#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/45/2214541.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214541_Fobs loop_ _publ_author_name 'Yang, E.' 'Song, Xu-Chun' 'Lin, You-Dan' 'Shen, Shuang-Zhen' _publ_section_title ; Poly[(\m~2~-1,3-di-4-pyridylpropane-\k^2^N:N')(\m~2~-terephthalato-\k^2^O:O')zinc(II)] ; _journal_coeditor_code BT2419 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2067 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.7563 _cell_length_b 16.3925 _cell_length_c 19.7019 _exptl_crystal_F_000 1760.00 _reflns_d_resolution_high 0.8401 _[local]_cod_data_source_file bt2419Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 534.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 115658.92 118663.47 3754.13 o 4 0 0 15239.35 16989.58 709.46 o 6 0 0 10376.04 10610.93 426.60 o 8 0 0 2138.24 1925.67 223.06 o 10 0 0 1126.06 1042.45 216.69 o 12 0 0 6690.76 6621.45 483.63 o 2 1 0 59885.54 65138.30 830.97 o 4 1 0 7503.77 6360.69 133.81 o 6 1 0 4995.00 5755.65 125.94 o 8 1 0 2650.66 2456.31 174.43 o 10 1 0 592.75 549.32 130.01 o 12 1 0 473.29 238.97 125.81 o 0 2 0 10751.41 8226.61 114.58 o 2 2 0 48254.86 50327.60 680.66 o 4 2 0 5026.29 4992.40 135.41 o 6 2 0 3400.24 3900.24 114.38 o 8 2 0 103.27 147.20 78.99 o 10 2 0 5300.19 5139.63 265.82 o 12 2 0 771.40 812.35 170.75 o 2 3 0 2865.91 1867.71 234.60 o 4 3 0 791.24 618.56 47.70 o 6 3 0 24714.05 25549.71 499.69 o 8 3 0 5288.19 5155.19 236.73 o 10 3 0 8096.22 7747.84 320.18 o 12 3 0 4717.19 4547.21 296.63 o 0 4 0 14336.45 13556.97 260.81 o 2 4 0 11605.52 10962.84 131.98 o 4 4 0 92542.18 99346.48 1459.27 o 6 4 0 3428.83 3529.34 128.22 o 8 4 0 27.24 24.27 68.57 o 10 4 0 2474.05 2802.70 214.02 o 12 4 0 1399.07 1379.00 177.57 o 2 5 0 2564.80 2257.27 64.90 o 4 5 0 12536.09 12589.67 169.59 o 6 5 0 2899.49 3181.42 114.22 o 8 5 0 2109.06 2395.96 176.72 o 10 5 0 14.38 58.61 81.31 o 12 5 0 606.51 484.84 130.37 o 0 6 0 19144.83 18505.31 367.50 o 2 6 0 360.05 411.61 40.77 o 4 6 0 24609.50 24970.19 1483.33 o 6 6 0 439.98 571.37 53.15 o 8 6 0 114.63 92.74 73.72 o 10 6 0 32.42 23.06 80.20 o 12 6 0 2651.23 2675.53 254.83 o 2 7 0 3522.56 3569.48 94.87 o 4 7 0 10079.51 10343.06 173.01 o 6 7 0 7688.12 7687.33 149.91 o 8 7 0 5848.82 5755.43 233.14 o 10 7 0 1961.38 1608.04 193.00 o 12 7 0 1161.31 850.78 179.98 o 0 8 0 2841.86 2413.23 128.59 o 2 8 0 31639.28 32775.25 284.04 o 4 8 0 4521.12 4569.26 113.72 o 6 8 0 19.31 26.58 40.87 o 8 8 0 32.29 -13.67 71.01 o 10 8 0 4069.70 3916.48 366.29 o 12 8 0 1704.08 1817.62 232.48 o 2 9 0 1389.96 1551.76 74.61 o 4 9 0 5.48 15.72 35.84 o 6 9 0 2849.44 2613.39 100.77 o 8 9 0 10.03 64.94 90.13 o 10 9 0 52.40 -4.23 106.05 o 12 9 0 291.69 274.30 150.10 o 0 10 0 3743.65 3203.22 163.87 o 2 10 0 2894.16 2980.15 101.73 o 4 10 0 4702.57 4459.42 129.79 o 6 10 0 131.48 144.82 52.49 o 8 10 0 210.41 144.47 87.52 o 10 10 0 2286.99 2040.30 214.82 o 12 10 0 811.85 736.85 265.71 o 2 11 0 1024.53 1070.12 78.10 o 4 11 0 10259.08 10331.81 197.84 o 6 11 0 2484.89 2699.30 118.64 o 8 11 0 15374.28 15083.63 390.99 o 10 11 0 5762.43 5685.60 380.03 o 0 12 0 133.64 112.76 78.62 o 2 12 0 1824.97 1750.08 109.65 o 4 12 0 43.97 52.57 51.49 o 6 12 0 24.58 17.04 52.94 o 8 12 0 1620.73 1652.88 187.11 o 10 12 0 533.49 499.53 186.15 o 2 13 0 12.02 0.52 59.87 o 4 13 0 1668.58 1542.03 108.87 o 6 13 0 24.92 -24.25 66.42 o 8 13 0 1700.58 1705.97 196.73 o 10 13 0 1527.95 1670.13 258.10 o 0 14 0 9533.58 9034.31 402.79 o 2 14 0 