#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214543.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214543_Fobs loop_ _publ_author_name 'Scharwitz, Michael' 'Oppel, Iris M.' 'Sheldrick, William S.' _publ_section_title ; Bis(\m-diethyldithiocarbamato)bis[(\h^5^-pentamethylcyclopentadienyl)iridium(III)] bis(perchlorate) ; _journal_coeditor_code BT2421 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2065 _journal_page_last m2066 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 20.2386 _cell_length_b 15.1259 _cell_length_c 25.6234 _exptl_crystal_F_000 4480.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file bt2421Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pbca in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1413.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 56081.11 65055.96 862.14 o 6 0 0 98334.42 105795.44 1335.60 o 8 0 0 982615.56 1072695.25 3335.41 o 10 0 0 871426.75 949942.06 3586.35 o 12 0 0 266925.91 278869.75 2164.77 o 14 0 0 58309.90 59168.23 1268.47 o 16 0 0 392886.50 405449.03 8253.91 o 18 0 0 172935.42 185493.56 3483.88 o 20 0 0 31245.08 32563.31 1915.07 o 22 0 0 38667.12 35552.52 2374.41 o 24 0 0 158606.31 164809.38 4211.75 o 4 1 0 55147.58 60418.57 573.31 o 6 1 0 54062.58 57013.96 1713.67 o 8 1 0 78109.91 81786.63 699.50 o 10 1 0 2560.20 2944.40 340.61 o 12 1 0 45239.57 46746.60 711.78 o 14 1 0 552.69 587.51 395.59 o 16 1 0 794.25 179.07 468.91 o 18 1 0 86.77 -633.61 633.61 o 20 1 0 1765.68 428.58 909.27 o 22 1 0 24211.92 22938.74 1482.47 o 24 1 0 26393.30 26850.88 1668.61 o 0 2 0 563830.25 500569.03 2529.88 o 2 2 0 448227.84 469607.63 3819.55 o 4 2 0 9800.90 10799.07 328.60 o 6 2 0 28960.81 28831.58 536.12 o 8 2 0 282507.75 314276.31 3044.93 o 10 2 0 290596.25 305903.13 3638.30 o 12 2 0 20347.12 18926.94 538.12 o 14 2 0 13957.17 14481.84 595.67 o 16 2 0 61351.14 63442.28 1209.17 o 18 2 0 72482.20 74489.59 1455.67 o 20 2 0 11544.64 9654.45 1106.13 o 22 2 0 3460.71 1375.36 1085.78 o 2 3 0 341174.41 340608.47 2759.55 o 4 3 0 3538.07 5090.10 351.19 o 6 3 0 197044.64 212538.47 1795.39 o 8 3 0 13570.92 13873.38 385.69 o 10 3 0 30944.10 32017.51 518.91 o 12 3 0 84715.80 88098.19 2264.38 o 14 3 0 69293.35 73684.34 1224.89 o 16 3 0 3942.30 3520.92 650.41 o 18 3 0 2434.16 1902.44 720.32 o 20 3 0 27947.73 30033.19 1163.22 o 22 3 0 39142.84 40471.70 1703.54 o 0 4 0 382980.38 369898.88 3109.34 o 2 4 0 298041.59 