#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/46/2214658.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214658_Fobs loop_ _publ_author_name 'Vembu, Nagarajan' 'Shafna, Karattu Chali' 'Sparkes, Hazel A.' 'Howard, Judith A. K.' _publ_section_title ; 2-Naphthyl benzenesulfonate ; _journal_coeditor_code GG2026 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3545 _journal_volume 63 _journal_year 2007 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.8910 _cell_length_b 10.8909 _cell_length_c 20.9578 _exptl_crystal_F_000 1184.00 _reflns_d_resolution_high 0.7013 _[local]_cod_data_source_file gg2026Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 07has016 in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 252.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 48430.07 44164.48 1707.84 o 4 0 0 49061.69 47119.93 972.77 o 6 0 0 51672.81 54370.70 1392.20 o 8 0 0 1.35 28.50 28.21 o 10 0 0 839.18 793.55 63.04 o 12 0 0 480.41 452.86 62.44 o 14 0 0 1090.44 1055.96 95.23 o 16 0 0 1646.28 1672.93 175.21 o 1 1 0 584.30 636.39 14.20 o 3 1 0 38440.91 37181.10 595.29 o 5 1 0 4029.53 4218.11 78.15 o 7 1 0 790.24 707.68 26.59 o 9 1 0 437.96 450.62 34.50 o 11 1 0 18.78 16.56 30.08 o 13 1 0 1146.79 1119.50 62.91 o 15 1 0 158.37 143.62 58.71 o 0 2 0 1006.13 1079.25 37.70 o 2 2 0 2710.84 2715.50 49.78 o 4 2 0 108.82 105.39 13.35 o 6 2 0 79.79 108.52 15.50 o 8 2 0 963.39 980.85 41.76 o 10 2 0 53.53 -1.84 25.49 o 12 2 0 5.77 23.89 40.59 o 14 2 0 72.85 61.36 52.93 o 16 2 0 191.34 158.62 69.20 o 1 3 0 458.26 396.07 17.10 o 3 3 0 348.79 301.67 15.64 o 5 3 0 525.08 610.81 24.49 o 7 3 0 968.18 978.70 37.33 o 9 3 0 49.29 88.74 24.71 o 11 3 0 290.88 212.93 44.10 o 13 3 0 465.41 616.23 50.07 o 15 3 0 39.81 42.56 79.91 o 0 4 0 0.78 -16.60 16.60 o 2 4 0 924.24 938.78 23.81 o 4 4 0 13.52 -4.98 11.93 o 6 4 0 1100.97 1110.15 48.23 o 8 4 0 2272.79 2268.68 68.59 o 10 4 0 296.06 323.43 35.56 o 12 4 0 999.05 1058.11 58.44 o 14 4 0 62.09 -15.80 60.59 o 16 4 0 559.65 657.82 167.11 o 1 5 0 47.27 39.03 12.06 o 3 5 0 53.93 71.87 14.63 o 5 5 0 248.02 243.05 27.95 o 7 5 0 3906.22 3867.57 81.82 o 9 5 0 3120.50 3176.71 86.07 o 11 5 0 280.93 285.21 44.35 o 13 5 0 2670.41 2634.22 136.07 o 15 5 0 301.55 176.12 89.42 o 0 6 