#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:33:09 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181066 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/46/2214633.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214633_Fobs loop_ _publ_author_name 'Boyle, Grant A.' 'Govender, Thavendran' 'Kruger, Hendrik G.' 'Maguire, Glenn E. M.' 'Naicker, Tricia' _publ_section_title ; (S)-(+)-2-Formamido-4-methylpentanoic acid ; _journal_coeditor_code EZ2086 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3445 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.6041 _cell_length_b 10.0758 _cell_length_c 9.2936 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.8111 _cod_data_source_file ez2086Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 7m_kznd5_0s in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 118.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2358.18 2357.73 39.65 o 4 0 0 464.27 454.19 10.73 o 6 0 0 505.83 528.92 15.34 o 8 0 0 1.42 1.66 0.50 o 10 0 0 38.24 38.44 1.64 o 1 1 0 4657.64 4493.69 229.82 o 2 1 0 78.14 61.24 0.49 o 3 1 0 4428.27 4692.27 59.25 o 4 1 0 70.87 70.94 0.65 o 5 1 0 1.43 2.27 0.49 o 6 1 0 147.58 148.91 2.93 o 7 1 0 47.04 47.12 1.01 o 8 1 0 35.14 33.15 0.81 o 9 1 0 28.97 29.32 0.76 o 10 1 0 48.61 45.60 1.05 o 11 1 0 21.71 22.15 0.89 o 0 2 0 77.92 74.04 1.21 o 1 2 0 4.30 6.42 0.87 o 2 2 0 0.11 0.44 0.11 o 3 2 0 265.62 243.06 11.42 o 4 2 0 144.14 150.90 2.46 o 5 2 0 469.56 464.79 7.27 o 6 2 0 2.10 3.01 0.35 o 7 2 0 63.29 67.14 1.04 o 8 2 0 70.96 68.58 1.14 o 9 2 0 49.95 48.82 0.99 o 10 2 0 32.81 35.21 0.99 o 11 2 0 0.05 0.15 0.46 o 1 3 0 421.74 427.19 5.25 o 2 3 0 248.16 238.72 3.59 o 3 3 0 3077.15 3164.89 99.46 o 4 3 0 339.80 366.16 5.61 o 5 3 0 1.34 0.83 0.27 o 6 3 0 217.82 208.94 3.45 o 7 3 0 61.45 57.63 1.36 o 8 3 0 2.84 3.27 0.45 o 9 3 0 107.77 100.33 1.67 o 10 3 0 3.08 3.89 0.55 o 11 3 0 0.18 -0.26 0.49 o 0 4 0 2336.13 2391.66 31.42 o 1 4 0 1059.00 1078.99 25.45 o 2 4 0 412.30 460.45 8.61 o 3 4 0 152.96 147.93 2.45 o 4 4 0 104.94 115.35 3.22 o 5 4 0 5.26 4.09 0.65 o 6 4 0 13.12 13.89 0.58 o 7 4 0 134.46 140.61 2.51 o 8 4 0 154.08 151.51 3.07 o 9 4 0 0.96 1.11 0.40 o 10 4 0 13.47 13.22 0.72 o 11 4 0 0.34 -0.49 0.49 o 1 5 0 0.00 1.17 0.52 o 2 5 0 149.93 179.87 