#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/45/2214565.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214565_Fobs loop_ _publ_author_name 'Huang, Jin-Shang' 'Li, Ming-Tian' _publ_section_title ; Bis[\m-2-hydroxy-N'-(4-hydroxy-2-oxidobenzylidene)benzohydrazide]bis[pyridinezinc(II)] dimethylformamide disolvate ; _journal_coeditor_code CF2107 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2170 _journal_page_last m2171 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.127 _cell_angle_gamma 90.000 _cell_length_a 24.5015 _cell_length_b 10.3868 _cell_length_c 28.8550 _exptl_crystal_F_000 3024.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file cf2107Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 051020bm in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 724.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 53.19 -0.54 0.90 o 2 0 0 60.43 59.61 10.30 o 3 0 0 188392.84 193711.45 5638.92 o 4 0 0 442.26 346.15 51.37 o 5 0 0 104.38 106.16 14.57 o 6 0 0 104511.37 99881.81 3469.35 o 7 0 0 2346.00 2114.22 64.52 o 8 0 0 3118.24 3017.18 87.96 o 9 0 0 10342.04 10069.68 257.46 o 10 0 0 2664.09 2407.78 77.02 o 11 0 0 3518.35 3418.16 108.18 o 12 0 0 19671.68 20870.65 518.01 o 13 0 0 3667.67 3694.52 148.66 o 14 0 0 3565.20 3586.48 113.08 o 15 0 0 19100.33 19078.99 598.70 o 16 0 0 1889.32 2079.12 110.75 o 17 0 0 1098.22 1380.66 94.11 o 18 0 0 14750.89 14174.78 469.18 o 19 0 0 993.82 994.12 86.34 o 20 0 0 59.99 13.16 70.17 o 21 0 0 8518.26 8300.04 311.81 o 22 0 0 1871.67 1616.75 117.86 o 23 0 0 531.41 529.34 96.45 o 24 0 0 1798.99 1798.28 130.50 o 25 0 0 8.52 39.50 54.43 o 26 0 0 7.17 -7.59 88.87 o 27 0 0 60.06 -115.42 76.95 o 28 0 0 147.56 110.00 111.63 o 1 1 0 235.50 290.50 22.54 o 2 1 0 384.23 248.44 19.24 o 3 1 0 29461.86 35579.61 1066.58 o 4 1 0 1809.79 1742.82 41.22 o 5 1 0 665.42 761.83 34.69 o 6 1 0 1102.05 1287.99 30.66 o 7 1 0 1875.04 1964.41 43.36 o 8 1 0 1780.18 1793.90 46.61 o 9 1 0 1764.34 1720.48 41.43 o 10 1 0 30.56 48.96 9.98 o 11 1 0 29.03 44.38 10.84 o 12 1 0 324.34 353.47 19.44 o 13 1 0 589.38 559.22 24.93 o 14 1 0 283.48 304.34 26.77 o 15 1 0 6935.25 7298.17 161.75 o 16 1 0 25.66 34.64 29.10 o 17 1 0 263.25 241.82 35.23 o 18 1 0 5622.38 5592.45 156.33 o 19 1 0 123.02 94.64 33.18 o 20 1 0 795.21 698.63 61.24 o 21 1 0 110.77 87.20 35.12 o 22 1 0 1.60 0.90 33.64 o 23 1 0 179.41 181.26 41.78 o 24 1 0 2109.78 2362.14 169.88 o 25 1 0 374.40 398.43 73.21 o 26 1 0 172.22 282.81 76.79 o 27 1 0 46.01 82.32 70.77 o 28 1 0 10.30 78.27 100.52 o 0 2 0 18531.93 20950.65 623.93 o 1 2 0 571.09 355.99 14.30 o 2 2 0 3168.53 2534.60 61.95 o 3 2 