#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:32:10 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181063 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/43/2214391.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214391_Fobs loop_ _publ_author_name 'Huang, Hai-Ping' 'Liu, Li-Xia' _publ_section_title ; Bis(\m-4-benzyl-3,5-diphenylpyrazolato-\k^2^N:N')bis[(4,4'-dimethyl-2,2'-bipyridine-\k^2^N,N')palladium(II)] bis(hexafluorophosphate) diethyl ether monosolvate monohydrate ; _journal_coeditor_code SI2018 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1875 _journal_page_last m1876 _journal_volume 63 _journal_year 2007 _space_group_IT_number 152 _symmetry_space_group_name_Hall 'P 31 2"' _symmetry_space_group_name_H-M 'P 31 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 22.1138 _cell_length_b 22.1138 _cell_length_c 12.8884 _exptl_crystal_F_000 2412.00 _reflns_d_resolution_high 0.7499 _cod_data_source_file si2018Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hhp20 in P3(1)21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 327.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z+1/3' '-x+y, -x, z+2/3' 'y, x, -z' 'x-y, -y, -z+2/3' '-x, -x+y, -z+1/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 27685.32 -1.00 1.00 o 1 1 0 38028.14 50404.36 1182.02 o -1 2 0 38654.83 48966.61 1204.12 o 0 2 0 95510.62 80190.30 4377.27 o 1 2 0 7036.36 8011.49 95.88 o 2 2 0 20484.51 20850.54 384.20 o -1 3 0 7043.51 7825.67 95.72 o 0 3 0 22842.49 25947.79 421.53 o 1 3 0 7030.90 7045.39 88.48 o 2 3 0 31784.83 32729.68 325.40 o 3 3 0 53475.24 62985.78 886.44 o -2 4 0 20572.17 21070.85 345.17 o -1 4 0 7309.81 7287.17 88.75 o 0 4 0 42129.50 51463.64 574.23 o 1 4 0 67912.37 75130.62 757.51 o 2 4 0 18973.16 17451.82 131.30 o 3 4 0 20200.27 22556.95 138.70 o 4 4 0 73108.66 68185.16 586.23 o -2 5 0 30522.44 31577.30 294.89 o -1 5 0 67964.46 76367.09 832.23 o 0 5 0 3852.23 4844.22 58.50 o 1 5 0 14807.61 16707.88 107.37 o 2 5 0 28103.18 27683.27 156.37 o 3 5 0 3226.42 3069.70 24.22 o 4 5 0 3312.79 3851.05 29.41 o 5 5 0 18635.92 17630.46 151.48 o -3 6 0 52456.28 61934.79 800.69 o -2 6 0 19263.12 17805.58 140.07 o -1 6 0 15023.88 17259.35 122.42 o 0 6 0 2904.32 3356.43 28.79 o 1 6 0 3539.42 3296.61 25.81 o 2 6 0 6640.88 5869.62 40.79 o 3 6 0 13924.29 15220.83 92.45 o 4 6 0 19220.72 20502.45 134.64 o 5 6 0 6563.69 7335.12 50.93 o 6 6 0 17394.46 16621.51 146.62 o -3 7 0 21245.12 23675.67 144.05 o -2 7 0 27151.37 26707.20 192.44 o -1 7 0 3211.31 2970.52 28.71 o 0 7 0 1387.10 1249.25 17.24 o 1 7 0 963.18 1197.76 16.06 o 2 7 0 1441.85 1419.48 15.90 o 3 7 0 1117.32 1635.89 