#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/46/2214645.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214645_Fobs loop_ _publ_author_name 'Gallucci, Judith C.' 'Dura, Robert D.' 'Paquette, Leo A.' _publ_section_title ; (11SR,13RS)-12-Oxa-9-azatetracyclo[7.4.1.0^2,7^.0^11,13^]tetradeca-2(7),3,5-trien-8-one ; _journal_coeditor_code FL2141 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3417 _journal_volume 63 _journal_year 2007 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.364 _cell_angle_gamma 90.000 _cell_length_a 7.1597 _cell_length_b 16.5327 _cell_length_c 8.7277 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.7704 _[local]_cod_data_source_file fl2141Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Paquette 1395 in Cc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 101.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2635.03 2500.36 36.68 o 4 0 0 1384.59 1489.83 23.49 o 6 0 0 558.46 590.99 18.13 o 8 0 0 55.87 62.64 10.72 o 1 1 0 3336.07 2959.28 33.65 o 3 1 0 2175.28 2205.30 28.85 o 5 1 0 5.26 5.71 1.29 o 7 1 0 140.94 136.77 7.01 o 9 1 0 15.37 4.53 5.81 o 0 2 0 16.74 -0.41 0.41 o 2 2 0 833.54 782.70 8.98 o 4 2 0 292.12 283.64 5.36 o 6 2 0 26.92 23.81 2.28 o 8 2 0 11.64 13.19 4.37 o 1 3 0 3532.86 3271.22 34.52 o 3 3 0 1912.73 1940.78 21.71 o 5 3 0 12.24 10.93 1.75 o 7 3 0 18.90 16.18 3.17 o 9 3 0 35.34 32.72 7.03 o 2 4 0 940.27 923.54 13.19 o 4 4 0 1417.21 1484.21 17.13 o 6 4 0 165.43 167.16 5.54 o 8 4 0 27.29 23.53 4.26 o 1 5 0 3074.76 3010.28 31.20 o 3 5 0 1028.03 1142.82 12.55 o 5 5 0 632.79 610.87 9.41 o 7 5 0 40.53 35.85 4.53 o 0 6 0 0.05 0.62 0.58 o 2 6 0 125.21 113.16 1.88 o 4 6 0 2.70 1.44 1.17 o 6 6 0 37.95 29.61 3.05 o 8 6 0 49.47 44.21 6.39 o 1 7 0 504.88 483.31 6.80 o 3 7 0 165.09 141.08 2.88 o 5 7 0 697.90 759.18 14.11 o 7 7 0 49.95 42.88 4.95 o 0 8 0 167.94 173.08 3.05 o 2 8 0 31.11 25.96 1.17 o 4 8 0 765.19 798.49 11.56 o 6 8 0 400.96 418.48 11.35 o 8 8 0 46.39 51.71 7.82 o 1 9 0 101.67 95.02 1.75 o 3 9 0 230.24 250.60 3.93 o 5 9 0 665.24 709.00 14.56 o 7 9 0 39.41 40.92 4.64 o 0 10 0 315.67 327.04 5.81 o 2 10 0 482.36 477.43 6.55 o 4 10 0 472.20 470.54 9.60 o 6 10 0 37.73 35.55 3.93 o 8 10 0 130.04 146.02 11.75 o 1 11 0 155.71 160.87 2.76 o 3 11 0 309.23 