0 1263.69 1302.34 60.59 o 2 6 0 1504.64 1557.07 39.36 o 4 6 0 1230.29 1286.52 38.14 o 6 6 0 1180.66 1099.76 51.74 o 8 6 0 1802.62 1850.18 61.32 o 10 6 0 338.18 354.47 45.01 o 12 6 0 287.64 125.59 66.33 o 14 6 0 30.81 13.62 81.04 o 1 7 0 488.42 491.05 28.90 o 3 7 0 198.28 246.01 55.49 o 5 7 0 404.25 382.31 32.67 o 7 7 0 1.53 -20.70 27.15 o 9 7 0 15.64 5.57 36.03 o 11 7 0 3.19 -11.13 61.49 o 13 7 0 1.19 -7.94 70.34 o 0 8 0 5147.70 4822.81 158.06 o 2 8 0 709.08 686.05 44.74 o 4 8 0 1307.61 1305.44 59.95 o 6 8 0 1909.21 1785.41 72.83 o 8 8 0 63.43 -7.86 38.25 o 10 8 0 547.97 565.81 75.90 o 12 8 0 128.29 91.17 75.63 o 14 8 0 111.38 162.74 137.80 o 1 9 0 1369.66 1328.22 70.96 o 3 9 0 8613.71 8009.89 201.33 o 5 9 0 359.72 375.08 43.16 o 7 9 0 1857.93 1917.43 158.38 o 9 9 0 544.78 655.94 77.99 o 11 9 0 455.00 291.19 99.76 o 13 9 0 887.24 1040.67 166.48 o 0 10 0 6128.15 5682.21 273.11 o 2 10 0 274.02 287.32 53.00 o 4 10 0 207.31 197.70 49.68 o 6 10 0 1168.01 1242.24 135.62 o 8 10 0 113.96 -10.23 56.19 o 10 10 0 7.31 7.48 91.66 o 12 10 0 274.85 486.35 154.63 o 1 11 0 549.34 544.67 122.52 o 3 11 0 1095.46 1142.56 85.45 o 5 11 0 1175.53 1222.89 97.27 o 7 11 0 45.90 14.95 67.65 o 9 11 0 200.61 183.32 109.74 o 0 12 0 614.17 701.47 102.88 o 2 12 0 198.40 234.93 66.41 o 4 12 0 99.59 125.90 90.41 o 6 12 0 928.66 1075.75 185.50 o 8 12 0 33.29 -97.89 97.89 o 1 13 0 3.42 14.08 73.89 o 3 13 0 677.08 824.19 249.72 o 5 13 0 118.81 65.09 132.50 o 7 13 0 168.99 430.86 122.21 o 0 14 0 2377.90 2347.58 187.68 o 2 14 0 482.81 578.02 85.38 o 4 14 0 7.33 -3.43 164.61 o 6 14 0 978.75 1146.04 159.00 o 1 15 0 2.78 -91.04 98.52 o 3 15 0 7.50 -109.12 109.12 o 1 1 1 248.99 255.37 9.69 o 2 1 1 6004.52 5793.27 65.06 o 3 1 1 12352.20 12303.13 142.62 o 4 1 1 13.18 -5.36 6.54 o 5 1 1 1379.50 1437.91 28.00 o 6 1 1 3901.79 4000.34 61.60 o 7 1 1 145.78 115.12 13.19 o 8 1 1 1172.34 1178.21 32.74 o 9 1 1 45.58 33.26 16.57 o 10 1 1 52.34 22.34 22.68 o 11 1 1 112.87 83.46 22.00 o 12 1 1 112.60 102.78 25.92 o 13 1 1 442.05 454.50 34.16 o 14 1 1 180.89 205.79 34.63 o 15 1 1 47.49 -0.59 38.94 o 16 1 1 2.95 -27.56 50.83 o 0 2 1 2155.07 2015.86 41.79 o 1 2 1 63809.24 59836.42 675.42 o 2 2 1 9826.26 10036.18 111.14 o 3 2 1 623.51 631.35 18.04 o 4 2 1 851.30 