2.95 o 3 5 0 69.89 58.58 0.87 o 4 5 0 0.08 -0.14 0.23 o 5 5 0 69.30 72.63 1.61 o 6 5 0 164.59 163.38 1.95 o 7 5 0 0.33 0.51 0.29 o 8 5 0 4.50 3.20 0.62 o 9 5 0 8.60 9.12 0.69 o 10 5 0 14.97 14.23 0.73 o 0 6 0 323.76 311.74 5.13 o 1 6 0 67.56 63.35 0.74 o 2 6 0 59.95 64.67 1.06 o 3 6 0 157.07 164.23 2.36 o 4 6 0 6.99 5.80 0.41 o 5 6 0 30.65 29.15 0.95 o 6 6 0 8.14 9.13 0.48 o 7 6 0 7.66 4.53 0.76 o 8 6 0 0.48 0.15 0.37 o 9 6 0 47.55 46.06 1.64 o 10 6 0 0.39 0.65 0.54 o 1 7 0 170.73 181.96 2.66 o 2 7 0 131.94 127.88 1.63 o 3 7 0 1.11 1.46 0.29 o 4 7 0 62.85 68.21 1.03 o 5 7 0 3.70 4.79 0.41 o 6 7 0 25.32 31.72 0.78 o 7 7 0 2.36 1.38 0.38 o 8 7 0 2.37 2.09 0.48 o 9 7 0 0.82 0.69 0.59 o 0 8 0 42.93 48.80 1.28 o 1 8 0 98.28 88.64 1.25 o 2 8 0 0.87 0.58 0.31 o 3 8 0 31.67 27.83 0.78 o 4 8 0 5.57 7.42 0.49 o 5 8 0 0.93 0.34 0.33 o 6 8 0 0.37 -0.30 0.39 o 7 8 0 0.60 0.47 0.42 o 8 8 0 1.79 1.35 0.57 o 9 8 0 12.85 15.53 1.14 o 1 9 0 40.66 40.71 0.89 o 2 9 0 30.11 29.87 0.81 o 3 9 0 47.88 47.14 1.09 o 4 9 0 20.91 20.49 0.74 o 5 9 0 1.03 0.82 0.42 o 6 9 0 1.78 0.80 0.61 o 7 9 0 1.26 1.19 0.59 o 8 9 0 10.49 13.92 1.06 o 0 10 0 1.22 1.90 0.60 o 1 10 0 1.27 1.17 0.41 o 2 10 0 12.20 12.56 0.65 o 3 10 0 3.65 3.34 0.46 o 4 10 0 2.60 2.09 0.55 o 5 10 0 0.50 0.41 0.62 o 6 10 0 6.76 6.04 0.80 o 7 10 0 15.76 16.25 0.97 o 1 11 0 4.54 5.58 0.55 o 2 11 0 22.12 19.38 0.89 o 3 11 0 11.19 11.57 0.90 o 4 11 0 0.41 0.16 0.61 o 5 11 0 0.50 0.20 0.66 o 0 12 0 6.34 6.09 1.25 o 1 12 0 9.91 8.79 0.75 o 2 12 0 3.13 3.34 0.74 o 3 12 0 0.03 0.16 0.65 o 1 0 1 7.51 10.73 0.42 o 2 0 1 166.12 176.98 2.60 o 3 0 1 279.53 278.65 3.90 o 4 0 1 111.00 122.82 1.78 o 5 0 1 159.03 150.26 2.46 o 6 0 1 218.54 208.06 3.96 o 7 0 1 6.58 8.04 0.42 o 8 0 1 2.14 1.64 0.37 o 9 0 1 1.52 2.20 0.40 o 10 0 1 8.83 8.72 0.56 o 11 0 1 3.35 3.96 0.58 o 0 1 1 20.66 27.77 0.20 o 1 1 1 208.98 204.26 1.37 o 2 1 1 6501.51 6871.06 272.44 o 3 1 1 322.64 300.36 3.59 o 4 1 1 913.53 913.91 15.52 o 5 1 1 48.54 45.99 0.44 o 6 1 1 101.33 87.72 0.90 o 7 1 1 2.12 2.29 0.24 o 8 1 1 2.64 2.24 0.26 o 9 1 1 10.17 9.77 0.39 o 10 1 1 4.86 5.80 0.40 o 11 1 1 6.41 8.15 0.48 o 0 2 1 2.02 3.58 0.23 o 1 2 1 3840.42 4018.76 61.58 o 2 2 1 70.80 77.88 1.08 o 3 2 1 2335.52 2360.15 26.25 o 4 2 1 56.49 59.57 0.62 o 5 2 1 208.64 