8353.06 8052.85 269.70 o 4 14 0 2703.20 2781.42 149.91 o 6 14 0 757.52 844.43 109.28 o 8 14 0 53.94 -35.08 124.68 o 2 15 0 490.95 432.78 108.01 o 4 15 0 3441.50 3348.92 201.49 o 6 15 0 6608.79 6579.69 232.38 o 8 15 0 3458.76 3607.16 318.13 o 0 16 0 2.74 97.31 122.27 o 2 16 0 790.51 824.12 135.25 o 4 16 0 100.84 13.06 87.70 o 6 16 0 8.75 51.51 108.24 o 8 16 0 337.04 350.52 310.46 o 2 17 0 37.54 39.39 91.71 o 4 17 0 1280.59 1187.72 157.79 o 6 17 0 395.94 648.33 156.82 o 0 18 0 2673.31 2745.80 301.99 o 2 18 0 3361.41 3179.23 225.57 o 4 18 0 775.95 758.78 149.14 o 2 19 0 178.02 203.47 116.89 o 1 1 1 15341.46 17417.13 218.38 o 2 1 1 1857.97 1646.91 30.86 o 3 1 1 2609.28 2639.17 57.77 o 4 1 1 10670.65 9984.40 131.71 o 5 1 1 3626.53 3777.80 76.29 o 6 1 1 10232.46 11268.15 202.73 o 7 1 1 9.42 -10.94 31.23 o 8 1 1 18772.30 17958.48 291.79 o 9 1 1 1504.86 1431.01 110.98 o 10 1 1 60.50 25.95 62.03 o 11 1 1 41.23 44.52 68.44 o 12 1 1 766.55 856.75 120.31 o 13 1 1 1655.21 1694.91 157.41 o 0 2 1 44927.50 49364.88 628.98 o 1 2 1 10366.15 9882.71 628.59 o 2 2 1 64377.08 62890.26 1962.45 o 3 2 1 1153.78 1004.77 36.38 o 4 2 1 326.83 317.20 28.96 o 5 2 1 15532.42 16146.13 244.94 o 6 2 1 889.17 902.70 45.59 o 7 2 1 7030.85 7292.31 139.87 o 8 2 1 214.31 304.98 64.00 o 9 2 1 5585.60 5602.43 184.92 o 10 2 1 811.62 673.69 96.55 o 11 2 1 1731.93 1922.26 142.24 o 12 2 1 824.50 834.16 119.18 o 13 2 1 92.75 99.73 84.05 o 1 3 1 3174.01 3438.25 50.27 o 2 3 1 64259.70 70094.84 584.84 o 3 3 1 52196.27 55076.71 494.00 o 4 3 1 14598.30 14191.49 186.68 o 5 3 1 1042.73 1024.58 48.66 o 6 3 1 324.44 304.73 37.05 o 7 3 1 94.27 93.48 36.08 o 8 3 1 3185.86 3111.02 135.09 o 9 3 1 469.95 357.17 75.81 o 10 3 1 2546.65 2408.03 143.49 o 11 3 1 158.83 113.94 74.55 o 12 3 1 78.28 5.53 70.98 o 13 3 1 1020.34 1080.86 132.17 o 0 4 1 10091.62 13384.43 164.90 o 1 4 1 8048.92 8396.56 81.63 o 2 4 1 345.35 367.61 23.81 o 3 4 1 68.61 71.79 18.12 o 4 4 1 5173.88 5384.46 76.30 o 5 4 1 1387.45 1508.74 52.17 o 6 4 1 49.07 34.34 26.68 o 7 4 1 2344.58 2303.92 82.76 o 8 4 1 81.23 22.86 49.68 o 9 4 1 1853.98 1757.41 113.05 o 10 4 1 195.49 79.02 60.51 o 11 4 1 497.79 454.73 87.49 o 12 4 1 82.82 64.11 74.25 o 13 4 1 48.90 16.80 79.96 o 1 5 1 100.50 95.82 19.54 o 2 5 1 3159.90 2882.23 49.00 o 3 5 1 1963.29 1629.40 92.59 o 4 5 1 23266.73 25449.06 207.86 o 5 5 1 1189.83 1038.09 42.83 o 6 5 1 923.96 946.37 46.26 o 7 5 1 347.59 440.09 47.86 o 8 5 1 5347.54 5102.18 160.11 o 9 5 1 1885.64 1827.30 115.95 o 10 5 1 3784.89 3805.53 163.04 o 11 5 1 1025.00 998.04 112.03 o 12 5 1 2024.51 1974.78 148.01 o 13 5 1 872.89 1030.19 133.18 o 0 6 1 3649.91 3423.53 96.09 o 1 6 1 526.84 579.77 31.65 o 2 6 1 3929.59 3631.41 59.68 o 3 6 1 1824.40 1738.77 50.60 o 4 6 1 4935.75 5194.32 76.82 o 5 6 1 9494.40 9751.05 107.77 o 6 6 1 1090.58 1051.34 49.09 o 7 6 1 4461.61 4307.75 108.79 o 8 6 1 186.80 200.12 60.07 o 9 6 1 3122.06 3054.41 142.44 o 10 6 1 161.56 190.65 69.30 o 11 6 1 788.36 786.90 106.20 o 12 6 1 2053.10 2081.66 154.09 o 13 6 1 836.37 887.63 136.17 o 1 7 1 2338.93 2507.23 58.30 o 2 7 1 1248.19 1092.94 39.72 o 3 7 1 1524.23 1604.24 47.09 o 4 7 1 442.84 497.07 32.82 o 5 7 1 142.50 170.08 27.97 o 6 7 1 7311.56 7880.24 104.73 o 7 7 1 782.99 829.18 57.40 o 8 7 1 2.84 -40.19 48.50 o 9 7 1 1016.42 934.81 98.35 o 10 7 1 262.29 112.46 68.91 o 11 7 1 12.42 36.00 79.18 o 12 7 1 50.05 84.30 86.91 o 13 7 1 36.65 0.39 123.46 o 0 8 1 1021.29 942.95 67.67 o 1 8 1 4989.68 5160.65 