#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214644.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214644_Fobs loop_ _publ_author_name 'Kishbaugh, Tara L. S.' 'Gribble, Gordon W.' 'Jasinski, Jerry P.' _publ_section_title ; 2-(4-Methoxybenzyl)-4-(phenylsulfonyl)-1,2,3,4-tetrahydropyrrolo[3,4-b]indole ; _journal_coeditor_code FL2139 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3411 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.472 _cell_angle_gamma 90.000 _cell_length_a 11.9290 _cell_length_b 9.3967 _cell_length_c 19.1976 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.7686 _[local]_cod_data_source_file fl2139Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TK-7 TLS-II-205 Kishbaugh/Gribble' _shelx_refln_list_code 4 _shelx_f_calc_maximum 311.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 261.92 0.45 14.86 o 2 0 0 17156.40 17741.60 242.43 o 3 0 0 97194.06 105228.26 1396.37 o 4 0 0 23085.82 25744.05 357.17 o 5 0 0 13352.81 14109.11 209.84 o 6 0 0 3762.31 3876.45 81.11 o 7 0 0 348.71 495.22 39.53 o 8 0 0 123.86 144.95 18.82 o 9 0 0 20.40 52.08 40.27 o 10 0 0 13.66 9.28 45.39 o 11 0 0 100.01 50.19 49.33 o 12 0 0 8.02 0.97 56.17 o 13 0 0 68.43 20.16 63.82 o 14 0 0 188.96 138.80 37.32 o 1 1 0 8814.16 8431.46 118.34 o 2 1 0 11715.31 11816.42 166.24 o 3 1 0 3600.07 3504.18 62.46 o 4 1 0 6690.72 6434.61 104.53 o 5 1 0 3311.57 3739.78 73.91 o 6 1 0 1789.40 1635.68 51.73 o 7 1 0 2829.61 2733.42 71.02 o 8 1 0 35.63 49.11 37.09 o 9 1 0 55.57 77.44 41.89 o 10 1 0 368.22 325.96 29.52 o 11 1 0 9.73 18.26 49.40 o 12 1 0 0.99 42.39 55.99 o 13 1 0 41.31 33.58 66.27 o 14 1 0 11.41 -46.02 72.93 o 0 2 0 16012.51 13760.08 192.34 o 1 2 0 474.03 418.92 21.84 o 2 2 0 16.90 21.52 19.66 o 3 2 0 627.63 558.48 27.55 o 4 2 0 1107.92 1199.05 38.13 o 5 2 0 449.60 417.65 31.35 o 6 2 0 52.99 58.75 30.89 o 7 2 0 25.57 27.13 33.33 o 8 2 0 16.95 -36.85 36.85 o 9 2 0 4.55 33.87 42.66 o 10 2 0 31.56 -11.08 47.08 o 11 2 0 70.32 -47.11 54.62 o 12 2 0 0.51 76.79 58.31 o 13 2 0 43.92 71.86 63.36 o 14 2 0 9.27 20.12 69.11 o 1 3 0 148.56 174.37 16.56 o 2 3 0 146.33 183.58 17.08 o 3 3 0 17.01 30.60 21.46 o 4 3 0 1015.40 944.65 37.56 o 5 3 0 613.57 683.48 36.94 o 6 3 0 46.95 47.99 31.40 o 7 3 0 87.84 102.92 17.05 o 8 3 0 45.02 22.52 40.25 o 9 3 0 149.74 