#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/43/2214397.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214397_Fobs loop_ _publ_author_name 'Yu, Xiao-Chun' 'Li, Shu-Yan' 'Zhong, Ping' _publ_section_title ; 4-Bromo-5-[(4-chlorobenzylidene)amino]-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile ; _journal_coeditor_code TK2157 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3098 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.0338 _cell_length_b 11.5819 _cell_length_c 34.4986 _exptl_crystal_F_000 2048.00 _reflns_d_resolution_high 0.7496 _[local]_cod_data_source_file tk2157Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zp58m in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 396.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 32585.49 36384.32 1324.28 o 4 0 0 60357.29 67764.91 2459.28 o 6 0 0 42934.99 49360.41 1797.01 o 8 0 0 1149.89 1059.32 89.19 o 10 0 0 4.09 15.67 30.85 o 2 1 0 1502.17 1267.56 35.15 o 4 1 0 57.58 50.84 8.06 o 6 1 0 6824.53 7185.42 191.51 o 8 1 0 5749.76 5726.29 157.55 o 10 1 0 453.38 574.25 48.59 o 0 2 0 65822.13 68713.75 3495.63 o 2 2 0 48332.51 53783.95 1233.05 o 4 2 0 761.92 924.64 30.04 o 6 2 0 14250.81 14931.09 389.65 o 8 2 0 17.35 24.51 19.02 o 10 2 0 30.71 24.32 33.00 o 12 2 0 5.69 20.10 44.19 o 2 3 0 46681.31 49825.26 1142.97 o 4 3 0 95.93 289.89 13.65 o 6 3 0 7961.58 6679.36 179.11 o 8 3 0 1429.58 1561.01 221.85 o 10 3 0 16.35 38.66 35.51 o 12 3 0 260.12 265.06 53.19 o 0 4 0 40700.79 46004.12 2341.93 o 2 4 0 5081.13 5545.01 146.19 o 4 4 0 5629.42 5758.23 137.12 o 6 4 0 8903.36 8880.26 337.30 o 8 4 0 556.24 371.19 39.35 o 10 4 0 19.26 9.76 38.24 o 12 4 0 57.07 -9.80 45.54 o 2 5 0 4391.43 4849.29 115.06 o 4 5 0 3252.46 2978.24 74.50 o 6 5 0 2307.70 2549.47 89.60 o 8 5 0 8.80 16.40 30.97 o 10 5 0 150.24 118.99 43.35 o 12 5 0 124.98 53.66 52.31 o 0 6 0 4156.78 5274.56 279.16 o 2 6 0 36928.33 42945.29 981.88 o 4 6 0 8089.33 8922.11 274.40 o 6 6 0 3370.41 3519.92 118.91 o 8 6 0 1063.23 1265.99 75.38 o 10 6 0 303.58 273.90 50.19 o 2 7 0 122.49 101.57 11.77 o 4 7 0 1.79 1.75 16.96 o 6 7 0 4441.23 4253.42 175.80 o 8 7 0 46.71 45.01 38.39 o 10 7 0 4.41 -32.13 43.00 o 0 8 0 3017.85 3075.69 123.94 o 2 8 0 306.14 211.72 33.79 o 4 8 0 1021.84 1180.64 60.27 o 6 8 0 853.19 851.66 97.11 o 8 8 0 4.24 32.90 55.57 o 10 8 0 15.46 19.48 150.34 o 2 9 0 505.65 532.80 71.34 o 4 9 0 177.04 143.43 