#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214542.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214542_Fobs loop_ _publ_author_name 'Gowda, B. Thimme' 'Foro, Sabine' 'Fuess, Hartmut' _publ_section_title ; 2,2,2-Trichloro-N-(2,4-dichlorophenyl)acetamide ; _journal_coeditor_code BT2420 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3391 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.3060 _cell_length_b 8.6250 _cell_length_c 18.3170 _exptl_crystal_F_000 1216.00 _reflns_d_resolution_high 0.8376 _[local]_cod_data_source_file bt2420Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' G76 PBCA' _shelx_refln_list_code 4 _shelx_f_calc_maximum 306.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4283.19 3717.83 19.41 o 4 0 0 36047.57 29366.93 258.44 o 6 0 0 1980.29 1638.79 19.05 o 8 0 0 6969.94 5134.27 43.32 o 10 0 0 882.15 671.39 18.30 o 12 0 0 51.11 27.20 4.35 o 14 0 0 289.41 345.87 10.89 o 16 0 0 1342.48 1635.26 38.48 o 2 1 0 4907.42 4728.86 24.81 o 4 1 0 7609.36 6882.73 38.17 o 6 1 0 5827.84 5363.15 38.12 o 8 1 0 6763.00 5947.21 47.91 o 10 1 0 28.22 26.25 3.26 o 12 1 0 32.06 46.51 5.03 o 14 1 0 500.35 530.36 16.08 o 16 1 0 113.29 125.45 7.89 o 0 2 0 3964.03 4750.15 28.74 o 2 2 0 9445.47 9857.05 47.39 o 4 2 0 14520.13 13371.88 65.14 o 6 2 0 6.33 19.04 2.18 o 8 2 0 4882.99 4421.51 42.19 o 10 2 0 4464.24 3619.95 45.03 o 12 2 0 64.23 63.93 5.30 o 14 2 0 270.70 228.61 9.94 o 16 2 0 33.14 51.41 7.07 o 2 3 0 2294.55 2196.61 20.93 o 4 3 0 1537.37 1483.22 18.97 o 6 3 0 4367.37 3538.77 34.06 o 8 3 0 10.80 7.89 2.72 o 10 3 0 616.13 573.25 15.82 o 12 3 0 3.75 6.39 4.90 o 14 3 0 340.27 298.02 11.03 o 16 3 0 172.86 239.31 8.58 o 0 4 0 20.49 12.51 2.45 o 2 4 0 865.21 933.49 15.73 o 4 4 0 4016.99 4283.66 37.47 o 6 4 0 154.09 146.03 4.49 o 8 4 0 8143.62 7173.26 63.09 o 10 4 0 5835.57 5075.00 59.23 o 12 4 0 137.55 122.19 6.67 o 14 4 0 515.61 624.43 18.41 o 2 5 0 1278.81 1333.59 21.23 o 4 5 0 3452.18 3303.84 36.15 o 6 5 0 725.52 685.28 17.74 o 8 5 0 1899.46 1604.22 30.33 o 10 5 0 1422.84 1350.64 31.48 o 12 5 0 273.95 273.82 9.94 o 14 5 0 242.55 291.39 9.94 o 0 6 0 10567.75 9961.67 76.91 o 2 6 0 2637.50 2664.14 34.59 o 4 6 0 4052.70 4064.43 44.94 o 6 6 0 101.09 97.82 5.17 o 8 6 0 846.53 847.52 24.44 o 10 6 0 64.29 72.09 6.12 o 12 6 0 31.01 19.86 5.17 o 2 7 0 899.84 806.14 21.03 o 4 7 0 363.24 367.64 11.85 o 6 7 0 343.78 344.32 9.81 o 8 7 0 1303.18 1231.10 30.24 o 10 7 0 228.02 231.71 8.71 o 12 7 0 336.44 392.00 11.85 o 0 8 0 262.57 226.96 7.49 o 2 8 0 5.98 6.80 3.13 o 4 8 0 196.21 179.93 6.40 o 6 8 0 101.86 95.10 5.03 o 8 8 0 72.01 80.12 5.99 o 10 8 0 538.88 537.73 16.92 o 2 9 0 1436.07 1071.71 23.55 o 4 9 0 530.93 398.27 11.86 o 6 9 0 479.77 461.90 13.36 o 8 9 0 1.82 -2.99 2.99 o 0 10 0 33.50 23.39 3.40 o 2 10 0 4.40 1.90 2.72 o 4 10 0 0.52 4.76 5.17 o 1 1 1 0.47 7.59 6.05 o 2 1 1 11341.68 11017.38 34.12 o 3 1 1 471.96 438.32 5.37 o 4 1 1 1389.00 993.94 8.92 o 5 1 1 1481.62 1196.87 24.30 o 6 1 1 2005.49 