291490.94 4099.84 o 4 4 0 9119.67 9522.94 422.47 o 6 4 0 39504.78 38537.62 660.95 o 8 4 0 116002.54 117472.81 1181.94 o 10 4 0 35952.25 35593.39 844.32 o 12 4 0 33181.39 35989.11 621.60 o 14 4 0 7334.90 7163.46 700.64 o 16 4 0 53220.88 52703.42 1191.69 o 18 4 0 15567.02 16024.92 944.96 o 20 4 0 7373.00 6593.22 921.83 o 22 4 0 9090.59 8907.22 1258.45 o 2 5 0 232241.44 220602.13 1700.32 o 4 5 0 194324.42 191099.70 2287.45 o 6 5 0 26825.98 26261.20 505.40 o 8 5 0 11173.46 10671.53 397.98 o 10 5 0 44533.18 48165.77 712.40 o 12 5 0 118438.91 122359.38 1324.32 o 14 5 0 68230.99 65158.32 1279.76 o 16 5 0 9779.11 8339.65 791.11 o 18 5 0 21141.86 20729.60 1081.96 o 20 5 0 35482.27 35606.86 1270.79 o 22 5 0 10802.99 11430.55 1102.55 o 0 6 0 834248.06 795099.38 12027.52 o 2 6 0 408037.25 386892.44 3925.94 o 4 6 0 41695.40 43481.43 628.35 o 6 6 0 213330.16 212226.38 3023.25 o 8 6 0 372287.44 379805.09 2046.47 o 10 6 0 244391.61 243049.98 2079.56 o 12 6 0 44837.37 44390.82 942.66 o 14 6 0 10887.90 10754.99 685.86 o 16 6 0 129800.15 133702.47 1917.03 o 18 6 0 100237.70 109296.50 1868.71 o 20 6 0 17827.19 17767.86 1119.10 o 22 6 0 26369.08 28109.46 1356.74 o 2 7 0 1147.65 748.51 473.06 o 4 7 0 83485.69 73517.30 1179.68 o 6 7 0 59382.00 58057.16 723.64 o 8 7 0 20584.25 20687.95 586.75 o 10 7 0 14175.89 12687.60 731.17 o 12 7 0 36166.18 37917.04 924.27 o 14 7 0 4448.98 4058.99 678.88 o 16 7 0 3295.90 2656.03 681.19 o 18 7 0 751.48 -20.18 799.26 o 20 7 0 10478.23 9206.33 1074.36 o 22 7 0 23941.06 23691.93 1348.09 o 0 8 0 45746.14 41659.13 1412.60 o 2 8 0 115989.62 117574.66 1570.92 o 4 8 0 20088.02 22448.64 645.07 o 6 8 0 22988.04 21031.75 591.06 o 8 8 0 101665.33 96477.45 1139.33 o 10 8 0 34175.77 34222.34 1066.65 o 12 8 0 11914.11 11502.59 737.57 o 14 8 0 691.20 437.41 658.90 o 16 8 0 36328.32 36442.97 1162.79 o 18 8 0 63545.89 67326.60 1679.57 o 20 8 0 11337.55 10172.16 1172.88 o 2 9 0 454235.13 456446.47 5964.29 o 4 9 0 525824.19 520539.59 3136.10 o 6 9 0 325306.53 323021.44 1856.26 o 8 9 0 1192.93 1111.22 736.06 o 10 9 0 123533.77 123170.34 1840.03 o 12 9 0 340687.56 340765.06 4554.36 o 14 9 0 368288.06 368413.56 3751.90 o 16 9 0 36708.40 34650.77 1141.28 o 18 9 0 22557.81 21396.44 1042.84 o 20 9 0 172753.20 185034.73 3503.95 o 0 10 0 20685.47 19688.62 1271.57 o 2 10 0 4121.31 3714.95 806.46 o 4 10 0 423.68 304.54 745.72 o 6 10 0 7124.53 7430.52 736.98 o 8 10 0 13140.09 