#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/45/2214563.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214563_Fobs loop_ _publ_author_name 'Stefanowicz, Piotr' 'Jaremko, Mariusz' 'Jaremko, \/Lukasz' 'Lis, Tadeusz' _publ_section_title ; Oxacyclohexane-2,6-dione (glutaric anhydride) ; _journal_coeditor_code BX2098 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3431 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.4100 _cell_length_b 7.5200 _cell_length_c 13.1800 _exptl_crystal_F_000 240.00 _reflns_d_resolution_high 0.7460 _[local]_cod_data_source_file bx2098Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jar12dc in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 64.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3114.02 3525.91 59.35 o 4 0 0 62.33 55.87 0.87 o 6 0 0 1.51 1.57 1.22 o 1 1 0 2398.94 2398.55 34.54 o 2 1 0 887.52 884.47 17.94 o 3 1 0 224.02 211.69 3.12 o 4 1 0 10.89 9.91 0.40 o 5 1 0 11.38 9.51 0.56 o 6 1 0 0.41 0.37 0.76 o 7 1 0 0.54 1.34 0.93 o 0 2 0 1481.44 1482.12 73.11 o 1 2 0 4158.60 4402.48 20.11 o 2 2 0 17.38 13.30 0.30 o 3 2 0 32.62 29.29 0.39 o 4 2 0 33.72 30.46 0.96 o 5 2 0 7.04 5.09 0.60 o 6 2 0 3.34 3.03 0.98 o 1 3 0 0.06 0.54 0.14 o 2 3 0 2.91 3.61 0.63 o 3 3 0 1.97 1.39 0.26 o 4 3 0 32.93 34.12 1.19 o 5 3 0 2.75 2.95 0.59 o 6 3 0 0.30 1.10 0.59 o 0 4 0 80.25 78.73 0.79 o 1 4 0 67.43 69.92 1.30 o 2 4 0 67.54 59.86 1.14 o 3 4 0 0.08 0.33 0.28 o 4 4 0 22.10 23.79 0.80 o 5 4 0 2.51 2.06 0.63 o 6 4 0 6.22 4.90 0.93 o 1 5 0 1.47 1.33 0.29 o 2 5 0 2.84 1.62 0.43 o 3 5 0 3.14 2.86 0.38 o 4 5 0 0.03 0.41 0.52 o 5 5 0 0.14 0.24 0.61 o 6 5 0 0.21 0.44 0.81 o 0 6 0 27.34 32.10 2.34 o 1 6 0 2.56 2.60 0.34 o 2 6 0 28.96 26.09 1.26 o 3 6 0 2.88 2.20 1.08 o 4 6 0 1.87 2.50 0.62 o 5 6 0 0.66 0.36 0.73 o 1 7 0 0.48 0.97 0.40 o 2 7 0 0.50 0.66 0.45 o 3 7 0 4.84 4.40 0.73 o 4 7 0 5.48 6.66 0.89 o 0 8 0 0.35 0.57 0.81 o 1 8 0 0.54 0.79 0.64 o 2 8 0 0.10 -0.30 0.46 o 3 8 0 3.38 3.53 0.74 o 1 9 0 1.12 1.26 0.64 o 2 9 0 2.77 2.23 0.80 o 1 0 1 124.98 134.72 2.38 o 2 0 1 486.71 522.34 5.41 o 3 0 1 23.13 22.45 0.35 o 4 0 1 0.64 0.87 0.27 o 5 0 1 36.82 35.23 1.04 o 6 0 1 0.17 1.16 0.78 o 7 0 1 5.60 5.62 1.52 o 0 1 1 544.32 583.46 5.20 o 1 1 1 1006.01 1055.21 5.48 o 2 1 1 345.83 382.69 2.61 o 3 1 1 494.66 513.24 6.00 o 4 1 1 28.34 27.28 0.41 o 5 1 1 0.68 0.65 0.25 o 6 1 1 5.13 4.24 0.61 o 7 1 1 0.59 0.96 0.99 o 0 2 1 870.89 870.84 3.81 o 1 2 1 1396.67 1507.97 14.89 o 2 