#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/43/2214395.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2214395_Fobs
loop_
_publ_author_name
'Song, Ah-Ran'
'Hwang, In-Chul'
'Ha, Kwang'
_publ_section_title
;
 Dichlorido-1\k^2^Cl-\m-[(1,2,5,6-\h:3,4,7,8-\h)-1,3,5,7-cyclooctatetraene]dimethyl-2\k^2^<i>C</i>-diplatinum(II)
;
_journal_coeditor_code           SK3133
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1878
_journal_volume                  63
_journal_year                    2007
_space_group_IT_number           62
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   7.8478
_cell_length_b                   10.3924
_cell_length_c                   15.4582
_exptl_crystal_F_000             1056.00
_reflns_d_resolution_high        0.7996
_[local]_cod_data_source_file    sk3133Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' cotPt2Me2Cl2'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            603.68
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z'
'-x-1/2, y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 12479.06 17264.51 309.18 o
4 0 0 850.54 843.01 114.76 o
6 0 0 3228.35 2444.32 510.67 o
8 0 0 10405.22 10652.29 1018.47 o
2 1 0 144313.66 144523.08 1968.81 o
4 1 0 3880.28 5868.82 240.01 o
6 1 0 10795.26 9818.04 674.20 o
8 1 0 2542.72 2439.75 397.22 o
0 2 0 364428.72 363661.19 2929.17 o
2 2 0 204.13 313.64 70.63 o
4 2 0 10660.11 10545.96 373.90 o
6 2 0 149.15 237.43 164.74 o
8 2 0 16193.45 15182.31 1190.60 o
2 3 0 145859.00 150864.83 1712.69 o
4 3 0 1731.42 2792.56 241.75 o
6 3 0 8529.29 8137.46 378.17 o
8 3 0 1537.42 1909.06 375.66 o
0 4 0 136454.92 156295.78 2200.46 o
2 4 0 158.05 258.81 52.79 o
4 4 0 11396.08 12625.74 561.84 o
6 4 0 15.12 252.35 100.65 o
8 4 0 13814.02 12910.13 1196.34 o
2 5 0 82429.51 86645.75 1034.78 o
4 5 0 841.83 1238.69 189.18 o
6 5 0 6798.74 6691.50 429.04 o
8 5 0 832.53 871.64 230.78 o
0 6 0 155964.00 178102.44 2834.49 o
2 6 0 4681.51 5376.60 264.91 o
4 6 0 1392.49 1612.85 236.11 o
6 6 0 635.75 961.94 191.44 o
8 6 0 4693.76 4454.57 562.73 o
2 7 0 34636.30 35464.53 715.06 o
4 7 0 251.55 272.51 113.75 o
6 7 0 3584.17 3693.07 379.35 o
8 7 0 208.34 709.02 220.58 o
0 8 0 57232.64 54425.65 3170.16 o
2 8 0 486.62 398.01 137.71 o
4 8 0 2404.57 2431.99 311.68 o
6 8 0 1.13 61.84 103.41 o
2 9 0 18816.97 19328.40 861.61 o
4 9 0 292.21 443.24 151.89 o
6 9 0 1819.96 2000.44 417.43 o
0 10 0 16167.53 17006.95 1093.06 o