1642.68 42.29 o 7 1 1 2043.46 1868.12 16.56 o 8 1 1 7218.19 6160.65 66.65 o 9 1 1 2332.28 1802.10 35.18 o 10 1 1 1261.78 1028.32 16.16 o 11 1 1 937.19 758.41 15.45 o 12 1 1 1242.19 1096.39 19.88 o 13 1 1 777.34 708.95 14.95 o 14 1 1 188.45 168.16 15.38 o 15 1 1 388.29 484.86 19.41 o 16 1 1 611.78 816.55 16.87 o 0 2 1 1752.03 1787.24 117.83 o 1 2 1 16321.47 19054.74 70.80 o 2 2 1 245.70 292.96 32.52 o 3 2 1 11159.04 10707.67 248.59 o 4 2 1 819.70 804.37 76.75 o 5 2 1 5323.30 4706.28 80.30 o 6 2 1 105.00 75.60 4.42 o 7 2 1 910.34 744.46 15.04 o 8 2 1 1370.83 1060.65 14.24 o 9 2 1 1110.72 894.24 14.36 o 10 2 1 6018.69 4939.43 65.04 o 11 2 1 37.17 41.00 3.32 o 12 2 1 165.63 118.58 6.12 o 13 2 1 155.95 140.23 5.44 o 14 2 1 587.04 641.14 13.79 o 15 2 1 520.79 557.47 15.68 o 16 2 1 43.63 63.58 4.60 o 1 3 1 24347.56 28287.58 127.01 o 2 3 1 18180.30 20416.55 64.59 o 3 3 1 1733.46 1804.07 16.61 o 4 3 1 6257.64 6148.55 72.48 o 5 3 1 6664.74 6410.43 72.70 o 6 3 1 9655.29 8626.35 117.69 o 7 3 1 362.91 371.93 7.46 o 8 3 1 481.74 460.78 24.95 o 9 3 1 34.49 45.54 4.69 o 10 3 1 338.70 313.31 14.71 o 11 3 1 0.52 -1.90 4.95 o 12 3 1 453.30 385.40 15.74 o 13 3 1 3.23 6.39 5.67 o 14 3 1 31.07 39.00 7.07 o 15 3 1 155.21 187.00 6.54 o 16 3 1 453.65 545.13 11.66 o 0 4 1 2610.08 3088.28 210.00 o 1 4 1 50.00 41.07 2.03 o 2 4 1 55.17 42.41 2.79 o 3 4 1 1231.17 1369.90 13.94 o 4 4 1 2712.67 2469.59 51.97 o 5 4 1 64.12 60.98 5.17 o 6 4 1 237.57 245.95 5.24 o 7 4 1 0.07 0.97 3.46 o 8 4 1 71.43 79.65 3.27 o 9 4 1 10.05 19.20 2.64 o 10 4 1 119.01 108.81 4.05 o 11 4 1 77.59 68.29 3.89 o 12 4 1 4.77 1.62 4.09 o 13 4 1 336.62 343.18 10.49 o 14 4 1 822.29 995.36 66.23 o 15 4 1 60.22 78.97 9.73 o 1 5 1 756.16 728.28 11.62 o 2 5 1 744.56 710.62 27.38 o 3 5 1 32.04 33.08 3.60 o 4 5 1 2011.46 2011.63 54.78 o 5 5 1 567.77 550.53 11.34 o 6 5 1 429.65 411.33 17.44 o 7 5 1 36.15 34.37 2.79 o 8 5 1 100.21 75.65 6.46 o 9 5 1 87.88 94.51 4.27 o 10 5 1 466.66 395.47 19.90 o 11 5 1 91.70 86.49 5.78 o 12 5 1 513.83 483.30 15.74 o 13 5 1 85.29 85.95 5.00 o 14 5 1 3.10 3.68 5.49 o 0 6 1 19039.83 18430.01 997.39 o 1 6 1 429.44 373.50 8.65 o 2 6 1 3.10 1.03 4.21 o 3 6 1 952.74 927.16 14.88 o 4 6 1 1558.66 1465.72 59.74 o 5 6 1 1863.02 1784.46 88.36 o 6 6 1 466.28 448.05 45.45 o 7 6 1 1719.17 1621.01 35.44 o 8 6 1 995.16 930.82 18.31 o 9 6 1 488.54 428.73 12.47 o 10 6 1 10.09 19.20 8.23 o 11 6 1 829.79 819.89 42.26 o 12 6 1 9.09 6.51 5.91 o 13 6 1 0.73 5.35 5.00 o 1 7 1 270.23 235.40 5.12 o 2 7 1 18.55 26.61 7.68 o 3 7 1 1.86 3.95 2.49 o 4 7 1 152.76 155.40 12.25 o 5 7 1 0.32 5.29 5.16 o 6 7 1 115.62 146.38 12.99 o 7 7 1 62.96 60.52 3.80 o 8 7 1 1241.96 1227.62 65.79 o 9 7 1 483.22 519.32 10.87 o 10 7 1 13.82 1.49 4.35 o 11 7 1 33.46 35.85 3.60 o 12 7 1 7.71 21.51 3.31 o 0 8 1 22.08 8.95 7.21 o 1 8 1 40.30 23.02 7.41 o 2 8 1 171.94 170.79 6.87 o 3 8 1 496.77 395.56 8.30 o 4 8 1 133.04 140.56 14.83 o 5 8 1 28.36 32.13 3.02 o 6 8 1 52.49 41.97 3.94 o 7 8 1 12.53 10.46 3.14 