761.08 17.52 o 5 2 1 14937.50 14752.03 182.46 o 6 2 1 5.86 -9.21 9.21 o 7 2 1 2008.00 2091.84 44.96 o 8 2 1 531.31 709.11 26.72 o 9 2 1 146.35 199.87 19.97 o 10 2 1 535.00 533.96 27.92 o 11 2 1 568.57 601.22 40.56 o 12 2 1 268.39 272.72 27.42 o 13 2 1 36.70 7.15 27.45 o 14 2 1 192.79 187.73 34.59 o 15 2 1 599.34 568.90 51.53 o 16 2 1 435.84 584.51 61.54 o 1 3 1 537.41 624.00 14.42 o 2 3 1 10640.53 9909.85 110.93 o 3 3 1 3.01 30.41 6.91 o 4 3 1 2845.58 2829.76 40.02 o 5 3 1 51.82 92.17 10.81 o 6 3 1 127.95 176.32 15.20 o 7 3 1 253.39 259.09 15.61 o 8 3 1 2241.04 2184.38 44.59 o 9 3 1 554.63 572.35 26.01 o 10 3 1 278.91 245.35 26.75 o 11 3 1 36.38 35.69 20.86 o 12 3 1 531.96 560.20 36.82 o 13 3 1 218.31 256.07 31.81 o 14 3 1 1079.69 1223.93 57.78 o 15 3 1 182.98 228.01 44.77 o 16 3 1 18.79 -116.60 127.20 o 0 4 1 3765.15 3886.49 107.30 o 1 4 1 1307.15 1369.58 24.43 o 2 4 1 0.16 -0.34 6.86 o 3 4 1 526.67 564.79 14.80 o 4 4 1 457.92 496.70 15.90 o 5 4 1 25.04 42.76 10.31 o 6 4 1 56.12 34.96 11.06 o 7 4 1 2.26 -3.61 11.63 o 8 4 1 2.85 -13.20 14.63 o 9 4 1 4.10 3.30 17.76 o 10 4 1 7.48 29.47 19.37 o 11 4 1 207.09 195.17 24.84 o 12 4 1 6.12 -26.71 26.71 o 13 4 1 25.94 -31.16 31.16 o 14 4 1 31.07 10.00 46.43 o 15 4 1 21.41 -19.07 52.24 o 16 4 1 17.39 -39.62 101.75 o 1 5 1 1721.60 1568.10 27.54 o 2 5 1 3183.48 3069.43 42.89 o 3 5 1 1278.50 1258.99 23.74 o 4 5 1 261.77 282.98 13.63 o 5 5 1 103.19 108.49 12.21 o 6 5 1 56.56 40.28 12.59 o 7 5 1 186.80 211.80 16.65 o 8 5 1 155.74 175.88 18.03 o 9 5 1 9.70 -11.81 17.50 o 10 5 1 3.26 -20.77 20.77 o 11 5 1 0.07 -24.78 24.78 o 12 5 1 8.38 1.02 32.74 o 13 5 1 104.65 21.02 46.06 o 14 5 1 173.05 148.34 54.20 o 15 5 1 23.78 12.77 56.61 o 16 5 1 1.76 -44.27 136.55 o 0 6 1 530.34 531.76 34.41 o 1 6 1 544.37 548.66 33.12 o 2 6 1 809.56 830.56 23.71 o 3 6 1 688.66 784.83 19.91 o 4 6 1 30.35 10.54 11.77 o 5 6 1 940.42 929.46 26.33 o 6 6 1 214.44 193.79 17.11 o 7 6 1 226.34 223.12 21.67 o 8 6 1 248.89 211.19 22.76 o 9 6 1 245.29 268.43 47.78 o 10 6 1 16.00 -5.66 25.71 o 11 6 1 998.11 1009.49 51.97 o 12 6 1 148.37 100.86 48.12 o 13 6 1 24.31 -30.85 48.30 o 14 6 1 0.23 -24.74 54.58 o 15 6 1 137.74 154.96 115.98 o 1 7 1 247.53 262.27 16.94 o 2 7 1 2416.25 2317.12 44.06 o 3 7 1 