11712.58 998.52 o 10 10 0 28049.26 27198.60 1138.86 o 12 10 0 2463.22 1736.13 919.72 o 14 10 0 1173.26 582.34 789.05 o 16 10 0 6655.75 5612.02 854.74 o 18 10 0 232.62 132.48 877.21 o 20 10 0 5737.89 4544.47 1190.78 o 2 11 0 144899.50 143152.16 2165.44 o 4 11 0 151122.97 153175.86 3641.49 o 6 11 0 35119.05 30923.54 1512.06 o 8 11 0 666.71 327.75 899.84 o 10 11 0 126946.44 125948.77 2129.41 o 12 11 0 229891.69 223169.94 2755.81 o 14 11 0 144158.05 143453.73 2569.38 o 16 11 0 25152.60 24703.85 1204.50 o 18 11 0 33420.41 34043.89 1308.56 o 0 12 0 2997.76 3023.17 1459.27 o 2 12 0 9388.29 9079.11 872.83 o 4 12 0 92.37 -184.66 833.33 o 6 12 0 9510.52 7407.85 1296.63 o 8 12 0 3183.20 4452.22 1285.07 o 10 12 0 1356.35 1626.31 999.56 o 12 12 0 4727.90 4411.59 1108.49 o 14 12 0 1895.85 918.23 998.24 o 16 12 0 2701.70 3746.40 938.05 o 2 13 0 892.13 636.57 833.04 o 4 13 0 24481.57 24615.86 1542.08 o 6 13 0 42409.52 45193.04 2897.34 o 8 13 0 1654.40 1285.44 1212.08 o 10 13 0 6350.33 4000.59 1106.18 o 12 13 0 5250.26 4066.37 1110.78 o 14 13 0 6161.96 4615.36 1165.39 o 16 13 0 1360.88 820.71 999.02 o 0 14 0 44702.80 46437.54 3922.01 o 2 14 0 8115.76 6757.62 928.46 o 4 14 0 1226.28 301.27 1049.33 o 6 14 0 1358.46 663.44 1306.11 o 8 14 0 13839.23 11781.61 2021.07 o 10 14 0 13933.78 13726.64 1525.81 o 12 14 0 5089.89 4635.56 1214.65 o 14 14 0 4402.18 3858.88 1290.62 o 2 15 0 69144.23 73536.91 1863.97 o 4 15 0 268550.94 300566.94 3438.85 o 6 15 0 115308.34 120081.74 2905.88 o 8 15 0 370.64 -120.18 1389.03 o 10 15 0 85573.51 87595.45 2697.98 o 12 15 0 167631.94 171233.25 6504.89 o 0 16 0 2280.56 1570.89 1285.69 o 2 16 0 1212.87 1266.46 1042.43 o 4 16 0 2367.30 2288.32 1090.92 o 6 16 0 62.46 -419.48 1086.16 o 8 16 0 826.42 -52.92 1441.44 o 10 16 0 8587.68 9793.88 1750.84 o 2 17 0 51290.54 56520.33 1848.37 o 4 17 0 72063.78 79525.31 2102.10 o 6 17 0 26920.49 26598.79 1651.32 o 3 1 1 10529.52 10273.31 252.95 o 4 1 1 364135.09 393766.56 3059.97 o 5 1 1 13112.61 13721.58 289.23 o 6 1 1 2295.02 2249.28 260.73 o 7 1 1 16539.36 16639.52 280.36 o 8 1 1 1950.41 1925.45 196.20 o 9 1 1 4934.22 5210.78 237.92 o 10 1 1 17064.84 16213.44 313.84 o 11 1 1 601.96 710.93 235.99 o 12 1 1 89321.59 91275.87 654.07 o 13 1 1 15.73 -8.93 265.83 o 14 1 1 69618.20 70324.75 653.35 o 15 1 1 3484.38 3212.04 336.11 o 16 1 1 19418.26 18685.13 508.12 o 17 1 1 515.79 1267.80 424.19 o 18 1 1 18166.84 18177.85 620.67 o 19 