2 10 0 180.43 277.39 97.66 o
4 10 0 1469.27 1522.80 393.04 o
6 10 0 8.46 550.70 259.64 o
2 11 0 8778.55 8893.65 1027.07 o
4 11 0 475.50 364.65 130.54 o
0 12 0 10391.45 10491.63 969.69 o
2 12 0 585.32 685.67 329.93 o
1 0 1 27201.07 27926.39 715.47 o
2 0 1 2663.89 2824.31 83.22 o
3 0 1 46385.01 43365.57 712.54 o
4 0 1 41565.25 39728.40 385.55 o
5 0 1 18331.18 18685.00 332.90 o
6 0 1 221.64 337.28 162.14 o
7 0 1 17263.41 14545.26 766.31 o
8 0 1 1614.52 1508.45 354.31 o
9 0 1 44.14 -121.32 121.32 o
0 1 1 11107.31 11767.44 153.08 o
1 1 1 18376.18 15508.33 151.29 o
2 1 1 9000.96 7224.21 129.06 o
3 1 1 63509.44 65425.26 711.03 o
4 1 1 158.74 217.77 47.34 o
5 1 1 50720.84 45665.95 532.83 o
6 1 1 18262.61 15680.31 596.26 o
7 1 1 505.45 635.16 154.94 o
8 1 1 170.35 138.37 102.03 o
9 1 1 123.92 207.90 120.35 o
1 2 1 25114.64 30488.09 358.73 o
2 2 1 4116.94 3142.34 82.43 o
3 2 1 69075.30 71232.98 605.23 o
4 2 1 36722.55 35600.93 476.72 o
5 2 1 11815.44 11042.01 279.39 o
6 2 1 422.56 429.81 127.34 o
7 2 1 12957.50 10268.53 458.62 o
8 2 1 1454.71 1475.21 232.11 o
9 2 1 27.58 177.36 112.41 o
0 3 1 6309.37 11605.68 266.20 o
1 3 1 384.05 231.65 38.88 o
2 3 1 46273.59 51827.96 385.63 o
3 3 1 36941.61 38616.21 482.73 o
4 3 1 5913.88 5852.75 204.23 o
5 3 1 39798.56 36504.42 924.05 o
6 3 1 6444.50 6044.04 251.71 o
7 3 1 1193.56 1457.59 217.91 o
8 3 1 158.93 305.28 125.07 o
9 3 1 109.39 232.98 117.90 o
1 4 1 10403.96 12199.85 210.90 o
2 4 1 2783.12 2933.09 104.66 o
3 4 1 54570.68 56826.64 466.60 o
4 4 1 23665.39 22249.31 417.48 o
5 4 1 9923.95 9595.96 296.39 o
6 4 1 371.28 469.72 94.09 o
7 4 1 9196.69 8141.30 488.64 o
8 4 1 1305.66 1368.61 218.35 o
9 4 1 46.68 103.72 128.77 o
0 5 1 1718.56 1414.28 139.80 o
1 5 1 1354.90 1211.64 96.14 o
2 5 1 12400.47 13023.82 226.77 o
3 5 1 19656.16 19066.56 267.00 o
4 5 1 488.76 489.30 90.43 o
5 5 1 25759.51 24109.01 501.17 o
6 5 1 8543.54 8276.82 327.31 o
7 5 1 768.18 1075.23 185.89 o
8 5 1 31.30 141.67 119.26 o
9 5 1 234.23 328.81 125.47 o
1 6 1 3845.70 3961.47 176.00 o
2 6 1 461.94 713.67 83.46 o
3 6 1 18513.30 17417.26 357.60 o
4 6 1 14896.05 14002.41 380.90 o
5 6 1 10631.68 10193.03 341.87 o
6 6 1 374.99 443.11 104.37 o
7 6 1 6735.99 5437.82 435.20 o
8 6 1 698.54 668.94 147.82 o
0 7 1 2947.85 3396.33 236.28 o
1 7 1 1661.11 1826.54 114.14 o
2 7 1 4233.46 4463.69 204.87 o
3 7 1 11494.70 12036.66 315.05 o
4 7 1 49.05 37.92 70.04 o