982.73 951.76 31.46 o 4 7 1 109.46 111.58 19.97 o 5 7 1 218.76 254.41 22.13 o 6 7 1 310.27 339.84 23.42 o 7 7 1 1663.63 1603.46 44.34 o 8 7 1 3712.49 3469.51 70.93 o 9 7 1 944.68 981.73 43.12 o 10 7 1 94.16 74.82 27.56 o 11 7 1 120.54 102.39 36.50 o 12 7 1 446.26 560.68 58.77 o 13 7 1 769.62 761.53 70.03 o 14 7 1 434.08 380.34 67.05 o 0 8 1 1196.04 1231.70 93.67 o 1 8 1 350.93 356.85 28.30 o 2 8 1 426.64 446.25 27.39 o 3 8 1 78.10 79.38 21.00 o 4 8 1 148.43 110.32 21.77 o 5 8 1 1014.74 992.85 38.50 o 6 8 1 965.85 1043.36 43.18 o 7 8 1 242.92 245.33 29.49 o 8 8 1 5.96 -21.92 26.22 o 9 8 1 1.14 -13.56 29.95 o 10 8 1 1005.87 1096.84 65.47 o 11 8 1 424.70 385.04 46.48 o 12 8 1 1.63 0.71 51.00 o 13 8 1 43.01 3.51 51.43 o 14 8 1 137.38 246.92 140.29 o 1 9 1 10.32 -4.31 25.65 o 2 9 1 43.16 16.74 21.49 o 3 9 1 348.42 365.05 37.19 o 4 9 1 7.79 14.49 24.29 o 5 9 1 220.85 244.65 42.98 o 6 9 1 19.46 4.80 25.59 o 7 9 1 73.95 79.54 30.08 o 8 9 1 28.46 1.99 31.61 o 9 9 1 214.59 148.01 38.51 o 10 9 1 95.56 80.74 44.56 o 11 9 1 9.39 -27.56 52.10 o 12 9 1 70.57 78.76 69.27 o 13 9 1 19.95 3.38 68.69 o 0 10 1 453.48 520.69 49.45 o 1 10 1 985.85 1014.61 60.68 o 2 10 1 76.62 77.36 26.00 o 3 10 1 204.78 240.72 32.48 o 4 10 1 61.35 48.02 28.40 o 5 10 1 1705.67 1680.21 60.45 o 6 10 1 531.24 680.63 56.65 o 7 10 1 218.65 211.85 34.69 o 8 10 1 3.20 -33.10 38.17 o 9 10 1 740.20 788.20 73.53 o 10 10 1 101.27 156.57 67.88 o 11 10 1 405.39 291.44 76.97 o 12 10 1 15.99 -117.22 117.22 o 1 11 1 551.47 623.49 46.67 o 2 11 1 1468.93 1417.39 63.10 o 3 11 1 135.90 124.56 31.90 o 4 11 1 1970.82 1890.60 65.52 o 5 11 1 187.07 249.57 41.27 o 6 11 1 2.39 -7.97 39.87 o 7 11 1 72.55 89.51 41.80 o 8 11 1 664.95 845.73 73.88 o 9 11 1 155.76 73.44 55.85 o 10 11 1 189.34 106.94 80.44 o 0 12 1 68.39 78.45 50.45 o 1 12 1 2282.63 2133.56 80.51 o 2 12 1 335.38 354.18 69.75 o 3 12 1 76.48 49.20 38.30 o 4 12 1 57.91 37.96 39.42 o 5 12 1 431.02 502.96 52.01 o 6 12 1 110.75 88.67 49.28 o 7 12 1 609.39 529.07 73.56 o 8 12 1 149.83 159.90 65.15 o 9 12 1 24.85 -64.75 94.15 o 1 13 1 4.28 36.49 40.76 o 2 13 1 518.63 531.66 57.48 o 3 13 1 192.98 240.23 48.79 o 4 13 1 321.57 329.29 51.35 o 5 13 1 6.26 7.91 42.09 o 6 13 1 14.10 -24.48 45.37 o 7 13 1 0.47 24.18 59.10 o 