1 1 122.98 562.93 529.18 o 20 1 1 76921.94 75063.54 1336.71 o 21 1 1 2956.62 2279.81 753.33 o 22 1 1 33043.20 31888.58 1134.88 o 23 1 1 7698.81 6916.65 900.28 o 24 1 1 8056.14 5806.63 902.00 o 0 2 1 24389.56 24659.86 713.74 o 1 2 1 122666.14 126617.80 1628.01 o 2 2 1 89739.26 92329.41 1764.64 o 3 2 1 328221.13 358615.28 6331.76 o 4 2 1 35.12 868.95 288.10 o 5 2 1 61674.43 63940.14 885.35 o 6 2 1 76102.23 81662.20 702.19 o 7 2 1 1141.39 1394.19 181.49 o 8 2 1 31861.10 34005.08 335.09 o 9 2 1 23359.68 23211.21 332.17 o 10 2 1 13323.71 12341.37 298.01 o 11 2 1 125677.03 126007.03 742.19 o 12 2 1 489.07 594.15 261.52 o 13 2 1 296666.97 314852.38 1206.86 o 14 2 1 21386.79 20859.92 435.84 o 15 2 1 101328.51 105538.48 888.49 o 16 2 1 42037.28 43852.96 740.90 o 17 2 1 374.57 419.32 439.77 o 18 2 1 18653.25 18987.16 636.94 o 19 2 1 59941.91 62046.68 942.91 o 20 2 1 3.85 46.10 614.43 o 21 2 1 116966.36 122338.30 1670.93 o 22 2 1 17003.35 16858.66 1019.75 o 23 2 1 47915.20 49993.04 1311.84 o 1 3 1 12391.25 12577.87 329.04 o 2 3 1 192007.78 186205.45 2016.52 o 3 3 1 19964.56 19583.25 340.09 o 4 3 1 381180.88 399127.66 1872.70 o 5 3 1 4226.87 4179.66 217.32 o 6 3 1 173816.42 179083.77 993.68 o 7 3 1 5105.27 5002.57 195.88 o 8 3 1 1594.60 1622.31 179.74 o 9 3 1 31523.61 33269.22 345.96 o 10 3 1 107960.55 112753.76 1075.63 o 11 3 1 42145.71 44590.13 625.17 o 12 3 1 421493.91 447881.13 2639.57 o 13 3 1 2959.86 3061.26 302.95 o 14 3 1 308900.16 325372.91 1821.99 o 15 3 1 7273.51 7112.66 482.98 o 16 3 1 23773.96 23352.94 640.50 o 17 3 1 106.82 -41.38 452.43 o 18 3 1 32686.34 33705.56 758.85 o 19 3 1 7489.06 8677.71 621.33 o 20 3 1 178217.41 187922.94 1601.31 o 21 3 1 16621.06 18251.77 851.17 o 22 3 1 151802.88 159996.63 1976.29 o 23 3 1 3087.50 3945.77 862.11 o 0 4 1 32387.19 31286.34 669.18 o 1 4 1 54168.11 55873.41 700.97 o 2 4 1 41686.12 40484.22 561.18 o 3 4 1 444342.38 417013.53 2078.48 o 4 4 1 7630.27 7324.93 273.81 o 5 4 1 180221.14 185479.83 1235.68 o 6 4 1 4896.28 4855.44 222.43 o 7 4 1 31590.88 33048.49 347.79 o 8 4 1 711.51 825.28 179.67 o 9 4 1 6182.01 6357.68 226.34 o 10 4 1 29410.78 30725.10 369.12 o 11 4 1 227161.86 243509.03 1667.93 o 12 4 1 962.04 681.17 265.52 o 13 4 1 195163.58 205119.16 1160.71 o 14 4 1 6273.62 6720.39 498.29 o 15 4 1 85248.47 88104.77 999.48 o 16 4 1 5502.71 5184.75 495.81 o 17 4 1 1700.03 1107.49 485.41 o 18 4 1 4091.73 4259.19 561.11 o 19 4 