182.47 4.35 o 6 2 1 93.27 95.18 1.32 o 7 2 1 32.64 29.84 0.54 o 8 2 1 63.05 65.03 0.75 o 9 2 1 2.29 2.29 0.32 o 10 2 1 0.13 0.03 0.32 o 11 2 1 1.41 0.72 0.38 o 0 3 1 1654.28 1587.49 17.12 o 1 3 1 190.61 186.93 1.47 o 2 3 1 816.52 824.45 7.26 o 3 3 1 1600.51 1620.20 23.56 o 4 3 1 260.38 255.83 2.55 o 5 3 1 21.38 23.83 0.42 o 6 3 1 72.42 73.15 0.65 o 7 3 1 55.15 52.25 1.22 o 8 3 1 9.09 6.87 0.33 o 9 3 1 29.92 31.21 0.63 o 10 3 1 6.39 6.19 0.42 o 11 3 1 0.18 0.23 0.36 o 0 4 1 25.53 28.41 0.44 o 1 4 1 184.71 186.01 1.61 o 2 4 1 1436.33 1521.33 12.64 o 3 4 1 578.48 631.82 6.34 o 4 4 1 267.52 268.00 2.77 o 5 4 1 320.94 327.16 3.02 o 6 4 1 142.72 142.96 1.23 o 7 4 1 68.30 65.44 0.89 o 8 4 1 10.38 10.40 0.39 o 9 4 1 5.32 6.23 0.40 o 10 4 1 5.82 5.94 0.41 o 11 4 1 2.33 2.38 0.42 o 0 5 1 130.33 135.85 1.85 o 1 5 1 271.85 268.29 2.08 o 2 5 1 134.58 124.67 1.32 o 3 5 1 50.25 50.56 0.52 o 4 5 1 93.41 90.87 0.94 o 5 5 1 324.39 328.75 2.84 o 6 5 1 265.91 263.04 3.03 o 7 5 1 57.55 54.71 0.64 o 8 5 1 24.80 26.62 0.52 o 9 5 1 0.64 0.19 0.29 o 10 5 1 7.14 7.94 0.46 o 0 6 1 23.34 22.43 0.51 o 1 6 1 141.21 131.36 1.09 o 2 6 1 186.86 187.58 2.01 o 3 6 1 15.32 16.43 0.37 o 4 6 1 61.30 60.18 0.97 o 5 6 1 81.58 81.20 0.97 o 6 6 1 9.20 8.01 0.33 o 7 6 1 40.16 40.43 0.68 o 8 6 1 0.60 0.37 0.29 o 9 6 1 1.06 1.82 0.35 o 10 6 1 0.83 0.88 0.40 o 0 7 1 66.05 65.59 0.91 o 1 7 1 118.68 116.77 0.79 o 2 7 1 38.53 37.22 0.58 o 3 7 1 14.77 12.91 0.37 o 4 7 1 54.67 60.48 0.99 o 5 7 1 2.59 1.97 0.26 o 6 7 1 18.85 18.47 0.47 o 7 7 1 4.31 3.97 0.33 o 8 7 1 0.76 0.73 0.32 o 9 7 1 0.60 0.69 0.37 o 0 8 1 0.42 -0.29 0.33 o 1 8 1 138.64 145.17 1.03 o 2 8 1 25.74 20.82 0.46 o 3 8 1 60.73 57.09 0.77 o 4 8 1 49.71 47.40 0.74 o 5 8 1 35.55 31.72 0.62 o 6 8 1 7.40 6.83 0.39 o 7 8 1 0.79 0.51 0.34 o 8 8 1 27.59 25.13 1.01 o 9 8 1 0.20 0.47 0.47 o 0 9 1 54.00 54.54 0.98 o 1 9 1 17.24 17.17 0.49 o 2 9 1 55.85 60.70 0.86 o 3 9 1 87.11 82.68 1.03 o 4 9 1 10.79 9.64 0.46 o 5 9 1 5.93 6.07 0.38 o 6 9 1 3.98 3.51 0.38 o 7 9 1 19.62 21.78 0.78 o 8 9 1 0.66 0.73 0.48 o 0 10 1 100.88 100.96 1.36 o 1 10 1 21.08 22.54 0.55 o 2 10 1 33.56 35.02 0.65 o 3 10 1 4.38 4.82 0.39 o 4 10 1 3.88 4.04 0.46 o 5 10 1 3.70 4.03 0.43 o 6 10 1 6.77 6.24 0.54 o 0 11 1 0.79 1.25 0.51 o 1 11 1 8.20 10.06 0.48 o 