0 14 1 80.53 5.70 63.30 o 1 14 1 701.74 581.08 60.76 o 2 14 1 51.22 40.33 49.41 o 3 14 1 73.80 46.82 53.62 o 4 14 1 4.14 14.95 50.58 o 5 14 1 203.29 204.87 56.53 o 6 14 1 87.38 48.01 108.49 o 1 15 1 7.30 -103.51 103.51 o 2 15 1 116.50 189.55 106.00 o 3 15 1 47.28 142.16 112.86 o 4 15 1 26.93 -21.20 106.00 o 0 0 2 13610.24 7443.68 280.59 o 1 0 2 2887.43 2777.48 62.50 o 2 0 2 550.28 544.36 20.44 o 3 0 2 16694.47 16945.83 310.55 o 4 0 2 6083.68 5850.02 118.26 o 5 0 2 7265.06 6760.27 135.13 o 6 0 2 2268.75 2264.52 103.41 o 7 0 2 821.18 960.06 31.62 o 8 0 2 977.86 907.91 41.40 o 9 0 2 2768.83 2727.77 76.38 o 10 0 2 430.90 432.95 36.93 o 11 0 2 337.82 432.22 40.62 o 12 0 2 31.14 12.70 32.18 o 13 0 2 339.84 421.51 61.56 o 14 0 2 274.56 300.96 56.62 o 15 0 2 37.40 47.39 56.29 o 16 0 2 2.19 -66.63 80.21 o 1 1 2 1114.12 1064.89 16.99 o 2 1 2 553.81 530.34 10.88 o 3 1 2 5369.49 5240.60 63.94 o 4 1 2 969.64 1191.06 21.19 o 5 1 2 209.53 238.59 14.54 o 6 1 2 2577.48 2597.20 44.35 o 7 1 2 766.54 741.41 22.45 o 8 1 2 244.36 192.96 18.88 o 9 1 2 371.37 367.05 23.27 o 10 1 2 52.90 21.35 22.03 o 11 1 2 38.43 35.50 21.20 o 12 1 2 78.41 76.63 25.58 o 13 1 2 17.93 1.51 27.82 o 14 1 2 460.78 471.51 40.82 o 15 1 2 1.10 -14.97 39.06 o 16 1 2 454.88 451.18 65.62 o 0 2 2 4334.09 4089.90 79.04 o 1 2 2 2542.10 2482.83 36.28 o 2 2 2 17819.59 17687.03 213.51 o 3 2 2 322.63 372.97 11.41 o 4 2 2 373.93 378.36 16.12 o 5 2 2 903.78 876.45 20.81 o 6 2 2 607.12 684.09 22.45 o 7 2 2 0.13 -11.44 11.44 o 8 2 2 1771.03 1777.77 39.76 o 9 2 2 0.17 -7.16 16.37 o 10 2 2 111.04 96.63 20.70 o 11 2 2 160.98 105.23 28.16 o 12 2 2 25.30 24.08 24.29 o 13 2 2 37.42 45.79 30.64 o 14 2 2 165.28 116.30 33.45 o 15 2 2 1.36 6.84 43.31 o 16 2 2 12.76 4.72 58.09 o 1 3 2 11068.09 10579.76 138.77 o 2 3 2 6340.75 5992.09 76.99 o 3 3 2 12675.73 12543.15 147.10 o 4 3 2 181.50 178.79 10.44 o 5 3 2 5296.29 5365.12 73.86 o 6 3 2 474.10 516.06 18.80 o 7 3 2 920.21 872.25 24.27 o 8 3 2 359.37 425.27 20.08 o 9 3 2 746.63 784.45 28.86 o 10 3 2 39.57 20.80 18.90 o 11 3 2 241.43 304.65 25.84 o 12 3 2 35.37 34.80 26.28 o 13 3 2 269.46 217.77 31.01 o 14 3 2 770.31 731.26 45.46 o 15 3 2 56.81 84.35 47.83 o 16 3 2 3.72 -91.45 192.67 o 0 4 2 3607.73 3921.58 96.34 o 1 4 2 891.14 