82.67 o 2 8 1 1510.29 1615.39 49.46 o 3 8 1 2947.15 3087.65 64.29 o 4 8 1 522.03 540.33 30.88 o 5 8 1 8343.40 8591.51 104.17 o 6 8 1 995.71 836.14 46.55 o 7 8 1 1886.33 1917.28 79.15 o 8 8 1 36.59 1.62 53.89 o 9 8 1 1074.02 1140.79 105.68 o 10 8 1 635.35 620.93 103.67 o 11 8 1 617.30 547.80 108.97 o 12 8 1 1607.51 1304.85 146.39 o 1 9 1 21024.18 21512.45 192.11 o 2 9 1 8.48 14.26 22.67 o 3 9 1 1469.31 1471.04 52.59 o 4 9 1 5513.13 5667.12 91.62 o 5 9 1 957.20 930.32 43.60 o 6 9 1 9840.26 9229.40 220.52 o 7 9 1 638.96 603.66 56.77 o 8 9 1 2985.31 3214.75 155.90 o 9 9 1 247.89 368.64 87.49 o 10 9 1 4786.73 4474.11 202.80 o 11 9 1 2521.64 2535.43 173.03 o 12 9 1 877.11 875.86 133.14 o 0 10 1 1183.05 1062.69 77.45 o 1 10 1 237.18 217.78 34.91 o 2 10 1 264.62 273.04 35.72 o 3 10 1 4135.68 4431.55 90.30 o 4 10 1 1653.17 1689.21 61.63 o 5 10 1 1566.33 1504.53 56.41 o 6 10 1 5.41 5.16 32.06 o 7 10 1 1892.03 1882.10 100.66 o 8 10 1 372.87 308.65 81.29 o 9 10 1 3566.64 3439.13 173.62 o 10 10 1 32.74 37.27 74.75 o 11 10 1 115.70 81.06 88.84 o 12 10 1 242.15 214.20 147.68 o 1 11 1 200.58 200.71 41.68 o 2 11 1 75.46 73.03 35.19 o 3 11 1 819.90 786.69 50.96 o 4 11 1 1028.45 1054.73 58.28 o 5 11 1 1137.42 1260.57 63.75 o 6 11 1 138.91 64.77 39.24 o 7 11 1 23.39 -4.67 42.67 o 8 11 1 330.84 319.44 89.84 o 9 11 1 279.24 211.78 91.56 o 10 11 1 51.02 86.72 91.49 o 11 11 1 34.71 -26.33 90.18 o 0 12 1 4182.79 4424.46 169.36 o 1 12 1 126.73 161.98 42.74 o 2 12 1 6010.74 5930.02 130.57 o 3 12 1 110.77 124.34 40.90 o 4 12 1 4988.60 5045.69 113.50 o 5 12 1 6099.41 6108.16 125.69 o 6 12 1 403.45 368.65 51.62 o 7 12 1 2676.02 2654.71 110.38 o 8 12 1 450.57 321.23 92.55 o 9 12 1 4073.87 3790.37 221.97 o 10 12 1 40.72 99.42 104.98 o 11 12 1 1041.87 1006.72 164.72 o 1 13 1 760.04 733.64 72.59 o 2 13 1 1180.41 1228.37 83.97 o 3 13 1 2432.41 2372.79 93.81 o 4 13 1 723.39 696.74 60.86 o 5 13 1 3456.21 3461.37 104.92 o 6 13 1 10743.41 10769.44 179.69 o 7 13 1 165.90 134.58 61.60 o 8 13 1 1976.88 2229.04 162.47 o 9 13 1 604.38 453.48 134.86 o 10 13 1 1477.25 1524.40 220.51 o 0 14 1 801.84 886.42 121.86 o 1 14 1 72.68 53.06 53.98 o 2 14 1 51.09 31.98 53.56 o 3 14 1 605.46 579.35 73.83 o 4 14 1 12.14 9.33 47.29 o 5 14 1 1585.08 1601.42 86.76 o 6 14 1 154.27 117.72 55.93 o 7 14 1 1549.08 1362.16 110.82 o 8 14 1 12.06 15.74 91.38 o 9 14 1 10.31 -5.29 124.79 o 1 15 1 2105.77 1989.37 116.30 o 2 15 1 489.90 348.86 71.77 o 3 15 1 981.26 990.63 93.66 o 4 15 1 232.51 262.33 69.70 o 5 15 1 937.98 891.17 87.47 o 6 15 1 516.44 527.04 81.96 o 7 15 1 231.68 265.10 85.50 o 8 15 1 639.80 846.85 145.57 o 0 16 1 5308.71 4808.46 236.29 o 1 16 1 818.10 704.11 89.44 o 2 16 1 2550.06 2583.29 134.44 o 3 16 1 1139.29 1092.72 103.43 o 4 16 1 1725.12 1957.88 123.31 o 5 16 1 759.99 765.03 95.96 o 6 16 1 1761.55 1915.67 132.68 o 7 16 1 1165.16 1398.10 155.00 o 1 17 1 1444.38 1407.56 114.00 o 2 17 1 544.75 505.98 87.79 o 3 17 1 216.97 238.18 74.70 o 4 17 1 873.79 901.52 104.13 o 5 17 1 289.26 244.85 80.23 o 6 17 1 1443.08 1451.74 137.17 o 0 18 1 8.29 -27.43 92.68 o 1 18 1 0.65 -26.67 65.17 o 2 18 1 111.27 82.71 72.34 o 3 18 1 97.02 61.77 72.25 o 4 18 1 3.45 -19.61 69.31 o 5 18 1 248.13 252.66 86.72 o 1 19 1 1543.45 1582.27 131.61 o 2 19 1 209.68 91.90 76.81 o 3 19 1 2064.98 2157.99 146.32 o 0 0 2 3033.20 2798.78 232.34 o 1 0 2 67.53 149.59 20.76 o 2 0 2 552.30 329.39 27.53 o 3 0 2 3666.66 3538.49 104.47 o 4 0 2 2.71 -29.08 34.61 o 5 0 2 19135.09 