o 8 8 1 337.44 326.71 40.25 o 9 8 1 214.85 202.74 8.92 o 10 8 1 244.42 279.45 20.90 o 1 9 1 55.82 33.58 2.82 o 2 9 1 90.62 84.05 13.33 o 3 9 1 26.92 30.99 2.72 o 4 9 1 4.58 4.82 2.70 o 5 9 1 13.35 10.35 4.01 o 6 9 1 74.14 64.22 10.20 o 7 9 1 2.06 1.47 3.46 o 8 9 1 26.22 21.75 2.41 o 0 10 1 66.00 36.12 3.47 o 1 10 1 15.46 9.03 1.81 o 2 10 1 32.52 21.39 2.11 o 3 10 1 42.36 42.87 6.46 o 4 10 1 145.43 114.88 4.63 o 0 0 2 7593.00 6155.02 23.58 o 1 0 2 599.51 599.83 12.69 o 2 0 2 456.70 394.50 5.72 o 3 0 2 23133.89 19098.87 641.54 o 4 0 2 8407.02 7386.78 66.99 o 5 0 2 26932.58 22354.75 90.21 o 6 0 2 24434.39 19958.96 213.61 o 7 0 2 19461.77 16782.79 190.61 o 8 0 2 10437.67 8506.39 64.80 o 9 0 2 4618.01 3758.32 38.12 o 10 0 2 1346.24 1045.22 16.46 o 11 0 2 3545.83 2930.45 30.27 o 12 0 2 2.36 26.70 10.20 o 13 0 2 1.95 17.05 3.27 o 14 0 2 744.19 756.41 24.63 o 15 0 2 12.91 8.98 4.94 o 16 0 2 116.36 98.05 4.85 o 17 0 2 238.76 280.20 21.38 o 1 1 2 1073.29 1055.41 41.70 o 2 1 2 668.85 540.29 7.35 o 3 1 2 27.19 32.55 3.06 o 4 1 2 809.46 748.81 8.33 o 5 1 2 5598.32 4785.37 28.64 o 6 1 2 2804.13 2363.78 17.85 o 7 1 2 2491.98 2302.04 19.14 o 8 1 2 97.47 41.12 2.93 o 9 1 2 4622.17 3484.27 44.80 o 10 1 2 460.70 332.32 6.79 o 11 1 2 106.51 100.47 3.75 o 12 1 2 2292.39 1938.60 28.18 o 13 1 2 1953.65 1821.19 28.13 o 14 1 2 16.64 15.29 3.95 o 15 1 2 70.82 107.13 5.34 o 16 1 2 118.37 149.89 5.72 o 0 2 2 7972.15 9272.28 391.82 o 1 2 2 9620.28 10830.92 264.01 o 2 2 2 2911.57 2867.87 32.23 o 3 2 2 43.51 30.86 2.18 o 4 2 2 23679.51 22805.04 80.34 o 5 2 2 73.05 125.46 8.50 o 6 2 2 3947.74 3433.31 79.80 o 7 2 2 44.80 63.61 8.64 o 8 2 2 328.64 286.01 19.55 o 9 2 2 432.54 362.24 7.80 o 10 2 2 435.05 319.49 10.29 o 11 2 2 136.35 120.20 4.83 o 12 2 2 55.90 71.28 3.83 o 13 2 2 97.93 84.41 5.03 o 14 2 2 1020.66 1098.81 23.24 o 15 2 2 177.13 170.32 6.20 o 16 2 2 161.40 217.92 8.78 o 1 3 2 11638.73 12703.37 277.58 o 2 3 2 129.82 123.34 2.79 o 3 3 2 3541.94 3593.97 90.68 o 4 3 2 96.77 99.06 2.45 o 5 3 2 2012.43 1777.06 16.34 o 6 3 2 77.98 81.63 2.50 o 7 3 2 511.24 478.71 19.16 o 8 3 2 1.29 1.91 2.55 o 9 3 2 217.94 200.66 12.66 o 10 3 2 4.24 7.50 3.19 o 11 3 2 21.65 35.27 3.55 o 12 3 2 1305.51 1344.96 51.71 o 13 3 2 7.77 3.96 6.87 o 14 3 2 12.03 1.24 10.20 o 15 3 2 115.14 131.03 5.39 o 16 3 2 11.49 12.75 3.50 o 0 4 2 4096.07 4582.08 182.09 o 1 4 2 699.71 877.74 29.65 o 2 4 2 1646.72 1620.26 17.53 o 3 4 2 4156.47 4226.24 110.65 o 4 4 2 10760.05 10978.04 211.98 o 5 4 2 2434.05 2157.80 76.04 o 6 4 2 4.57 9.46 1.86 o 7 4 2 290.76 246.16 6.47 o 8 4 2 90.43 77.67 3.27 o 9 4 2 1770.26 1521.19 43.68 o 10 4 2 60.82 55.97 7.35 o 11 4 2 49.88 46.16 3.94 o 12 4 2 352.11 350.43 20.50 o 13 4 2 99.57 82.76 4.98 o 14 4 2 170.22 219.53 6.45 o 15 4 2 357.80 504.90 21.26 o 1 5 2 846.14 988.07 142.18 o 2 5 2 5661.20 6079.37 326.70 o 3 5 2 916.04 1038.64 55.69 o 4 5 2 625.88 551.94 29.81 o 5 5 2 638.96 669.56 67.47 o 6 5 2 352.80 364.31 27.24 o 7 5 2 57.79 63.06 3.29 o 8 5 2 