25.29 o 6 9 0 0.41 -31.18 31.18 o 8 9 0 27.32 14.62 40.11 o 10 9 0 10.95 27.75 58.82 o 0 10 0 25.91 -0.68 19.42 o 2 10 0 898.15 980.75 49.11 o 4 10 0 1324.79 1205.51 70.01 o 6 10 0 59.98 133.97 42.72 o 8 10 0 299.81 350.14 55.44 o 2 11 0 2.56 16.07 24.39 o 4 11 0 6.09 -12.51 32.64 o 6 11 0 679.33 786.14 63.30 o 8 11 0 121.80 120.59 54.45 o 0 12 0 286.78 286.50 62.07 o 2 12 0 763.05 737.62 57.54 o 4 12 0 80.20 72.59 38.86 o 6 12 0 5.22 8.66 40.28 o 4 13 0 110.45 61.16 48.22 o 6 13 0 143.07 195.82 51.56 o 0 14 0 72.54 75.09 65.08 o 2 14 0 4.44 -41.38 58.24 o 2 15 0 49.13 87.44 73.42 o 1 1 1 3093.59 3059.28 55.89 o 2 1 1 5161.37 5309.62 92.53 o 3 1 1 18131.30 20017.82 364.85 o 4 1 1 179.83 137.80 7.78 o 5 1 1 3732.17 3951.13 76.20 o 6 1 1 2172.44 2361.95 49.07 o 7 1 1 1918.03 2003.99 44.75 o 8 1 1 16.17 -9.06 11.25 o 9 1 1 186.12 180.28 15.97 o 10 1 1 18.97 31.70 20.56 o 11 1 1 5.93 -16.37 24.65 o 0 2 1 12050.09 12375.12 367.85 o 1 2 1 1894.48 1971.04 32.09 o 2 2 1 48469.30 52219.13 893.34 o 3 2 1 14906.28 16323.54 281.05 o 4 2 1 174.80 146.24 8.60 o 5 2 1 1411.73 1261.94 28.22 o 6 2 1 514.54 688.94 19.69 o 7 2 1 151.47 141.39 11.84 o 8 2 1 90.48 100.08 13.10 o 9 2 1 276.89 253.44 22.86 o 10 2 1 2.75 -18.28 22.45 o 11 2 1 2.63 49.80 27.86 o 12 2 1 0.98 -34.06 34.06 o 1 3 1 10439.28 10614.14 207.54 o 2 3 1 16522.90 17570.81 286.44 o 3 3 1 4558.94 4673.38 78.38 o 4 3 1 27437.31 31109.95 506.49 o 5 3 1 2507.73 2600.59 56.15 o 6 3 1 7.69 15.38 8.61 o 7 3 1 282.96 230.98 14.87 o 8 3 1 74.39 95.29 17.53 o 9 3 1 102.44 93.04 22.55 o 10 3 1 27.69 3.07 24.98 o 11 3 1 62.12 107.59 37.07 o 12 3 1 15.20 79.16 33.37 o 13 3 1 5.43 12.86 50.97 o 0 4 1 6222.98 6793.68 204.35 o 1 4 1 54.77 83.42 6.13 o 2 4 1 4309.51 4386.72 82.55 o 3 4 1 140.07 296.72 8.81 o 4 4 1 15148.71 16041.74 263.09 o 5 4 1 3450.93 3120.38 55.47 o 6 4 1 524.21 669.86 21.41 o 7 4 1 12.14 -2.67 14.63 o 8 4 1 397.78 456.58 31.12 o 9 4 1 1915.09 2109.53 73.29 o 10 4 1 121.09 112.03 27.96 o 11 4 1 122.81 179.85 33.70 o 12 4 1 13.88 -11.85 31.12 o 1 5 1 6248.99 5984.63 111.73 o 2 5 1 3714.23 4665.79 78.44 o 3 5 1 1007.08 839.42 20.78 o 4 5 1 2611.21 2553.73 45.98 o 5 5 1 196.44 193.80 10.82 o 6 5 1 506.99 547.27 25.83 o 7 5 1 290.82 323.62 27.05 o 8 5 1 158.59 130.67 23.76 o 9 5 1 111.33 84.62 25.97 o 10 5 1 194.83 216.54 38.99 o 11 5 1 0.14 38.84 31.96 o 12 5 1 6.34 24.10 43.71 o 0 6 1 2074.08 