0 11852.22 12934.81 247.58 o 4 2 0 4890.34 4706.13 156.04 o 5 2 0 1058.64 767.63 30.25 o 6 2 0 7821.58 8229.93 184.48 o 7 2 0 4.25 20.17 8.17 o 8 2 0 565.05 442.59 19.23 o 9 2 0 3150.91 3392.08 71.22 o 10 2 0 924.31 843.85 28.43 o 11 2 0 0.05 6.00 13.24 o 12 2 0 2317.61 2435.29 68.38 o 13 2 0 412.26 385.71 29.12 o 14 2 0 55.31 65.59 19.20 o 15 2 0 39.20 51.10 20.19 o 16 2 0 539.23 486.58 36.52 o 17 2 0 4.17 -11.35 24.37 o 18 2 0 176.30 233.80 38.72 o 19 2 0 2.00 -6.48 27.80 o 20 2 0 244.12 259.83 40.88 o 21 2 0 403.54 494.61 51.50 o 22 2 0 4.99 5.02 31.86 o 23 2 0 25.76 24.04 36.23 o 24 2 0 360.27 499.39 57.12 o 25 2 0 34.60 31.80 48.09 o 26 2 0 59.88 -24.84 63.48 o 27 2 0 60.14 64.02 69.30 o 28 2 0 51.76 65.82 104.04 o 1 3 0 265.41 306.41 16.24 o 2 3 0 580.92 583.59 30.43 o 3 3 0 12420.26 13596.68 292.81 o 4 3 0 3229.33 3586.01 79.00 o 5 3 0 18194.53 18617.72 354.46 o 6 3 0 352.01 413.70 22.91 o 7 3 0 901.19 896.34 38.18 o 8 3 0 710.83 714.12 35.50 o 9 3 0 7799.08 7822.35 148.14 o 10 3 0 933.86 902.46 54.28 o 11 3 0 126.30 136.91 16.11 o 12 3 0 5837.44 5516.98 127.29 o 13 3 0 170.50 171.55 24.92 o 14 3 0 182.16 190.85 25.75 o 15 3 0 3561.28 3681.00 99.08 o 16 3 0 317.51 286.26 32.04 o 17 3 0 509.94 521.48 57.30 o 18 3 0 113.38 45.17 28.67 o 19 3 0 230.49 156.46 36.79 o 20 3 0 25.74 -10.19 30.61 o 21 3 0 641.44 721.27 60.77 o 22 3 0 282.35 357.10 49.42 o 23 3 0 836.67 892.27 69.67 o 24 3 0 912.51 956.47 74.02 o 25 3 0 334.09 320.27 65.64 o 26 3 0 677.94 789.12 99.02 o 27 3 0 1035.78 1065.58 180.45 o 28 3 0 169.66 279.21 146.85 o 0 4 0 7992.06 7573.40 250.19 o 1 4 0 955.05 903.06 43.50 o 2 4 0 512.93 453.08 25.22 o 3 4 0 56154.36 59414.14 1230.14 o 4 4 0 834.89 836.08 33.93 o 5 4 0 782.36 774.60 31.27 o 6 4 0 73463.80 78110.78 1442.15 o 7 4 0 1932.61 2089.18 58.94 o 8 4 0 383.46 373.23 27.10 o 9 4 0 139020.55 145384.44 2670.59 o 10 4 0 2029.52 2001.34 71.19 o 11 4 0 130.12 104.78 18.87 o 12 4 0 25552.09 25168.40 488.78 o 13 4 0 2061.93 1922.13 64.93 o 14 4 0 885.58 858.43 53.04 o 15 4 0 17859.49 16095.20 402.91 o 16 4 0 537.30 452.87 38.40 o 17 4 0 15.21 2.14 23.90 o 18 4 0 48.82 72.75 28.28 o 19 4 0 9.88 17.69 31.75 o 20 4 0 0.76 1.86 33.41 o 21 4 0 2774.59 2775.72 113.41 o 22 4 0 296.95 341.52 49.08 o 23 4 0 0.78 22.15 36.65 o 24 4 0 925.42 941.06 88.17 o 25 4 0 473.21 553.82 77.50 o 26 4 0 0.87 21.52 51.25 o 27 4 0 301.88 421.05 188.57 o 1 5 0 811.74 893.07 50.29 o 2 5 0 364.77 388.39 35.65 o 3 5 0 1329.50 1328.56 54.48 o 4 5 0 1015.06 896.14 41.21 o 5 5 0 146.98 161.56 28.80 o 6 5 0 2638.97 2472.89 80.55 o 7 5 0 560.13 582.48 31.98 o 8 5 0 121.76 83.60 20.49 o 9 5 0 