171.04 163.80 14.77 o 9 5 2 4621.09 4294.45 223.51 o 10 5 2 27.94 25.65 3.72 o 11 5 2 14.55 20.39 7.96 o 12 5 2 5.56 -5.75 12.51 o 13 5 2 278.84 266.91 6.84 o 14 5 2 87.76 95.22 8.91 o 0 6 2 806.73 743.84 65.81 o 1 6 2 1465.66 1665.87 136.66 o 2 6 2 10.61 37.47 15.50 o 3 6 2 262.38 282.32 23.56 o 4 6 2 353.20 379.25 18.12 o 5 6 2 597.23 578.73 46.64 o 6 6 2 592.08 589.36 53.05 o 7 6 2 1493.44 1417.13 141.66 o 8 6 2 1030.32 988.98 19.15 o 9 6 2 253.36 227.76 31.72 o 10 6 2 89.87 83.65 10.88 o 11 6 2 219.86 210.85 7.21 o 12 6 2 160.71 162.46 5.62 o 13 6 2 1.17 0.72 4.27 o 1 7 2 132.12 123.58 18.85 o 2 7 2 1004.88 911.24 117.09 o 3 7 2 69.41 42.15 4.62 o 4 7 2 502.06 517.66 84.51 o 5 7 2 316.99 331.73 29.82 o 6 7 2 977.73 925.67 90.36 o 7 7 2 2.86 -0.68 5.33 o 8 7 2 29.05 45.98 4.42 o 9 7 2 336.65 330.89 30.58 o 10 7 2 261.67 235.98 19.61 o 11 7 2 412.19 407.06 15.54 o 12 7 2 68.66 75.63 7.14 o 0 8 2 100.41 83.47 16.12 o 1 8 2 6.65 15.45 9.32 o 2 8 2 6.71 3.05 4.96 o 3 8 2 98.53 104.57 12.24 o 4 8 2 99.90 109.94 24.01 o 5 8 2 513.83 518.49 92.76 o 6 8 2 151.37 156.77 35.18 o 7 8 2 303.95 306.87 58.29 o 8 8 2 105.09 115.87 16.19 o 9 8 2 22.44 25.39 3.02 o 10 8 2 66.19 58.89 7.69 o 1 9 2 1079.10 724.13 22.01 o 2 9 2 273.61 240.40 30.23 o 3 9 2 383.42 345.79 55.59 o 4 9 2 143.54 112.48 23.95 o 5 9 2 492.45 443.59 63.46 o 6 9 2 19.01 9.63 3.21 o 7 9 2 98.11 76.76 3.56 o 8 9 2 21.41 25.37 6.12 o 0 10 2 45.69 23.50 8.23 o 1 10 2 6.14 0.57 2.55 o 2 10 2 53.02 22.47 3.33 o 3 10 2 0.62 2.17 2.59 o 1 1 3 7432.82 7469.73 307.98 o 2 1 3 38220.78 38546.73 114.96 o 3 1 3 17265.19 15869.10 362.08 o 4 1 3 9654.33 8571.62 167.19 o 5 1 3 9335.09 8566.26 259.19 o 6 1 3 34.00 32.25 1.97 o 7 1 3 3819.72 3263.60 74.20 o 8 1 3 132.38 151.20 3.51 o 9 1 3 188.88 190.90 4.36 o 10 1 3 42.48 36.33 2.87 o 11 1 3 331.98 283.88 6.74 o 12 1 3 1285.81 1273.66 23.17 o 13 1 3 55.52 60.06 5.17 o 14 1 3 11.29 6.50 7.07 o 15 1 3 77.77 85.77 4.86 o 16 1 3 308.69 381.64 18.05 o 0 2 3 27040.42 30161.12 1000.88 o 1 2 3 28598.49 33328.46 399.97 o 2 2 3 726.23 609.85 43.14 o 3 2 3 920.25 1028.08 44.56 o 4 2 3 3168.74 2735.45 58.68 o 5 2 3 2785.96 2634.08 19.78 o 6 2 3 288.67 246.03 6.68 o 7 2 3 5656.83 5075.93 178.43 o 8 2 3 4166.30 3662.05 111.75 o 9 2 3 143.59 122.54 8.10 o 10 2 3 12.26 5.26 3.46 o 11 2 3 3267.06 2872.77 33.28 o 12 2 3 57.33 71.52 4.32 o 13 2 3 0.97 -3.79 6.43 o 14 2 3 729.21 842.04 18.09 o 15 2 3 271.50 345.59 7.60 o 16 2 3 779.65 946.52 19.40 o 1 3 3 4083.83 4467.99 30.05 o 2 3 3 1062.53 1076.12 82.61 o 3 3 3 3230.73 3212.76 159.43 o 4 3 3 1224.64 1239.15 51.56 o 5 3 3 743.39 764.55 44.20 o 6 3 3 9710.28 9225.71 352.84 o 7 3 3 7248.09 6450.95 203.13 o 8 3 3 22.35 42.71 7.55 o 9 3 3 347.08 273.18 6.13 o 10 3 3 5522.00 4883.55 312.82 o 11 3 3 514.17 492.38 35.92 o 12 3 3 4017.99 3968.40 195.45 o 13 3 3 6.16 29.39 10.06 o 14 3 3 186.85 210.81 6.19 o 15 3 3 23.51 27.27 3.79 o 16 3 3 17.24 17.37 3.20 o 0 4 3 256.65 262.72 26.77 o 1 4 3 400.66 429.05 