2 1 251.93 274.97 2.82 o 3 2 1 2.96 1.76 0.17 o 4 2 1 2.49 2.64 0.25 o 5 2 1 15.26 14.55 0.44 o 6 2 1 11.43 12.04 0.72 o 0 3 1 605.81 628.85 4.26 o 1 3 1 20.97 23.77 0.24 o 2 3 1 470.14 497.72 8.53 o 3 3 1 6.57 6.88 0.24 o 4 3 1 7.07 8.20 0.34 o 5 3 1 32.26 32.21 0.59 o 6 3 1 0.67 0.89 0.38 o 0 4 1 78.63 66.41 1.33 o 1 4 1 28.13 27.31 0.61 o 2 4 1 30.49 29.04 0.51 o 3 4 1 1.43 1.70 0.23 o 4 4 1 14.55 10.05 0.47 o 5 4 1 13.61 12.93 0.57 o 6 4 1 1.10 1.11 0.55 o 0 5 1 2.81 2.43 0.28 o 1 5 1 18.00 19.21 0.38 o 2 5 1 14.76 15.02 0.37 o 3 5 1 21.93 22.23 0.54 o 4 5 1 17.05 14.25 0.57 o 5 5 1 9.47 9.78 0.57 o 6 5 1 16.74 18.11 1.12 o 0 6 1 1.49 1.30 0.29 o 1 6 1 14.83 14.56 0.33 o 2 6 1 5.26 5.00 0.33 o 3 6 1 4.75 4.44 0.44 o 4 6 1 11.32 10.56 0.63 o 5 6 1 1.09 1.92 0.48 o 0 7 1 2.48 3.59 0.65 o 1 7 1 2.25 2.23 0.32 o 2 7 1 13.22 11.80 0.38 o 3 7 1 4.58 4.14 0.51 o 4 7 1 3.29 2.12 0.46 o 5 7 1 1.34 1.65 1.12 o 0 8 1 10.53 11.47 0.87 o 1 8 1 10.15 10.55 0.52 o 2 8 1 0.23 0.88 0.38 o 3 8 1 5.93 5.37 0.55 o 4 8 1 1.02 2.62 1.30 o 0 9 1 0.86 0.77 0.50 o 1 9 1 4.54 6.18 0.52 o 2 9 1 3.35 2.67 0.53 o 1 0 2 1232.31 1239.51 14.18 o 2 0 2 11.70 10.56 0.25 o 3 0 2 390.91 395.39 7.82 o 4 0 2 16.85 17.06 0.40 o 5 0 2 4.00 3.82 0.54 o 6 0 2 0.22 0.19 0.62 o 7 0 2 0.01 0.77 1.26 o 0 1 2 2278.14 2454.35 30.19 o 1 1 2 499.34 502.32 5.40 o 2 1 2 314.06 311.38 4.78 o 3 1 2 53.03 51.70 0.49 o 4 1 2 19.39 16.58 0.38 o 5 1 2 10.48 9.77 0.44 o 6 1 2 0.66 1.01 0.46 o 7 1 2 2.79 3.78 1.02 o 0 2 2 2774.26 2965.70 60.02 o 1 2 2 588.29 627.62 5.89 o 2 2 2 367.07 361.01 5.50 o 3 2 2 121.69 126.46 1.32 o 4 2 2 23.11 23.29 0.49 o 5 2 2 7.43 7.14 0.37 o 6 2 2 1.68 1.22 0.43 o 7 2 2 2.34 3.03 1.13 o 0 3 2 473.99 465.14 11.94 o 1 3 2 233.14 223.75 3.33 o 2 3 2 292.88 307.63 2.17 o 3 3 2 4.87 5.30 0.45 o 4 3 2 25.79 25.89 0.59 o 5 3 2 6.33 6.15 0.43 o 6 3 2 6.76 6.27 0.55 o 0 4 2 2.86 2.85 0.27 o 1 4 2 560.15 612.41 8.66 o 2 4 2 74.35 70.25 0.90 o 3 4 2 25.44 22.62 0.59 o 4 4 2 17.11 18.45 0.53 o 5 4 2 9.37 8.21 0.58 o 6 4 2 3.76 4.53 0.53 o 0 5 2 86.71 78.18 1.68 o 1 5 2 140.79 148.03 2.36 o 2 5 2 77.85 79.08 1.05 o 3 5 2 5.18 4.42 0.31 o 4 5 2 8.55 7.95 0.52 o 5 5 2 2.80 2.33 0.45 o 6 5 2 2.12 2.73 0.90 o 0 6 2 1.39 2.41 0.59 o 1 6 2 36.08 41.72 0.86 o 2 6 2 8.53 8.60 0.38 o 3 6 2 38.85 37.67 0.84 o 4 6 2 0.31 0.82 0.39 o 5 6 2 5.60 6.42 0.59 o 0 7 2 13.02 15.05 1.52 o 1 7 2 15.40 15.68 0.45 o 2 7 2 26.54 27.81 0.58 o 3 7 2 1.42 1.49 0.37 o 4 7 