18935.30 359.60 o 6 0 2 1159.04 1095.00 88.00 o 7 0 2 26329.06 27118.92 515.85 o 8 0 2 30.25 5.57 64.66 o 9 0 2 5672.70 5945.60 266.44 o 10 0 2 16.92 71.64 95.03 o 11 0 2 15566.51 15375.81 469.57 o 12 0 2 70.82 -17.77 99.77 o 13 0 2 1961.35 1837.06 200.70 o 1 1 2 16772.35 17811.83 300.14 o 2 1 2 2053.47 2067.63 39.46 o 3 1 2 14644.36 14459.96 115.97 o 4 1 2 1261.60 1024.99 49.93 o 5 1 2 4053.46 4490.89 112.42 o 6 1 2 743.44 905.21 57.78 o 7 1 2 2726.21 2808.00 95.96 o 8 1 2 50.40 87.58 52.96 o 9 1 2 70.91 54.59 56.57 o 10 1 2 103.73 -7.34 59.65 o 11 1 2 624.04 635.36 101.04 o 12 1 2 717.02 631.05 104.21 o 13 1 2 1454.00 1653.61 148.99 o 0 2 2 7097.74 5782.29 85.13 o 1 2 2 4891.77 4348.90 243.64 o 2 2 2 188.65 216.15 22.30 o 3 2 2 1284.09 1186.00 38.64 o 4 2 2 2828.35 2777.56 51.42 o 5 2 2 1346.56 1648.65 52.99 o 6 2 2 449.57 509.88 38.14 o 7 2 2 3083.71 3124.09 101.10 o 8 2 2 5.53 -12.62 47.72 o 9 2 2 172.62 204.68 68.29 o 10 2 2 604.86 589.51 93.46 o 11 2 2 39.78 5.52 64.02 o 12 2 2 91.05 46.39 73.15 o 13 2 2 3.43 21.92 77.61 o 1 3 2 97730.12 103328.89 1183.44 o 2 3 2 18916.86 17726.11 687.67 o 3 3 2 82975.32 86696.18 1047.18 o 4 3 2 1574.57 1615.30 47.30 o 5 3 2 13507.59 13941.92 180.78 o 6 3 2 191.65 166.99 29.19 o 7 3 2 1130.89 1212.58 69.83 o 8 3 2 10.63 -0.21 44.86 o 9 3 2 2014.16 1909.22 116.28 o 10 3 2 11.28 24.44 60.41 o 11 3 2 593.04 524.56 90.73 o 12 3 2 158.71 71.47 76.14 o 13 3 2 1409.95 1548.10 146.74 o 0 4 2 15977.88 17205.26 231.40 o 1 4 2 554.82 622.68 29.32 o 2 4 2 1139.78 923.90 41.08 o 3 4 2 11130.73 11403.23 115.42 o 4 4 2 2981.70 3342.37 64.58 o 5 4 2 15398.74 15945.30 145.67 o 6 4 2 542.81 560.37 37.17 o 7 4 2 5839.57 5783.49 131.58 o 8 4 2 350.61 454.81 70.45 o 9 4 2 2624.42 2672.45 132.33 o 10 4 2 883.73 756.31 94.94 o 11 4 2 1775.05 1781.67 130.45 o 12 4 2 100.66 125.74 77.89 o 13 4 2 20.53 34.64 87.22 o 1 5 2 19322.74 19948.05 146.64 o 2 5 2 2770.06 3679.77 57.20 o 3 5 2 15968.15 16396.25 155.29 o 4 5 2 3908.26 3712.91 87.12 o 5 5 2 7688.71 8363.83 115.15 o 6 5 2 1232.85 1453.83 54.92 o 7 5 2 306.80 334.68 42.94 o 8 5 2 434.85 533.75 75.26 o 9 5 2 2.35 36.80 55.98 o 10 5 2 0.44 20.27 61.23 o 11 5 2 1493.15 1376.36 124.13 o 12 5 2 56.43 23.14 79.61 o 13 5 2 1174.76 1084.04 143.50 o 0 6 2 3546.87 4446.23 90.39 o 1 6 2 16492.82 16930.15 134.37 o 2 6 2 902.21 874.74 34.98 o 3 6 2 20781.37 21403.54 488.20 o 4 6 2 45.39 41.31 19.70 o 5 6 2 87.15 64.43 24.62 o 6 6 2 29.92 38.33 26.19 o 7 6 2 4266.24 4261.48 103.16 o 8 6 2 212.04 213.94 62.13 o 9 6 2 6045.28 6134.69 187.38 o 10 6 2 70.89 89.12 68.14 o 11 6 2 1185.44 1075.52 124.86 o 12 6 2 2.28 -52.80 77.89 o 13 6 2 19.01 -25.64 85.19 o 1 7 2 18417.27 17199.77 141.39 o 2 7 2 638.61 732.21 34.93 o 3 7 2 5575.31 5498.06 76.72 o 4 7 2 1961.11 1863.32 57.40 o 5 7 2 1792.20 1807.23 55.08 o 6 7 2 881.41 1000.92 50.36 o 7 7 2 944.99 935.40 61.55 o 8 7 2 16.62 5.30 54.36 o 9 7 2 1150.80 1136.52 110.72 o 10 7 2 4.36 -2.58 64.83 o 11 7 2 4378.74 4066.68 187.29 o 12 7 2 0.06 -16.03 79.51 o 13 7 2 2688.18 2892.97 282.48 o 0 8 2 519.03 500.81 55.86 o 1 8 2 2.78 -2.88 22.52 o 2 8 2 460.59 525.31 35.25 o 3 8 2 2782.07 2708.60 62.22 o 4 8 2 5.96 -9.94 20.89 o 5 8 2 5004.04 5147.25 86.25 o 6 8 2 19.79 35.69 29.92 o 7 8 2 10537.80 10988.44 202.65 o 8 8 2 0.75 -10.14 49.49 o 9 8 2 5206.25 5406.05 185.50 o 10 8 2 11.35 53.66 72.15 o 11 8 2 619.08 623.68 111.95 o 12 8 2 15.84 -39.57 82.34 o 1 9 2 55.45 42.09 25.76 o 2 9 2 629.55 