23.86 o 2 4 3 448.18 537.45 41.59 o 3 4 3 241.62 256.97 10.15 o 4 4 3 2710.49 2662.22 123.03 o 5 4 3 374.04 395.09 18.06 o 6 4 3 1361.98 1234.30 46.09 o 7 4 3 3178.00 2869.83 190.10 o 8 4 3 839.15 815.04 68.68 o 9 4 3 0.23 5.45 4.69 o 10 4 3 196.70 204.75 19.87 o 11 4 3 1084.65 1063.45 81.25 o 12 4 3 13.43 10.29 5.23 o 13 4 3 10.86 11.54 3.79 o 14 4 3 259.27 277.38 6.94 o 15 4 3 18.06 33.48 8.77 o 1 5 3 700.37 733.60 37.54 o 2 5 3 86.10 131.53 8.03 o 3 5 3 130.45 107.74 12.52 o 4 5 3 56.71 62.66 6.87 o 5 5 3 3430.74 3526.35 173.38 o 6 5 3 147.08 168.69 13.61 o 7 5 3 285.31 282.84 22.54 o 8 5 3 509.17 445.72 18.95 o 9 5 3 2957.02 2734.32 295.16 o 10 5 3 53.45 40.12 5.98 o 11 5 3 198.12 186.65 24.43 o 12 5 3 973.06 974.09 18.05 o 13 5 3 384.89 423.38 25.75 o 14 5 3 224.82 244.63 24.85 o 0 6 3 100.63 90.78 16.53 o 1 6 3 1952.17 1915.59 56.23 o 2 6 3 130.29 135.39 29.94 o 3 6 3 958.20 1070.16 164.64 o 4 6 3 1142.39 1150.31 210.24 o 5 6 3 1603.49 1636.69 243.85 o 6 6 3 1294.67 1445.82 255.23 o 7 6 3 26.45 32.56 9.32 o 8 6 3 1110.18 1149.37 84.81 o 9 6 3 568.89 552.17 56.24 o 10 6 3 116.23 137.52 7.01 o 11 6 3 101.13 94.03 4.66 o 12 6 3 9.82 10.69 3.40 o 13 6 3 83.85 92.54 8.78 o 1 7 3 46.87 45.75 5.17 o 2 7 3 1052.91 1013.04 140.01 o 3 7 3 900.95 932.22 216.86 o 4 7 3 1003.66 986.97 198.99 o 5 7 3 31.35 46.00 3.81 o 6 7 3 20.63 36.35 7.55 o 7 7 3 211.08 206.03 38.86 o 8 7 3 84.28 83.66 18.02 o 9 7 3 20.34 26.92 3.51 o 10 7 3 10.30 6.33 3.16 o 11 7 3 109.19 110.01 8.37 o 12 7 3 6.69 12.87 3.81 o 0 8 3 51.00 153.39 77.26 o 1 8 3 33.14 29.43 6.39 o 2 8 3 51.34 40.89 4.76 o 3 8 3 242.30 217.34 26.61 o 4 8 3 641.79 606.11 118.73 o 5 8 3 116.56 128.41 16.60 o 6 8 3 87.22 109.31 19.79 o 7 8 3 5.22 4.62 5.19 o 8 8 3 65.45 54.17 8.57 o 9 8 3 23.74 30.12 2.88 o 10 8 3 1.96 -1.72 4.40 o 1 9 3 1.71 0.68 3.36 o 2 9 3 3.08 -4.05 4.05 o 3 9 3 91.46 73.56 3.30 o 4 9 3 34.89 29.45 2.64 o 5 9 3 115.48 75.52 3.56 o 6 9 3 0.02 -1.94 3.93 o 7 9 3 0.36 -0.03 4.01 o 0 10 3 5.17 3.15 1.20 o 1 10 3 145.76 76.43 10.14 o 2 10 3 83.90 57.62 5.58 o 3 10 3 165.93 98.93 4.15 o 0 0 4 4061.68 3768.49 75.58 o 1 0 4 16973.92 14503.69 145.98 o 2 0 4 1524.89 1363.97 14.10 o 3 0 4 18421.49 19139.85 236.17 o 4 0 4 38848.88 36710.29 116.84 o 5 0 4 1183.28 998.96 12.94 o 6 0 4 1763.98 1519.19 16.54 o 7 0 4 221.39 152.63 6.67 o 8 0 4 1033.36 1032.10 15.86 o 9 0 4 731.21 593.68 11.52 o 10 0 4 2685.59 2341.87 28.03 o 11 0 4 4286.11 4137.75 266.50 o 12 0 4 324.83 328.13 7.26 o 13 0 4 3138.26 3473.28 137.48 o 14 0 4 607.73 607.20 13.45 o 15 0 4 61.60 55.04 4.05 o 16 0 4 4.36 4.04 3.50 o 1 1 4 2632.50 2306.38 43.47 o 2 1 4 3028.88 2966.22 106.72 o 3 1 4 6741.95 6771.75 192.72 o 4 1 4 880.59 794.71 15.55 o 5 1 4 4909.06 4578.12 120.90 o 6 1 4 516.33 407.85 13.17 o 7 1 4 8991.68 8366.21 57.73 o 8 1 4 864.72 826.43 14.64 o 9 1 4 331.13 323.72 10.83 o 10 1 4 500.64 471.81 9.99 o 11 1 4 32.02 37.81 4.07 o 12 1 4 1.35 1.77 8.29 o 13 1 4 150.61 148.14 7.21 o 14 1 4 41.73 