1806.41 60.79 o 1 6 1 148.62 168.91 10.21 o 2 6 1 3636.29 3832.75 65.88 o 3 6 1 84.35 63.71 7.91 o 4 6 1 27.49 34.36 11.83 o 5 6 1 4926.76 4937.74 112.36 o 6 6 1 3748.25 3658.52 96.05 o 7 6 1 578.46 630.08 35.75 o 8 6 1 45.51 45.64 24.13 o 9 6 1 492.93 618.35 40.07 o 10 6 1 116.60 82.43 31.13 o 11 6 1 116.56 175.19 35.24 o 1 7 1 13951.82 14409.27 265.17 o 2 7 1 2093.60 2124.31 39.45 o 3 7 1 11467.89 11213.62 241.74 o 4 7 1 1742.77 1809.77 47.77 o 5 7 1 2322.63 2190.15 56.97 o 6 7 1 17.72 -16.04 19.96 o 7 7 1 1315.43 1281.15 65.08 o 8 7 1 9.60 -16.37 24.82 o 9 7 1 395.06 359.51 36.19 o 10 7 1 201.96 282.21 36.30 o 11 7 1 7.23 -34.31 34.31 o 0 8 1 6380.36 7215.66 192.56 o 1 8 1 709.73 705.55 19.27 o 2 8 1 1277.78 1204.12 29.75 o 3 8 1 7.02 26.19 12.58 o 4 8 1 25.44 19.25 13.73 o 5 8 1 974.12 1016.86 46.32 o 6 8 1 28.57 71.73 23.39 o 7 8 1 711.75 877.59 45.10 o 8 8 1 565.96 483.10 37.21 o 9 8 1 65.91 143.49 31.06 o 10 8 1 15.85 11.60 33.14 o 1 9 1 1785.00 1830.17 41.60 o 2 9 1 193.96 161.52 17.00 o 3 9 1 2936.58 2811.85 69.79 o 4 9 1 282.80 229.55 23.78 o 5 9 1 325.42 313.73 35.98 o 6 9 1 24.96 29.71 23.19 o 7 9 1 22.17 -24.94 24.94 o 8 9 1 173.21 76.02 31.77 o 9 9 1 11.09 -10.36 35.72 o 10 9 1 0.30 -12.32 34.27 o 0 10 1 532.11 566.96 25.99 o 1 10 1 535.25 552.91 31.16 o 2 10 1 2411.40 2289.01 59.84 o 3 10 1 187.28 205.98 24.15 o 4 10 1 23.95 43.97 19.44 o 5 10 1 1243.86 1135.08 53.54 o 6 10 1 17.10 15.00 31.99 o 7 10 1 342.97 392.89 36.87 o 8 10 1 530.57 512.10 43.08 o 9 10 1 6.55 -22.37 34.98 o 1 11 1 619.40 688.66 34.54 o 2 11 1 157.09 101.01 19.04 o 3 11 1 207.77 198.92 21.43 o 4 11 1 21.28 31.56 22.52 o 5 11 1 663.56 633.31 70.49 o 6 11 1 3.27 15.19 28.01 o 7 11 1 21.20 33.01 29.94 o 8 11 1 0.32 6.35 34.65 o 0 12 1 241.37 260.64 59.99 o 1 12 1 385.03 370.17 57.71 o 2 12 1 119.95 107.85 39.23 o 3 12 1 0.72 -7.56 28.13 o 4 12 1 45.80 25.35 25.70 o 5 12 1 17.88 2.25 26.58 o 6 12 1 111.42 82.88 31.46 o 7 12 1 118.15 127.22 37.31 o 1 13 1 814.79 840.54 46.81 o 2 13 1 6.04 -25.03 53.40 o 3 13 1 60.33 82.43 56.40 o 4 13 1 158.41 175.39 31.44 o 5 13 1 135.83 91.34 32.56 o 6 13 1 8.13 -2.36 31.93 o 0 14 1 0.80 6.01 43.72 o 1 14 1 42.89 34.06 36.69 o 2 14 1 27.76 -49.89 56.90 o 5 14 1 27.07 31.84 45.06 o 1 15 1 6.92 -10.19 44.37 o 2 15 1 42.33 112.63 72.42 o 0 0 2 4073.53 -0.69 0.69 o 1 0 2 9130.05 10427.58 270.70 o 2 0 2 10871.50 11270.92 291.58 o 