5644.71 5298.29 123.45 o 10 5 0 1945.58 2005.61 65.17 o 11 5 0 671.64 588.16 38.67 o 12 5 0 911.73 849.22 54.05 o 13 5 0 621.98 621.72 47.48 o 14 5 0 14.48 -2.99 23.11 o 15 5 0 6366.97 6358.98 187.49 o 16 5 0 2284.98 1914.02 73.34 o 17 5 0 822.89 787.20 58.52 o 18 5 0 404.24 404.39 48.13 o 19 5 0 123.67 158.16 38.74 o 20 5 0 2.78 -18.03 32.02 o 21 5 0 592.71 615.66 59.81 o 22 5 0 23.35 91.63 39.07 o 23 5 0 6.36 -14.58 39.01 o 24 5 0 183.42 205.64 58.82 o 25 5 0 0.24 -71.68 47.79 o 26 5 0 14.60 25.12 54.22 o 27 5 0 193.86 233.21 90.04 o 0 6 0 10449.58 10678.82 500.70 o 1 6 0 259.11 217.84 58.52 o 2 6 0 38.39 40.65 28.93 o 3 6 0 14706.86 14781.27 389.32 o 4 6 0 75.96 45.72 18.34 o 5 6 0 2018.35 2018.70 60.03 o 6 6 0 4228.83 3938.78 97.17 o 7 6 0 453.05 437.51 30.78 o 8 6 0 11.78 -8.02 17.36 o 9 6 0 473.38 435.74 37.45 o 10 6 0 286.87 264.50 32.19 o 11 6 0 209.66 251.60 29.83 o 12 6 0 6226.99 5833.62 141.34 o 13 6 0 3457.99 3006.86 97.70 o 14 6 0 2379.96 2374.79 82.38 o 15 6 0 189.47 121.37 36.16 o 16 6 0 40.61 18.62 34.88 o 17 6 0 1.06 -2.60 26.32 o 18 6 0 1178.79 1225.95 73.42 o 19 6 0 0.19 26.73 34.83 o 20 6 0 4.65 50.90 37.04 o 21 6 0 651.11 711.35 63.83 o 22 6 0 15.45 -31.32 38.70 o 23 6 0 40.81 63.49 41.00 o 24 6 0 160.11 216.17 61.25 o 25 6 0 130.95 89.06 69.05 o 26 6 0 10.70 -14.86 57.81 o 1 7 0 125.69 128.95 37.73 o 2 7 0 282.10 332.09 51.45 o 3 7 0 292.92 340.43 51.10 o 4 7 0 80.56 98.75 36.35 o 5 7 0 6.14 21.18 23.02 o 6 7 0 702.87 811.81 146.26 o 7 7 0 77.81 53.38 27.75 o 8 7 0 78.90 120.18 31.12 o 9 7 0 35.84 28.03 27.56 o 10 7 0 527.50 431.14 47.02 o 11 7 0 228.56 330.88 45.44 o 12 7 0 1412.83 1236.05 75.06 o 13 7 0 35.70 39.91 35.11 o 14 7 0 318.96 246.82 53.07 o 15 7 0 2843.71 2700.50 207.24 o 16 7 0 40.39 32.98 39.25 o 17 7 0 199.81 220.78 48.13 o 18 7 0 2080.72 2055.13 110.45 o 19 7 0 45.23 -13.29 60.22 o 20 7 0 319.88 377.17 60.60 o 21 7 0 603.90 686.50 78.96 o 22 7 0 158.26 242.87 59.12 o 23 7 0 169.07 114.37 82.91 o 24 7 0 343.36 228.49 88.06 o 25 7 0 9.69 58.10 70.31 o 1 8 0 583.53 551.88 68.98 o 2 8 0 58.39 0.32 37.11 o 3 8 0 12146.37 11357.36 390.44 o 4 8 0 805.92 769.43 77.97 o 5 8 0 126.90 169.50 50.47 o 6 8 0 7883.69 7473.73 279.52 o 7 8 0 600.69 622.39 74.14 o 8 8 0 137.42 219.27 49.57 o 9 8 0 886.19 825.62 83.46 o 10 8 0 335.02 366.67 99.43 o 11 8 0 531.11 417.95 71.24 o 12 8 0 8622.01 7958.55 423.75 o 13 8 0 602.38 607.23 79.27 o 14 8 0 0.81 2.51 55.81 o 15 8 0 1314.07 1533.20 243.85 o 16 8 0 1123.30 1167.61 108.81 o 17 8 0 9.28 -3.16 51.83 o 18 8 0 2087.69 2253.13 151.71 o 19 8 0 930.84 850.70 167.17 o 20 8 0 24.80 2.59 90.76 o 21 8 0 665.88 638.61 