675.01 39.62 o 3 9 2 1587.75 1756.87 56.07 o 4 9 2 224.76 265.37 35.22 o 5 9 2 1017.56 953.70 41.89 o 6 9 2 230.40 242.53 35.19 o 7 9 2 1005.70 1034.12 70.88 o 8 9 2 48.71 59.47 55.33 o 9 9 2 12.96 10.18 66.85 o 10 9 2 10.94 27.93 73.38 o 11 9 2 122.09 104.44 86.47 o 12 9 2 3.08 -1.83 90.77 o 0 10 2 513.50 575.71 66.72 o 1 10 2 1779.63 2114.78 68.79 o 2 10 2 428.15 521.72 42.90 o 3 10 2 1191.22 1146.77 53.83 o 4 10 2 46.66 49.98 30.78 o 5 10 2 9579.51 9131.50 167.03 o 6 10 2 106.96 105.48 36.04 o 7 10 2 7691.40 8275.33 193.25 o 8 10 2 172.21 134.59 66.37 o 9 10 2 2249.37 2154.72 158.36 o 10 10 2 21.86 -13.18 81.44 o 11 10 2 684.14 724.84 131.90 o 1 11 2 18291.84 18368.81 200.36 o 2 11 2 775.08 725.38 54.87 o 3 11 2 13290.68 13263.00 168.09 o 4 11 2 202.24 186.40 37.85 o 5 11 2 946.78 936.47 60.23 o 6 11 2 20.70 -11.55 34.03 o 7 11 2 904.11 804.40 74.53 o 8 11 2 6.70 -49.03 62.64 o 9 11 2 355.35 401.20 112.34 o 10 11 2 96.39 129.36 94.73 o 11 11 2 1888.85 1716.18 171.24 o 0 12 2 563.06 515.46 82.59 o 1 12 2 3069.78 3249.73 110.53 o 2 12 2 1.29 -6.04 36.37 o 3 12 2 3635.13 3702.14 105.07 o 4 12 2 1100.40 1068.87 67.32 o 5 12 2 17.53 -19.00 38.64 o 6 12 2 8.21 20.27 42.64 o 7 12 2 1440.11 1341.47 92.48 o 8 12 2 76.08 95.53 86.88 o 9 12 2 468.42 366.59 122.83 o 10 12 2 3.60 -14.53 105.63 o 1 13 2 896.75 821.68 74.70 o 2 13 2 12.80 39.45 46.68 o 3 13 2 1293.95 1231.12 85.11 o 4 13 2 9.12 7.58 40.38 o 5 13 2 6.76 -12.92 41.34 o 6 13 2 37.80 -16.80 46.89 o 7 13 2 240.85 253.20 68.77 o 8 13 2 114.40 60.70 84.08 o 9 13 2 234.08 277.30 125.49 o 10 13 2 4.24 18.11 112.17 o 0 14 2 228.94 103.96 83.27 o 1 14 2 621.38 606.37 78.64 o 2 14 2 427.03 310.54 62.75 o 3 14 2 2906.76 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13 788.75 794.15 135.67 o 10 8 13 270.53 518.98 203.14 o 1 9 13 966.70 1090.10 118.91 o 2 9 13 526.29 556.26 101.21 o 3 9 13 2709.80 2728.50 163.52 o 4 9 13 1461.18 1394.06 130.83 o 5 9 13 60.65 42.82 81.46 o 6 9 13 4695.16 4791.04 259.00 o 7 9 13 69.63 51.22 91.08 o 8 9 13 2170.84 2110.17 187.59 o 9 9 13 248.23 174.66 114.22 o 0 10 13 4991.16 5065.38 289.10 o 1 10 13 2.12 -42.94 66.04 o 2 10 13 1434.71 1436.54 135.11 o 3 10 13 220.63 197.16 83.69 o 4 10 13 129.13 114.38 79.18 o 5 10 13 654.91 661.38 124.59 o 6 10 13 85.08 54.45 89.80 o 7 10 13 551.56 595.65 128.56 o 8 10 13 96.48 -36.04 91.61 o 9 10 13 141.97 201.87 128.69 o 1 11 13 57.60 37.53 76.81 o 2 11 13 14.58 78.08 81.05 o 3 11 13 74.60 30.28 79.01 o 4 11 13 81.41 58.56 85.32 o 5 11 13 349.36 407.15 103.84 o 6 11 13 2166.10 2434.11 191.99 o 7 11 13 581.17 551.52 130.97 o 8 11 13 320.69 427.23 130.79 o 0 12 13 5524.29 5814.97 416.78 o 1 12 13 0.71 -46.55 74.63 o 2 12 13 4249.26 4108.62 209.58 o 3 12 13 596.95 461.35 107.79 o 4 12 13 344.85 403.77 98.61 o 5 12 13 392.31 443.48 111.33 o 6 12 13 344.83 287.35 112.73 o 7 12 13 582.26 518.76 136.18 o 1 13 13 911.50 910.55 132.04 o 2 13 13 751.76 701.82 114.69 o 3 13 13 20.29 -5.55 78.65 o 4 13 13 3461.34 3612.64 194.79 o 5 13 13 384.91 346.81 112.53 o 6 13 13 913.83 991.72 158.71 o 0 14 13 211.34 217.05 132.07 o 1 14 13 788.66 721.97 130.21 o 2 14 13 3.55 24.78 83.95 o 3 14 13 178.72 68.30 88.93 o 4 14 13 202.61 156.26 95.64 o 5 14 13 113.46 56.93 102.79 o 1 15 13 97.72 51.74 86.55 o 2 15 13 727.74 719.55 118.08 o 3 15 13 264.62 176.47 93.96 o 4 15 13 477.90 480.99 119.52 o 0 16 13 2240.85 2685.81 271.59 o 1 16 13 0.93 0.62 94.52 o 2 16 13 3839.86 3519.91 427.72 o 0 0 14 