1 61604.43 64908.84 1037.45 o 20 4 1 6751.27 7766.82 652.92 o 21 4 1 94773.30 100204.16 1324.16 o 22 4 1 4009.29 4809.01 770.78 o 23 4 1 57993.04 58244.20 1431.71 o 1 5 1 61306.77 57967.41 637.57 o 2 5 1 25121.58 25844.57 474.77 o 3 5 1 74786.39 74232.11 680.64 o 4 5 1 80509.21 77897.80 914.49 o 5 5 1 26733.07 24749.65 360.94 o 6 5 1 79279.06 80641.50 716.49 o 7 5 1 104867.68 106659.24 1169.88 o 8 5 1 1947.19 1845.17 217.98 o 9 5 1 135144.31 137719.61 664.55 o 10 5 1 80855.63 83541.38 654.98 o 11 5 1 22315.15 21403.44 417.44 o 12 5 1 54971.20 57045.73 761.56 o 13 5 1 4054.18 3760.88 407.96 o 14 5 1 30070.86 31041.70 647.89 o 15 5 1 32481.37 33588.21 839.10 o 16 5 1 34811.30 36645.52 770.58 o 17 5 1 65846.75 67879.38 1024.98 o 18 5 1 66.94 28.94 541.41 o 19 5 1 52843.41 54303.32 1003.88 o 20 5 1 43056.11 43574.07 966.80 o 21 5 1 2922.67 2930.23 646.43 o 22 5 1 33549.06 34425.59 973.19 o 23 5 1 9385.87 9006.45 890.94 o 0 6 1 222505.86 212887.16 1689.23 o 1 6 1 4937.84 3687.94 404.78 o 2 6 1 118749.13 113879.85 831.65 o 3 6 1 7405.96 7041.56 328.17 o 4 6 1 27664.98 26290.30 407.91 o 5 6 1 45538.23 45484.72 464.82 o 6 6 1 40170.57 38908.59 529.14 o 7 6 1 15908.07 15755.54 350.20 o 8 6 1 226495.47 220646.06 1003.83 o 9 6 1 1651.96 1138.87 263.57 o 10 6 1 87349.50 84706.92 690.75 o 11 6 1 1058.63 1039.40 339.15 o 12 6 1 9599.00 8715.75 443.45 o 13 6 1 24269.88 25281.62 583.62 o 14 6 1 14676.70 13615.75 519.96 o 15 6 1 1555.62 1141.55 448.74 o 16 6 1 55208.38 57958.97 981.87 o 17 6 1 3580.37 3000.67 551.98 o 18 6 1 83791.38 88699.98 1223.51 o 19 6 1 54.31 568.53 578.71 o 20 6 1 16132.01 15685.44 770.37 o 21 6 1 8560.88 7325.03 723.53 o 22 6 1 20912.30 19713.69 880.12 o 1 7 1 268964.22 256906.83 2314.82 o 2 7 1 37029.23 33911.16 616.04 o 3 7 1 31782.84 29771.48 528.18 o 4 7 1 48147.86 47860.86 559.96 o 5 7 1 22173.72 19961.37 414.25 o 6 7 1 20383.74 20499.92 390.62 o 7 7 1 45947.91 42961.48 490.41 o 8 7 1 26.20 -57.54 257.98 o 9 7 1 111143.54 111549.72 907.77 o 10 7 1 17076.33 16294.82 582.05 o 11 7 1 76782.64 76130.51 827.78 o 12 7 1 39837.67 39796.48 679.49 o 13 7 1 216.26 201.94 419.23 o 14 7 1 49658.32 49387.65 775.71 o 15 7 1 32778.36 32332.15 704.68 o 16 7 1 3109.22 2293.17 512.79 o 17 7 1 82719.74 84241.42 1384.22 o 18 7 1 5226.73 5435.63 640.53 o 19 7 1 31263.11 30477.68 931.21 o 20 7 1 8866.40 8050.73 725.19 o 21 7 1 1789.40 1501.38 689.69 o 22 7 1 6515.52 6060.94 