3 0 2 1070.95 1023.65 30.59 o 4 0 2 64492.63 68980.18 1770.38 o 5 0 2 2783.65 3062.29 85.16 o 6 0 2 1035.35 825.18 31.63 o 7 0 2 3.94 -7.01 13.45 o 8 0 2 6982.62 7302.54 272.44 o 9 0 2 217.30 328.28 25.99 o 10 0 2 168.70 159.40 29.20 o 11 0 2 7.47 34.04 49.39 o 1 1 2 90.11 26.71 9.43 o 2 1 2 34.42 8.31 2.80 o 3 1 2 1506.98 1509.70 30.36 o 4 1 2 10848.29 10474.27 193.10 o 5 1 2 64.76 51.27 7.40 o 6 1 2 9827.05 9358.38 174.80 o 7 1 2 188.77 237.39 21.40 o 8 1 2 983.78 922.64 26.59 o 9 1 2 306.31 324.08 19.74 o 10 1 2 807.23 719.44 34.59 o 11 1 2 331.73 287.20 39.34 o 12 1 2 158.15 179.04 65.08 o 0 2 2 32572.22 37430.36 1107.49 o 1 2 2 17337.81 19443.57 377.43 o 2 2 2 92468.34 100891.91 1724.50 o 3 2 2 1500.70 1649.65 31.17 o 4 2 2 9536.60 10523.45 194.00 o 5 2 2 2279.04 2548.39 51.16 o 6 2 2 2298.11 3065.96 61.63 o 7 2 2 8.17 34.56 13.90 o 8 2 2 1698.11 1513.20 39.97 o 9 2 2 306.25 282.39 23.60 o 10 2 2 22.78 55.29 23.85 o 11 2 2 67.53 118.69 29.30 o 12 2 2 37.54 42.34 35.74 o 1 3 2 57260.86 61690.55 1186.98 o 2 3 2 2422.88 3195.38 57.12 o 3 3 2 5028.04 5178.92 86.65 o 4 3 2 5800.79 6315.38 105.63 o 5 3 2 3757.00 3884.65 75.29 o 6 3 2 2381.52 2769.24 56.54 o 7 3 2 3740.54 3902.81 83.84 o 8 3 2 341.62 308.95 22.68 o 9 3 2 662.04 593.07 34.92 o 10 3 2 414.57 413.37 44.36 o 11 3 2 11.19 61.53 28.53 o 12 3 2 130.03 97.20 32.46 o 13 3 2 2.30 55.81 74.00 o 0 4 2 22713.08 25381.38 752.14 o 1 4 2 969.09 962.64 24.07 o 2 4 2 20674.65 22392.58 407.23 o 3 4 2 4876.55 5172.40 91.78 o 4 4 2 13167.84 14407.33 236.77 o 5 4 2 1358.91 1503.50 29.75 o 6 4 2 788.83 840.81 25.28 o 7 4 2 763.78 736.09 30.52 o 8 4 2 1475.61 1582.89 57.65 o 9 4 2 117.04 77.88 24.87 o 10 4 2 256.31 238.87 30.79 o 11 4 2 25.19 5.56 29.78 o 12 4 2 57.39 41.58 57.02 o 1 5 2 1493.40 1386.94 33.77 o 2 5 2 2128.67 2460.30 45.62 o 3 5 2 1388.83 1321.44 29.15 o 4 5 2 4363.30 3892.02 71.02 o 5 5 2 1897.96 1651.20 37.26 o 6 5 2 1920.29 1602.50 53.06 o 7 5 2 2510.92 2253.71 73.79 o 8 5 2 529.20 584.62 44.97 o 9 5 2 147.98 169.73 28.38 o 10 5 2 663.58 518.67 38.70 o 11 5 2 79.95 91.39 33.60 o 12 5 2 11.93 -1.97 35.51 o 0 6 2 13550.81 13702.54 410.11 o 1 6 2 1354.01 1383.85 31.37 o 2 6 2 5846.48 5525.98 92.85 o 3 6 2 71.91 54.20 8.70 o 4 6 2 1154.90 874.43 25.46 o 5 6 2 3114.15 2984.12 66.30 o 6 6 2 1293.05 981.10 36.65 o 7 6 2 2512.81 2589.80 83.55 o 8 6 2 599.72 428.58 32.81 o 9 6 2 0.41 -24.64 