84.56 121.59 86.18 o 1 0 14 318.19 357.53 82.59 o 2 0 14 587.44 398.75 100.53 o 3 0 14 1246.57 1230.77 137.50 o 4 0 14 145.94 132.58 88.34 o 5 0 14 6953.12 7097.07 289.56 o 6 0 14 947.37 966.43 144.84 o 7 0 14 8298.46 7969.68 329.58 o 8 0 14 2582.01 2370.58 213.09 o 9 0 14 2886.73 3260.39 296.56 o 10 0 14 856.27 863.52 259.06 o 11 0 14 814.49 743.77 255.41 o 1 1 14 7447.08 7008.73 163.32 o 2 1 14 16.28 18.28 45.39 o 3 1 14 7866.86 7974.24 238.75 o 4 1 14 513.63 585.21 81.53 o 5 1 14 2027.10 1858.15 128.15 o 6 1 14 49.54 31.54 63.28 o 7 1 14 167.46 126.95 78.35 o 8 1 14 619.71 623.81 111.26 o 9 1 14 34.87 3.53 76.77 o 10 1 14 1435.03 1470.92 168.87 o 11 1 14 138.02 280.17 177.47 o 0 2 14 701.66 747.19 101.08 o 1 2 14 54.26 66.69 46.94 o 2 2 14 1488.99 1550.37 97.18 o 3 2 14 116.26 140.19 60.59 o 4 2 14 863.13 963.68 92.47 o 5 2 14 1238.94 1203.04 110.61 o 6 2 14 1858.50 1629.62 132.91 o 7 2 14 3052.37 3021.40 171.57 o 8 2 14 514.04 596.55 109.88 o 9 2 14 767.14 761.11 107.68 o 10 2 14 140.58 96.03 97.34 o 11 2 14 5.17 -29.06 114.78 o 1 3 14 6454.37 6207.63 158.88 o 2 3 14 188.89 144.13 51.45 o 3 3 14 2938.08 2841.56 132.94 o 4 3 14 803.10 660.39 81.14 o 5 3 14 56.68 -13.24 69.64 o 6 3 14 2976.57 3072.75 182.55 o 7 3 14 308.05 326.37 99.11 o 8 3 14 72.16 67.85 90.49 o 9 3 14 1552.45 1462.20 138.82 o 10 3 14 120.67 96.62 103.59 o 11 3 14 1323.25 850.72 187.11 o 0 4 14 172.87 184.85 76.93 o 1 4 14 1398.01 1365.25 88.55 o 2 4 14 199.31 170.77 59.72 o 3 4 14 11430.68 12020.03 273.00 o 4 4 14 1300.10 937.82 162.95 o 5 4 14 12306.46 12957.11 462.29 o 6 4 14 43.26 39.29 86.94 o 7 4 14 7374.30 7664.17 279.08 o 8 4 14 424.87 394.88 103.15 o 9 4 14 4503.64 4572.88 208.63 o 10 4 14 266.41 221.18 114.64 o 1 5 14 854.71 779.06 83.71 o 2 5 14 12.75 45.52 58.45 o 3 5 14 1837.31 2037.58 123.89 o 4 5 14 695.21 688.64 93.13 o 5 5 14 222.94 250.25 96.29 o 6 5 14 610.38 679.06 129.80 o 7 5 14 500.22 616.95 119.20 o 8 5 14 100.53 95.85 90.59 o 9 5 14 7.09 17.56 87.37 o 10 5 14 7.40 -14.75 112.03 o 0 6 14 24.10 -5.26 78.83 o 1 6 14 196.07 271.42 72.94 o 2 6 14 342.50 397.82 87.93 o 3 6 14 931.87 930.20 99.59 o 4 6 14 895.17 708.25 123.64 o 5 6 14 13.70 -1.35 82.22 o 6 6 14 6.12 50.42 87.01 o 7 6 14 304.77 256.69 100.28 o 8 6 14 0.99 -22.83 85.30 o 9 6 14 879.17 838.66 148.26 o 10 6 14 16.82 -35.81 111.78 o 1 7 14 8737.81 8628.89 233.48 o 2 7 14 398.36 435.96 92.30 o 3 7 14 3299.84 3483.30 174.90 o 4 7 14 216.00 302.62 86.96 o 5 7 14 2586.83 2635.60 178.42 o 6 7 14 92.23 29.56 91.23 o 7 7 14 703.06 606.84 126.43 o 8 7 14 3.68 -0.35 92.79 o 9 7 14 187.38 161.23 110.39 o 10 7 14 19.33 25.08 132.34 o 0 8 14 2400.90 2548.64 206.65 o 1 8 14 575.38 502.91 89.90 o 2 8 14 51.51 91.19 72.01 o 3 8 14 1074.45 1055.50 119.39 o 4 8 14 49.40 -18.83 69.24 o 5 8 14 1730.33 1910.04 178.79 o 6 8 14 106.46 180.43 104.97 o 7 8 14 2725.70 2998.33 204.50 o 8 8 14 1.27 18.62 97.67 o 9 8 14 2220.35 2258.20 202.60 o 1 9 14 332.88 247.25 85.84 o 2 9 14 4.50 12.89 69.74 o 3 9 14 37.47 29.00 73.05 o 4 9 14 25.43 -54.44 70.94 o 5 9 14 147.93 194.93 108.73 o 6 9 14 177.88 237.07 113.97 o 7 9 14 115.99 0.85 91.72 o 8 9 14 4.03 -59.16 104.62 o 9 9 14 5.36 -66.02 122.58 o 0 10 14 2909.26 2839.06 229.09 o 1 10 14 106.58 36.93 76.96 o 2 10 14 435.95 414.07 101.30 o 3 10 14 1303.06 1313.37 136.68 o 4 10 14 102.23 93.20 84.96 o 5 10 14 3063.25 3253.70 233.78 o 6 10 14 100.38 89.80 96.43 o 7 10 14 2157.57 2290.84 199.38 o 8 10 14 9.45 -9.26 