797.78 o 0 8 1 222451.75 230552.52 4228.88 o 1 8 1 19086.58 18410.40 586.90 o 2 8 1 141039.22 134500.00 1056.66 o 3 8 1 15366.59 13600.99 506.34 o 4 8 1 31.26 -63.25 363.79 o 5 8 1 37405.77 36325.60 546.28 o 6 8 1 63487.59 61451.63 585.59 o 7 8 1 2429.53 2144.68 325.63 o 8 8 1 90478.38 87486.04 975.61 o 9 8 1 22478.69 21535.64 669.77 o 10 8 1 87692.96 86353.87 1061.71 o 11 8 1 1993.72 1654.31 487.76 o 12 8 1 5886.27 4852.07 492.46 o 13 8 1 27101.06 26710.70 654.69 o 14 8 1 5136.84 4504.98 494.80 o 15 8 1 18214.84 17474.85 632.59 o 16 8 1 51833.03 51493.78 874.96 o 17 8 1 59.02 25.00 532.95 o 18 8 1 64557.14 67319.55 1192.50 o 19 8 1 4890.34 4720.90 697.55 o 20 8 1 1449.94 996.99 703.41 o 21 8 1 9569.42 8870.25 864.07 o 1 9 1 91147.37 89900.45 1011.63 o 2 9 1 37891.63 35475.50 768.42 o 3 9 1 9065.12 7951.93 490.67 o 4 9 1 62574.38 60479.80 844.65 o 5 9 1 403.09 111.09 404.74 o 6 9 1 17063.29 16053.28 485.79 o 7 9 1 75.17 -120.71 365.55 o 8 9 1 1119.69 954.72 454.27 o 9 9 1 72.14 -45.17 517.19 o 10 9 1 5652.40 5143.28 583.40 o 11 9 1 17116.04 15081.70 683.00 o 12 9 1 45610.61 45625.40 938.06 o 13 9 1 2881.80 1735.08 496.10 o 14 9 1 39612.42 39634.20 802.26 o 15 9 1 179.24 110.77 491.96 o 16 9 1 4366.84 3711.47 558.95 o 17 9 1 1363.68 886.44 579.39 o 18 9 1 6330.27 5710.98 657.17 o 19 9 1 81.84 2.99 725.17 o 20 9 1 14295.91 15109.71 899.65 o 0 10 1 10524.20 9640.59 788.54 o 1 10 1 3933.20 2878.05 490.82 o 2 10 1 9407.33 8864.02 578.85 o 3 10 1 42085.53 40385.57 836.22 o 4 10 1 327.31 -205.33 482.41 o 5 10 1 35910.97 36999.08 719.53 o 6 10 1 10403.07 9645.46 506.30 o 7 10 1 3422.92 3325.78 507.89 o 8 10 1 10021.79 8480.33 628.58 o 9 10 1 6.07 -89.57 549.45 o 10 10 1 12607.81 10597.59 705.36 o 11 10 1 5592.13 5605.42 634.70 o 12 10 1 1223.25 390.97 594.96 o 13 10 1 9647.28 9464.79 660.70 o 14 10 1 27.11 -156.82 521.49 o 15 10 1 16421.23 16700.69 697.46 o 16 10 1 14020.36 12634.53 680.73 o 17 10 1 3362.52 3165.74 602.28 o 18 10 1 9919.71 8555.95 698.23 o 19 10 1 2632.99 3091.62 726.00 o 1 11 1 81033.16 80907.10 1160.53 o 2 11 1 230.24 -106.03 516.00 o 3 11 1 18907.16 17602.80 729.52 o 4 11 1 3867.62 3664.78 579.25 o 5 11 1 1576.20 787.22 561.36 o 6 11 1 1310.61 848.47 631.00 o 7 11 1 100324.09 100093.88 1451.34 o 8 11 1 54.59 -466.18 653.03 o 9 11 1 67363.83 63197.52 1176.04 o 10 11 1 67.85 188.53 626.51 o 11 11 1 22019.86 19863.42 852.73 o 12 11 1 2751.46 3251.14 