2 2.48 3.03 0.56 o 0 8 2 6.84 5.05 0.61 o 1 8 2 5.25 4.88 0.50 o 2 8 2 0.64 0.88 0.37 o 3 8 2 1.23 0.90 0.44 o 4 8 2 1.47 1.45 0.84 o 0 9 2 0.07 1.18 0.61 o 1 9 2 1.18 1.12 0.45 o 2 9 2 0.83 1.21 0.52 o 1 0 3 494.12 554.27 5.29 o 2 0 3 3.06 2.64 0.18 o 3 0 3 82.90 69.78 0.70 o 4 0 3 112.65 112.44 0.96 o 5 0 3 31.67 32.89 1.04 o 6 0 3 2.27 1.73 0.63 o 7 0 3 5.75 5.27 1.45 o 0 1 3 37.46 37.44 0.81 o 1 1 3 647.39 694.83 8.91 o 2 1 3 54.53 59.34 0.73 o 3 1 3 104.58 101.10 0.70 o 4 1 3 42.67 40.69 0.49 o 5 1 3 92.47 97.50 1.22 o 6 1 3 14.08 15.34 0.70 o 7 1 3 12.32 12.56 1.52 o 0 2 3 361.54 365.63 1.50 o 1 2 3 204.06 208.66 1.92 o 2 2 3 11.25 13.85 0.36 o 3 2 3 4.22 5.63 0.20 o 4 2 3 101.41 102.73 1.07 o 5 2 3 19.02 19.26 0.42 o 6 2 3 11.59 11.00 0.58 o 7 2 3 1.30 1.06 0.77 o 0 3 3 1.39 1.78 0.27 o 1 3 3 113.21 121.54 1.21 o 2 3 3 121.91 129.08 1.68 o 3 3 3 31.47 31.75 0.73 o 4 3 3 4.52 4.00 0.33 o 5 3 3 15.46 15.41 0.49 o 6 3 3 12.01 13.13 0.65 o 0 4 3 123.56 127.23 3.10 o 1 4 3 101.01 107.56 0.81 o 2 4 3 32.36 33.58 0.67 o 3 4 3 57.69 62.68 0.87 o 4 4 3 0.82 1.10 0.30 o 5 4 3 11.34 10.53 0.66 o 6 4 3 1.07 1.42 0.47 o 0 5 3 83.09 86.72 1.99 o 1 5 3 6.14 4.65 0.31 o 2 5 3 39.31 39.99 0.64 o 3 5 3 5.47 5.68 0.36 o 4 5 3 0.48 0.71 0.31 o 5 5 3 1.39 1.70 0.45 o 6 5 3 0.88 0.84 0.99 o 0 6 3 51.40 47.06 1.15 o 1 6 3 34.13 30.82 0.45 o 2 6 3 57.29 58.12 0.94 o 3 6 3 5.99 4.84 0.35 o 4 6 3 9.10 7.87 0.53 o 5 6 3 1.40 2.11 0.57 o 0 7 3 3.74 4.94 0.70 o 1 7 3 51.03 56.03 0.62 o 2 7 3 6.21 4.94 0.42 o 3 7 3 7.11 7.83 0.50 o 4 7 3 2.94 3.67 0.61 o 0 8 3 2.70 3.53 0.66 o 1 8 3 11.64 10.78 0.68 o 2 8 3 11.70 11.03 0.53 o 3 8 3 5.88 5.36 0.55 o 4 8 3 1.24 0.49 1.32 o 0 9 3 12.66 14.72 0.86 o 1 9 3 2.80 2.00 0.51 o 2 9 3 2.40 2.76 0.54 o 0 0 4 757.60 758.28 1.46 o 1 0 4 6.63 5.90 0.17 o 2 0 4 56.92 65.67 1.30 o 3 0 4 65.47 60.96 0.68 o 4 0 4 111.40 114.39 1.40 o 5 0 4 47.43 55.15 1.84 o 6 0 4 5.63 5.07 0.69 o 0 1 4 520.87 506.50 7.21 o 1 1 4 212.79 209.30 2.08 o 2 1 4 72.97 65.91 0.95 o 3 1 4 43.05 43.40 0.46 o 4 1 4 24.02 26.56 0.58 o 5 1 4 8.41 7.53 0.34 o 6 1 4 1.50 2.24 0.43 o 0 2 4 95.10 82.33 1.79 o 1 2 4 177.96 176.47 3.05 o 2 2 4 89.12 96.13 1.22 o 3 2 4 92.76 93.05 0.69 o 4 2 4 85.99 92.27 0.88 o 5 2 4 4.64 4.25 0.32 o 6 2 4 3.46 3.93 0.45 o 0 3 4 14.69 15.55 0.64 o 1 3 4 67.08 66.78 1.08 o 2 3 4 149.42 149.88 1.51 o 3 3 4 8.19 6.68 0.38 o 4 3 4 52.01 54.29 0.58 o 5 3 4 1.16 1.03 0.32 o 6 3 4 2.67 3.24 0.47 o 0 4 4 756.81 