102.02 o 1 11 14 4711.60 4683.78 219.05 o 2 11 14 282.07 242.38 95.87 o 3 11 14 2477.73 2706.52 178.50 o 4 11 14 12.70 -46.46 78.54 o 5 11 14 1415.57 1399.95 163.08 o 6 11 14 5.70 38.01 93.22 o 7 11 14 2.02 17.49 101.54 o 0 12 14 2.69 70.58 132.08 o 1 12 14 105.29 53.16 86.57 o 2 12 14 172.93 88.45 89.68 o 3 12 14 377.97 413.26 109.72 o 4 12 14 343.01 433.36 104.82 o 5 12 14 1306.54 1393.93 167.37 o 6 12 14 189.62 199.37 108.26 o 7 12 14 2017.86 2005.73 220.16 o 1 13 14 761.71 754.59 127.48 o 2 13 14 0.24 -38.61 84.99 o 3 13 14 845.30 762.49 125.23 o 4 13 14 22.13 -78.88 87.36 o 5 13 14 448.45 463.72 130.99 o 6 13 14 229.53 308.11 137.19 o 0 14 14 638.27 631.51 197.23 o 1 14 14 143.78 80.59 95.99 o 2 14 14 708.60 637.41 122.75 o 3 14 14 508.96 425.76 111.07 o 4 14 14 774.09 663.74 137.52 o 5 14 14 2012.88 1860.19 276.77 o 1 15 14 2775.78 2872.17 194.12 o 2 15 14 5.92 -26.33 82.14 o 3 15 14 1684.23 2003.62 165.11 o 1 1 15 14240.35 13396.34 304.17 o 2 1 15 3354.38 3131.32 141.74 o 3 1 15 1845.26 2005.84 121.95 o 4 1 15 142.45 159.48 66.83 o 5 1 15 37.93 22.50 67.43 o 6 1 15 400.61 419.56 92.67 o 7 1 15 203.68 250.97 87.90 o 8 1 15 202.41 168.14 91.45 o 9 1 15 802.89 799.80 127.23 o 10 1 15 116.81 87.14 132.15 o 0 2 15 15029.52 14875.25 510.55 o 1 2 15 1033.87 903.38 80.43 o 2 2 15 1842.34 1998.55 110.00 o 3 2 15 2951.99 2941.27 139.68 o 4 2 15 1001.27 712.05 103.91 o 5 2 15 9960.77 9780.58 286.20 o 6 2 15 207.35 219.27 83.44 o 7 2 15 5139.68 5051.69 212.53 o 8 2 15 2.42 36.04 79.96 o 9 2 15 3150.82 3170.42 197.25 o 10 2 15 453.40 411.42 157.61 o 1 3 15 238.45 200.67 57.35 o 2 3 15 144.00 146.54 56.52 o 3 3 15 3813.28 3923.70 172.04 o 4 3 15 662.49 475.84 92.89 o 5 3 15 2137.10 1945.03 170.77 o 6 3 15 147.30 98.24 81.47 o 7 3 15 347.48 334.70 106.30 o 8 3 15 56.63 77.58 89.92 o 9 3 15 718.12 689.36 135.38 o 10 3 15 3.70 24.99 121.89 o 0 4 15 2329.00 2100.04 153.44 o 1 4 15 595.81 559.14 78.27 o 2 4 15 223.79 184.73 64.92 o 3 4 15 11.58 31.90 62.38 o 4 4 15 1014.02 887.58 98.63 o 5 4 15 81.88 32.67 84.51 o 6 4 15 57.29 -18.95 85.42 o 7 4 15 346.03 296.31 102.17 o 8 4 15 118.61 63.45 93.15 o 9 4 15 330.75 334.99 115.24 o 10 4 15 219.70 153.80 114.23 o 1 5 15 5971.54 6189.66 199.10 o 2 5 15 281.91 241.69 74.47 o 3 5 15 3871.48 3838.86 165.80 o 4 5 15 1489.08 1186.35 212.20 o 5 5 15 6046.08 5960.68 265.27 o 6 5 15 1497.51 1773.22 233.81 o 7 5 15 14.72 52.13 87.90 o 8 5 15 936.46 873.37 143.67 o 9 5 15 579.98 560.14 134.24 o 10 5 15 557.39 557.73 174.02 o 0 6 15 2400.20 2292.13 195.89 o 1 6 15 129.01 92.65 65.87 o 2 6 15 2770.47 2670.11 159.20 o 3 6 15 2556.75 2723.10 159.12 o 4 6 15 1885.36 1990.99 136.26 o 5 6 15 4065.10 4294.18 236.33 o 6 6 15 13.17 111.29 97.22 o 7 6 15 3658.65 3701.42 220.14 o 8 6 15 25.47 19.39 98.73 o 9 6 15 1950.67 1906.50 189.22 o 1 7 15 191.41 154.67 72.14 o 2 7 15 47.40 83.45 72.83 o 3 7 15 303.18 350.28 91.46 o 4 7 15 462.03 355.34 94.34 o 5 7 15 603.46 525.75 128.83 o 6 7 15 55.77 48.75 93.85 o 7 7 15 5.86 28.19 91.57 o 8 7 15 20.89 80.31 100.87 o 9 7 15 1023.46 1149.83 168.26 o 0 8 15 529.13 551.00 135.50 o 1 8 15 185.61 159.59 75.06 o 2 8 15 285.49 290.83 89.33 o 3 8 15 333.41 318.63 92.91 o 4 8 15 1717.36 1815.07 149.29 o 5 8 15 871.69 849.10 149.17 o 6 8 15 37.37 -26.50 94.28 o 7 8 15 683.78 643.89 148.97 o 8 8 15 104.53 99.20 118.85 o 9 8 15 689.15 757.87 169.71 o 1 9 15 6356.00 6299.93 236.96 o 2 9 15 14.88 -34.62 74.03 o 3 9 15 1803.21 1781.81 151.81 o 4 9 