70.12 4.71 o 15 1 4 161.69 174.41 7.01 o 16 1 4 127.41 134.01 6.33 o 0 2 4 93714.27 112403.33 2187.78 o 1 2 4 18687.34 20336.13 1109.82 o 2 2 4 491.63 597.53 11.05 o 3 2 4 12414.00 13353.36 458.29 o 4 2 4 3540.41 3782.00 224.87 o 5 2 4 78.28 57.74 2.61 o 6 2 4 1317.89 1145.37 64.44 o 7 2 4 3583.96 3136.01 165.92 o 8 2 4 3831.57 3453.61 188.88 o 9 2 4 63.22 85.12 12.72 o 10 2 4 1664.89 1544.29 27.07 o 11 2 4 1749.87 1619.70 32.29 o 12 2 4 99.38 96.13 7.75 o 13 2 4 0.34 10.91 6.46 o 14 2 4 30.65 39.11 6.26 o 15 2 4 22.94 25.80 3.74 o 16 2 4 50.11 55.28 6.05 o 1 3 4 1157.72 1165.63 61.05 o 2 3 4 772.78 766.40 21.54 o 3 3 4 504.38 515.42 19.17 o 4 3 4 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45.45 3.12 o 7 8 8 206.59 199.90 4.48 o 8 8 8 0.49 1.53 3.60 o 1 9 8 201.44 214.28 8.30 o 2 9 8 197.07 236.77 5.13 o 3 9 8 561.37 578.21 11.48 o 4 9 8 36.33 39.16 2.74 o 5 9 8 112.94 112.48 3.08 o 1 1 9 1627.92 1657.51 24.10 o 2 1 9 2179.85 2247.58 74.78 o 3 1 9 1333.13 1302.69 33.04 o 4 1 9 2593.62 2304.44 24.54 o 5 1 9 4859.47 4941.84 248.00 o 6 1 9 19.05 21.98 3.03 o 7 1 9 833.65 741.71 46.16 o 8 1 9 142.53 179.42 5.19 o 9 1 9 2211.81 2234.53 30.30 o 10 1 9 4.95 15.06 9.65 o 11 1 9 236.56 209.09 6.40 o 12 1 9 516.16 468.92 10.77 o 13 1 9 528.33 547.16 25.49 o 14 1 9 15.96 14.71 2.77 o 15 1 9 597.34 592.70 21.36 o 0 2 9 9947.55 11674.46 135.56 o 1 2 9 14.57 20.81 3.55 o 2 2 9 1276.53 1255.35 54.67 o 3 2 9 3647.91 3691.37 106.36 o 4 2 9 782.00 893.90 15.84 o 5 2 9 3959.02 3638.01 32.75 o 6 2 9 15.37 11.03 6.87 o 7 2 9 997.26 1024.07 19.08 o 8 2 9 0.23 -2.99 5.58 o 9 2 9 2048.79 1909.43 41.40 o 10 2 9 61.72 58.08 3.99 o 11 2 9 938.73 920.15 19.02 o 12 2 9 55.55 58.48 3.74 o 13 2 9 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5 9 8.15 3.30 4.36 o 6 5 9 274.21 298.13 6.54 o 7 5 9 22.28 25.60 3.62 o 8 5 9 4.33 5.22 4.62 o 9 5 9 351.46 335.63 7.13 o 10 5 9 807.81 786.33 26.42 o 11 5 9 1.16 9.49 3.00 o 12 5 9 166.00 155.78 5.17 o 13 5 9 0.48 4.87 2.61 o 0 6 9 1.79 55.84 32.09 o 1 6 9 2816.86 3103.01 37.00 o 2 6 9 32.52 30.85 3.67 o 3 6 9 346.89 347.48 10.08 o 4 6 9 567.76 597.97 12.55 o 5 6 9 1364.66 1401.31 23.27 o 6 6 9 184.40 218.52 11.70 o 7 6 9 245.51 262.81 6.29 o 8 6 9 276.60 297.37 14.71 o 9 6 9 308.20 245.67 5.68 o 10 6 9 256.56 268.51 6.40 o 11 6 9 105.35 95.86 3.61 o 1 7 9 343.06 371.26 13.28 o 2 7 9 9.21 13.89 10.27 o 3 7 9 4.48 12.52 3.22 o 4 7 9 192.52 213.07 7.08 o 5 7 9 116.57 120.30 4.61 o 6 7 9 365.02 347.08 7.02 o 7 7 9 119.74 128.29 4.27 o 8 7 9 1.58 2.63 2.58 o 9 7 9 590.21 623.10 24.15 o 10 7 9 22.00 32.76 2.35 o 0 8 9 638.63 703.40 15.69 o 1 8 9 4.07 3.74 5.96 o 2 8 9 0.97 -4.04 5.34 o 3 8 9 15.49 18.49 3.07 o 4 8 9 22.53 36.76 3.36 o 5 8 9 429.37 387.43 9.54 o 6 8 9 76.75 100.06 3.56 o 7 8 9 34.14 32.57 2.69 o 8 8 9 4.83 5.63 7.82 o 1 9 9 0.05 -0.08 2.91 o 2 9 9 2.16 2.91 4.08 o 3 9 9 0.05 3.48 3.82 o 4 9 9 3.72 4.74 2.53 o 0 0 10 28062.03 35400.63 970.22 o 1 0 10 9694.10 11585.09 102.02 o 2 0 10 