762.85 18.64 o 2 4 2 0.02 -4.16 8.44 o 3 4 2 977.29 1096.49 22.25 o 4 4 2 428.58 500.38 15.73 o 5 4 2 1885.37 1727.28 32.04 o 6 4 2 7.92 5.35 11.29 o 7 4 2 701.32 689.47 23.14 o 8 4 2 349.27 356.65 20.14 o 9 4 2 685.11 752.27 32.96 o 10 4 2 367.50 347.38 26.02 o 11 4 2 2935.21 2726.40 59.81 o 12 4 2 484.02 438.52 35.11 o 13 4 2 395.15 348.78 40.20 o 14 4 2 1.08 10.80 43.88 o 15 4 2 247.23 172.71 57.90 o 16 4 2 131.22 198.28 160.87 o 1 5 2 84.79 122.29 11.19 o 2 5 2 495.78 419.74 16.78 o 3 5 2 70.51 95.15 10.04 o 4 5 2 157.46 243.71 13.83 o 5 5 2 198.56 217.96 14.74 o 6 5 2 25.48 3.33 12.12 o 7 5 2 8.83 5.74 13.43 o 8 5 2 8158.08 7586.19 107.11 o 9 5 2 201.54 191.72 23.49 o 10 5 2 41.02 11.08 22.59 o 11 5 2 68.88 64.75 28.35 o 12 5 2 531.77 597.12 47.21 o 13 5 2 284.25 367.63 56.53 o 14 5 2 2320.80 2488.44 99.60 o 15 5 2 161.90 124.97 60.16 o 0 6 2 708.98 770.85 40.49 o 1 6 2 182.46 245.72 28.99 o 2 6 2 357.02 391.84 19.77 o 3 6 2 3679.49 3762.57 60.36 o 4 6 2 50.71 38.76 13.41 o 5 6 2 194.75 164.28 21.98 o 6 6 2 96.13 98.02 16.72 o 7 6 2 541.95 620.47 32.82 o 8 6 2 40.83 56.42 20.10 o 9 6 2 432.99 470.55 42.09 o 10 6 2 236.35 210.61 33.66 o 11 6 2 763.21 890.67 70.17 o 12 6 2 64.91 69.01 36.73 o 13 6 2 96.87 43.41 47.61 o 14 6 2 151.43 119.94 56.91 o 15 6 2 30.27 -83.79 92.51 o 1 7 2 485.18 541.59 25.98 o 2 7 2 1078.72 1023.80 30.00 o 3 7 2 507.19 543.21 28.11 o 4 7 2 0.89 3.35 15.33 o 5 7 2 838.96 919.37 35.93 o 6 7 2 230.88 211.40 24.14 o 7 7 2 342.40 383.49 32.63 o 8 7 2 9.46 5.37 21.55 o 9 7 2 27.18 -10.28 22.95 o 10 7 2 34.19 15.63 30.26 o 11 7 2 2.63 -32.50 33.14 o 12 7 2 3.61 -36.69 36.69 o 13 7 2 65.30 24.16 50.72 o 14 7 2 53.46 91.54 60.74 o 0 8 2 3416.70 3468.98 102.12 o 1 8 2 869.34 916.77 35.19 o 2 8 2 68.84 78.04 20.43 o 3 8 2 22.09 28.60 19.54 o 4 8 2 1177.40 1132.73 36.79 o 5 8 2 1043.44 1034.44 39.35 o 6 8 2 603.81 721.32 36.70 o 7 8 2 54.91 61.69 25.73 o 8 8 2 259.96 317.45 32.55 o 9 8 2 8.40 -31.40 31.40 o 10 8 2 485.32 487.94 48.93 o 11 8 2 79.66 34.06 43.11 o 12 8 2 0.02 26.30 61.73 o 13 8 2 0.08 -50.60 60.17 o 14 8 2 110.77 -120.96 130.94 o 1 9 2 901.10 878.83 40.67 o 2 9 2 183.12 175.12 24.30 o 3 9 2 1934.73 1928.69 54.13 o 4 9 2 11.83 2.03 24.19 o 5 9 2 3.24 -2.81 25.24 o 6 9 