157.63 23.65 o 10 3 0 2.77 -48.09 48.09 o 11 3 0 1.74 66.68 50.93 o 12 3 0 1.78 61.62 56.76 o 13 3 0 0.15 -9.45 63.76 o 14 3 0 0.00 44.89 72.59 o 0 4 0 662.15 664.82 30.95 o 1 4 0 23.49 25.33 23.36 o 2 4 0 300.10 285.11 27.31 o 3 4 0 239.95 230.08 20.83 o 4 4 0 1714.05 1759.95 52.06 o 5 4 0 26.28 51.62 14.53 o 6 4 0 159.96 171.42 17.34 o 7 4 0 794.47 758.30 49.15 o 8 4 0 11.54 -18.12 42.36 o 9 4 0 443.74 428.36 39.20 o 10 4 0 75.63 83.70 25.65 o 11 4 0 9.71 -14.76 53.27 o 12 4 0 111.99 75.57 62.42 o 13 4 0 7.54 -20.80 65.71 o 14 4 0 9.05 40.57 72.95 o 1 5 0 169.85 166.33 16.65 o 2 5 0 913.35 1273.43 44.95 o 3 5 0 230.69 177.89 15.57 o 4 5 0 237.09 269.83 24.33 o 5 5 0 1296.10 1470.61 54.38 o 6 5 0 610.62 736.81 47.09 o 7 5 0 9.91 -1.00 40.39 o 8 5 0 224.49 220.68 24.37 o 9 5 0 722.21 767.16 61.54 o 10 5 0 133.50 106.19 27.78 o 11 5 0 43.22 25.54 59.89 o 12 5 0 17.22 43.96 61.44 o 13 5 0 12.71 -32.97 70.95 o 0 6 0 876.27 752.94 42.04 o 1 6 0 0.95 28.58 28.77 o 2 6 0 194.78 212.57 19.52 o 3 6 0 225.58 222.67 20.22 o 4 6 0 259.05 270.36 27.02 o 5 6 0 135.45 141.32 18.97 o 6 6 0 25.65 -7.76 39.21 o 7 6 0 311.83 349.11 35.21 o 8 6 0 4.72 -47.11 47.11 o 9 6 0 74.21 94.55 26.58 o 10 6 0 81.49 37.43 57.82 o 11 6 0 12.67 -23.36 62.28 o 12 6 0 106.90 79.70 41.72 o 1 7 0 384.24 363.49 28.17 o 2 7 0 286.40 321.42 29.56 o 3 7 0 191.82 227.65 20.36 o 4 7 0 139.31 176.64 20.47 o 5 7 0 2.99 45.05 41.80 o 6 7 0 76.11 77.89 44.74 o 7 7 0 46.06 -0.68 48.79 o 8 7 0 135.48 134.69 26.85 o 9 7 0 0.96 94.79 57.15 o 10 7 0 34.87 -63.12 63.12 o 11 7 0 44.49 104.82 34.17 o 12 7 0 6.78 86.05 72.79 o 0 8 0 717.09 782.00 55.50 o 1 8 0 169.14 150.03 22.49 o 2 8 0 20.02 6.26 41.09 o 3 8 0 15.07 13.21 44.75 o 4 8 0 19.41 74.67 46.06 o 5 8 0 15.51 -13.31 47.95 o 6 8 0 12.41 100.08 24.02 o 7 8 0 0.60 -10.51 52.52 o 8 8 0 0.16 -59.49 59.49 o 9 8 0 23.33 30.06 65.38 o 10 8 0 1.34 -18.75 68.11 o 11 8 0 5.10 -76.79 76.79 o 1 9 0 129.08 109.89 24.54 o 2 9 0 29.44 88.59 47.36 o 3 9 0 13.22 3.56 47.38 o 4 9 0 32.36 -1.64 51.17 o 5 9 0 8.54 19.94 51.63 o 6 9 0 12.40 -15.78 58.64 o 7 9 0 0.78 80.96 56.22 o 8 9 0 50.12 12.35 63.34 o 9 9 0 16.49 -71.58 71.58 o 10 9 0 13.68 -5.74 74.72 o 0 10 0 1.85 80.71 51.79 o 1 10 0 2.72 68.27 35.55 o 2 10 0 1.92 17.76 52.13 o 3 10 0 46.64 -18.46 57.60 o 