5 7 1 14367.94 13123.95 410.53 o
6 7 1 5792.32 5343.40 325.26 o
7 7 1 141.92 193.21 75.09 o
8 7 1 129.57 253.67 200.01 o
1 8 1 3696.78 3696.09 230.59 o
2 8 1 104.31 218.83 71.24 o
3 8 1 10658.11 10928.45 377.69 o
4 8 1 8414.95 8313.52 349.81 o
5 8 1 4703.18 4797.26 314.67 o
6 8 1 406.01 484.93 110.34 o
7 8 1 3055.12 2800.20 266.53 o
0 9 1 110.92 196.57 125.58 o
1 9 1 100.68 214.04 86.47 o
2 9 1 5812.45 6038.77 280.81 o
3 9 1 5624.22 5702.55 345.86 o
4 9 1 673.25 935.52 158.04 o
5 9 1 7101.77 7178.50 440.23 o
6 9 1 1286.42 1318.07 171.94 o
7 9 1 139.16 269.88 127.02 o
1 10 1 1816.73 2045.72 238.38 o
2 10 1 176.86 274.44 89.07 o
3 10 1 6309.97 5839.24 394.87 o
4 10 1 3040.88 3021.46 311.85 o
5 10 1 1459.56 1436.36 213.26 o
6 10 1 113.88 303.27 214.26 o
0 11 1 6.10 107.77 134.80 o
1 11 1 7.76 106.54 91.20 o
2 11 1 1380.67 1522.29 338.04 o
3 11 1 2552.54 2338.68 304.63 o
4 11 1 40.70 70.71 98.25 o
5 11 1 3058.00 2734.83 333.18 o
1 12 1 756.53 1075.12 179.31 o
2 12 1 38.62 377.43 177.08 o
3 12 1 1736.51 1711.49 333.55 o
0 0 2 79797.45 56952.82 4083.91 o
1 0 2 115376.72 128352.21 1862.82 o
2 0 2 704.29 1641.28 85.14 o
3 0 2 28428.60 32717.16 1163.35 o
4 0 2 2361.94 2573.19 128.13 o
5 0 2 1540.24 1505.63 105.26 o
6 0 2 3995.28 3981.44 455.26 o
7 0 2 9237.45 9027.52 431.09 o
8 0 2 4347.26 3639.76 506.68 o
9 0 2 919.08 1265.82 286.79 o
1 1 2 109936.71 122756.48 631.14 o
2 1 2 14646.90 12415.63 143.21 o
3 1 2 17946.91 13413.21 326.83 o
4 1 2 14019.31 13737.36 235.35 o
5 1 2 3674.55 3729.33 127.67 o
6 1 2 4153.38 4442.43 247.97 o
7 1 2 1633.82 1626.82 223.56 o
8 1 2 237.12 392.19 132.87 o
9 1 2 5934.16 5030.65 427.90 o
0 2 2 75010.32 79379.98 589.25 o
1 2 2 84468.23 88331.61 664.73 o
2 2 2 13008.77 13187.91 166.68 o
3 2 2 20739.89 19883.66 206.04 o
4 2 2 36.62 324.80 46.06 o
5 2 2 526.14 572.53 78.66 o
6 2 2 522.24 608.07 131.57 o
7 2 2 9985.18 9007.31 428.95 o
8 2 2 2717.38 3137.41 272.67 o
9 2 2 868.58 883.38 170.67 o
1 3 2 56538.12 55206.67 375.06 o
2 3 2 17701.02 18222.99 260.89 o
3 3 2 35570.35 36516.47 662.70 o
4 3 2 8085.45 8320.66 241.15 o
5 3 2 23.23 352.38 74.65 o
6 3 2 2930.94 3187.91 242.14 o
7 3 2 2715.19 2387.52 277.54 o
8 3 2 34.44 168.31 102.20 o
9 3 2 6278.26 6146.26 377.65 o
0 4 2 34897.30 38483.44 627.47 o
1 4 2 62263.27 67133.50 536.73 o
2 4 2 14417.22 16574.81 222.37 o
3 4 2 14186.29 14090.94 288.73 o
4 4 2 10.45 217.91 64.30 o
5 4 2 12.51 153.61 64.33 o
6 4 2 166.45 221.78 77.18 o