24.64 o 10 6 2 308.13 343.91 56.26 o 11 6 2 3.35 -31.69 31.69 o 1 7 2 857.81 861.11 22.53 o 2 7 2 776.14 692.53 17.81 o 3 7 2 281.83 251.65 16.32 o 4 7 2 513.25 483.97 22.25 o 5 7 2 1330.62 1231.08 37.67 o 6 7 2 148.72 105.08 19.50 o 7 7 2 48.35 23.49 29.66 o 8 7 2 140.10 156.41 44.36 o 9 7 2 13.61 38.52 28.39 o 10 7 2 129.12 107.91 45.06 o 11 7 2 2.15 4.73 33.62 o 0 8 2 41.83 85.12 16.59 o 1 8 2 161.28 188.63 11.03 o 2 8 2 30.02 98.27 11.16 o 3 8 2 69.49 84.60 13.74 o 4 8 2 141.47 193.60 16.89 o 5 8 2 5492.59 5293.64 134.01 o 6 8 2 11.87 17.18 22.57 o 7 8 2 282.68 229.54 29.61 o 8 8 2 2.78 -24.77 24.77 o 9 8 2 49.32 75.61 30.48 o 10 8 2 88.99 57.03 37.48 o 1 9 2 104.01 143.98 13.86 o 2 9 2 0.30 11.53 13.63 o 3 9 2 98.04 108.77 16.22 o 4 9 2 0.43 5.33 17.02 o 5 9 2 396.71 351.89 25.15 o 6 9 2 3.89 2.75 22.64 o 7 9 2 172.28 80.09 27.98 o 8 9 2 1.93 -18.55 28.09 o 9 9 2 183.72 244.79 36.40 o 10 9 2 5.08 1.64 35.02 o 0 10 2 116.78 109.59 24.77 o 1 10 2 42.79 34.77 15.13 o 2 10 2 16.99 18.80 15.20 o 3 10 2 1574.66 1540.87 46.17 o 4 10 2 196.67 171.39 25.82 o 5 10 2 48.37 54.54 33.47 o 6 10 2 61.01 48.93 26.81 o 7 10 2 20.60 -4.99 27.92 o 8 10 2 181.52 140.91 33.81 o 9 10 2 22.01 -34.85 34.98 o 1 11 2 58.91 55.35 21.80 o 2 11 2 27.17 46.90 20.43 o 3 11 2 175.01 200.52 26.79 o 4 11 2 83.74 141.67 26.56 o 5 11 2 36.02 38.07 26.03 o 6 11 2 60.64 27.21 27.69 o 7 11 2 111.04 100.74 32.74 o 8 11 2 19.18 40.75 36.01 o 0 12 2 24.49 14.42 34.09 o 1 12 2 191.74 240.36 35.93 o 2 12 2 237.21 280.70 29.84 o 3 12 2 1.90 -13.76 21.11 o 4 12 2 0.77 21.13 37.67 o 5 12 2 8.66 -25.86 25.86 o 6 12 2 10.41 -22.49 28.91 o 7 12 2 20.28 -1.76 33.75 o 1 13 2 3.13 -25.81 25.81 o 2 13 2 20.06 -14.18 39.63 o 3 13 2 38.33 17.31 38.59 o 4 13 2 218.08 258.24 33.86 o 5 13 2 3.42 -21.25 38.65 o 6 13 2 9.67 73.83 34.03 o 0 14 2 35.10 84.74 46.66 o 1 14 2 19.62 42.21 35.60 o 2 14 2 32.79 40.38 62.74 o 4 14 2 59.84 193.73 63.91 o 5 14 2 50.27 106.62 56.15 o 1 15 2 50.33 86.75 90.86 o 2 15 2 5.05 -62.07 62.07 o 1 1 3 433.78 581.06 17.41 o 2 1 3 3810.50 4574.76 80.19 o 3 1 3 2215.55 2230.11 43.90 o 4 1 3 0.47 6.80 5.23 o 5 1 3 3057.46 3361.77 65.71 o 6 1 3 27.68 47.53 9.07 o 7 1 3 7.70 -2.29 9.68 o 8 1 3 3.23 23.81 11.63 o 9 1 3 21.94 27.84 14.87 o 10 1 3 21.62 61.85 21.66 o 11 1 3 0.00 12.89 28.64 o 12 1 3 40.52 60.40 60.91 o 0 2 3 7705.87 7444.54 222.56 o 1 2 3 5079.89 5992.93 127.49 o 