4 10 0 63.29 84.75 56.75 o 5 10 0 42.18 26.20 64.47 o 6 10 0 7.02 58.39 63.96 o 7 10 0 1.34 45.34 66.93 o 8 10 0 22.07 92.63 71.25 o 1 11 0 10.19 81.49 59.82 o 2 11 0 53.40 85.81 63.73 o 3 11 0 4.32 -47.41 65.86 o 4 11 0 42.62 97.12 33.80 o 5 11 0 5.30 90.88 66.00 o 6 11 0 0.41 -75.83 75.83 o 0 12 0 8.80 43.45 70.75 o 1 12 0 10.15 121.08 71.02 o 2 12 0 70.47 118.51 73.37 o -14 1 1 20.25 17.34 69.70 o -13 1 1 9.40 6.11 60.69 o -12 1 1 102.25 98.98 52.73 o -11 1 1 121.58 188.61 25.56 o -10 1 1 2.37 -39.94 44.05 o -9 1 1 869.09 613.47 50.96 o -8 1 1 731.72 750.53 48.57 o -7 1 1 411.66 507.74 39.39 o -6 1 1 1726.93 1567.96 49.52 o -5 1 1 2528.13 2783.69 61.26 o -4 1 1 547.78 516.44 27.76 o -3 1 1 3289.67 3702.97 64.36 o -2 1 1 428.18 365.64 19.61 o -1 1 1 348.16 363.82 16.15 o 0 1 1 166.71 122.05 9.24 o 1 1 1 2345.43 2261.54 39.44 o 2 1 1 6378.17 6470.28 97.47 o 3 1 1 4246.42 4197.88 72.56 o 4 1 1 1059.44 1097.61 36.27 o 5 1 1 1396.50 1339.43 44.07 o 6 1 1 6175.06 6912.14 122.02 o 7 1 1 13.59 -20.87 35.64 o 8 1 1 546.56 342.39 31.91 o 9 1 1 1258.63 1401.44 65.14 o 10 1 1 3.67 -46.20 49.86 o 11 1 1 106.22 50.23 53.96 o 12 1 1 206.13 257.36 31.21 o 13 1 1 0.55 -67.50 67.50 o 14 1 1 48.04 80.69 70.52 o -14 2 1 1.26 22.61 70.48 o -13 2 1 81.77 6.72 62.86 o -12 2 1 229.22 263.56 30.48 o -11 2 1 38.58 21.57 51.15 o -10 2 1 67.15 73.89 47.20 o -9 2 1 934.44 849.84 53.93 o -8 2 1 77.25 66.20 35.64 o -7 2 1 684.38 699.19 42.47 o -6 2 1 50.63 3.93 28.58 o -5 2 1 863.16 867.23 36.51 o -4 2 1 38.06 25.40 22.86 o -3 2 1 2402.35 2162.90 46.76 o -2 2 1 2864.12 2764.49 51.98 o -1 2 1 832.30 896.15 26.93 o 0 2 1 6227.79 5237.58 81.25 o 1 2 1 3713.19 3258.48 56.85 o 2 2 1 1350.93 1133.50 32.89 o 3 2 1 1381.46 1285.29 37.54 o 4 2 1 262.00 193.92 15.36 o 5 2 1 312.89 305.80 29.67 o 6 2 1 114.35 104.11 15.64 o 7 2 1 48.61 66.81 16.64 o 8 2 1 291.27 282.03 24.98 o 9 2 1 908.74 752.41 57.06 o 10 2 1 432.65 509.93 40.33 o 11 2 1 8.57 -54.83 54.83 o 12 2 1 535.68 441.80 38.18 o 13 2 1 181.02 193.66 35.55 o 14 2 1 0.41 -49.59 73.45 o -14 3 1 0.23 -17.76 73.29 o -13 3 1 10.92 -68.77 68.77 o -12 3 1 21.40 62.96 54.63 o -11 3 1 2.91 80.90 49.32 o -10 3 1 55.92 83.27 46.67 o -9 3 1 12.65 54.24 21.57 o -8 3 1 0.60 -37.71 37.71 o -7 3 1 145.97 127.87 17.84 o -6 3 1 1248.01 1228.66 48.48 