306.02 6.39 o 5 11 0 430.69 465.08 11.61 o 7 11 0 4.29 2.08 4.05 o 0 12 0 104.11 105.84 3.17 o 2 12 0 229.14 232.31 4.33 o 4 12 0 263.21 260.91 6.68 o 6 12 0 84.30 83.61 5.68 o 1 13 0 671.85 689.97 9.70 o 3 13 0 37.97 35.66 2.12 o 5 13 0 18.97 20.87 3.50 o 7 13 0 186.23 239.10 16.07 o 0 14 0 1.51 2.24 2.68 o 2 14 0 161.24 154.32 3.86 o 4 14 0 390.70 442.04 10.49 o 6 14 0 83.67 77.51 7.91 o 1 15 0 6.50 10.05 1.65 o 3 15 0 24.48 24.25 2.86 o 5 15 0 24.12 17.31 4.93 o 0 16 0 2.20 0.25 2.27 o 2 16 0 4.81 4.53 2.12 o 4 16 0 108.51 100.60 5.84 o 6 16 0 3.19 -5.12 5.12 o 1 17 0 23.76 21.65 2.86 o 3 17 0 147.66 127.67 12.16 o 5 17 0 20.22 22.00 6.39 o 0 18 0 290.76 270.40 21.64 o 2 18 0 6.46 3.77 2.54 o 4 18 0 134.67 137.51 9.20 o 1 19 0 15.24 7.34 3.81 o 3 19 0 43.71 54.54 6.62 o 0 20 0 9.56 6.87 7.78 o 2 20 0 22.50 22.75 6.51 o 1 21 0 23.15 20.54 7.72 o -9 1 1 31.90 41.04 7.01 o -7 1 1 13.65 12.65 5.56 o -5 1 1 224.24 200.50 3.46 o -3 1 1 622.37 637.66 7.43 o -1 1 1 5425.88 4698.69 41.96 o 1 1 1 1843.11 1654.64 17.75 o 3 1 1 1479.66 1515.72 17.48 o 5 1 1 123.95 124.28 2.91 o 7 1 1 267.12 286.98 8.30 o -8 2 1 71.71 68.46 5.81 o -6 2 1 49.26 46.02 2.76 o -4 2 1 64.45 56.49 1.75 o -2 2 1 1030.06 960.76 9.89 o 0 2 1 3913.11 3444.11 41.23 o 2 2 1 1822.71 1791.70 18.41 o 4 2 1 302.99 315.31 5.34 o 6 2 1 237.93 216.42 6.59 o 8 2 1 21.68 17.86 5.15 o -9 3 1 33.91 45.74 6.81 o -7 3 1 69.51 65.34 3.96 o -5 3 1 5.54 5.65 1.46 o -3 3 1 300.01 290.14 3.79 o -1 3 1 9842.35 9153.65 100.30 o 1 3 1 911.50 884.42 9.39 o 3 3 1 350.63 399.96 4.93 o 5 3 1 27.15 17.13 1.75 o 7 3 1 269.75 273.28 19.16 o -8 4 1 82.91 83.97 5.51 o -6 4 1 70.35 65.53 3.75 o -4 4 1 1162.93 1167.27 14.14 o -2 4 1 278.05 261.55 3.34 o 0 4 1 2871.67 2668.81 29.05 o 2 4 1 180.02 179.02 2.46 o 4 4 1 473.31 530.69 7.32 o 6 4 1 106.16 103.13 4.64 o 8 4 1 9.03 9.39 4.64 o -7 5 1 92.25 76.17 4.45 o -5 5 1 648.98 640.20 9.79 o -3 5 1 15.29 12.38 1.17 o -1 5 1 2613.40 2493.67 26.10 o 1 5 1 1166.68 1162.66 13.37 o 3 5 1 300.29 297.62 3.75 o 5 5 1 21.80 21.72 1.88 o 7 5 1 57.16 43.00 3.75 o -8 6 1 6.92 6.18 4.08 o -6 6 1 622.23 620.14 14.71 o -4 6 1 243.82 258.64 4.34 o -2 6 1 248.74 257.62 3.30 o 0 6 1 1499.31 1503.03 14.95 o 2 6 1 2748.65 2845.91 29.41 o 4 6 1 406.64 418.09 8.24 