797.68 2.22 o 1 4 4 36.94 37.14 0.44 o 2 4 4 293.69 294.20 5.34 o 3 4 4 8.62 8.88 0.46 o 4 4 4 7.28 7.65 0.45 o 5 4 4 4.31 3.27 0.49 o 6 4 4 0.35 0.60 0.61 o 0 5 4 8.25 9.55 0.43 o 1 5 4 20.56 18.34 0.46 o 2 5 4 38.69 41.91 0.91 o 3 5 4 79.10 84.90 0.95 o 4 5 4 3.13 2.23 0.38 o 5 5 4 5.93 4.84 0.55 o 0 6 4 0.71 2.08 0.93 o 1 6 4 110.56 112.78 2.08 o 2 6 4 63.91 64.28 0.84 o 3 6 4 2.98 3.46 0.36 o 4 6 4 1.64 2.58 0.38 o 5 6 4 0.34 1.14 0.52 o 0 7 4 0.14 1.38 0.50 o 1 7 4 0.80 1.14 0.30 o 2 7 4 17.12 17.52 0.57 o 3 7 4 3.10 2.53 0.44 o 4 7 4 2.23 2.35 0.55 o 0 8 4 10.35 11.18 1.49 o 1 8 4 3.96 4.68 0.52 o 2 8 4 5.27 5.09 0.49 o 3 8 4 4.74 4.06 0.50 o 4 8 4 0.29 1.35 1.25 o 0 9 4 1.56 2.44 0.68 o 1 9 4 1.30 1.98 0.50 o 2 9 4 3.90 3.95 1.02 o 1 0 5 21.74 19.18 0.52 o 2 0 5 1.01 1.54 0.21 o 3 0 5 0.95 0.93 0.28 o 4 0 5 1.40 1.05 0.32 o 5 0 5 17.11 15.30 1.08 o 6 0 5 0.23 0.02 0.71 o 0 1 5 8.77 8.86 0.36 o 1 1 5 204.12 181.22 1.89 o 2 1 5 221.01 231.80 2.36 o 3 1 5 136.18 134.68 1.12 o 4 1 5 154.02 173.61 1.13 o 5 1 5 39.78 38.55 1.25 o 6 1 5 6.02 5.90 0.65 o 0 2 5 49.88 53.83 1.45 o 1 2 5 403.66 425.56 5.28 o 2 2 5 24.85 21.31 0.27 o 3 2 5 62.66 64.61 0.81 o 4 2 5 44.62 46.72 1.03 o 5 2 5 2.25 1.35 0.33 o 6 2 5 3.84 3.23 0.59 o 0 3 5 193.86 185.28 5.66 o 1 3 5 18.29 20.49 0.34 o 2 3 5 6.63 6.24 0.24 o 3 3 5 207.75 228.34 2.60 o 4 3 5 86.54 90.98 1.69 o 5 3 5 6.23 7.39 0.49 o 6 3 5 24.82 31.75 0.90 o 0 4 5 68.01 61.56 1.67 o 1 4 5 30.54 33.60 0.87 o 2 4 5 92.01 92.50 1.40 o 3 4 5 112.67 114.82 1.81 o 4 4 5 7.44 6.78 0.46 o 5 4 5 17.95 21.89 0.68 o 6 4 5 2.92 3.47 0.92 o 0 5 5 34.96 33.26 0.90 o 1 5 5 15.36 15.70 0.37 o 2 5 5 96.10 98.33 1.09 o 3 5 5 54.50 58.66 0.87 o 4 5 5 4.68 5.17 0.45 o 5 5 5 11.22 12.90 0.81 o 0 6 5 0.41 1.02 0.46 o 1 6 5 9.72 8.56 0.40 o 2 6 5 4.57 4.03 0.32 o 3 6 5 4.73 3.94 0.39 o 4 6 5 5.19 5.43 0.53 o 5 6 5 5.57 6.68 0.92 o 0 7 5 0.22 0.75 0.48 o 1 7 5 6.49 5.02 0.50 o 2 7 5 12.17 12.89 0.58 o 3 7 5 9.27 8.53 0.55 o 4 7 5 4.78 3.76 0.62 o 0 8 5 4.66 4.70 0.68 o 1 8 5 0.13 0.54 0.42 o 2 8 5 0.31 0.94 0.41 o 3 8 5 0.14 1.04 0.44 o 0 9 5 2.91 4.11 0.79 o 1 9 5 0.61 0.49 0.44 o 2 9 5 1.12 0.39 1.01 o 0 0 6 18.24 26.43 0.86 o 1 0 6 198.04 234.31 1.23 o 2 0 6 367.25 404.84 5.96 o 3 0 6 36.92 36.60 0.91 o 4 0 6 83.44 91.03 3.90 o 5 0 6 8.37 7.45 0.79 o 6 0 6 0.03 1.18 0.67 o 0 1 6 90.78 86.72 0.79 o 1 1 6 610.22 633.21 3.91 o 2 1 6 243.43 279.89 2.15 o 3 1 6 106.14 112.42 1.79 o 4 1 6 72.04 