18.27 o 4 7 0 7674.26 6604.67 46.38 o 5 7 0 4853.54 3460.67 29.67 o 6 7 0 5347.74 5946.15 44.64 o 7 7 0 2568.48 2737.76 38.58 o -4 8 0 72976.13 68078.45 577.96 o -3 8 0 2894.33 2829.06 32.56 o -2 8 0 6903.92 6185.47 48.53 o -1 8 0 865.87 1097.20 15.80 o 0 8 0 167.09 -4.26 4.62 o 1 8 0 289.87 86.18 6.63 o 2 8 0 370.16 324.95 8.69 o 3 8 0 11276.45 12207.57 78.53 o 4 8 0 4184.22 4335.93 34.20 o 5 8 0 15928.33 15044.95 95.30 o 6 8 0 6295.31 7126.46 52.79 o 7 8 0 2031.17 2162.74 27.10 o 8 8 0 21103.70 22209.84 207.22 o -4 9 0 3156.99 3667.17 31.95 o -3 9 0 14018.67 15299.74 103.83 o -2 9 0 1491.26 1447.04 19.36 o -1 9 0 272.00 63.06 6.40 o 0 9 0 527.11 1222.20 16.91 o 1 9 0 2008.79 2386.68 26.73 o 2 9 0 2218.19 2310.80 25.36 o 3 9 0 3111.94 2208.00 21.98 o 4 9 0 41.16 99.69 7.47 o 5 9 0 3565.66 3614.32 31.64 o 6 9 0 1769.91 1683.74 22.82 o 7 9 0 3324.07 3422.03 39.77 o 8 9 0 940.22 813.12 21.98 o 9 9 0 6649.96 6738.46 92.29 o -5 10 0 18928.85 18148.06 200.37 o -4 10 0 19937.22 21095.90 138.74 o -3 10 0 1349.21 1960.00 23.34 o -2 10 0 286.23 255.96 9.51 o -1 10 0 2103.46 2535.53 27.17 o 0 10 0 5334.00 3860.22 35.02 o 1 10 0 7721.91 7251.13 58.61 o 2 10 0 2848.55 2967.69 27.51 o 3 10 0 2592.88 1987.45 21.64 o 4 10 0 5294.27 5219.01 42.16 o 5 10 0 3100.71 3537.83 34.57 o 6 10 0 12197.00 11847.87 87.93 o 7 10 0 4774.33 4844.25 46.36 o 8 10 0 14967.59 15888.99 118.40 o 9 10 0 5661.92 5592.22 55.94 o 10 10 0 6766.31 6482.10 90.77 o -5 11 0 6595.92 7406.66 59.87 o -4 11 0 7352.83 6314.44 54.13 o -3 11 0 11680.65 12530.49 96.73 o -2 11 0 2104.69 2148.60 27.10 o -1 11 0 7589.44 7143.45 60.69 o 0 11 0 652.48 727.77 16.01 o 1 11 0 5811.16 5761.23 50.31 o 2 11 0 693.00 713.25 15.06 o 3 11 0 329.44 352.75 11.42 o 4 11 0 786.18 645.59 16.28 o 5 11 0 588.23 491.04 18.17 o 6 11 0 1294.80 1359.35 24.04 o 7 11 0 1654.20 1465.42 31.43 o 8 11 0 609.90 577.20 19.39 o 9 11 0 5253.18 5406.16 58.02 o 10 11 0 1251.44 1300.77 27.87 o 11 11 0 8.87 -9.28 16.15 o -6 12 0 17622.78 17144.03 193.99 o -5 12 0 4617.18 3201.89 34.57 o -4 12 0 4381.79 4519.38 46.84 o -3 12 0 2934.70 2065.72 27.12 o -2 12 0 2655.76 2664.99 32.10 o -1 12 0 5848.94 5806.57 53.00 o 0 12 0 15243.64 14312.18 102.76 o 1 12 0 3836.95 3960.05 41.82 o 2 12 0 9093.10 8365.32 64.95 o 3 12 0 2203.85 2367.88 31.00 o 4 12 0 3196.11 3542.06 37.79 o 5 12 0 2706.18 2509.78 31.95 o 6 12 0 1610.88 1625.90 26.83 o 7 12 0 939.30 1161.74 25.62 o 8 12 0 1814.83 1869.90 31.94 o 9 12 0 520.11 495.99 25.14 o 10 12 0 645.76 721.43 23.92 o 11 12 0 483.05 486.89 23.55 o 12 12 0 1674.16 1752.34 54.52 o -6 13 0 5077.50 5690.89 52.18 o -5 13 0 16086.24 15040.89 111.51 