2 11 1 18.24 20.94 0.69 o 3 11 1 11.05 11.15 0.54 o 4 11 1 7.68 8.71 0.56 o 5 11 1 0.83 0.71 0.47 o 0 12 1 0.18 0.61 0.53 o 1 12 1 0.33 0.09 0.44 o 2 12 1 1.42 1.81 0.49 o 0 0 2 14055.74 12856.01 169.63 o 1 0 2 1259.24 1196.53 23.24 o 2 0 2 218.20 219.74 2.34 o 3 0 2 39.29 52.63 0.51 o 4 0 2 22.94 18.08 0.42 o 5 0 2 461.54 485.74 7.31 o 6 0 2 82.85 90.73 1.56 o 7 0 2 3.75 5.30 0.39 o 8 0 2 8.74 7.65 0.45 o 9 0 2 29.73 32.31 0.88 o 10 0 2 42.62 41.00 1.04 o 11 0 2 3.07 3.38 0.56 o 0 1 2 193.80 163.12 1.95 o 1 1 2 2769.80 2855.24 30.02 o 2 1 2 61.22 69.76 0.50 o 3 1 2 185.71 172.34 1.52 o 4 1 2 587.46 585.87 6.62 o 5 1 2 177.23 176.70 2.73 o 6 1 2 151.78 149.20 2.76 o 7 1 2 18.81 19.66 0.45 o 8 1 2 30.06 28.59 0.54 o 9 1 2 44.92 45.24 0.65 o 10 1 2 32.65 32.30 0.71 o 11 1 2 13.20 13.79 0.56 o 0 2 2 0.48 0.50 0.12 o 1 2 2 487.39 483.50 3.13 o 2 2 2 71.49 74.27 0.38 o 3 2 2 56.42 56.78 0.61 o 4 2 2 26.96 22.82 0.40 o 5 2 2 85.13 86.37 1.81 o 6 2 2 12.00 12.21 0.38 o 7 2 2 166.78 171.42 1.58 o 8 2 2 57.03 56.29 0.86 o 9 2 2 16.35 14.41 0.48 o 10 2 2 35.01 35.55 0.73 o 11 2 2 1.92 1.18 0.40 o 0 3 2 49.26 53.77 0.56 o 1 3 2 935.12 998.60 7.22 o 2 3 2 154.74 158.51 1.13 o 3 3 2 755.41 794.63 4.20 o 4 3 2 39.97 39.28 0.40 o 5 3 2 0.03 0.37 0.18 o 6 3 2 98.65 95.66 0.87 o 7 3 2 126.43 114.58 4.24 o 8 3 2 8.06 8.51 0.38 o 9 3 2 51.93 46.64 0.72 o 10 3 2 7.19 9.36 0.45 o 11 3 2 1.71 1.99 0.43 o 0 4 2 4.81 2.33 0.36 o 1 4 2 206.55 225.42 1.62 o 2 4 2 973.84 1000.92 8.58 o 3 4 2 119.99 129.15 1.00 o 4 4 2 331.53 313.24 3.00 o 5 4 2 4.40 3.76 0.24 o 6 4 2 24.60 23.79 0.46 o 7 4 2 14.60 13.25 0.40 o 8 4 2 60.56 59.34 0.76 o 9 4 2 10.72 8.37 0.53 o 10 4 2 0.66 0.42 0.35 o 11 4 2 1.12 0.41 0.44 o 0 5 2 313.74 281.74 2.20 o 1 5 2 156.26 148.84 1.00 o 2 5 2 148.72 151.99 1.19 o 3 5 2 20.44 18.91 0.37 o 4 5 2 67.25 70.71 0.84 o 5 5 2 193.59 194.79 2.06 o 6 5 2 32.20 31.29 0.50 o 7 5 2 24.25 23.15 0.47 o 8 5 2 5.31 5.79 0.38 o 9 5 2 0.67 0.49 0.32 o 10 5 2 2.62 2.70 0.40 o 0 6 2 146.76 139.18 2.11 o 1 6 2 35.36 38.76 0.44 o 2 6 2 17.15 21.36 0.37 o 3 6 2 159.65 160.38 1.67 o 4 6 2 39.10 39.46 0.48 o 5 6 2 167.66 168.86 1.89 o 6 6 2 10.23 9.09 0.36 o 7 6 2 1.70 1.69 0.30 o 8 6 2 6.05 7.69 0.44 o 9 6 2 12.67 11.57 0.50 o 10 6 2 16.66 17.97 0.65 o 0 7 2 