7 4 2 9604.97 8938.48 496.63 o
8 4 2 2086.11 2315.11 274.89 o
9 4 2 545.36 967.38 166.45 o
1 5 2 56800.96 59356.68 676.23 o
2 5 2 10674.50 10014.71 191.90 o
3 5 2 7333.48 6866.02 179.64 o
4 5 2 3989.77 4252.14 236.45 o
5 5 2 592.64 684.62 110.07 o
6 5 2 1780.35 1939.28 182.54 o
7 5 2 818.26 679.96 155.79 o
8 5 2 0.85 -47.41 103.43 o
9 5 2 3865.55 3488.60 734.44 o
0 6 2 12115.08 11473.94 393.82 o
1 6 2 42587.21 44418.09 526.97 o
2 6 2 367.62 463.09 52.92 o
3 6 2 9509.41 9445.88 211.52 o
4 6 2 1508.29 1642.77 164.57 o
5 6 2 6.01 166.74 76.18 o
6 6 2 1694.05 1765.07 182.59 o
7 6 2 5435.71 4767.59 405.92 o
8 6 2 1888.88 1591.55 195.57 o
1 7 2 31765.50 31453.17 473.97 o
2 7 2 5019.12 5486.60 225.69 o
3 7 2 1488.51 1814.41 118.69 o
4 7 2 3044.43 3495.02 252.05 o
5 7 2 716.05 816.27 124.32 o
6 7 2 1598.95 1784.09 185.59 o
7 7 2 409.38 477.01 82.58 o
8 7 2 7.01 220.28 145.35 o
0 8 2 10568.99 10527.71 413.36 o
1 8 2 19373.64 18966.03 448.52 o
2 8 2 1406.75 1552.92 184.82 o
3 8 2 4630.12 4987.94 300.57 o
4 8 2 125.62 212.90 83.91 o
5 8 2 0.12 122.84 74.94 o
6 8 2 443.38 541.05 123.85 o
7 8 2 2528.34 2825.25 245.29 o
1 9 2 9887.58 9944.84 346.36 o
2 9 2 3075.58 3164.19 271.14 o
3 9 2 2491.05 2687.59 279.19 o
4 9 2 1485.56 1573.15 196.65 o
5 9 2 6.62 179.60 83.60 o
6 9 2 757.57 761.44 138.94 o
0 10 2 4487.10 4532.42 487.81 o
1 10 2 6768.49 7050.09 391.46 o
2 10 2 1944.75 1770.11 168.67 o
3 10 2 2040.67 1885.34 243.79 o
4 10 2 0.76 32.41 83.45 o
5 10 2 77.50 104.77 104.58 o
6 10 2 43.33 144.17 90.61 o
1 11 2 5197.17 5528.96 402.25 o
2 11 2 1345.24 1107.36 297.54 o
3 11 2 785.77 722.80 175.61 o
4 11 2 647.21 658.43 164.87 o
5 11 2 1.21 101.62 100.11 o
0 12 2 1357.75 1330.83 286.02 o
1 12 2 2409.32 2710.38 333.57 o
2 12 2 269.80 236.25 161.31 o
3 12 2 929.74 1070.75 291.60 o
1 0 3 54473.09 63257.13 1135.48 o
2 0 3 1877.35 1870.34 108.83 o
3 0 3 204.12 382.25 54.58 o
4 0 3 106571.52 111653.06 1537.40 o
5 0 3 5660.75 5829.64 197.20 o
6 0 3 2341.86 2481.01 262.31 o
7 0 3 39.34 271.91 111.19 o
8 0 3 2881.22 2773.82 430.67 o
9 0 3 723.37 800.81 245.16 o
0 1 3 790.90 2832.05 163.20 o
1 1 3 14024.86 14275.20 258.33 o
2 1 3 61195.48 58322.29 1180.94 o
3 1 3 3523.31 3767.17 100.97 o
4 1 3 6475.16 5916.25 128.98 o
5 1 3 722.84 890.14 79.80 o
6 1 3 30044.68 28585.71 512.11 o
7 1 3 3192.95 3331.60 265.71 o
8 1 3 1101.78 1066.55 187.33 o
9 1 3 151.46 343.77 135.97 o
1 2 3 7828.62 6932.19 117.51 o