699.76 o 13 11 1 279.58 487.34 653.34 o 14 11 1 999.96 1201.46 627.00 o 15 11 1 44429.20 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-372.65 971.82 o 7 3 27 84073.26 82551.48 2029.12 o 8 3 27 56.04 254.40 1067.49 o 9 3 27 104417.36 112286.64 2750.90 o 10 3 27 1825.78 2240.14 1306.11 o 0 4 27 70690.39 73755.78 2667.67 o 1 4 27 2303.96 3051.83 807.02 o 2 4 27 31764.42 32042.35 1381.19 o 3 4 27 8718.22 8294.50 1124.90 o 4 4 27 365.07 233.91 964.65 o 5 4 27 14396.17 13658.58 1180.00 o 6 4 27 33171.86 34887.50 1501.38 o 7 4 27 13497.49 12763.07 1246.52 o 8 4 27 80427.48 87208.98 2042.69 o 9 4 27 1769.92 900.87 1125.50 o 1 5 27 20153.65 20233.58 1313.18 o 2 5 27 7332.53 8249.34 1111.99 o 3 5 27 3141.70 2012.19 961.84 o 4 5 27 38518.31 40684.68 1569.04 o 5 5 27 983.56 811.23 1021.12 o 6 5 27 42180.40 45719.52 1668.38 o 7 5 27 18404.52 17026.89 1321.30 o 8 5 27 3263.44 3468.57 1141.78 o 0 6 27 1177.49 876.27 1809.07 o 1 6 27 5305.55 4696.60 1044.59 o 2 6 27 609.52 234.48 1026.93 o 3 6 27 50375.04 52549.86 1718.94 o 4 6 27 228.06 534.31 1097.62 o 5 6 27 71035.58 75101.29 1922.93 o 6 6 27 2108.07 1729.20 1172.42 o 7 6 27 19334.02 20907.65 1412.13 o 1 7 27 8191.96 7404.84 1492.67 o 2 7 27 36071.39 38819.00 1602.06 o 3 7 27 4872.36 5772.51 1192.91 o 4 7 27 87305.35 96231.59 2264.65 o 5 7 27 24.39 319.87 1109.14 o 6 7 27 63173.83 65828.52 1946.25 o 0 8 27 28580.13 31616.38 3052.81 o 1 8 27 4675.21 4013.03 1601.22 o 2 8 27 8927.34 9992.27 2356.74 o 3 8 27 19227.90 18368.41 1824.11 o 0 0 28 1671.42 148.40 1731.34 o 1 0 28 55.30 -754.22 1160.42 o 2 0 28 42.84 37.61 1159.97 o 3 0 28 141.86 -598.85 1211.17 o 4 0 28 2065.14 1369.29 1250.82 o 5 0 28 4083.31 3126.44 1276.12 o 6 0 28 275.27 183.73 1759.61 o 7 0 28 10271.23 7766.29 2084.67 o 8 0 28 214.62 190.80 1865.61 o 9 0 28 428.29 91.87 1780.81 o 1 1 28 6830.26 6781.93 895.94 o 2 1 28 110385.23 115232.67 1792.74 o 3 1 28 19263.14 19745.00 1042.64 o 4 1 28 177104.34 183356.55 2851.89 o 5 1 28 5188.18 5116.70 1097.09 o 6 1 28 105354.80 106251.55 2114.54 o 7 1 28 5655.29 6102.82 1266.53 o 8 1 28 10522.30 8173.52 1414.12 o 9 1 28 11136.89 9661.90 1556.48 o 0 2 28 25364.38 27615.96 1653.90 o 1 2 28 221.74 5.28 838.66 o 2 2 28 3219.73 4015.25 902.67 o 3 2 28 104.21 -475.96 878.70 o 4 2 28 251.04 -455.34 932.85 o 5 2 28 75.84 -534.76 1065.18 o 6 2 28 2064.74 2464.09 1004.16 o 7 2 28 1460.69 845.75 1075.50 o 8 2 28 11103.45 12245.13 