7432.32 8166.97 148.99 o 3 0 10 1608.83 1932.42 63.96 o 4 0 10 2940.85 3124.58 121.49 o 5 0 10 1782.85 1443.65 63.98 o 6 0 10 398.38 393.80 17.37 o 7 0 10 967.75 834.13 18.92 o 8 0 10 2745.29 2676.22 30.63 o 9 0 10 3191.34 2855.99 77.16 o 10 0 10 3018.26 2792.71 168.09 o 11 0 10 1578.72 1356.46 23.70 o 12 0 10 24.71 26.82 4.22 o 13 0 10 523.29 471.08 12.75 o 14 0 10 25.35 20.40 2.99 o 15 0 10 924.11 959.99 36.31 o 1 1 10 4100.65 4650.87 42.63 o 2 1 10 4841.95 5037.36 40.61 o 3 1 10 2971.36 3015.84 102.46 o 4 1 10 60.78 47.45 4.01 o 5 1 10 26.31 51.20 5.17 o 6 1 10 627.47 527.88 11.24 o 7 1 10 107.63 106.21 4.08 o 8 1 10 9.22 12.62 3.22 o 9 1 10 5313.30 5304.57 133.37 o 10 1 10 56.17 63.09 10.75 o 11 1 10 56.05 66.60 4.35 o 12 1 10 109.90 104.97 4.29 o 13 1 10 162.96 138.50 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174.33 14.29 o 3 7 10 357.34 367.27 16.01 o 4 7 10 1.96 6.68 4.90 o 5 7 10 0.73 -4.90 7.55 o 6 7 10 26.96 51.02 3.94 o 7 7 10 177.42 169.28 4.42 o 8 7 10 10.20 5.69 3.06 o 9 7 10 178.19 194.32 4.70 o 0 8 10 218.13 297.26 28.32 o 1 8 10 418.14 459.36 57.85 o 2 8 10 37.27 45.53 4.90 o 3 8 10 57.02 78.76 8.30 o 4 8 10 131.12 175.71 13.00 o 5 8 10 435.71 503.58 17.99 o 6 8 10 5.39 5.80 2.77 o 7 8 10 83.47 72.46 2.93 o 1 9 10 631.48 839.63 83.34 o 2 9 10 153.27 171.49 23.55 o 1 1 11 3205.72 3856.50 121.59 o 2 1 11 2081.73 2168.55 53.85 o 3 1 11 1126.74 1099.58 54.45 o 4 1 11 743.85 655.38 32.22 o 5 1 11 266.81 244.58 10.01 o 6 1 11 1.83 2.36 5.03 o 7 1 11 602.37 518.32 26.32 o 8 1 11 1304.66 1147.34 67.52 o 9 1 11 235.72 243.68 6.01 o 10 1 11 299.02 279.91 12.12 o 11 1 11 177.52 185.86 5.34 o 12 1 11 65.05 49.27 3.41 o 13 1 11 145.97 131.42 4.13 o 14 1 11 460.63 441.36 9.34 o 0 2 11 5.13 19.83 13.46 o 1 2 11 513.04 577.77 16.23 o 2 2 11 251.78 310.63 6.69 o 3 2 11 2305.47 2319.01 34.34 o 4 2 11 61.21 72.68 3.95 o 5 2 11 2995.07 2912.85 105.30 o 6 2 11 3.62 1.66 3.80 o 7 2 11 145.37 114.29 4.52 o 8 2 11 3920.68 3689.95 36.61 o 9 2 11 462.48 469.20 19.96 o 10 2 11 1175.25 1097.25 35.14 o 11 2 11 33.19 31.62 3.49 o 12 2 11 32.47 35.85 4.22 o 13 2 11 14.79 4.98 4.71 o 14 2 11 348.78 312.20 9.54 o 1 3 11 1131.67 1222.78 23.08 o 2 3 11 4893.38 5055.56 124.16 o 3 3 11 1178.66 1181.05 55.88 o 4 3 11 556.47 513.45 16.09 o 5 3 11 76.67 63.38 3.98 o 6 3 11 7863.74 7350.04 192.28 o 7 3 11 3.75 6.33 3.98 o 8 3 11 668.32 656.49 19.30 o 9 3 11 258.02 284.28 6.35 o 10 3 11 1604.41 1611.58 26.65 o 11 3 11 1702.44 1575.16 25.71 o 12 3 11 344.48 302.20 17.50 o 13 3 11 57.05 57.37 2.96 o 0 4 11 642.72 808.89 17.55 o 1 4 11 2614.73 2976.28 36.96 o 2 4 11 26.20 30.86 4.07 o 3 4 11 38.63 66.24 8.70 o 4 4 11 1292.25 1160.06 47.14 o 5 4 11 210.65 229.63 7.35 o 6 4 11 3.52 1.34 3.44 o 7 4 11 124.54 115.57 4.62 o 8 4 11 196.10 188.86 5.39 o 9 4 11 34.61 27.33 4.42 o 10 4 11 13.32 1.96 5.55 o 11 4 11 1.08 -1.00 4.66 o 12 4 11 149.53 177.10 11.02 o 13 4 11 23.81 26.59 2.45 o 1 5 11 60.12 56.43 4.80 o 2 5 11 466.20 513.54 11.65 o 