75.80 1.07 o 5 1 6 2.47 2.12 0.41 o 6 1 6 0.95 1.06 0.52 o 0 2 6 482.53 488.04 13.96 o 1 2 6 268.07 277.06 3.89 o 2 2 6 16.00 14.95 0.44 o 3 2 6 201.79 200.06 1.86 o 4 2 6 26.69 26.65 0.62 o 5 2 6 4.51 5.15 0.64 o 6 2 6 1.20 1.19 0.50 o 0 3 6 131.47 133.44 5.19 o 1 3 6 191.85 198.80 3.05 o 2 3 6 106.08 100.57 1.55 o 3 3 6 57.61 59.31 1.33 o 4 3 6 5.71 6.49 0.44 o 5 3 6 3.42 3.05 0.44 o 6 3 6 0.88 1.14 0.58 o 0 4 6 12.02 12.98 0.62 o 1 4 6 3.47 3.56 0.27 o 2 4 6 8.08 7.59 0.39 o 3 4 6 5.35 6.74 0.35 o 4 4 6 8.16 8.24 0.51 o 5 4 6 2.40 2.55 0.48 o 6 4 6 4.27 4.13 1.30 o 0 5 6 24.24 22.75 0.71 o 1 5 6 3.39 3.25 0.30 o 2 5 6 6.83 6.76 0.40 o 3 5 6 11.92 13.39 0.52 o 4 5 6 0.28 0.97 0.40 o 5 5 6 7.48 8.88 0.65 o 0 6 6 9.07 9.49 0.69 o 1 6 6 8.38 9.00 0.51 o 2 6 6 1.12 1.54 0.33 o 3 6 6 0.30 0.76 0.36 o 4 6 6 2.17 2.59 0.49 o 5 6 6 2.60 3.07 1.41 o 0 7 6 0.38 0.95 0.46 o 1 7 6 5.16 6.47 0.50 o 2 7 6 10.85 13.24 0.56 o 3 7 6 1.37 2.21 0.49 o 4 7 6 1.35 2.75 0.61 o 0 8 6 6.92 5.54 0.86 o 1 8 6 3.82 3.98 0.60 o 2 8 6 8.98 9.13 0.64 o 3 8 6 5.07 5.05 0.77 o 0 9 6 6.79 7.50 1.47 o 1 9 6 1.82 2.07 0.64 o 1 0 7 489.89 530.47 6.60 o 2 0 7 15.96 13.76 0.38 o 3 0 7 107.38 118.90 1.81 o 4 0 7 94.55 97.27 1.03 o 5 0 7 9.53 7.02 0.83 o 6 0 7 0.05 0.83 0.83 o 0 1 7 29.48 27.30 0.75 o 1 1 7 42.91 40.83 0.60 o 2 1 7 57.56 55.92 0.77 o 3 1 7 2.78 2.54 0.27 o 4 1 7 22.66 23.60 0.49 o 5 1 7 17.63 15.41 0.65 o 6 1 7 1.52 2.36 0.62 o 0 2 7 0.09 0.46 0.19 o 1 2 7 31.10 27.92 0.39 o 2 2 7 75.01 84.14 0.52 o 3 2 7 32.36 32.02 0.51 o 4 2 7 93.38 104.34 1.36 o 5 2 7 11.45 12.56 0.69 o 6 2 7 9.09 9.35 0.74 o 0 3 7 157.53 142.90 2.43 o 1 3 7 104.13 104.94 1.22 o 2 3 7 16.62 16.00 0.41 o 3 3 7 178.82 195.37 4.08 o 4 3 7 25.85 25.30 0.62 o 5 3 7 10.69 10.67 0.71 o 6 3 7 4.58 5.00 1.45 o 0 4 7 9.80 12.02 0.45 o 1 4 7 5.09 4.66 0.35 o 2 4 7 32.03 29.91 0.82 o 3 4 7 61.13 66.17 0.86 o 4 4 7 1.98 2.17 0.50 o 5 4 7 14.54 17.49 0.79 o 0 5 7 0.88 1.43 0.35 o 1 5 7 7.11 6.59 0.40 o 2 5 7 17.33 18.67 0.83 o 3 5 7 17.66 15.88 0.73 o 4 5 7 3.55 3.29 0.52 o 5 5 7 9.96 11.26 0.79 o 0 6 7 0.06 0.70 0.58 o 1 6 7 0.18 0.53 0.31 o 2 6 7 18.33 16.57 0.57 o 3 6 7 7.48 6.89 0.53 o 4 6 7 3.98 4.44 0.58 o 5 6 7 1.25 1.31 1.18 o 0 7 7 0.62 0.63 0.60 o 1 7 7 3.41 2.82 0.50 o 2 7 7 2.23 2.79 0.53 o 3 7 7 3.60 3.31 0.56 o 4 7 7 3.05 2.34 1.03 o 0 8 7 0.48 0.90 0.71 o 1 8 7 3.02 3.12 0.57 o 2 8 7 4.49 5.39 0.65 o 3 8 7 3.78 2.54 1.26 o 0 9 7 1.05 1.43 1.06 o 1 9 7 0.73 