o -4 13 0 81.80 117.30 10.08 o -3 13 0 2560.57 1940.53 28.75 o -2 13 0 571.72 593.55 16.85 o -1 13 0 3660.86 3816.52 39.08 o 0 13 0 460.75 599.18 19.48 o 1 13 0 459.18 560.19 17.60 o 2 13 0 2601.09 2793.87 33.92 o 3 13 0 1405.84 1228.19 24.96 o 4 13 0 1342.83 1562.04 29.84 o 5 13 0 4558.77 4428.04 47.45 o 6 13 0 2488.86 2410.82 37.54 o 7 13 0 715.12 646.44 31.07 o 8 13 0 454.95 426.59 19.74 o 9 13 0 688.42 828.51 26.31 o 10 13 0 723.77 759.68 25.26 o 11 13 0 307.19 312.32 21.36 o 12 13 0 157.16 165.06 19.30 o 13 13 0 194.15 217.74 29.45 o -7 14 0 2274.01 2492.44 44.95 o -6 14 0 6404.80 7288.69 62.54 o -5 14 0 3528.11 3547.85 40.75 o -4 14 0 5269.42 5169.49 50.43 o -3 14 0 418.41 444.35 20.73 o -2 14 0 9018.09 8283.19 67.80 o -1 14 0 518.36 622.98 17.16 o 0 14 0 19301.71 18541.53 138.79 o 1 14 0 2126.01 1973.90 29.28 o 2 14 0 2620.08 2604.65 34.20 o 3 14 0 2835.06 3138.85 39.09 o 4 14 0 2720.20 2446.90 35.57 o 5 14 0 78.10 21.44 12.03 o 6 14 0 3203.96 3236.02 45.04 o 7 14 0 522.46 514.45 21.74 o 8 14 0 44.27 -13.49 13.49 o 9 14 0 1186.43 1288.12 41.19 o 10 14 0 1158.59 1199.63 31.61 o 11 14 0 361.07 396.37 24.38 o 12 14 0 1342.29 1495.44 37.91 o 13 14 0 158.00 171.48 20.20 o 14 14 0 715.32 778.55 59.13 o -7 15 0 2031.55 2140.36 29.55 o -6 15 0 1621.91 1496.74 26.64 o -5 15 0 2997.43 3494.41 41.73 o -4 15 0 710.85 568.38 16.14 o -3 15 0 2172.37 2312.08 30.41 o -2 15 0 2434.65 2562.06 33.10 o -1 15 0 2180.86 2001.82 29.10 o 0 15 0 1757.93 1792.47 29.77 o 1 15 0 2676.92 2830.01 35.99 o 2 15 0 309.20 292.80 15.85 o 3 15 0 341.94 270.49 15.31 o 4 15 0 877.45 875.85 23.11 o 5 15 0 245.59 306.17 17.19 o 6 15 0 354.60 426.00 20.76 o 7 15 0 331.43 338.21 19.85 o 8 15 0 728.96 752.63 26.52 o 9 15 0 68.83 47.00 16.14 o 10 15 0 234.13 217.49 19.68 o 11 15 0 129.44 104.79 18.65 o 12 15 0 443.23 430.19 25.15 o 13 15 0 305.04 285.67 27.62 o 14 15 0 91.31 52.39 22.75 o -8 16 0 20712.20 21789.31 225.47 o -7 16 0 3237.57 3254.23 39.45 o -6 16 0 12474.79 12215.92 101.37 o -5 16 0 666.26 560.84 19.49 o -4 16 0 3181.13 3541.33 39.22 o -3 16 0 1316.95 1139.95 22.67 o -2 16 0 2604.29 2597.23 33.71 o -1 16 0 2640.03 2684.83 37.15 o 0 16 0 879.09 996.89 23.94 o 1 16 0 279.05 276.32 15.26 o 2 16 0 2517.44 2526.82 36.36 o 3 16 0 339.75 334.09 16.45 o 4 16 0 2792.81 2894.31 42.63 o 5 16 0 1044.01 1071.16 29.38 o 6 16 0 2769.62 2963.57 47.51 o 7 16 0 225.37 205.18 18.58 o 8 16 0 465.61 448.16 32.35 o 9 16 0 472.27 405.45 23.11 o 10 16 0 151.76 147.43 21.79 o 11 16 0 59.72 47.15 19.24 o 12 16 0 237.67 213.40 25.54 o 13 16 0 191.00 172.45 25.38 o -8 17 0 989.43 844.92 25.03 o -7 17 0 4723.67 4794.44 56.34 o -6 