2 1219.41 1251.62 46.60 o 7 9 2 299.20 285.77 33.39 o 8 9 2 2558.42 2470.68 69.18 o 9 9 2 18.37 -26.51 39.64 o 10 9 2 7.96 -41.28 41.28 o 11 9 2 54.61 -10.74 44.85 o 12 9 2 460.71 613.34 83.02 o 13 9 2 33.88 66.95 122.83 o 0 10 2 587.95 679.20 72.05 o 1 10 2 1666.26 1543.08 68.88 o 2 10 2 23.65 34.95 23.51 o 3 10 2 238.41 226.78 32.11 o 4 10 2 497.17 588.56 44.40 o 5 10 2 2281.40 2281.71 69.98 o 6 10 2 85.44 107.95 32.53 o 7 10 2 219.07 160.13 35.77 o 8 10 2 79.47 29.41 40.43 o 9 10 2 1041.15 1104.71 82.16 o 10 10 2 15.75 -29.74 46.28 o 11 10 2 576.13 698.94 101.84 o 12 10 2 1.05 95.83 87.62 o 1 11 2 30.89 -26.76 26.76 o 2 11 2 400.68 455.79 40.78 o 3 11 2 16.92 -27.89 27.89 o 4 11 2 122.07 117.14 39.71 o 5 11 2 7.43 -18.38 32.29 o 6 11 2 24.24 9.98 33.51 o 7 11 2 0.28 -44.82 44.82 o 8 11 2 36.36 91.56 52.18 o 9 11 2 0.01 49.53 57.11 o 10 11 2 32.48 -29.01 71.77 o 0 12 2 423.12 423.47 64.15 o 1 12 2 233.22 281.11 43.61 o 2 12 2 99.32 164.49 40.32 o 3 12 2 26.87 1.00 34.71 o 4 12 2 101.13 66.36 35.26 o 5 12 2 283.83 251.16 46.08 o 6 12 2 206.54 135.80 46.97 o 7 12 2 431.35 336.60 63.88 o 8 12 2 2.77 -40.80 57.50 o 9 12 2 74.39 129.98 67.09 o 1 13 2 0.01 10.00 39.44 o 2 13 2 46.21 38.86 45.18 o 3 13 2 6.60 27.55 52.62 o 4 13 2 19.84 24.18 48.37 o 5 13 2 0.01 -42.03 43.95 o 6 13 2 0.06 76.56 66.10 o 7 13 2 29.09 6.29 61.83 o 8 13 2 184.75 193.29 127.20 o 0 14 2 72.09 17.79 63.70 o 1 14 2 20.90 -5.09 46.34 o 2 14 2 1.77 -47.44 48.14 o 3 14 2 1.83 10.40 50.59 o 4 14 2 22.30 -27.74 48.31 o 5 14 2 21.21 4.14 75.04 o 6 14 2 1.11 51.13 106.62 o 7 14 2 3.13 -15.59 112.24 o 1 15 2 38.98 45.33 86.40 o 2 15 2 7.22 -83.55 103.51 o 3 15 2 9.63 -103.51 103.51 o 1 1 3 479.38 456.74 11.11 o 2 1 3 5078.70 4949.71 71.74 o 3 1 3 4954.12 4482.86 60.37 o 4 1 3 3110.65 3211.08 48.16 o 5 1 3 426.43 472.39 15.67 o 6 1 3 5.45 5.46 10.88 o 7 1 3 1509.64 1377.19 29.81 o 8 1 3 2070.88 2068.60 39.72 o 9 1 3 510.49 496.23 26.73 o 10 1 3 16.82 1.66 19.75 o 11 1 3 43.69 22.42 21.75 o 12 1 3 293.51 272.09 30.43 o 13 1 3 1184.12 1300.43 50.04 o 14 1 3 124.38 81.30 41.33 o 15 1 3 304.51 187.71 43.88 o 16 1 3 268.07 369.91 57.99 o 0 2 3 44768.05 41459.20 740.86 o 1 2 3 16871.79 16804.94 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