0.78 1.19 o 0 0 8 106.94 101.54 6.32 o 1 0 8 37.89 41.55 0.40 o 2 0 8 34.63 44.21 0.91 o 3 0 8 28.22 28.53 1.32 o 4 0 8 7.53 7.30 0.74 o 5 0 8 1.00 1.09 0.57 o 6 0 8 0.15 0.45 0.79 o 0 1 8 34.88 29.67 0.55 o 1 1 8 35.42 32.46 0.68 o 2 1 8 89.01 88.64 1.06 o 3 1 8 36.41 38.01 0.61 o 4 1 8 51.52 53.58 1.34 o 5 1 8 18.76 17.71 0.63 o 6 1 8 1.93 1.76 0.77 o 0 2 8 36.49 34.67 1.25 o 1 2 8 76.47 76.66 0.88 o 2 2 8 66.96 65.99 1.05 o 3 2 8 16.37 16.55 0.45 o 4 2 8 5.05 5.45 0.41 o 5 2 8 1.23 1.06 0.48 o 6 2 8 2.29 3.59 0.81 o 0 3 8 47.83 44.95 1.50 o 1 3 8 56.83 57.49 1.45 o 2 3 8 45.14 45.98 0.54 o 3 3 8 7.83 7.87 0.51 o 4 3 8 15.21 14.16 0.73 o 5 3 8 4.72 4.71 0.55 o 0 4 8 13.99 15.48 0.66 o 1 4 8 29.07 24.46 0.63 o 2 4 8 35.11 36.48 0.63 o 3 4 8 36.31 40.54 0.66 o 4 4 8 6.66 6.78 0.63 o 5 4 8 6.26 6.19 0.65 o 0 5 8 43.87 45.41 0.85 o 1 5 8 40.69 42.18 0.63 o 2 5 8 107.54 118.37 2.19 o 3 5 8 3.19 3.96 0.65 o 4 5 8 3.22 3.26 0.55 o 5 5 8 1.05 0.69 0.79 o 0 6 8 3.06 1.00 0.93 o 1 6 8 2.12 1.29 0.37 o 2 6 8 30.49 32.96 0.81 o 3 6 8 14.75 14.88 0.83 o 4 6 8 2.73 3.47 0.58 o 0 7 8 8.31 9.59 1.53 o 1 7 8 9.98 9.88 0.82 o 2 7 8 3.57 3.73 0.59 o 3 7 8 1.88 2.30 0.69 o 0 8 8 2.12 2.39 1.23 o 1 8 8 1.08 1.06 0.62 o 2 8 8 2.13 2.66 0.75 o 1 0 9 19.55 17.04 0.57 o 2 0 9 2.40 2.24 0.38 o 3 0 9 25.68 22.83 0.68 o 4 0 9 11.31 10.84 0.71 o 5 0 9 15.71 15.49 0.93 o 6 0 9 2.21 1.74 0.97 o 0 1 9 17.07 14.69 0.45 o 1 1 9 24.76 23.53 0.50 o 2 1 9 6.85 7.41 0.53 o 3 1 9 17.17 14.88 0.56 o 4 1 9 44.55 49.16 0.75 o 5 1 9 9.74 8.86 0.59 o 0 2 9 118.48 120.86 2.68 o 1 2 9 1.04 1.32 0.25 o 2 2 9 9.47 9.95 0.40 o 3 2 9 0.38 0.68 0.26 o 4 2 9 25.74 27.57 0.64 o 5 2 9 3.40 2.39 0.56 o 6 2 9 1.07 1.43 1.18 o 0 3 9 3.42 2.98 0.49 o 1 3 9 34.06 32.43 1.12 o 2 3 9 27.64 26.53 0.66 o 3 3 9 10.61 8.73 0.58 o 4 3 9 3.04 2.74 0.54 o 5 3 9 10.91 12.57 0.71 o 0 4 9 6.20 5.89 0.53 o 1 4 9 35.13 35.69 0.54 o 2 4 9 0.49 1.02 0.33 o 3 4 9 8.21 7.79 0.59 o 4 4 9 2.82 3.43 0.59 o 5 4 9 2.18 2.23 0.59 o 0 5 9 35.11 31.18 1.33 o 1 5 9 2.83 2.67 0.39 o 2 5 9 7.51 7.06 0.43 o 3 5 9 4.38 4.01 0.59 o 4 5 9 3.03 3.18 0.60 o 0 6 9 0.46 1.93 1.10 o 1 6 9 8.67 7.74 0.60 o 2 6 9 3.29 2.90 0.47 o 3 6 9 2.10 3.81 0.70 o 4 6 9 1.47 1.82 0.69 o 0 7 9 0.23 0.84 0.90 o 1 7 9 9.64 7.65 0.84 o 2 7 9 7.51 9.20 0.90 o 3 7 9 4.38 4.89 0.77 o 0 8 9 3.17 3.20 1.32 o 1 8 9 2.35 2.30 1.23 o 2 8 9 1.54 1.72 1.06 o 0 0 10 124.38 130.58 5.47 o 1 0 10 7.28 7.10 0.50 o 2 0 10 0.33 1.05 