17 0 1453.77 1511.24 31.55 o -5 17 0 2678.34 2552.92 37.98 o -4 17 0 1266.95 1517.75 34.46 o -3 17 0 2854.43 3105.38 42.78 o -2 17 0 364.22 389.71 16.79 o -1 17 0 231.95 241.50 16.35 o 0 17 0 180.45 147.49 14.51 o 1 17 0 439.91 375.51 18.13 o 2 17 0 790.68 907.18 24.71 o 3 17 0 955.16 889.94 27.40 o 4 17 0 822.50 847.63 26.92 o 5 17 0 39.53 38.17 15.91 o 6 17 0 484.59 428.93 28.17 o 7 17 0 787.05 842.14 28.41 o 8 17 0 7.59 -14.94 14.94 o 9 17 0 368.11 309.45 22.22 o 10 17 0 135.88 123.41 20.39 o 11 17 0 74.05 79.00 23.45 o 12 17 0 116.27 105.19 26.79 o -9 18 0 6573.07 6658.40 102.87 o -8 18 0 15049.84 15948.76 137.04 o -7 18 0 1622.46 1386.65 41.38 o -6 18 0 1573.01 1600.49 34.36 o -5 18 0 4497.49 4379.85 52.89 o -4 18 0 2797.22 2578.29 38.93 o -3 18 0 287.92 212.38 16.52 o -2 18 0 2536.20 2572.09 40.94 o -1 18 0 350.18 303.05 19.49 o 0 18 0 60.55 25.21 13.08 o 1 18 0 127.89 108.57 20.84 o 2 18 0 2010.09 2225.86 38.14 o 3 18 0 673.02 736.13 25.90 o 4 18 0 3618.36 3529.03 53.11 o 5 18 0 899.89 903.70 29.71 o 6 18 0 642.40 740.43 27.73 o 7 18 0 248.71 278.43 20.83 o 8 18 0 65.84 72.85 18.11 o 9 18 0 378.21 409.87 26.85 o 10 18 0 370.69 369.32 29.71 o 11 18 0 123.06 73.14 26.71 o -9 19 0 5726.57 5578.74 65.14 o -8 19 0 580.90 584.30 22.07 o -7 19 0 980.42 1181.33 28.19 o -6 19 0 2416.32 2299.28 39.68 o -5 19 0 99.19 59.86 19.42 o -4 19 0 856.16 884.25 26.23 o -3 19 0 391.05 370.78 19.38 o -2 19 0 746.15 880.27 28.51 o -1 19 0 124.59 93.64 15.94 o 0 19 0 117.20 45.28 15.15 o 1 19 0 375.95 343.85 20.76 o 2 19 0 272.39 244.42 21.00 o 3 19 0 78.26 87.22 18.47 o 4 19 0 507.54 558.00 27.20 o 5 19 0 491.26 480.92 26.75 o 6 19 0 227.15 259.95 25.75 o 7 19 0 353.15 344.86 26.64 o 8 19 0 63.88 62.30 19.55 o 9 19 0 257.29 273.84 31.78 o 10 19 0 241.88 286.34 34.64 o -10 20 0 6803.31 6519.84 103.10 o -9 20 0 5351.96 5600.53 63.27 o -8 20 0 1724.79 1770.20 35.99 o -7 20 0 647.14 535.04 22.14 o -6 20 0 3347.61 3355.22 48.72 o -5 20 0 256.69 341.86 22.04 o -4 20 0 2771.35 2826.46 45.31 o -3 20 0 950.28 854.97 27.30 o -2 20 0 2087.56 2291.97 44.97 o -1 20 0 411.28 424.19 22.19 o 0 20 0 652.11 548.98 33.52 o 1 20 0 425.67 415.30 24.62 o 2 20 0 1443.86 1445.51 38.50 o 3 20 0 397.20 395.95 24.79 o 4 20 0 1058.47 1115.25 35.88 o 5 20 0 313.28 336.51 23.67 o 6 20 0 111.56 86.40 20.79 o 7 20 0 359.66 312.08 30.02 o 8 20 0 785.25 888.45 48.28 o -10 21 0 1332.34 1370.32 32.60 o -9 21 0 504.05 426.72 20.58 o -8 21 0 473.46 451.75 21.06 o -7 21 0 607.95 634.40 23.73 o -6 21 0 424.46 572.56 23.39 o -5 21 0 1088.40 1102.15 30.88 o -4 21 0 786.32 846.60 27.77 o -3 21 0 639.29 676.75 28.35 o -2 21 0 286.99 257.64 