3 5 11 912.19 1014.27 28.68 o 4 5 11 215.24 219.98 5.92 o 5 5 11 18.49 11.25 8.02 o 6 5 11 15.67 20.92 3.17 o 7 5 11 230.70 190.07 10.14 o 8 5 11 10.01 10.20 7.62 o 9 5 11 64.32 62.04 3.70 o 10 5 11 3.44 3.81 3.17 o 11 5 11 273.74 262.86 7.69 o 12 5 11 123.85 123.26 3.88 o 0 6 11 4247.94 5938.60 497.09 o 1 6 11 3.48 4.68 7.84 o 2 6 11 441.21 523.40 11.66 o 3 6 11 145.84 151.14 5.27 o 4 6 11 526.50 579.67 17.45 o 5 6 11 21.32 40.88 8.43 o 6 6 11 102.13 96.52 6.05 o 7 6 11 35.53 49.08 3.52 o 8 6 11 134.74 139.78 4.37 o 9 6 11 97.47 86.01 3.74 o 10 6 11 56.92 61.84 4.28 o 1 7 11 366.17 417.43 53.13 o 2 7 11 624.18 734.83 78.77 o 3 7 11 23.75 26.14 4.62 o 4 7 11 114.82 130.25 4.49 o 5 7 11 52.43 59.57 7.07 o 6 7 11 16.92 18.89 8.30 o 7 7 11 576.39 545.96 38.74 o 8 7 11 105.24 92.63 5.85 o 9 7 11 27.68 32.13 3.47 o 0 8 11 80.97 139.50 7.55 o 1 8 11 603.16 716.43 157.35 o 2 8 11 14.90 44.92 9.25 o 3 8 11 129.72 132.83 7.42 o 4 8 11 26.00 32.12 2.83 o 5 8 11 167.63 162.47 22.46 o 6 8 11 14.26 9.47 5.58 o 0 0 12 15690.27 21198.88 446.04 o 1 0 12 219.67 251.44 12.25 o 2 0 12 594.88 618.46 13.01 o 3 0 12 693.55 667.53 18.01 o 4 0 12 409.03 388.41 31.00 o 5 0 12 3394.99 3262.05 76.11 o 6 0 12 1677.51 1697.31 67.17 o 7 0 12 6505.45 6264.91 202.72 o 8 0 12 282.95 222.98 10.48 o 9 0 12 2.80 -0.38 5.67 o 10 0 12 49.40 87.63 4.13 o 11 0 12 648.60 624.74 12.48 o 12 0 12 176.28 174.29 12.39 o 13 0 12 559.85 482.53 25.16 o 14 0 12 83.43 125.76 4.76 o 1 1 12 62.57 64.50 8.64 o 2 1 12 806.56 1014.05 22.74 o 3 1 12 1901.30 1918.86 110.53 o 4 1 12 618.50 607.61 13.05 o 5 1 12 1075.65 1000.57 53.66 o 6 1 12 8.71 16.24 3.17 o 7 1 12 2340.62 2196.71 102.57 o 8 1 12 56.28 43.55 4.90 o 9 1 12 1757.64 1611.78 57.72 o 10 1 12 106.08 90.68 5.31 o 11 1 12 899.54 833.82 28.34 o 12 1 12 244.32 236.92 7.42 o 13 1 12 67.90 81.79 3.36 o 14 1 12 118.61 129.15 3.54 o 0 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8 4 12 357.52 347.92 16.62 o 9 4 12 247.11 211.07 14.23 o 10 4 12 734.18 677.92 20.54 o 11 4 12 140.26 125.11 11.02 o 12 4 12 93.50 88.00 3.20 o 1 5 12 536.40 598.78 13.08 o 2 5 12 20.81 27.81 4.18 o 3 5 12 484.80 501.63 11.45 o 4 5 12 137.72 172.50 24.97 o 5 5 12 178.77 176.86 9.53 o 6 5 12 81.02 61.44 5.44 o 7 5 12 1667.20 1518.01 89.91 o 8 5 12 476.21 465.16 55.00 o 9 5 12 554.62 541.84 34.02 o 10 5 12 77.00 77.57 3.27 o 11 5 12 76.47 96.58 3.27 o 0 6 12 681.26 994.38 20.57 o 1 6 12 77.13 82.63 5.61 o 2 6 12 11.11 12.31 3.66 o 3 6 12 232.50 249.71 6.48 o 4 6 12 0.00 3.49 3.95 o 5 6 12 256.02 242.46 19.81 o 6 6 12 200.90 214.28 20.08 o 7 6 12 661.92 626.13 29.54 o 8 6 12 0.48 -4.65 4.78 o 9 6 12 103.90 96.85 5.58 o 10 6 12 0.29 0.87 4.28 o 1 7 12 22.45 24.37 7.00 o 2 7 12 251.53 300.75 27.37 o 3 7 12 515.58 542.51 11.27 o 4 7 12 110.81 132.29 4.67 o 5 7 12 67.32 63.16 13.33 o 6 7 12 9.25 14.51 2.81 o 7 7 12 59.74 47.25 5.58 o 8 7 12 21.00 27.10 4.56 o 0 8 12 17.80 18.53 5.58 o 1 8 12 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