672.76 659.54 7.08 o 1 7 2 165.65 172.72 1.25 o 2 7 2 50.62 44.86 0.61 o 3 7 2 33.58 32.03 0.53 o 4 7 2 72.99 73.99 0.77 o 5 7 2 48.80 46.52 0.81 o 6 7 2 2.97 3.36 0.34 o 7 7 2 18.07 17.69 0.59 o 8 7 2 4.40 3.77 0.43 o 9 7 2 4.95 4.87 0.46 o 0 8 2 10.53 11.37 0.56 o 1 8 2 197.74 194.90 1.45 o 2 8 2 40.45 37.08 0.52 o 3 8 2 52.53 51.07 0.64 o 4 8 2 70.00 66.69 0.85 o 5 8 2 1.40 0.92 0.31 o 6 8 2 3.95 4.03 0.37 o 7 8 2 6.22 7.53 0.50 o 8 8 2 7.91 9.00 0.52 o 0 9 2 20.51 18.98 0.68 o 1 9 2 26.64 26.75 0.51 o 2 9 2 126.97 125.03 1.18 o 3 9 2 6.25 5.75 0.37 o 4 9 2 28.88 25.84 0.65 o 5 9 2 9.42 9.97 0.48 o 6 9 2 1.46 1.86 0.38 o 7 9 2 1.48 1.98 0.44 o 0 10 2 2.94 2.86 0.52 o 1 10 2 2.65 3.23 0.35 o 2 10 2 12.72 12.42 0.49 o 3 10 2 22.94 22.50 0.62 o 4 10 2 1.42 1.15 0.37 o 5 10 2 5.80 7.07 0.47 o 6 10 2 0.85 0.93 0.37 o 0 11 2 2.62 2.54 0.57 o 1 11 2 11.01 12.06 0.58 o 2 11 2 24.94 27.20 0.80 o 3 11 2 3.65 4.12 0.45 o 4 11 2 13.04 14.51 0.67 o 5 11 2 6.28 7.36 0.62 o 0 12 2 3.58 5.02 0.80 o 1 12 2 15.79 16.03 0.75 o 2 12 2 3.17 2.44 0.48 o 1 0 3 21.20 25.10 0.45 o 2 0 3 223.23 229.02 2.30 o 3 0 3 78.03 67.71 5.33 o 4 0 3 462.23 516.49 4.56 o 5 0 3 23.94 25.84 0.65 o 6 0 3 124.95 126.57 2.02 o 7 0 3 26.19 26.58 0.62 o 8 0 3 66.98 70.73 1.11 o 9 0 3 0.06 -0.26 0.41 o 10 0 3 3.30 2.22 0.51 o 11 0 3 30.39 34.26 1.03 o 0 1 3 36.17 29.53 0.75 o 1 1 3 131.64 150.38 0.85 o 2 1 3 190.87 194.99 1.11 o 3 1 3 327.70 335.54 1.79 o 4 1 3 4.30 5.41 0.21 o 5 1 3 135.91 154.32 2.15 o 6 1 3 24.92 23.97 0.38 o 7 1 3 82.70 81.17 0.83 o 8 1 3 10.81 9.31 0.50 o 9 1 3 8.73 8.87 0.44 o 10 1 3 4.49 4.05 0.40 o 11 1 3 4.87 6.44 0.48 o 0 2 3 113.54 134.94 1.71 o 1 2 3 1328.50 1420.51 10.27 o 2 2 3 93.61 87.05 0.68 o 3 2 3 185.05 181.57 1.31 o 4 2 3 39.63 40.74 0.48 o 5 2 3 111.16 103.22 0.92 o 6 2 3 16.56 17.55 0.44 o 7 2 3 28.77 30.00 0.60 o 8 2 3 49.26 52.74 0.71 o 9 2 3 23.68 21.97 0.60 o 10 2 3 6.04 7.28 0.45 o 11 2 3 0.71 0.51 0.41 o 0 3 3 18.79 13.45 0.28 o 1 3 3 241.36 244.02 2.15 o 2 3 3 1472.26 1542.08 8.96 o 3 3 3 5.35 5.93 0.19 o 4 3 3 3.30 3.28 0.19 o 5 3 3 125.76 124.23 0.81 o 6 3 3 122.45 120.44 1.37 o 7 3 3 13.65 14.68 0.45 o 8 3 3 7.16 6.52 0.37 o 9 3 3 1.70 1.32 0.23 o 10 3 3 3.90 3.74 0.44 o 11 3 3 0.48 0.32 0.44 o 0 4 3 166.69 179.56 3.02 o 