o 6 6 1 33.19 27.89 3.17 o 8 6 1 65.91 62.09 5.74 o -7 7 1 8.71 7.94 3.34 o -5 7 1 312.06 265.52 6.39 o -3 7 1 13.54 9.55 0.87 o -1 7 1 974.74 980.22 9.76 o 1 7 1 747.69 726.48 8.01 o 3 7 1 251.85 288.40 5.15 o 5 7 1 402.42 433.49 8.68 o 7 7 1 99.32 86.55 6.12 o -8 8 1 34.93 33.08 6.84 o -6 8 1 32.31 20.30 3.75 o -4 8 1 119.93 121.44 2.76 o -2 8 1 1014.63 1091.27 12.32 o 0 8 1 1768.58 1803.29 35.85 o 2 8 1 393.51 430.56 5.63 o 4 8 1 598.21 627.95 9.09 o 6 8 1 129.73 127.16 7.62 o 8 8 1 8.27 10.80 5.99 o -7 9 1 22.82 18.12 5.15 o -5 9 1 1549.39 1680.84 31.62 o -3 9 1 740.21 757.40 9.60 o -1 9 1 1490.43 1653.34 19.16 o 1 9 1 281.53 270.64 3.63 o 3 9 1 759.35 821.56 12.16 o 5 9 1 90.72 90.54 4.05 o 7 9 1 187.25 192.99 9.31 o -8 10 1 72.88 83.74 8.65 o -6 10 1 362.33 398.52 13.61 o -4 10 1 340.32 328.20 11.95 o -2 10 1 888.59 920.88 10.38 o 0 10 1 512.60 540.32 6.44 o 2 10 1 48.60 45.17 1.75 o 4 10 1 74.58 68.65 3.34 o 6 10 1 29.95 27.33 4.34 o -7 11 1 53.21 41.61 5.93 o -5 11 1 50.10 46.17 3.50 o -3 11 1 328.73 335.60 5.81 o -1 11 1 450.76 447.18 5.39 o 1 11 1 71.11 65.54 1.68 o 3 11 1 256.50 287.08 5.54 o 5 11 1 143.12 142.85 7.62 o 7 11 1 88.04 96.61 8.21 o -6 12 1 45.65 43.26 6.18 o -4 12 1 115.71 104.15 7.01 o -2 12 1 12.34 11.05 1.29 o 0 12 1 16.53 16.99 1.29 o 2 12 1 483.16 514.60 7.72 o 4 12 1 152.46 164.47 5.45 o 6 12 1 22.55 21.91 3.75 o -7 13 1 6.31 6.20 5.51 o -5 13 1 627.11 744.93 17.37 o -3 13 1 236.45 247.32 5.54 o -1 13 1 767.54 853.03 12.36 o 1 13 1 46.55 43.90 1.75 o 3 13 1 19.82 13.65 3.09 o 5 13 1 33.97 33.23 4.16 o 7 13 1 29.27 23.51 7.43 o -6 14 1 137.05 149.47 9.68 o -4 14 1 497.72 575.49 14.63 o -2 14 1 587.23 630.11 9.37 o 0 14 1 196.02 191.00 4.61 o 2 14 1 6.12 5.91 1.68 o 4 14 1 74.21 67.32 5.56 o 6 14 1 17.44 16.90 4.80 o -5 15 1 45.80 37.42 4.55 o -3 15 1 194.00 197.20 5.79 o -1 15 1 55.87 52.70 2.36 o 1 15 1 146.39 135.27 3.75 o 3 15 1 6.07 13.23 3.27 o 5 15 1 64.69 62.15 7.01 o -6 16 1 61.34 68.75 7.92 o -4 16 1 21.81 17.19 3.92 o -2 16 1 216.89 193.38 5.08 o 0 16 1 303.67 322.26 9.48 o 2 16 1 82.94 78.53 9.89 o 4 16 1 17.56 22.42 6.39 o -5 17 1 98.45 101.66 7.51 o -3 17 1 165.57 169.89 6.86 o -1 17 1 19.22 16.66 2.49 o 1 17 1 165.81 173.57 10.92 o 3 17 1 23.53 23.45 6.18 o 5 17 1 19.92 17.84 