o -5 3 1 2.73 25.77 26.07 o -4 3 1 1513.27 1472.27 44.13 o -3 3 1 850.29 747.97 31.59 o -2 3 1 3626.14 3683.91 67.57 o -1 3 1 6084.72 5527.40 90.61 o 0 3 1 135.51 154.15 13.46 o 1 3 1 766.76 835.01 30.99 o 2 3 1 895.01 874.77 32.83 o 3 3 1 584.60 655.74 30.83 o 4 3 1 96.43 85.00 12.66 o 5 3 1 171.40 151.49 15.05 o 6 3 1 241.60 204.73 19.72 o 7 3 1 221.25 262.94 26.34 o 8 3 1 445.51 479.53 45.73 o 9 3 1 129.68 160.93 23.79 o 10 3 1 257.19 258.43 26.35 o 11 3 1 0.27 -54.56 54.56 o 12 3 1 29.69 98.96 57.82 o 13 3 1 145.74 -52.10 72.78 o 14 3 1 25.58 83.09 72.06 o -14 4 1 103.02 125.97 37.61 o -13 4 1 1.24 45.77 64.91 o -12 4 1 119.84 199.55 30.31 o -11 4 1 0.29 -52.49 52.49 o -10 4 1 73.25 11.85 52.17 o -9 4 1 1004.40 910.55 64.76 o -8 4 1 599.56 654.38 54.58 o -7 4 1 3.79 48.88 33.56 o -6 4 1 61.95 -4.68 33.28 o -5 4 1 437.20 496.41 35.71 o -4 4 1 657.10 752.14 37.23 o -3 4 1 2535.42 2903.21 64.84 o -2 4 1 2414.95 2129.25 52.04 o -1 4 1 366.78 452.59 28.59 o 0 4 1 2230.74 2309.93 53.35 o 1 4 1 760.46 784.40 33.91 o 2 4 1 1717.39 1568.94 46.03 o 3 4 1 10.21 1.23 26.20 o 4 4 1 1813.79 1900.02 56.09 o 5 4 1 52.65 54.21 15.28 o 6 4 1 237.41 221.67 21.17 o 7 4 1 121.03 96.79 19.86 o 8 4 1 156.35 142.49 22.99 o 9 4 1 91.82 154.36 24.79 o 10 4 1 1.03 57.31 48.00 o 11 4 1 16.69 33.03 54.97 o 12 4 1 93.40 123.45 32.69 o 13 4 1 4.88 10.78 68.36 o -13 5 1 9.11 -41.46 72.00 o -12 5 1 2.81 55.31 62.67 o -11 5 1 2.66 -48.16 57.19 o -10 5 1 0.02 -0.86 52.04 o -9 5 1 32.24 27.38 49.22 o -8 5 1 70.36 66.08 23.07 o -7 5 1 174.97 191.08 21.26 o -6 5 1 610.50 561.95 44.91 o -5 5 1 57.04 66.79 33.78 o -4 5 1 7.06 39.19 28.93 o -3 5 1 202.25 152.99 15.75 o -2 5 1 1215.52 1415.82 47.75 o -1 5 1 1070.73 1176.08 43.08 o 0 5 1 650.50 600.18 33.99 o 1 5 1 29.21 19.66 15.07 o 2 5 1 1103.76 1290.09 45.37 o 3 5 1 29.86 40.59 14.10 o 4 5 1 79.02 89.91 15.66 o 5 5 1 67.37 25.33 33.53 o 6 5 1 5.04 -6.58 36.12 o 7 5 1 296.74 336.70 33.08 o 8 5 1 94.07 137.49 23.25 o 9 5 1 160.65 194.61 26.90 o 10 5 1 80.77 31.55 53.19 o 11 5 1 2.36 -9.19 60.39 o 12 5 1 40.85 39.28 65.88 o 13 5 1 15.22 26.59 70.68 o -13 6 1 1.84 -22.00 75.31 o -12 6 1 1.93 82.62 66.68 o -11 6 1 52.59 -22.39 64.16 o -10 6 1 0.00 -20.93 58.31 o -9 6 1 11.08 -27.54 52.26 o -8 6 1 28.01 46.52 46.27 o -7 6 1 182.07 193.51 