15 602.29 719.09 118.36 o 5 9 15 1073.99 1115.52 167.63 o 6 9 15 288.29 443.74 135.00 o 7 9 15 1069.54 933.21 154.38 o 8 9 15 1188.42 1363.19 175.76 o 0 10 15 97.01 60.03 104.14 o 1 10 15 205.71 174.49 88.76 o 2 10 15 1260.29 1236.70 139.28 o 3 10 15 792.78 768.42 123.06 o 4 10 15 456.92 587.11 116.60 o 5 10 15 22.20 12.78 102.16 o 6 10 15 60.71 -98.49 98.49 o 7 10 15 767.48 788.48 147.15 o 8 10 15 43.58 -101.10 113.75 o 1 11 15 397.12 421.28 108.38 o 2 11 15 10.41 -16.02 82.60 o 3 11 15 593.59 362.82 107.81 o 4 11 15 367.84 326.93 113.88 o 5 11 15 1333.59 1126.90 174.95 o 6 11 15 18.33 2.37 99.67 o 7 11 15 167.51 81.61 115.52 o 0 12 15 447.49 349.90 169.63 o 1 12 15 1.41 -19.62 83.34 o 2 12 15 361.43 195.21 101.55 o 3 12 15 671.83 658.78 127.52 o 4 12 15 69.38 65.17 106.97 o 5 12 15 1444.74 1467.91 176.66 o 6 12 15 75.99 -41.63 104.38 o 1 13 15 3150.73 2929.60 201.30 o 2 13 15 416.50 388.85 117.60 o 3 13 15 5678.89 6119.35 306.31 o 4 13 15 214.77 220.89 104.97 o 5 13 15 78.56 111.04 122.23 o 0 14 15 6.41 -132.74 132.74 o 1 14 15 67.96 7.49 108.12 o 2 14 15 189.32 183.92 101.91 o 3 14 15 6.26 9.38 93.20 o 0 0 16 4541.34 4582.04 343.28 o 1 0 16 4062.89 3848.48 198.68 o 2 0 16 1534.43 1543.41 159.70 o 3 0 16 5179.74 5768.22 269.63 o 4 0 16 419.90 275.32 96.59 o 5 0 16 3996.47 4188.06 289.74 o 6 0 16 82.91 13.64 100.59 o 7 0 16 1461.48 1446.37 220.04 o 8 0 16 288.10 395.32 161.41 o 9 0 16 693.53 673.79 200.05 o 10 0 16 2623.32 2520.98 297.31 o 1 1 16 3445.12 2871.29 340.02 o 2 1 16 5171.39 5248.75 180.59 o 3 1 16 1053.86 1240.64 108.09 o 4 1 16 1779.42 1386.72 325.56 o 5 1 16 81.96 104.26 79.49 o 6 1 16 1721.54 1897.44 146.81 o 7 1 16 74.07 110.79 84.99 o 8 1 16 6359.21 6460.29 253.66 o 9 1 16 260.38 286.72 117.79 o 10 1 16 2898.16 3065.59 245.90 o 0 2 16 690.07 397.45 174.20 o 1 2 16 4720.80 4588.58 149.67 o 2 2 16 3237.63 3216.23 141.10 o 3 2 16 796.75 754.36 94.78 o 4 2 16 2522.03 1400.58 422.43 o 5 2 16 122.94 60.59 86.93 o 6 2 16 25.81 101.93 85.78 o 7 2 16 23.04 78.07 91.07 o 8 2 16 162.91 75.60 96.13 o 9 2 16 148.81 108.92 105.16 o 10 2 16 0.44 -57.62 141.62 o 1 3 16 155.92 118.61 52.58 o 2 3 16 918.58 996.84 96.84 o 3 3 16 1613.21 1728.55 133.04 o 4 3 16 4613.48 3786.40 532.56 o 5 3 16 15.81 29.61 86.42 o 6 3 16 5053.74 5108.86 259.62 o 7 3 16 328.35 272.79 103.08 o 8 3 16 2073.23 2247.52 188.82 o 9 3 16 6.66 -49.51 95.46 o 0 4 16 6539.02 6222.51 282.85 o 1 4 16 5.35 31.74 58.57 o 2 4 16 8758.70 8513.16 215.08 o 3 4 16 1177.80 1252.18 113.31 o 4 4 16 3419.83 2893.28 455.05 o 5 4 16 16.44 -1.61 85.50 o 6 4 16 181.85 160.36 102.75 o 7 4 16 339.34 381.50 114.94 o 8 4 16 308.74 370.14 119.00 o 9 4 16 56.28 36.91 105.69 o 1 5 16 20.59 -9.54 61.07 o 2 5 16 355.73 232.61 85.61 o 3 5 16 139.23 32.38 64.05 o 4 5 16 986.42 961.10 104.33 o 5 5 16 626.64 514.31 125.04 o 6 5 16 1110.79 1319.28 165.67 o 7 5 16 11.29 7.81 90.12 o 8 5 16 341.68 427.32 121.79 o 9 5 16 1.24 -67.32 94.91 o 0 6 16 589.03 788.20 144.16 o 1 6 16 28.08 -36.32 61.66 o 2 6 16 1453.08 1576.29 136.41 o 3 6 16 2547.35 2614.72 164.15 o 4 6 16 404.31 422.03 97.51 o 5 6 16 485.33 437.38 111.35 o 6 6 16 292.03 195.17 112.42 o 7 6 16 6.23 48.11 94.65 o 8 6 16 12.59 -70.98 92.51 o 9 6 16 421.20 421.36 147.66 o 1 7 16 571.09 678.26 101.74 o 2 7 16 1325.67 1454.77 138.45 o 3 7 16 63.20 79.37 80.46 o 4 7 16 5678.77 5996.65 288.85 o 5 7 16 241.13 368.45 119.66 o 6 7 16 5568.14 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