6.48 o -4 18 1 33.87 27.04 5.15 o -2 18 1 254.86 282.44 9.74 o 0 18 1 301.73 335.25 12.36 o 2 18 1 290.07 335.97 10.72 o 4 18 1 89.83 89.08 7.68 o -3 19 1 13.76 10.30 4.05 o -1 19 1 60.88 68.56 6.80 o 1 19 1 165.99 150.24 8.00 o 3 19 1 328.18 395.47 17.76 o -2 20 1 0.28 -2.81 5.15 o 0 20 1 41.47 36.73 5.40 o 2 20 1 66.54 61.02 11.33 o -1 21 1 173.32 167.61 16.69 o 1 21 1 142.97 119.28 11.35 o -8 0 2 69.21 61.82 7.42 o -6 0 2 1788.05 1911.02 47.39 o -4 0 2 267.32 274.47 5.36 o -2 0 2 8676.23 8074.74 97.26 o 0 0 2 1092.93 1036.49 14.84 o 2 0 2 4459.70 4327.71 73.36 o 4 0 2 1506.17 1558.24 25.55 o 6 0 2 140.45 111.69 5.36 o 8 0 2 0.64 8.65 6.59 o -9 1 2 210.15 282.34 12.98 o -7 1 2 11.39 11.23 4.53 o -5 1 2 1060.39 1055.90 13.53 o -3 1 2 93.30 109.63 1.75 o -1 1 2 141.94 155.38 1.75 o 1 1 2 1583.07 1489.23 16.78 o 3 1 2 917.89 968.10 10.97 o 5 1 2 315.68 315.07 5.54 o 7 1 2 25.45 17.79 3.71 o -8 2 2 39.04 34.79 4.45 o -6 2 2 262.70 244.70 6.04 o -4 2 2 23.69 21.22 2.06 o -2 2 2 312.65 293.81 3.05 o 0 2 2 3696.54 3446.23 40.96 o 2 2 2 1027.57 991.49 11.19 o 4 2 2 152.98 151.34 2.87 o 6 2 2 198.39 193.07 5.39 o 8 2 2 8.47 8.61 5.15 o -9 3 2 56.53 57.94 6.84 o -7 3 2 179.69 188.62 6.84 o -5 3 2 167.49 158.05 2.91 o -3 3 2 446.11 437.34 4.75 o -1 3 2 10276.20 9602.50 104.59 o 1 3 2 3976.16 3758.23 38.10 o 3 3 2 902.83 945.55 12.65 o 5 3 2 442.79 485.80 12.78 o 7 3 2 17.70 11.13 4.53 o -8 4 2 75.23 68.52 6.10 o -6 4 2 1366.59 1524.49 27.39 o -4 4 2 254.38 277.05 3.63 o -2 4 2 5465.14 5411.75 51.81 o 0 4 2 144.80 135.11 2.06 o 2 4 2 660.55 661.97 8.01 o 4 4 2 228.67 245.61 4.33 o 6 4 2 180.00 165.47 5.93 o 8 4 2 13.98 2.38 5.93 o -9 5 2 161.34 179.78 11.37 o -7 5 2 53.62 43.59 4.74 o -5 5 2 625.52 646.51 8.88 o -3 5 2 859.68 938.45 9.86 o -1 5 2 4793.51 4845.29 51.14 o 1 5 2 106.97 108.12 1.68 o 3 5 2 35.69 32.57 1.29 o 5 5 2 52.50 47.44 5.36 o 7 5 2 15.46 10.62 3.56 o -8 6 2 3.28 5.31 4.16 o -6 6 2 203.16 210.95 6.51 o -4 6 2 154.61 140.23 2.87 o -2 6 2 334.47 394.54 4.93 o 0 6 2 1247.24 1308.64 15.87 o 2 6 2 1855.20 1948.22 24.11 o 4 6 2 125.59 125.79 2.76 o 6 6 2 93.97 76.15 4.26 o 8 6 2 3.48 2.34 5.04 o -7 7 2 41.06 37.06 5.04 o -5 7 2 402.33 417.00 7.80 o -3 7 2 64.81 49.68 1.46 o -1 7 2 1822.58 1877.53 19.88 o 1 7 2 67.89 