#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214584.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214584_Fobs loop_ _publ_author_name 'Wang, Qiang' 'Wang, Daqi' _publ_section_title ; Di-\m-chlorido-bis(chlorido{2-[4-(dimethylamino)benzylideneamino]pyridine-\kN}mercury(II)) ; _journal_coeditor_code CI2406 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2074 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.597 _cell_angle_beta 79.807 _cell_angle_gamma 79.619 _cell_length_a 8.9474 _cell_length_b 9.0853 _cell_length_c 10.2019 _exptl_crystal_F_000 468.00 _reflns_d_resolution_high 0.8407 _[local]_cod_data_source_file ci2406Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 060907b in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 167.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 20209.35 19857.01 790.81 o 2 0 0 17009.38 17753.85 579.06 o 3 0 0 5594.55 5622.52 227.71 o 4 0 0 2371.66 2518.64 124.29 o 5 0 0 1504.61 1604.82 62.61 o 6 0 0 727.76 694.95 65.65 o 7 0 0 1218.28 1202.28 63.79 o 8 0 0 777.04 879.98 55.43 o 9 0 0 320.50 350.85 39.66 o 10 0 0 239.37 285.81 61.51 o -10 1 0 9.92 11.70 33.49 o -9 1 0 152.68 184.31 32.29 o -8 1 0 654.89 657.95 47.51 o -7 1 0 2460.72 2598.79 119.55 o -6 1 0 3996.81 4240.88 154.54 o -5 1 0 6934.15 7409.57 248.75 o -4 1 0 3345.76 3544.41 121.59 o -3 1 0 10619.58 10887.32 357.40 o -2 1 0 4199.11 4341.17 103.55 o -1 1 0 984.71 1080.69 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