23.20 o -6 6 1 74.46 54.16 40.70 o -5 6 1 38.11 35.32 35.76 o -4 6 1 216.55 198.56 19.04 o -3 6 1 2.89 7.02 31.26 o -2 6 1 688.76 787.15 43.85 o -1 6 1 126.41 139.29 15.89 o 0 6 1 0.12 -2.22 30.35 o 1 6 1 499.08 509.75 37.51 o 2 6 1 109.00 165.36 16.78 o 3 6 1 7.18 -11.06 31.49 o 4 6 1 90.91 90.94 17.05 o 5 6 1 88.62 89.39 19.59 o 6 6 1 13.93 13.89 38.64 o 7 6 1 1.59 13.98 44.05 o 8 6 1 1.13 84.98 45.34 o 9 6 1 16.66 -9.44 54.94 o 10 6 1 10.85 23.54 58.03 o 11 6 1 70.66 -50.04 62.86 o 12 6 1 1.30 32.03 70.41 o -12 7 1 0.54 -13.21 76.79 o -11 7 1 85.65 1.61 68.83 o -10 7 1 34.66 79.98 63.66 o -9 7 1 53.75 47.61 57.75 o -8 7 1 106.49 133.02 27.15 o -7 7 1 89.00 13.19 51.80 o -6 7 1 37.05 45.59 45.13 o -5 7 1 476.72 504.94 49.43 o -4 7 1 32.28 -21.29 40.50 o -3 7 1 9.05 15.98 38.21 o -2 7 1 36.87 70.08 17.25 o -1 7 1 26.82 -1.93 35.30 o 0 7 1 59.25 36.05 35.60 o 1 7 1 195.59 191.16 19.04 o 2 7 1 287.73 292.75 23.17 o 3 7 1 139.29 160.88 20.16 o 4 7 1 242.16 249.67 22.24 o 5 7 1 9.57 62.57 41.34 o 6 7 1 61.90 92.26 22.50 o 7 7 1 92.29 70.60 25.81 o 8 7 1 16.34 -51.43 56.76 o 9 7 1 3.02 -20.41 56.10 o 10 7 1 5.20 -38.07 64.18 o 11 7 1 15.03 -15.07 67.04 o 12 7 1 8.02 47.31 74.40 o -11 8 1 64.73 92.94 76.67 o -10 8 1 76.34 -52.51 69.65 o -9 8 1 46.02 53.13 63.88 o -8 8 1 53.09 134.51 28.72 o -7 8 1 111.63 102.06 55.14 o -6 8 1 9.74 18.25 49.56 o -5 8 1 259.72 268.85 26.75 o -4 8 1 124.57 164.63 22.52 o -3 8 1 34.56 46.63 41.12 o -2 8 1 575.75 518.01 36.29 o -1 8 1 231.95 221.02 22.70 o 0 8 1 116.34 156.30 21.99 o 1 8 1 25.19 -33.44 44.81 o 2 8 1 16.64 -30.72 42.93 o 3 8 1 277.84 261.03 23.85 o 4 8 1 45.44 8.29 45.47 o 5 8 1 349.88 458.56 38.48 o 6 8 1 3.30 -17.62 50.68 o 7 8 1 5.44 50.18 53.33 o 8 8 1 106.68 114.53 60.27 o 9 8 1 2.08 46.68 61.57 o 10 8 1 13.43 -70.32 70.32 o 11 8 1 14.53 -37.87 73.88 o -10 9 1 29.53 27.81 73.90 o -9 9 1 32.18 -2.86 68.22 o -8 9 1 104.58 130.98 68.38 o -7 9 1 12.60 37.69 60.60 o -6 9 1 13.71 42.93 56.90 o -5 9 1 436.19 435.60 36.66 o -4 9 1 57.82 30.31 34.67 o -3 9 1 90.90 101.40 24.97 o -2 9 1 16.39 54.78 48.40 o -1 9 1 8.19 -49.52 49.52 o 0 9 1 457.19 410.24 39.27 o 1 9 1 277.95 245.97 26.07 o 2 9 1 110.01 136.27 25.47 o 3 9 1 0.00 -35.55 49.65 o 4 9 1 147.79 158.85 27.51 o 5 9 1 87.81 32.39 56.44 o 6 9 1 102.68 39.88 