2 2 3 3359.30 3823.88 95.79 o
3 2 3 9849.62 9361.74 160.04 o
4 2 3 94390.23 91980.78 601.28 o
5 2 3 253.46 391.44 48.52 o
6 2 3 3374.74 2938.67 238.86 o
7 2 3 382.97 647.22 124.00 o
8 2 3 2500.78 2578.94 245.54 o
9 2 3 1663.96 1634.12 234.45 o
0 3 3 706.59 1530.60 117.16 o
1 3 3 23831.38 23749.45 255.47 o
2 3 3 34989.88 34599.41 312.59 o
3 3 3 1028.86 1093.46 78.41 o
4 3 3 404.30 372.69 45.49 o
5 3 3 82.65 239.16 54.55 o
6 3 3 30910.36 28336.74 456.28 o
7 3 3 2286.15 2581.34 240.83 o
8 3 3 1185.76 1150.17 168.77 o
9 3 3 45.65 240.27 106.79 o
1 4 3 2571.99 2165.30 87.68 o
2 4 3 743.90 1093.78 78.97 o
3 4 3 8005.90 7988.53 175.13 o
4 4 3 68921.09 67500.33 696.96 o
5 4 3 8.99 118.11 63.43 o
6 4 3 4574.51 4689.15 216.29 o
7 4 3 429.34 625.76 133.11 o
8 4 3 1547.17 1679.81 203.51 o
9 4 3 1475.48 1447.23 219.86 o
0 5 3 1606.82 2376.39 224.19 o
1 5 3 11747.60 11886.65 208.90 o
2 5 3 42483.49 42053.48 394.40 o
3 5 3 1175.89 1366.29 97.00 o
4 5 3 1994.19 2005.39 156.84 o
5 5 3 57.90 102.10 62.14 o
6 5 3 17046.11 16445.39 370.18 o
7 5 3 1774.44 2010.25 223.73 o
8 5 3 622.97 653.70 136.51 o
1 6 3 12315.89 12567.76 266.17 o
2 6 3 228.72 339.67 50.62 o
3 6 3 315.52 372.39 55.82 o
4 6 3 41111.09 38002.63 572.41 o
5 6 3 1355.52 1573.80 153.77 o
6 6 3 3045.16 2751.70 227.18 o
7 6 3 11.09 315.69 72.41 o
8 6 3 1014.52 963.27 143.60 o
0 7 3 717.82 1228.94 171.64 o
1 7 3 3768.07 3950.15 181.49 o
2 7 3 28142.51 27168.36 408.39 o
3 7 3 797.80 843.16 85.70 o
4 7 3 2167.59 2314.06 208.41 o
5 7 3 301.07 266.07 85.75 o
6 7 3 8593.85 8984.43 362.98 o
7 7 3 858.40 946.51 123.94 o
8 7 3 507.26 739.56 179.91 o
1 8 3 2651.51 2880.18 197.61 o
2 8 3 159.97 253.39 65.11 o
3 8 3 1150.50 1272.82 149.67 o
4 8 3 20574.87 18828.28 504.69 o
5 8 3 81.06 234.92 88.85 o
6 8 3 1636.36 1516.01 172.33 o
7 8 3 60.83 347.45 97.03 o
0 9 3 324.30 652.79 196.04 o
1 9 3 2451.72 2607.52 200.83 o
2 9 3 9229.30 8999.03 302.49 o
3 9 3 297.81 403.25 115.63 o
4 9 3 134.44 291.59 96.35 o
5 9 3 34.97 9.53 78.70 o
6 9 3 5384.10 5674.04 444.45 o
1 10 3 446.78 607.22 103.92 o
2 10 3 2.66 84.71 64.58 o
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4 10 3 9748.40 10089.33 497.50 o
5 10 3 7.37 98.06 75.30 o
6 10 3 1112.54 1110.64 175.05 o
0 11 3 731.08 774.61 338.53 o
1 11 3 1221.77 1483.80 192.67 o
2 11 3 3820.31 3676.03 375.36 o
3 11 3 154.83 247.96 109.30 o
4 11 3 27.59 50.51 94.64 o
1 12 3 770.54 758.49 141.18 o