76.90 1.58 o 3 7 2 824.72 897.52 12.07 o 5 7 2 62.79 51.81 3.05 o 7 7 2 134.62 132.43 7.10 o -8 8 2 82.87 78.33 10.72 o -6 8 2 35.92 30.85 3.75 o -4 8 2 483.04 486.64 8.04 o -2 8 2 2006.27 2106.96 29.26 o 0 8 2 326.14 338.71 3.93 o 2 8 2 295.04 317.03 4.34 o 4 8 2 67.58 53.46 4.33 o 6 8 2 54.07 41.22 3.96 o -7 9 2 81.22 78.17 5.39 o -5 9 2 152.65 163.44 11.13 o -3 9 2 273.73 247.50 3.79 o -1 9 2 1518.82 1649.46 24.11 o 1 9 2 299.23 310.48 6.80 o 3 9 2 113.14 84.21 2.46 o 5 9 2 63.37 57.85 3.96 o 7 9 2 88.47 93.40 8.74 o -8 10 2 40.69 50.23 14.42 o -6 10 2 0.53 -0.17 2.46 o -4 10 2 101.21 96.41 3.05 o -2 10 2 821.81 880.15 10.77 o 0 10 2 696.73 732.28 9.07 o 2 10 2 765.54 854.84 11.29 o 4 10 2 32.10 26.99 2.88 o 6 10 2 142.06 141.94 9.07 o -7 11 2 16.96 14.81 5.39 o -5 11 2 150.32 140.62 9.89 o -3 11 2 397.31 417.65 6.53 o -1 11 2 372.78 415.90 5.81 o 1 11 2 69.29 66.35 1.75 o 3 11 2 381.04 407.11 9.48 o 5 11 2 427.61 465.61 13.76 o 7 11 2 186.27 201.33 12.26 o -6 12 2 196.96 213.44 9.60 o -4 12 2 734.71 731.47 14.02 o -2 12 2 216.85 228.63 7.01 o 0 12 2 39.95 36.91 1.75 o 2 12 2 146.57 147.39 7.01 o 4 12 2 399.18 427.13 10.89 o 6 12 2 26.61 18.32 10.10 o -7 13 2 43.51 43.59 8.30 o -5 13 2 9.24 3.89 3.05 o -3 13 2 501.24 514.53 9.14 o -1 13 2 316.58 317.15 5.22 o 1 13 2 224.10 226.78 4.45 o 3 13 2 369.93 366.05 9.02 o 5 13 2 11.92 7.09 3.43 o -6 14 2 32.48 32.61 5.39 o -4 14 2 38.01 40.30 5.36 o -2 14 2 527.73 510.71 9.50 o 0 14 2 7.69 9.66 1.75 o 2 14 2 757.89 839.63 17.53 o 4 14 2 17.84 11.72 3.86 o 6 14 2 106.81 108.02 11.33 o -5 15 2 36.72 29.51 4.16 o -3 15 2 241.57 254.61 7.52 o -1 15 2 485.00 504.76 9.07 o 1 15 2 204.09 232.16 9.89 o 3 15 2 55.61 57.43 6.39 o 5 15 2 105.39 117.22 10.10 o -6 16 2 79.03 79.36 9.56 o -4 16 2 7.94 3.35 3.09 o -2 16 2 50.37 45.87 3.12 o 0 16 2 192.92 198.39 7.83 o 2 16 2 107.96 87.89 4.64 o 4 16 2 58.26 56.39 5.67 o -5 17 2 100.42 113.00 8.45 o -3 17 2 42.00 30.50 4.53 o -1 17 2 135.53 126.53 5.63 o 1 17 2 142.55 128.18 6.14 o 3 17 2 31.78 23.93 4.73 o 5 17 2 20.29 20.64 7.53 o -4 18 2 6.64 3.84 5.39 o -2 18 2 233.18 216.44 7.78 o 0 18 2 1.71 2.45 3.27 o 2 18 2 130.99 134.15 6.79 o 4 18 2 6.72 1.56 7.01 o -3 19 2 5.24 12.03 5.56 o -1 19 2 55.69 49.72 5.18 o 1 19 2 60.13 71.30 6.19 o 3 