21.42 o -1 21 0 395.85 418.24 22.56 o 0 21 0 116.60 80.49 17.03 o 1 21 0 40.61 49.78 17.81 o 2 21 0 261.35 286.80 23.05 o 3 21 0 255.65 284.31 22.95 o 4 21 0 422.52 416.87 26.62 o 5 21 0 469.01 398.35 28.62 o 6 21 0 74.09 70.30 26.00 o 7 21 0 277.32 335.41 51.75 o -11 22 0 2.08 -19.51 19.51 o -10 22 0 653.08 750.89 26.79 o -9 22 0 696.82 883.67 30.37 o -8 22 0 54.32 -10.90 19.00 o -7 22 0 323.70 328.29 20.74 o -6 22 0 2818.72 2979.12 48.57 o -5 22 0 41.55 31.86 16.15 o -4 22 0 3680.62 3711.36 62.39 o -3 22 0 68.92 129.71 19.74 o -2 22 0 1417.77 1462.39 36.38 o -1 22 0 40.59 8.92 15.72 o 0 22 0 211.13 233.04 21.83 o 1 22 0 38.51 33.01 18.06 o 2 22 0 584.44 501.43 27.84 o 3 22 0 40.54 24.47 19.16 o 4 22 0 118.16 122.44 26.84 o 5 22 0 275.98 305.15 34.67 o -11 23 0 477.79 486.78 23.91 o -10 23 0 656.27 668.52 27.20 o -9 23 0 1204.19 1229.10 36.43 o -8 23 0 793.81 780.38 28.39 o -7 23 0 224.33 217.52 19.89 o -6 23 0 493.32 406.31 22.97 o -5 23 0 901.54 920.09 30.29 o -4 23 0 513.27 545.29 27.26 o -3 23 0 344.20 332.17 26.82 o -2 23 0 263.61 306.44 22.19 o -1 23 0 47.06 27.03 17.47 o 0 23 0 261.68 248.02 23.32 o 1 23 0 154.47 180.75 22.65 o 2 23 0 361.73 310.38 27.61 o 3 23 0 243.21 216.14 34.12 o 4 23 0 16.23 -14.73 26.88 o -12 24 0 1402.12 1335.90 50.74 o -11 24 0 283.32 322.58 21.92 o -10 24 0 1126.28 1211.95 35.01 o -9 24 0 50.22 24.52 16.99 o -8 24 0 422.66 418.98 23.90 o -7 24 0 801.58 829.03 29.11 o -6 24 0 643.14 752.15 42.01 o -5 24 0 473.69 508.37 27.23 o -4 24 0 1075.71 1159.07 40.68 o -3 24 0 236.95 238.40 21.63 o -2 24 0 611.64 558.15 27.09 o -1 24 0 155.86 184.78 24.27 o 0 24 0 1692.68 1890.46 51.18 o 1 24 0 147.64 139.31 30.98 o 2 24 0 1150.34 1224.61 73.05 o -12 25 0 123.36 150.29 25.44 o -11 25 0 352.48 349.89 22.91 o -10 25 0 248.72 251.50 21.28 o -9 25 0 484.90 475.70 26.37 o -8 25 0 3.38 -15.70 15.70 o -7 25 0 236.22 257.86 21.41 o -6 25 0 233.61 223.45 20.62 o -5 25 0 297.24 380.20 25.81 o -4 25 0 437.02 438.57 27.46 o -3 25 0 27.27 3.97 19.51 o -2 25 0 360.92 357.01 29.38 o -1 25 0 159.47 229.27 33.76 o 0 25 0 577.46 618.89 43.09 o 1 25 0 192.37 255.33 36.07 o -13 26 0 215.46 233.55 30.19 o -12 26 0 1314.13 1523.54 38.93 o -11 26 0 135.72 131.65 20.01 o -10 26 0 146.74 148.72 20.70 o -9 26 0 332.06 296.05 22.79 o -8 26 0 72.21 43.14 18.24 o -7 26 0 331.71 299.95 25.20 o -6 26 0 118.15 81.06 20.68 o -5 26 0 467.19 486.55 31.89 o -4 26 0 121.49 105.78 25.13 o -3 26 0 241.14 260.52 34.21 o -2 26 0 1170.08 1345.89 58.44 o -1 26 0 184.71 226.19 34.51 o -13 27 0 166.78 169.27 20.89 o -12 27 0 403.40 424.33 25.59 o -11 27 0 61.91 48.86 18.97 o -10 27 0 137.40 117.84 