2 12 3 15.16 25.76 189.35 o
3 12 3 31.11 204.60 107.12 o
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1 0 4 30605.80 31044.09 834.62 o
2 0 4 7868.04 7702.81 214.98 o
3 0 4 40640.53 39042.91 493.95 o
4 0 4 7690.80 7152.00 274.82 o
5 0 4 4936.96 5286.03 202.72 o
6 0 4 9829.66 9162.84 413.05 o
7 0 4 2808.07 2903.99 433.86 o
8 0 4 2773.94 2649.93 434.74 o
9 0 4 426.26 660.81 215.01 o
1 1 4 26230.92 21913.71 451.74 o
2 1 4 35747.94 32307.42 622.87 o
3 1 4 1254.70 1303.83 79.13 o
4 1 4 15457.62 14000.22 224.25 o
5 1 4 1976.65 2422.21 134.25 o
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9 1 4 4257.98 3232.79 342.34 o
0 2 4 74027.17 71503.79 1035.69 o
1 2 4 20617.42 22835.17 394.29 o
2 2 4 9952.93 10364.44 176.59 o
3 2 4 32414.23 31901.28 336.43 o
4 2 4 3062.06 3423.13 120.34 o
5 2 4 5716.95 5695.51 179.94 o
6 2 4 8453.09 8178.02 364.28 o
7 2 4 3313.34 3490.25 278.39 o
8 2 4 2116.91 2242.08 236.70 o
9 2 4 478.70 262.96 168.95 o
1 3 4 100046.05 106285.33 608.71 o
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5 3 4 38.82 271.26 58.51 o
6 3 4 409.01 630.65 82.28 o
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0 4 4 50442.94 48709.62 635.31 o
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3 4 4 20635.63 20264.83 280.76 o
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6 4 4 5749.50 5627.48 225.81 o
7 4 4 2918.01 2907.45 263.01 o
8 4 4 1402.87 1740.63 211.27 o
9 4 4 501.01 561.34 119.36 o
1 5 4 33935.14 33141.73 334.42 o
2 5 4 19405.53 17575.90 263.60 o
3 5 4 75.13 300.17 47.74 o
4 5 4 8253.76 8153.64 242.26 o
5 5 4 1200.44 1614.54 138.99 o
6 5 4 302.70 690.78 94.94 o
7 5 4 3724.09 3916.76 311.56 o
8 5 4 1137.59 1523.05 182.16 o
0 6 4 20544.41 20489.52 474.59 o
1 6 4 16413.10 16636.11 276.12 o
2 6 4 3130.44 3121.67 144.69 o
3 6 4 15294.40 14599.08 295.63 o
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5 6 4 3905.66 4274.97 230.81 o
6 6 4 3611.21 4022.89 252.59 o
7 6 4 2095.92 2358.56 235.62 o
8 6 4 1075.29 1049.24 190.47 o
1 7 4 12042.03 11920.49 274.96 o
2 7 4 9832.25 9520.55 301.45 o
3 7 4 65.34 168.88 50.16 o
4 7 4 4815.00 4867.29 322.52 o
5 7 4 1273.72 1406.07 157.82 o
6 7 4 281.45 531.12 106.48 o
7 7 4 3048.04 3016.30 230.87 o
8 7 4 583.14 665.06 186.19 o
0 8 4 10104.78 10046.49 381.94 o
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1 3 17 526.08 1135.21 276.61 o
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