19 2 22.27 23.65 6.17 o -2 20 2 10.80 9.07 4.53 o 0 20 2 38.71 34.10 5.15 o 2 20 2 79.13 84.66 9.75 o -1 21 2 64.03 62.62 7.53 o -9 1 3 166.96 203.46 15.45 o -7 1 3 525.54 560.52 14.66 o -5 1 3 131.11 113.35 2.62 o -3 1 3 996.81 1036.72 9.47 o -1 1 3 120.29 114.40 1.58 o 1 1 3 33.84 37.10 0.87 o 3 1 3 1.15 2.88 0.87 o 5 1 3 196.70 192.90 8.04 o 7 1 3 22.79 20.49 5.77 o -8 2 3 173.67 189.73 8.59 o -6 2 3 701.26 754.13 14.79 o -4 2 3 206.82 230.55 3.05 o -2 2 3 440.15 427.58 4.37 o 0 2 3 153.75 150.07 2.88 o 2 2 3 1066.67 1159.66 13.40 o 4 2 3 632.56 655.61 9.02 o 6 2 3 274.19 269.14 7.92 o 8 2 3 11.36 12.78 4.66 o -9 3 3 63.74 62.05 7.27 o -7 3 3 332.03 355.66 10.20 o -5 3 3 148.20 150.30 3.50 o -3 3 3 3740.45 4019.28 37.51 o -1 3 3 1651.52 1617.53 17.41 o 1 3 3 3350.40 3467.17 36.70 o 3 3 3 689.91 681.35 9.18 o 5 3 3 53.16 51.44 4.12 o 7 3 3 54.46 58.16 5.15 o -8 4 3 36.87 28.95 4.64 o -6 4 3 1106.14 1124.91 19.61 o -4 4 3 362.36 352.07 4.51 o -2 4 3 7.50 8.49 0.62 o 0 4 3 2304.58 2381.15 29.28 o 2 4 3 789.56 825.97 10.20 o 4 4 3 284.93 293.80 5.09 o 6 4 3 38.77 29.00 3.34 o 8 4 3 2.78 1.36 5.22 o -9 5 3 54.81 62.58 7.72 o -7 5 3 152.30 162.38 6.33 o -5 5 3 68.30 53.82 2.33 o -3 5 3 474.43 530.99 6.22 o -1 5 3 472.90 476.83 5.68 o 1 5 3 474.29 538.84 6.73 o 3 5 3 37.81 37.62 2.06 o 5 5 3 1135.81 1229.01 24.46 o 7 5 3 9.80 13.04 3.63 o -8 6 3 4.91 8.50 5.04 o -6 6 3 268.73 292.69 8.30 o -4 6 3 678.96 694.27 8.61 o -2 6 3 1763.66 1885.83 20.05 o 0 6 3 228.38 232.26 3.21 o 2 6 3 608.20 681.71 8.42 o 4 6 3 246.78 245.72 4.80 o 6 6 3 149.49 142.24 6.10 o -7 7 3 115.02 121.23 7.01 o -5 7 3 102.86 101.23 3.05 o -3 7 3 2927.29 3246.85 36.95 o -1 7 3 1097.94 1109.47 11.97 o 1 7 3 1299.47 1376.61 28.64 o 3 7 3 342.95 380.33 5.81 o 5 7 3 122.92 129.80 5.04 o 7 7 3 32.64 42.19 5.73 o -8 8 3 38.22 40.11 5.93 o -6 8 3 149.56 156.33 5.51 o -4 8 3 307.45 307.19 8.86 o -2 8 3 53.04 47.97 1.29 o 0 8 3 196.46 210.57 3.17 o 2 8 3 8.72 7.50 1.44 o 4 8 3 67.49 62.79 2.76 o 6 8 3 87.78 92.36 9.27 o -7 9 3 301.08 339.90 13.55 o -5 9 3 282.33 310.27 5.93 o -3 9 3 117.62 103.95 2.46 o -1 9 3 343.76 375.67 4.85 o 1 9 3 239.99 257.17 3.79 o 3 9 3 274.21 298.59 5.45 o 5 9 3 463.02 505.56 14.65 o 7 9 3 69.32 71.90 8.08 o -8 10 3 81.08 80.58 9.48 o -6 