2 2 3 14592.39 16627.67 286.07 o 3 2 3 1409.50 1738.93 32.76 o 4 2 3 60.34 65.67 6.28 o 5 2 3 776.25 1015.73 24.35 o 6 2 3 806.25 714.76 20.45 o 7 2 3 4470.62 4628.43 90.62 o 8 2 3 336.20 272.05 17.17 o 9 2 3 523.78 455.62 27.66 o 10 2 3 358.12 364.13 31.87 o 11 2 3 234.84 275.18 32.87 o 12 2 3 12.82 63.45 42.55 o 13 2 3 61.94 124.98 75.59 o 1 3 3 2613.53 2342.37 44.60 o 2 3 3 7971.74 8128.41 149.98 o 3 3 3 5097.46 5298.31 88.60 o 4 3 3 278.43 346.10 16.98 o 5 3 3 626.84 603.69 17.36 o 6 3 3 26.50 20.85 11.26 o 7 3 3 451.89 445.97 18.45 o 8 3 3 727.36 871.91 35.12 o 9 3 3 605.03 621.93 70.52 o 10 3 3 33.54 34.46 25.68 o 11 3 3 31.70 34.80 27.64 o 12 3 3 51.48 31.14 42.83 o 13 3 3 16.74 -19.10 51.47 o 0 4 3 27092.53 28738.88 851.13 o 1 4 3 2279.74 2114.63 41.12 o 2 4 3 12013.10 13005.51 237.93 o 3 4 3 2631.14 2505.59 46.59 o 4 4 3 7892.76 8238.77 137.07 o 5 4 3 426.80 503.43 14.78 o 6 4 3 1449.11 1189.99 38.33 o 7 4 3 5722.10 5856.69 145.44 o 8 4 3 2202.04 2158.80 107.78 o 9 4 3 133.50 139.20 25.94 o 10 4 3 254.08 319.59 32.01 o 11 4 3 27.28 63.01 39.04 o 12 4 3 28.07 14.13 33.96 o 1 5 3 9614.27 9769.87 192.08 o 2 5 3 713.58 812.90 18.48 o 3 5 3 21550.77 23365.81 425.79 o 4 5 3 109.95 109.79 10.68 o 5 5 3 4133.46 4042.79 79.79 o 6 5 3 758.19 678.78 28.07 o 7 5 3 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6 12 12 4.35 53.59 34.00 o 7 12 12 40.88 74.15 50.68 o 1 13 12 228.97 259.35 44.11 o 2 13 12 24.90 28.30 31.25 o 3 13 12 83.73 51.24 65.12 o 4 13 12 67.73 92.34 33.30 o 5 13 12 51.36 107.61 42.35 o 0 14 12 101.53 95.45 68.58 o 1 14 12 7.21 -24.38 48.08 o 2 14 12 11.61 -28.07 38.77 o 3 14 12 11.45 9.04 45.10 o 4 14 12 6.84 -21.13 49.16 o 1 1 13 3835.66 4046.27 69.33 o 2 1 13 576.53 573.19 13.94 o 3 1 13 2040.80 2004.42 38.48 o 4 1 13 4407.70 4118.56 84.94 o 5 1 13 149.97 88.20 10.66 o 6 1 13 2.80 12.36 9.78 o 7 1 13 606.22 518.56 23.65 o 8 1 13 0.86 28.90 15.69 o 9 1 13 319.23 289.96 29.41 o 10 1 13 125.12 143.26 44.56 o 11 1 13 361.41 407.41 37.74 o 12 1 13 8.76 -8.02 39.06 o 0 2 13 3562.64 3472.36 85.08 o 1 2 13 553.55 540.84 13.72 o 2 2 13 358.41 469.95 16.64 o 3 2 13 4450.43 4568.31 87.91 o 4 2 13 162.40 106.10 7.97 o 5 2 13 334.95 200.22 11.78 o 6 2 13 1581.69 1512.39 42.40 o 7 2 13 586.50 584.76 25.01 o 8 2 13 57.84 36.10 16.33 o 9 2 13 92.73 165.66 21.49 o 10 2 13 70.36 26.15 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