0.46 o 3 0 10 1.85 2.42 0.58 o 4 0 10 4.85 5.07 0.60 o 5 0 10 0.13 0.11 0.62 o 0 1 10 65.77 60.17 1.57 o 1 1 10 119.90 119.90 0.76 o 2 1 10 10.94 9.30 0.35 o 3 1 10 73.65 74.79 0.95 o 4 1 10 1.60 1.36 0.34 o 5 1 10 0.35 0.63 0.44 o 0 2 10 44.52 44.01 1.49 o 1 2 10 48.27 46.82 0.84 o 2 2 10 12.49 11.98 0.44 o 3 2 10 12.29 11.00 0.48 o 4 2 10 9.84 10.52 0.57 o 5 2 10 4.64 4.86 0.68 o 0 3 10 17.67 21.59 0.71 o 1 3 10 94.26 95.21 1.75 o 2 3 10 35.37 31.82 0.91 o 3 3 10 2.33 2.30 0.51 o 4 3 10 8.05 8.48 0.65 o 5 3 10 2.06 2.60 0.52 o 0 4 10 52.02 47.25 1.00 o 1 4 10 12.15 12.01 0.82 o 2 4 10 70.43 69.77 3.78 o 3 4 10 2.36 2.38 0.52 o 4 4 10 5.26 4.71 0.55 o 5 4 10 1.78 2.21 1.16 o 0 5 10 11.83 10.96 0.78 o 1 5 10 9.62 8.95 0.51 o 2 5 10 11.02 9.90 1.11 o 3 5 10 5.86 5.67 0.65 o 4 5 10 0.04 0.58 0.54 o 0 6 10 8.16 8.43 1.26 o 1 6 10 17.23 15.98 0.67 o 2 6 10 4.74 2.22 0.57 o 3 6 10 3.01 2.73 0.67 o 0 7 10 0.48 0.60 1.20 o 1 7 10 0.51 0.20 0.74 o 2 7 10 0.49 0.23 0.61 o 1 0 11 5.19 3.81 0.39 o 2 0 11 27.84 23.64 0.76 o 3 0 11 24.49 22.38 0.89 o 4 0 11 11.58 11.99 1.02 o 5 0 11 9.72 10.53 1.41 o 0 1 11 55.17 61.68 0.90 o 1 1 11 4.02 3.82 0.32 o 2 1 11 9.52 8.13 0.43 o 3 1 11 3.06 3.06 0.43 o 4 1 11 0.73 1.19 0.42 o 5 1 11 2.16 1.58 0.69 o 0 2 11 61.06 60.22 1.61 o 1 2 11 25.08 28.13 0.89 o 2 2 11 24.43 21.10 0.53 o 3 2 11 40.61 39.55 1.21 o 4 2 11 3.55 3.09 0.67 o 5 2 11 0.83 0.99 0.82 o 0 3 11 0.00 0.31 0.35 o 1 3 11 43.27 44.74 0.55 o 2 3 11 10.36 9.01 0.54 o 3 3 11 7.40 5.62 0.57 o 4 3 11 3.17 3.11 0.74 o 0 4 11 0.66 1.40 0.42 o 1 4 11 21.60 18.88 0.56 o 2 4 11 10.05 9.52 0.61 o 3 4 11 5.95 5.64 0.60 o 4 4 11 1.35 1.93 0.62 o 0 5 11 3.88 4.07 0.59 o 1 5 11 2.89 2.07 0.44 o 2 5 11 0.36 0.95 0.48 o 3 5 11 0.93 1.28 0.61 o 0 6 11 0.54 0.70 0.64 o 1 6 11 3.57 2.37 0.49 o 2 6 11 0.66 1.41 0.63 o 3 6 11 4.01 3.40 0.92 o 0 7 11 0.10 -0.30 1.27 o 1 7 11 0.86 0.22 0.79 o 2 7 11 1.01 0.47 1.23 o 0 0 12 15.05 17.19 1.36 o 1 0 12 83.13 94.01 3.13 o 2 0 12 1.57 1.64 0.55 o 3 0 12 42.46 42.63 2.11 o 4 0 12 1.81 1.27 0.78 o 5 0 12 1.65 1.42 1.01 o 0 1 12 304.25 347.67 6.10 o 1 1 12 70.58 71.16 1.54 o 2 1 12 31.34 29.46 0.67 o 3 1 12 0.86 1.13 0.40 o 4 1 12 5.42 4.18 0.57 o 5 1 12 0.45 0.57 0.74 o 0 2 12 10.62 8.06 0.85 o 1 2 12 18.14 17.92 0.47 o 2 2 12 25.81 24.95 0.51 o 3 2 12 1.08 1.74 0.45 o 4 2 12 0.28 0.56 0.59 o 0 3 12 1.76 1.86 0.42 o 1 3 12 31.63 30.59 0.61 o 2 3 12 4.55 4.18 0.59 o 3 3 12 2.27 2.76 0.56 o 4 3 12 3.05 