10 3 48.86 42.62 3.56 o -4 10 3 211.60 222.52 5.33 o -2 10 3 126.51 133.39 2.28 o 0 10 3 196.94 201.58 3.50 o 2 10 3 114.70 114.25 2.68 o 4 10 3 265.17 268.96 9.27 o 6 10 3 56.38 55.16 5.84 o -7 11 3 73.79 78.07 9.48 o -5 11 3 51.55 39.91 5.15 o -3 11 3 56.21 49.53 2.43 o -1 11 3 189.18 173.32 3.34 o 1 11 3 337.72 371.33 5.54 o 3 11 3 51.12 35.90 2.33 o 5 11 3 65.47 60.29 7.80 o -6 12 3 0.02 5.11 3.34 o -4 12 3 237.48 230.70 6.44 o -2 12 3 210.01 211.17 3.81 o 0 12 3 176.99 168.15 3.79 o 2 12 3 189.07 174.56 4.08 o 4 12 3 44.78 42.49 3.56 o 6 12 3 29.76 27.47 5.49 o -7 13 3 86.76 81.02 8.51 o -5 13 3 19.23 12.73 3.50 o -3 13 3 20.67 19.16 1.85 o -1 13 3 533.84 596.06 10.03 o 1 13 3 201.58 183.44 3.93 o 3 13 3 35.15 25.70 3.05 o 5 13 3 116.16 113.20 7.39 o -6 14 3 67.46 69.36 6.83 o -4 14 3 42.55 44.48 3.66 o -2 14 3 23.64 27.07 1.85 o 0 14 3 24.26 16.75 1.98 o 2 14 3 30.03 23.27 3.92 o 4 14 3 190.98 200.14 17.93 o -5 15 3 31.47 26.76 4.22 o -3 15 3 182.70 171.83 7.62 o -1 15 3 10.45 7.66 1.98 o 1 15 3 127.67 143.88 7.83 o 3 15 3 70.92 57.61 4.38 o 5 15 3 194.94 218.25 21.22 o -6 16 3 1.02 5.30 8.86 o -4 16 3 7.06 7.49 4.53 o -2 16 3 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88.79 13.19 o 1 7 9 39.67 31.46 4.49 o 3 7 9 8.46 8.09 6.02 o -4 8 9 98.79 106.21 6.95 o -2 8 9 52.45 42.47 5.15 o 0 8 9 41.90 40.87 6.26 o 2 8 9 43.54 38.77 5.34 o -5 9 9 214.41 245.93 12.55 o -3 9 9 62.33 56.76 12.36 o -1 9 9 47.88 51.24 5.93 o 1 9 9 3.04 9.37 6.39 o -4 10 9 232.90 232.75 16.16 o -2 10 9 0.24 0.11 4.16 o 0 10 9 106.34 121.19 14.84 o 2 10 9 9.96 8.06 6.26 o -3 11 9 28.66 24.99 6.30 o -1 11 9 137.45 130.78 11.75 o 1 11 9 18.37 14.48 8.65 o -2 12 9 10.14 13.17 8.24 o 0 12 9 27.19 41.61 8.30 o -4 0 10 24.02 18.13 4.95 o -2 0 10 92.57 75.83 6.18 o 0 0 10 260.12 297.14 23.08 o 2 0 10 50.13 35.03 10.30 o -5 1 10 178.84 172.64 9.70 o -3 1 10 24.61 28.47 4.55 o -1 1 10 36.23 42.84 4.34 o 1 1 10 51.18 44.39 10.10 o -4 2 10 6.84 10.63 4.34 o -2 2 10 5.77 4.19 3.56 o 0 2 10 18.68 16.63 4.05 o 2 2 10 38.49 33.79 6.92 o -5 3 10 73.83 73.67 7.24 o -3 3 10 39.66 36.36 4.45 o -1 3 10 2.57 2.57 4.53 o 1 3 10 7.77 6.26 5.36 o -4 4 10 105.52 108.12 7.53 o -2 4 10 33.47 29.42 11.33 o 0 4 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