 18 9 0 12.91 49.07 24.26 o 19 9 0 491.01 565.02 45.60 o 20 9 0 137.48 218.10 42.08 o 21 9 0 3.99 -23.08 23.08 o 22 9 0 3.39 8.49 27.23 o 23 9 0 36.33 65.97 39.13 o 24 9 0 5.06 -6.48 33.64 o 0 10 0 5550.00 5413.75 99.14 o 1 10 0 3458.82 3819.53 64.61 o 2 10 0 1746.63 2135.42 44.20 o 3 10 0 250.08 272.32 16.98 o 4 10 0 1153.05 1197.59 35.70 o 5 10 0 4611.92 4628.95 80.36 o 6 10 0 594.44 476.32 27.66 o 7 10 0 2.41 -10.49 11.73 o 8 10 0 19.59 7.68 14.06 o 9 10 0 2261.40 2344.52 92.79 o 10 10 0 798.64 859.70 39.63 o 11 10 0 1368.51 1267.15 48.94 o 12 10 0 6.48 2.98 17.11 o 13 10 0 255.41 213.12 48.70 o 14 10 0 168.11 190.82 27.79 o 15 10 0 3976.53 4083.05 95.52 o 16 10 0 428.33 476.37 40.05 o 17 10 0 82.12 49.36 25.29 o 18 10 0 349.98 317.18 37.71 o 19 10 0 475.76 410.72 42.25 o 20 10 0 0.57 -22.14 22.14 o 21 10 0 230.36 161.35 34.33 o 22 10 0 4.15 7.65 26.91 o 23 10 0 1.93 -25.76 25.76 o 0 11 0 106.11 99.00 18.27 o 1 11 0 4.13 14.87 9.31 o 2 11 0 26.58 44.75 21.65 o 3 11 0 7493.05 8111.75 96.16 o 4 11 0 1205.56 1266.01 33.82 o 5 11 0 2227.08 2137.15 43.40 o 6 11 0 3215.18 3466.10 72.34 o 7 11 0 174.02 124.11 19.88 o 8 11 0 427.23 318.63 36.66 o 9 11 0 175.40 162.72 24.50 o 10 11 0 15.06 16.90 21.37 o 11 11 0 177.85 139.41 23.87 o 12 11 0 831.82 942.46 44.97 o 13 11 0 926.13 807.42 44.21 o 14 11 0 106.43 63.63 23.49 o 15 11 0 68.38 103.57 25.95 o 16 11 0 576.13 668.84 67.02 o 17 11 0 17.36 -24.65 24.65 o 18 11 0 394.66 324.68 38.82 o 19 11 0 88.18 48.82 35.52 o 20 11 0 37.08 27.03 27.63 o 21 11 0 0.65 13.43 28.09 o 22 11 0 290.20 308.54 42.95 o 0 12 0 1237.36 1237.88 48.60 o 1 12 0 122.03 106.49 19.83 o 2 12 0 540.31 633.23 31.01 o 3 12 0 1660.06 1682.34 50.59 o 4 12 0 320.77 336.70 28.62 o 5 12 0 1.13 -1.41 13.04 o 6 12 0 1392.93 1565.50 50.41 o 8 12 0 101.75 110.99 25.89 o 9 12 0 80.60 75.94 20.26 o 10 12 0 24.66 20.15 20.79 o 11 12 0 157.41 163.38 25.42 o 12 12 0 628.64 604.33 39.88 o 13 12 0 4.34 7.14 18.88 o 14 12 0 5.70 4.14 20.24 o 15 12 0 227.15 194.39 31.36 o 16 12 0 179.72 203.47 32.43 o 17 12 0 1.71 30.15 24.70 o 18 12 0 265.48 216.35 33.61 o 19 12 0 47.14 41.02 27.70 o 20 12 0 34.68 57.53 29.40 o 21 12 0 30.93 35.07 30.24 o 22 12 0 148.86 113.04 50.47 o 0 13 0 4838.21 5485.14 112.31 o 1 13 0 838.55 919.05 36.59 o 2 13 0 67.68 87.95 14.87 o 3 13 0 2209.40 