1 4 3 211.13 218.99 1.76 o 2 4 3 224.24 231.44 2.01 o 3 4 3 521.48 516.74 3.54 o 4 4 3 83.20 76.89 0.60 o 5 4 3 225.65 221.34 1.70 o 6 4 3 4.50 5.50 0.31 o 7 4 3 37.02 36.30 0.65 o 8 4 3 38.08 37.98 0.70 o 9 4 3 13.86 15.36 0.55 o 10 4 3 1.59 0.79 0.40 o 0 5 3 51.66 49.74 0.68 o 1 5 3 83.82 84.13 0.59 o 2 5 3 92.87 88.16 0.69 o 3 5 3 36.92 32.28 0.51 o 4 5 3 281.80 265.47 2.20 o 5 5 3 22.65 20.62 0.43 o 6 5 3 146.10 140.33 1.19 o 7 5 3 71.75 65.25 0.80 o 8 5 3 6.68 5.52 0.41 o 9 5 3 3.80 2.58 0.39 o 10 5 3 11.78 13.02 0.56 o 0 6 3 1.47 1.44 0.27 o 1 6 3 315.70 313.13 2.92 o 2 6 3 128.48 133.94 1.28 o 3 6 3 27.02 25.75 0.51 o 4 6 3 30.75 27.35 0.50 o 5 6 3 18.41 18.94 0.47 o 6 6 3 44.15 41.87 0.68 o 7 6 3 56.94 54.16 0.88 o 8 6 3 9.82 9.04 0.49 o 9 6 3 13.09 15.45 0.62 o 0 7 3 20.15 21.18 0.58 o 1 7 3 31.28 32.35 0.44 o 2 7 3 114.52 112.84 0.97 o 3 7 3 68.28 67.87 0.76 o 4 7 3 45.69 44.09 0.71 o 5 7 3 38.29 35.78 0.68 o 6 7 3 2.65 3.18 0.36 o 7 7 3 15.23 13.72 0.58 o 8 7 3 8.14 10.28 0.54 o 9 7 3 11.38 12.63 0.60 o 0 8 3 28.50 27.70 0.68 o 1 8 3 95.42 96.33 1.02 o 2 8 3 61.93 59.29 0.72 o 3 8 3 54.35 51.40 0.72 o 4 8 3 128.24 117.98 1.08 o 5 8 3 0.28 0.34 0.31 o 6 8 3 0.92 0.73 0.35 o 7 8 3 6.28 5.56 0.49 o 8 8 3 26.15 29.11 0.80 o 0 9 3 51.39 49.78 1.10 o 1 9 3 41.55 39.94 0.73 o 2 9 3 94.28 94.62 0.99 o 3 9 3 52.68 47.79 0.78 o 4 9 3 13.26 12.84 0.50 o 5 9 3 11.48 12.90 0.56 o 6 9 3 0.85 1.76 0.39 o 7 9 3 21.25 22.97 0.78 o 0 10 3 235.57 234.98 3.64 o 1 10 3 71.34 76.02 1.07 o 2 10 3 10.50 11.39 0.52 o 3 10 3 18.68 19.75 0.62 o 4 10 3 1.86 1.23 0.39 o 5 10 3 1.43 1.70 0.43 o 6 10 3 13.54 13.99 0.62 o 0 11 3 4.43 4.21 0.75 o 1 11 3 3.18 2.82 0.48 o 2 11 3 26.82 27.90 0.77 o 3 11 3 21.13 20.85 0.71 o 4 11 3 6.52 8.93 0.63 o 0 0 4 1552.63 1635.59 20.14 o 1 0 4 267.73 305.96 1.43 o 2 0 4 73.72 84.44 0.77 o 3 0 4 41.40 38.42 0.56 o 4 0 4 244.57 256.98 2.48 o 5 0 4 48.22 43.06 1.48 o 6 0 4 3.74 3.17 0.51 o 7 0 4 0.28 0.47 0.34 o 8 0 4 20.99 21.13 0.75 o 9 0 4 0.45 0.37 0.43 o 10 0 4 22.53 22.99 0.89 o 11 0 4 0.03 0.41 0.54 o 0 1 4 693.12 590.48 88.91 o 1 1 4 228.17 263.73 1.65 o 2 1 4 285.35 300.21 1.81 o 3 1 4 798.29 830.52 4.65 o 4 1 4 152.21 161.57 1.19 o 5 1 4 99.80 100.64 1.68 o 6 1 4 1.86 1.65 0.24 o 7 1 4 14.99 13.76 0.41 o 8 