20.72 o -9 27 0 386.40 437.58 27.99 o -8 27 0 69.71 39.38 21.72 o -7 27 0 360.15 370.66 30.33 o -6 27 0 68.84 33.16 26.07 o -5 27 0 281.30 287.90 32.25 o -4 27 0 11.50 -22.64 26.73 o -14 28 0 672.13 772.55 74.02 o -13 28 0 322.09 339.71 29.59 o -12 28 0 229.30 217.80 27.63 o -11 28 0 80.87 67.48 24.64 o -10 28 0 367.00 357.63 30.54 o -9 28 0 265.97 325.30 49.35 o -8 28 0 778.17 952.65 45.28 o -7 28 0 274.10 270.09 39.64 o -14 29 0 93.91 77.34 27.23 o -13 29 0 201.33 207.98 33.82 o -12 29 0 115.33 106.98 32.84 o -11 29 0 128.37 139.29 33.55 o -10 29 0 228.63 228.99 36.18 o -1 1 1 5666.36 5289.75 146.55 o 0 1 1 107397.47 74601.41 3559.05 o 1 1 1 5229.72 5481.13 79.32 o -3 2 1 7181.52 7003.47 95.40 o -2 2 1 2614.20 2101.54 30.63 o -1 2 1 5011.48 5443.37 79.35 o 0 2 1 446.28 993.29 15.96 o 1 2 1 5683.91 6229.15 112.03 o 2 2 1 2775.01 2236.24 47.15 o -5 3 1 6503.02 6749.41 54.38 o -4 3 1 27832.13 22553.49 309.85 o -3 3 1 2457.64 913.61 17.87 o -2 3 1 6345.67 6273.74 82.35 o -1 3 1 5724.97 6375.79 90.96 o 0 3 1 631.80 520.38 19.93 o 1 3 1 1873.50 2101.40 37.51 o 2 3 1 21220.65 23331.98 189.56 o 3 3 1 17147.37 15644.41 122.38 o -7 4 1 9098.10 11926.94 87.36 o -6 4 1 15368.67 19096.60 131.55 o -5 4 1 12199.15 10734.77 77.47 o -4 4 1 7847.61 10498.53 85.73 o -3 4 1 28190.02 23291.68 234.93 o -2 4 1 2478.20 1910.20 27.30 o -1 4 1 1724.65 1919.49 31.82 o 0 4 1 32244.17 31815.33 253.29 o 1 4 1 14573.27 15199.32 123.76 o 2 4 1 13044.33 13182.48 146.31 o 3 4 1 41113.64 40233.63 271.54 o 4 4 1 2745.23 3077.25 27.76 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369.30 25.44 o -6 20 2 490.56 379.13 25.89 o -5 20 2 876.40 960.32 36.38 o -4 20 2 980.16 1102.66 39.34 o -3 20 2 2265.88 2267.33 47.35 o -2 20 2 306.55 269.00 23.25 o -1 20 2 1196.00 1265.41 37.62 o 0 20 2 698.72 597.35 28.71 o 1 20 2 22.11 17.58 17.62 o 2 20 2 635.13 779.63 32.30 o 3 20 2 442.35 452.50 29.82 o 4 20 2 159.71 115.81 25.41 o 5 20 2 337.69 285.20 28.17 o 6 20 2 197.63 196.03 26.72 o 7 20 2 143.19 137.35 26.17 o 8 20 2 125.52 101.25 38.41 o -28 21 2 319.00 282.26 35.00 o -27 21 2 71.22 19.93 26.85 o -26 21 2 96.20 94.31 23.64 o -25 21 2 45.79 46.95 23.65 o -24 21 2 310.18 283.55 44.24 o -23 21 2 416.34 439.11 42.52 o -22 21 2 784.22 808.39 39.12 o -21 21 2 545.44 638.22 36.69 o -20 21 2 936.09 950.38 47.00 o -19 21 2 1079.99 1156.11 41.05 o -18 21 2 2249.85 2385.65 55.04 o -17 21 2 1662.53 1899.82 83.53 o -16 21 2 2163.67 2236.57 59.95 o -15 21 2 334.96 355.91 26.44 o -14 21 2 374.99 312.61 24.84 o -13 21 2 317.75 313.02 25.33 o -12 21 2 283.59 237.57 23.98 o -11 21 2 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