59.11 o 7 9 1 11.16 99.67 61.28 o 8 9 1 4.72 19.98 62.57 o 9 9 1 42.09 88.29 70.33 o -8 10 1 0.05 15.64 74.97 o -7 10 1 25.01 -61.51 68.61 o -6 10 1 48.23 13.21 65.07 o -5 10 1 5.13 98.35 57.39 o -4 10 1 31.83 0.91 58.26 o -3 10 1 5.21 25.20 53.17 o -2 10 1 11.05 40.32 26.65 o -1 10 1 0.13 48.32 50.34 o 0 10 1 0.13 -13.94 50.84 o 1 10 1 1.00 -10.74 53.08 o 2 10 1 1.16 -57.65 57.65 o 3 10 1 18.53 -0.88 57.67 o 4 10 1 4.20 106.48 59.23 o 5 10 1 33.12 119.89 62.66 o 6 10 1 0.32 39.92 63.32 o 7 10 1 2.03 75.18 65.89 o 8 10 1 29.08 -66.07 78.12 o -6 11 1 26.74 45.57 72.74 o -5 11 1 9.11 -37.21 70.27 o -4 11 1 1.68 32.56 63.26 o -3 11 1 51.66 -10.96 65.57 o -2 11 1 8.04 77.22 60.94 o -1 11 1 38.81 37.82 62.00 o 0 11 1 2.02 104.10 60.12 o 1 11 1 16.66 -63.66 63.66 o 2 11 1 31.61 -27.83 63.57 o 3 11 1 4.48 44.73 63.85 o 4 11 1 7.40 48.00 68.47 o 5 11 1 0.23 9.60 70.41 o 6 11 1 0.98 137.41 71.52 o -2 12 1 6.03 -49.86 74.42 o -1 12 1 1.33 -20.61 74.63 o 0 12 1 27.11 8.90 70.70 o 1 12 1 5.84 93.66 70.88 o 2 12 1 5.58 49.09 73.83 o -15 0 2 12.36 -53.72 77.69 o -14 0 2 60.02 76.32 47.88 o -13 0 2 47.12 25.34 59.28 o -12 0 2 83.97 92.53 26.90 o -11 0 2 37.43 83.32 49.76 o -10 0 2 66.24 2.18 43.99 o -9 0 2 50.33 -6.31 38.30 o -8 0 2 0.02 22.14 34.44 o -7 0 2 1806.30 2000.59 58.41 o -6 0 2 159.42 160.32 15.29 o -5 0 2 208.71 175.79 16.13 o -4 0 2 1969.93 2358.02 50.79 o -3 0 2 12600.88 13132.83 186.11 o -2 0 2 6157.94 5900.34 87.43 o -1 0 2 175.18 204.91 13.50 o 0 0 2 10099.48 9731.85 133.95 o 1 0 2 9162.28 9565.82 134.21 o 2 0 2 3297.95 3196.36 55.85 o 3 0 2 10410.34 10732.25 157.89 o 4 0 2 1455.92 1476.99 41.97 o 5 0 2 3.02 8.61 26.32 o 6 0 2 2846.65 2976.60 70.69 o 7 0 2 9.08 19.62 33.85 o 8 0 2 617.05 623.52 46.30 o 9 0 2 49.56 -8.94 44.32 o 10 0 2 141.98 144.81 25.53 o 11 0 2 150.05 85.09 57.09 o 12 0 2 114.88 73.59 58.82 o 13 0 2 174.70 250.54 35.36 o 14 0 2 0.00 28.43 72.45 o -15 1 2 59.52 -34.05 79.87 o -14 1 2 94.75 96.25 70.55 o -13 1 2 3.07 -60.69 60.69 o -12 1 2 53.89 107.72 55.80 o -11 1 2 275.23 251.85 26.03 o -10 1 2 0.11 -37.08 43.05 o -9 1 2 1.84 29.79 36.85 o -8 1 2 164.89 190.91 18.70 o -7 1 2 10.39 50.61 30.74 o -6 1 2 3350.21 3787.57 78.07 o -5 1 2 672.69 901.29 36.51 o -4 1 2 2616.31 2734.78 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