2203.35 64.10 o 4 13 0 248.77 320.72 26.91 o 5 13 0 908.89 788.50 38.46 o 6 13 0 2027.82 2125.01 70.40 o 7 13 0 188.41 245.92 33.74 o 8 13 0 9.36 7.39 16.70 o 9 13 0 194.86 210.75 27.54 o 10 13 0 631.04 641.93 39.81 o 11 13 0 100.58 139.69 25.85 o 12 13 0 252.57 216.82 29.99 o 13 13 0 856.57 852.99 48.00 o 14 13 0 109.35 108.42 26.45 o 15 13 0 182.31 176.05 30.91 o 16 13 0 367.10 396.65 40.30 o 17 13 0 4.81 -4.41 23.01 o 18 13 0 57.82 70.67 33.14 o 19 13 0 138.25 113.78 39.11 o 20 13 0 4.68 1.18 27.47 o 21 13 0 97.17 96.31 37.53 o 0 14 0 102.95 137.46 25.61 o 1 14 0 573.22 608.82 37.95 o 2 14 0 490.87 614.15 65.42 o 3 14 0 151.79 148.86 22.06 o 4 14 0 15.16 29.05 17.41 o 5 14 0 873.60 965.04 50.88 o 6 14 0 11.53 5.97 17.89 o 7 14 0 9.41 4.96 17.87 o 8 14 0 220.29 217.65 30.36 o 9 14 0 287.45 293.91 41.47 o 10 14 0 6.97 0.34 22.55 o 11 14 0 1155.60 1034.21 66.96 o 12 14 0 95.14 75.49 25.02 o 13 14 0 10.85 17.68 20.91 o 14 14 0 421.54 559.41 44.44 o 15 14 0 153.61 148.19 63.71 o 16 14 0 63.48 50.54 25.96 o 17 14 0 48.54 82.09 29.09 o 18 14 0 9.10 3.87 27.46 o 19 14 0 70.65 84.21 32.91 o 20 14 0 86.94 101.10 35.19 o 0 15 0 4481.69 4419.96 161.41 o 1 15 0 0.40 0.02 16.64 o 2 15 0 1203.10 1412.38 50.70 o 3 15 0 1240.03 1438.80 51.91 o 4 15 0 0.46 -15.84 15.84 o 5 15 0 107.35 105.25 22.71 o 6 15 0 713.69 645.88 39.25 o 7 15 0 106.21 54.90 20.92 o 8 15 0 499.21 441.00 42.82 o 9 15 0 492.62 521.05 65.07 o 10 15 0 618.98 667.07 44.02 o 11 15 0 0.09 -18.15 18.15 o 12 15 0 28.55 33.34 21.57 o 13 15 0 42.46 35.92 23.27 o 14 15 0 26.74 1.30 22.11 o 15 15 0 220.44 177.06 53.38 o 16 15 0 104.00 127.16 37.77 o 17 15 0 0.86 11.18 26.05 o 18 15 0 7.27 2.13 27.92 o 19 15 0 128.78 130.18 34.99 o 1 16 0 317.96 359.02 111.26 o 2 16 0 1758.46 1875.72 77.66 o 3 16 0 8.94 -16.92 16.92 o 4 16 0 854.09 816.33 43.75 o 5 16 0 106.56 90.75 23.16 o 6 16 0 41.49 14.34 19.71 o 7 16 0 100.19 107.44 24.59 o 8 16 0 1743.94 1792.06 75.85 o 9 16 0 186.78 145.67 28.13 o 10 16 0 55.93 82.00 34.25 o 11 16 0 583.28 503.89 41.79 o 12 16 0 24.23 20.26 26.95 o 13 16 0 14.80 5.88 22.69 o 14 16 0 703.91 734.92 51.41 o 15 16 0 25.37 16.89 27.10 o 16 16 0 2.92 16.86 27.90 o 17 16 0 334.92 310.47 42.88 o 18 16 0 32.65 65.19 39.67 o 0 17 0 125.90 162.32 50.99 o 1 17 0 254.96 327.07 43.53 o 2 17 0 28.34 64.82 29.31 o 3 17 