210.52 o 22 8 0 237.39 308.33 118.13 o 23 8 0 10.99 81.28 104.58 o 1 9 0 851.80 869.17 123.55 o 2 9 0 596.83 683.37 150.37 o 3 9 0 1161.80 1166.72 147.93 o 4 9 0 457.53 456.80 70.63 o 5 9 0 139.96 175.44 54.17 o 6 9 0 11.02 -22.34 42.66 o 7 9 0 386.54 375.69 65.96 o 8 9 0 4.85 32.38 43.36 o 9 9 0 215.58 165.25 67.46 o 10 9 0 309.52 403.55 69.27 o 11 9 0 484.05 554.48 112.17 o 12 9 0 85.04 9.93 50.62 o 13 9 0 570.52 571.40 82.17 o 14 9 0 142.35 173.89 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123.82 o 9 11 0 439.73 569.82 91.57 o 10 11 0 30.13 3.72 52.13 o 11 11 0 17.18 -15.41 69.90 o 12 11 0 213.30 211.03 74.76 o 13 11 0 0.72 70.69 92.39 o 14 11 0 18.10 21.37 58.62 o 15 11 0 428.71 499.25 95.21 o 16 11 0 50.58 26.64 71.58 o 0 12 0 505.64 421.04 119.21 o 1 12 0 38.77 39.96 62.32 o 2 12 0 72.57 153.15 72.22 o 3 12 0 1349.69 1564.30 139.14 o 4 12 0 123.38 57.62 78.84 o 5 12 0 49.78 15.71 82.37 o 6 12 0 382.90 436.97 99.98 o 7 12 0 133.01 273.90 76.79 o 8 12 0 4.28 -54.11 56.13 o 9 12 0 468.48 503.39 92.52 o 10 12 0 190.15 134.38 70.13 o 11 12 0 6.54 -9.01 79.66 o 12 12 0 63.88 36.52 71.24 o 13 12 0 322.78 608.53 104.64 o 1 13 0 194.42 276.19 84.75 o 2 13 0 238.59 249.73 125.99 o 3 13 0 1.43 -4.53 75.53 o 4 13 0 143.76 149.33 87.28 o 5 13 0 69.30 68.53 78.35 o 6 13 0 67.68 28.45 75.46 o -29 1 1 0.83 -26.99 71.96 o -28 1 1 3.73 18.89 68.16 o -27 1 1 13.59 18.27 91.85 o -26 1 1 43.68 41.90 41.16 o -25 1 1 946.51 985.71 87.29 o -24 1 1 140.45 149.44 50.96 o -23 1 1 497.31 535.25 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320.30 320.18 19.61 o 11 1 1 27687.28 29318.16 555.13 o 12 1 1 1026.67 1069.56 40.65 o 13 1 1 664.10 653.05 40.13 o 14 1 1 8009.37 7785.88 189.29 o 15 1 1 428.75 407.39 31.15 o 16 1 1 177.28 79.57 25.65 o 17 1 1 6947.48 6376.91 185.13 o 18 1 1 621.81 526.66 47.18 o 19 1 1 384.16 402.35 43.74 o 20 1 1 5838.23 5326.33 218.94 o 21 1 1 1164.17 1097.39 100.19 o 22 1 1 497.83 481.50 51.90 o 23 1 1 868.70 759.92 62.65 o 24 1 1 143.01 145.05 55.86 o 25 1 1 10.09 -33.93 57.00 o 26 1 1 45.98 -24.44 61.18 o 27 1 1 123.10 191.85 77.88 o 28 1 1 12.27 -40.64 74.32 o -29 2 1 119.40 4.34 107.83 o -28 2 1 808.97 815.59 117.19 o -27 2 1 401.66 373.60 90.24 o -26 2 1 323.63 342.70 55.72 o -25 2 1 2497.76 2545.15 111.38 o -24 2 1 171.09 223.12 46.34 o -23 2 1 211.92 267.20 46.61 o -22 2 1 1274.03 1291.63 76.44 o -21 2 1 265.63 310.98 43.89 o -20 2 1 12.36 10.16 30.23 o -19 2 1 7899.92 7827.17 205.15 o -18 2 1 2976.34 2996.28 103.75 o -17 2 1 544.25 528.07 45.44 o -16 2 1 11010.61 10959.85 232.54 o -15 2 1 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