1601.03 o 9 2 28 541.53 531.11 1388.47 o 1 3 28 14.69 1119.25 820.32 o 2 3 28 320.64 453.89 795.10 o 3 3 28 0.15 348.88 1000.31 o 4 3 28 2357.57 1963.81 1024.40 o 5 3 28 1.11 -266.55 963.47 o 6 3 28 704.33 756.38 1068.84 o 7 3 28 0.69 574.19 1104.23 o 8 3 28 1686.96 1348.10 1070.47 o 0 4 28 44542.83 47710.39 1978.67 o 1 4 28 48.00 422.45 822.49 o 2 4 28 30265.04 30944.21 1695.81 o 3 4 28 1141.19 969.63 948.02 o 4 4 28 111.74 457.41 1061.21 o 5 4 28 6090.28 6686.18 1117.04 o 6 4 28 18070.05 18227.54 1382.72 o 7 4 28 3292.17 3868.44 1095.51 o 1 5 28 12424.13 12553.35 1193.00 o 2 5 28 32168.85 31970.13 1447.75 o 3 5 28 6435.92 5341.30 1135.86 o 4 5 28 89136.88 93064.79 2371.03 o 5 5 28 3145.65 4092.90 1140.74 o 6 5 28 45040.37 48504.32 1713.10 o 0 6 28 9932.34 8946.43 2360.27 o 1 6 28 56.16 18.00 1440.97 o 2 6 28 2086.49 1939.39 1053.11 o 3 6 28 37.14 -393.50 1119.14 o 4 6 28 5.04 27.12 1095.19 o 5 6 28 1032.32 1262.76 1161.94 o 1 7 28 834.37 400.53 1418.66 o 1 1 29 26062.87 26629.54 1396.36 o 2 1 29 912.65 1468.91 838.05 o 3 1 29 1507.57 1775.76 850.27 o 4 1 29 5124.60 6446.32 966.32 o 5 1 29 1331.79 1845.18 1007.89 o 6 1 29 2829.12 3395.94 1109.34 o 7 1 29 7209.24 7155.96 1632.41 o 0 2 29 73003.80 76364.06 2279.61 o 1 2 29 589.98 593.29 866.83 o 2 2 29 40515.06 41468.38 1333.90 o 3 2 29 1123.62 1119.67 854.42 o 4 2 29 1667.83 661.02 999.83 o 5 2 29 800.46 1222.84 1079.31 o 6 2 29 30892.00 30408.21 1476.18 o 1 3 29 72030.10 72365.11 1621.80 o 2 3 29 206.21 28.57 1031.03 o 3 3 29 13992.10 13932.73 1210.08 o 4 3 29 906.18 302.03 1072.16 o 5 3 29 5694.56 4594.60 1138.38 o 6 3 29 708.36 954.44 1131.63 o 0 4 29 59297.48 61501.84 2130.19 o 1 4 29 4717.59 4177.20 1057.25 o 2 4 29 33850.71 34218.89 1535.62 o 3 4 29 21105.54 20946.22 1426.84 o 4 4 29 1958.36 2167.49 1038.48 o 5 4 29 21241.20 21308.84 1405.98 o 1 5 29 45131.75 46501.14 1698.31 o 2 5 29 10928.40 10420.14 1243.39 o 3 5 29 3833.77 3415.74 1183.40 o 0 0 30 88056.52 95181.27 3575.75 o 1 0 30 22129.29 20702.83 1673.94 o 2 0 30 61860.96 64556.55 2189.80 o 3 0 30 180610.70 189247.92 3373.94 o 4 0 30 11256.83 10348.29 1433.17 o 1 1 30 667.49 206.59 927.26 o 2 1 30 61.07 -914.07 914.07 o 3 1 30 74.61 -277.84 920.40 o 4 1 30 4418.61 2532.90 1170.28 o 0 2 30 18720.75 20308.21 1685.41 o 1 2 30 4793.16 4854.62 932.21 o 2 2 30 9682.87 10588.84 1022.00 o 3 2 30 24870.63 26662.36 1470.37 o 1 3 30 25813.99 27048.45 1265.88 o