2.96 0.57 o 0 4 12 25.95 28.07 0.86 o 1 4 12 0.53 0.65 0.44 o 2 4 12 1.01 1.33 0.49 o 3 4 12 2.39 2.93 0.61 o 4 4 12 1.56 0.57 1.04 o 0 5 12 1.06 1.69 0.53 o 1 5 12 1.46 2.61 0.45 o 2 5 12 13.90 13.95 1.54 o 3 5 12 0.74 1.05 0.77 o 0 6 12 0.69 1.39 0.80 o 1 6 12 2.05 2.17 0.53 o 2 6 12 0.12 0.94 0.69 o 0 7 12 0.29 0.29 1.09 o 1 7 12 0.01 0.31 1.25 o 1 0 13 59.84 57.62 1.81 o 2 0 13 0.76 1.56 0.52 o 3 0 13 24.02 22.60 0.89 o 4 0 13 8.42 10.85 1.07 o 0 1 13 37.55 36.83 0.86 o 1 1 13 0.43 1.15 0.34 o 2 1 13 3.54 3.23 0.38 o 3 1 13 1.80 1.34 0.46 o 4 1 13 2.29 2.29 0.57 o 0 2 13 15.38 17.08 0.91 o 1 2 13 3.59 3.78 0.37 o 2 2 13 38.31 37.34 0.56 o 3 2 13 1.97 2.13 0.47 o 4 2 13 8.65 9.87 0.75 o 0 3 13 2.74 3.12 0.54 o 1 3 13 15.09 14.06 0.46 o 2 3 13 0.16 0.81 0.46 o 3 3 13 0.37 0.91 0.56 o 4 3 13 0.30 -0.12 1.14 o 0 4 13 2.87 3.79 0.61 o 1 4 13 1.17 0.98 0.46 o 2 4 13 4.39 4.09 0.57 o 3 4 13 1.98 1.26 0.57 o 0 5 13 0.04 0.48 0.81 o 1 5 13 1.71 2.43 0.84 o 2 5 13 0.56 0.29 0.50 o 0 6 13 0.07 0.43 0.70 o 1 6 13 2.79 2.93 0.59 o 0 0 14 35.26 35.10 1.59 o 1 0 14 6.53 6.64 0.67 o 2 0 14 16.45 14.08 0.72 o 3 0 14 13.55 14.19 2.05 o 4 0 14 0.03 0.48 0.88 o 0 1 14 1.55 1.32 0.53 o 1 1 14 0.40 1.16 0.39 o 2 1 14 2.18 1.87 0.39 o 3 1 14 1.82 1.72 0.43 o 4 1 14 1.63 0.78 0.59 o 0 2 14 1.89 1.55 0.60 o 1 2 14 12.31 11.72 0.58 o 2 2 14 1.02 1.59 0.42 o 3 2 14 1.62 2.34 0.51 o 0 3 14 21.34 26.69 1.67 o 1 3 14 17.69 16.38 0.53 o 2 3 14 0.32 0.87 0.44 o 3 3 14 0.13 0.68 0.49 o 0 4 14 5.12 6.11 0.72 o 1 4 14 2.88 4.41 0.65 o 2 4 14 10.40 11.30 0.83 o 0 5 14 0.13 1.01 0.75 o 1 5 14 12.93 16.48 0.86 o 2 5 14 0.88 2.00 1.28 o 0 6 14 1.05 1.11 1.29 o 1 0 15 3.60 3.36 0.68 o 2 0 15 0.26 0.14 0.64 o 3 0 15 0.95 2.10 0.71 o 0 1 15 3.58 4.38 0.76 o 1 1 15 3.12 2.76 0.45 o 2 1 15 0.50 0.86 0.44 o 3 1 15 0.42 1.31 0.51 o 0 2 15 0.07 0.87 0.55 o 1 2 15 15.69 15.33 0.58 o 2 2 15 5.48 5.77 0.55 o 3 2 15 2.63 2.11 0.96 o 0 3 15 0.02 0.43 0.71 o 1 3 15 0.86 1.28 0.51 o 2 3 15 0.52 1.75 0.48 o 3 3 15 5.01 3.20 1.25 o 0 4 15 2.57 3.73 0.89 o 1 4 15 0.03 0.66 0.57 o 0 0 16 16.32 20.18 1.66 o 1 0 16 7.78 8.38 1.38 o 2 0 16 0.60 0.64 0.61 o 0 1 16 15.07 17.67 1.14 o 1 1 16 2.45 2.74 0.51 o 2 1 16 1.02 1.68 0.47 o 0 2 16 0.82 0.81 0.62 o 1 2 16 0.99 1.61 0.53 o 2 2 16 0.14 1.01 0.68 o 0 3 16 6.68 8.19 1.84 o 1 3 16 0.05 -0.02 1.25 o 0 4 16 0.10 0.07 1.24 o 1 0 17 0.01 0.64 1.08 o 0 1 17 0.96 1.45 1.32 o 1 1 17 0.74 0.65 0.93 o 1 2 17 0.95 0.50 1.00 o