1 4 13.99 14.05 0.49 o 9 1 4 41.32 41.12 0.73 o 10 1 4 1.41 2.04 0.38 o 11 1 4 4.26 4.82 0.49 o 0 2 4 2.88 2.35 0.19 o 1 2 4 424.13 430.41 3.19 o 2 2 4 135.04 137.22 0.66 o 3 2 4 255.00 286.26 1.80 o 4 2 4 238.97 240.30 1.56 o 5 2 4 119.69 112.07 0.88 o 6 2 4 29.92 29.60 0.52 o 7 2 4 61.08 65.30 0.73 o 8 2 4 29.07 27.43 0.65 o 9 2 4 0.38 0.55 0.34 o 10 2 4 3.90 3.43 0.43 o 0 3 4 33.43 29.06 0.39 o 1 3 4 108.02 116.66 1.02 o 2 3 4 109.58 113.45 1.01 o 3 3 4 22.71 22.38 0.31 o 4 3 4 227.64 236.14 2.04 o 5 3 4 25.33 26.77 0.45 o 6 3 4 31.78 34.10 0.54 o 7 3 4 42.45 43.88 0.68 o 8 3 4 31.37 30.68 0.65 o 9 3 4 3.50 3.75 0.42 o 10 3 4 12.50 14.02 0.61 o 0 4 4 453.53 488.98 7.51 o 1 4 4 46.91 50.67 0.46 o 2 4 4 225.91 228.04 1.90 o 3 4 4 177.18 179.31 1.49 o 4 4 4 117.17 111.20 0.96 o 5 4 4 12.77 12.04 0.38 o 6 4 4 124.10 120.80 0.99 o 7 4 4 78.20 76.27 0.84 o 8 4 4 2.58 2.34 0.37 o 9 4 4 21.15 20.12 0.70 o 10 4 4 4.46 5.63 0.50 o 0 5 4 154.09 157.08 1.75 o 1 5 4 77.40 82.41 0.81 o 2 5 4 150.72 151.07 1.65 o 3 5 4 14.25 12.17 0.39 o 4 5 4 57.33 57.98 0.62 o 5 5 4 211.48 194.22 2.30 o 6 5 4 154.31 155.25 1.65 o 7 5 4 33.00 32.68 0.67 o 8 5 4 18.57 17.18 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0.56 o 9 4 6 3.38 3.39 0.51 o 0 5 6 253.31 240.09 4.77 o 1 5 6 6.70 5.11 0.29 o 2 5 6 43.74 45.82 0.71 o 3 5 6 108.02 104.61 1.16 o 4 5 6 15.52 14.62 0.53 o 5 5 6 75.54 72.64 0.96 o 6 5 6 87.62 87.04 1.05 o 7 5 6 3.44 3.33 0.43 o 8 5 6 11.10 10.07 0.61 o 0 6 6 269.48 266.52 4.93 o 1 6 6 4.42 4.54 0.32 o 2 6 6 21.85 19.77 0.50 o 3 6 6 68.30 67.79 0.78 o 4 6 6 81.13 80.55 1.00 o 5 6 6 63.20 67.13 0.98 o 6 6 6 8.27 7.40 0.47 o 7 6 6 8.73 8.94 0.54 o 8 6 6 2.33 2.49 0.47 o 0 7 6 6.20 5.86 0.60 o 1 7 6 96.92 91.85 1.20 o 2 7 6 30.39 30.88 0.64 o 3 7 6 39.82 39.81 0.79 o 4 7 6 0.15 0.24 0.38 o 5 7 6 24.84 25.83 0.74 o 6 7 6 2.72 3.56 0.43 o 7 7 6 0.36 0.24 0.40 o 0 8 6 9.26 8.05 0.67 o 1 8 6 0.27 0.29 0.36 o 2 8 6 2.83 2.62 0.40 o 3 8 6 14.05 13.95 0.61 o 4 8 6 27.01 27.10 0.79 o 5 8 6 7.50 8.22 0.55 o 6 8 6 2.50 4.02 0.48 o 0 9 6 8.94 9.97 0.77 o 1 9 6 13.32 13.01 0.61 o 2 9 6 20.23 20.67 0.74 o 3 9 6 0.52 1.03 0.41 o 4 9 6 4.02 3.92 0.53 o 5 9 6 1.77 2.02 0.50 o 0 10 6 3.43 3.92 0.76 o 1 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