0 3.39 -3.76 48.46 o 4 17 0 88.40 134.53 49.31 o 5 17 0 99.97 99.80 26.27 o 6 17 0 75.78 59.55 24.16 o 7 17 0 0.18 10.20 21.10 o 8 17 0 31.22 56.02 23.89 o 9 17 0 0.95 11.01 22.00 o 10 17 0 13.87 11.91 23.24 o 11 17 0 17.73 5.99 23.94 o 13 17 0 14.54 -7.27 23.57 o 14 17 0 2.75 -23.80 23.83 o 15 17 0 0.43 7.83 26.76 o 16 17 0 0.38 -16.54 27.66 o 0 18 0 1162.98 1376.57 105.75 o 1 18 0 955.47 992.97 65.91 o 2 18 0 657.76 640.06 72.27 o 3 18 0 477.75 554.42 54.22 o 4 18 0 260.61 270.36 61.24 o 5 18 0 1089.77 1275.24 72.89 o 6 18 0 469.76 411.37 49.65 o 7 18 0 172.55 161.72 30.66 o 8 18 0 596.36 642.91 84.11 o 9 18 0 88.15 42.46 34.96 o 10 18 0 19.32 28.90 25.83 o 11 18 0 669.97 718.58 52.10 o 12 18 0 92.92 84.54 30.92 o 13 18 0 3.09 11.69 51.01 o 14 18 0 125.49 80.24 38.16 o 15 18 0 42.14 -8.61 31.73 o 0 19 0 151.28 276.12 64.36 o 1 19 0 71.43 71.11 34.77 o 2 19 0 22.88 27.87 30.41 o 3 19 0 9.74 28.07 72.40 o 4 19 0 11.12 -10.33 30.11 o 5 19 0 2.16 4.37 29.48 o 6 19 0 112.92 97.07 37.56 o 7 19 0 46.05 -12.91 30.81 o 8 19 0 0.06 9.90 31.09 o 9 19 0 25.47 51.88 28.16 o 10 19 0 9.92 -2.07 25.45 o 11 19 0 36.29 31.75 28.05 o 12 19 0 6.19 6.12 34.62 o 13 19 0 30.68 -15.52 27.56 o 0 20 0 49.51 48.40 47.88 o 1 20 0 170.42 223.39 44.54 o 2 20 0 224.71 282.74 137.47 o 3 20 0 172.86 234.96 45.78 o 4 20 0 182.85 292.42 50.15 o 5 20 0 312.66 431.80 54.06 o 6 20 0 15.36 -22.73 31.34 o 7 20 0 8.15 79.81 45.48 o 8 20 0 161.94 143.48 49.76 o 9 20 0 9.62 -7.00 34.49 o 10 20 0 8.37 23.37 35.92 o 0 21 0 24.89 -4.15 46.32 o 1 21 0 4.52 10.71 35.28 o 2 21 0 12.62 -30.49 30.49 o 3 21 0 149.18 177.71 58.07 o 4 21 0 4.73 58.90 37.94 o 5 21 0 18.86 -16.90 58.13 o 6 21 0 4.48 -38.80 38.80 o 7 21 0 75.14 93.05 75.91 o -26 1 1 1.05 33.97 37.29 o -25 1 1 5.77 8.24 33.71 o -24 1 1 527.03 568.46 199.69 o -23 1 1 2.01 -23.93 30.81 o -22 1 1 2.77 39.90 30.26 o -21 1 1 1900.04 2105.98 88.86 o -20 1 1 6.88 25.75 26.19 o -19 1 1 105.56 100.93 31.00 o -18 1 1 291.55 230.58 35.46 o -17 1 1 444.47 473.03 42.95 o -16 1 1 167.62 247.43 33.17 o -15 1 1 877.78 864.12 48.86 o -14 1 1 225.16 205.75 28.62 o -13 1 1 4923.24 4752.56 105.83 o -11 1 1 6018.33 6275.08 116.29 o -10 1 1 2723.24 2783.24 68.63 o -9 1 1 948.40 1234.36 59.82 o -8 1 1 1206.33 792.64 73.57 o 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