#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/46/2214684.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214684_Fobs loop_ _publ_author_name '\"Ozkinali, Sevil' 'U\,car, Ibrahim' 'Kocaokutgen, Hasan' 'Bulut, Ahmet' _publ_section_title ; 25,27-Bis(acryloyloxy)-5,11,17,23-tetra-tert-butyl-26,28-dihydroxycalix[4]arene ; _journal_coeditor_code HB2469 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3396 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.047 _cell_angle_gamma 90.000 _cell_length_a 15.8896 _cell_length_b 26.4819 _cell_length_c 10.3522 _exptl_crystal_F_000 1578.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file hb2469Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TEST STRUCTURE D:\DATA\HASAN8_C2C\HASAN8' _shelx_refln_list_code 4 _shelx_f_calc_maximum 545.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 893.62 368.44 129.24 o 4 0 0 59897.05 51036.42 3256.24 o 6 0 0 779.62 497.12 73.88 o 8 0 0 7748.43 6761.58 318.35 o 10 0 0 1573.61 1513.15 81.69 o 12 0 0 429.71 497.59 64.50 o 14 0 0 250.11 282.01 62.77 o 16 0 0 52.27 41.18 64.78 o 18 0 0 4.93 -32.78 69.02 o 3 1 0 3308.46 1985.34 83.58 o 5 1 0 661.05 704.63 60.32 o 7 1 0 3720.74 3101.48 110.24 o 9 1 0 1193.67 1074.05 47.60 o 11 1 0 21.29 18.89 43.85 o 13 1 0 81.50 73.05 45.05 o 15 1 0 226.69 252.52 44.88 o 17 1 0 8.07 10.07 47.17 o 19 1 0 19.80 36.85 52.17 o 2 2 0 6054.81 4341.57 162.69 o 4 2 0 12144.91 12551.96 1017.06 o 6 2 0 773.51 811.27 52.18 o 8 2 0 1703.48 1574.93 76.51 o 10 2 0 240.85 268.22 46.14 o 12 2 0 54.58 59.08 44.66 o 14 2 0 406.84 446.87 46.97 o 16 2 0 0.45 -35.89 47.02 o 18 2 0 17.05 7.10 49.00 o 1 3 0 4317.16 3839.10 98.74 o 3 3 0 2999.01 2965.80 100.97 o 5 3 0 1357.17 1490.39 61.16 o 7 3 0 11274.61 11289.61 395.09 o 9 3 0 2.14 7.91 45.59 o 11 3 0 2.80 8.35 44.52 o 13 3 0 2.32 64.69 45.03 o 15 3 0 932.42 898.13 45.51 o 17 3 0 11.84 27.44 46.37 o 19 3 0 56.80 13.12 51.78 o 0 4 0 109.70 204.50 121.46 o 2 4 0 1927.67 1958.45 71.86 o 4 4 0 263.63 238.12 58.22 o 6 4 0 60.11 99.38 48.62 o 8 4 0 816.45 713.92 50.62 o 10 4 0 1263.19 1205.97 48.80 o 12 4 0 14.27 7.91 43.21 o 14 4 0 485.21 553.30 45.25 o 16 4 0 3.01 42.12 46.63 o 18 4 0 0.71 51.15 50.79 o 1 5 0 1124.01 1220.33 79.21 o 3 5 0 6667.66 5872.77 426.95 o 5 5 0 1641.93 1684.84 56.83 o 7 5 0 3055.64 3024.07 78.76 o 9 5 0 637.37 657.70 49.14 o 11 5 0 122.61 163.99 44.69 o 13 5 0 346.33 381.49 44.96 o 15 5 0 169.39 167.87 44.28 o 17 5 0 32.06 39.29 46.89 o 19 5 0 8.96 71.15 52.12 o 0 6 0 71326.06 70206.48 1481.56 o 2 6 0 3303.21 2923.17 72.92 o 4 6 0 611.80 571.12 57.10 o 6 6 0 66.56 133.23 43.63 o 8 6 0 2483.67 2415.39 76.40 o 10 6 0 1.38 50.67 47.88 o 12 6 0 95.08 151.62 43.51 o 14 6 0 468.45 474.89 44.16 o 16 6 0 99.96 28.72 46.65 o 18 6 0 24.77 31.43 48.67 o 1 7 0 3460.79 3558.98 79.59 o 3 7 0 163.72 237.14 59.28 o 5 7 0 39.92 33.65 47.21 o 7 7 0 1581.39 1585.26 46.02 o 9 7 0 371.00 357.47 45.18 o 11 7 0 11.84 17.39 45.95 o 13 7 0 33.22 37.24 42.70 o 15 7 0 83.51 52.03 45.45 o 17 7 0 41.07 37.04 47.50 o 19 7 0 14.01 74.68 52.21 o 0 8 0 46625.55 45570.58 639.12 o 2 8 0 21.51 67.77 63.43 o 4 8 0 3669.78 3145.16 93.73 o 6 8 0 684.19 769.66 46.39 o 8 8 0 152.74 137.25 41.31 o 10 8 0 119.29 169.94 45.42 o 12 8 0 41.49 41.93 42.02 o 14 8 0 138.35 196.49 45.27 o 16 8 0 0.02 14.23 47.19 o 18 8 0 1.02 -8.07 51.50 o 1 9 0 378.78 284.36 63.56 o 3 9 0 6431.90 6126.29 119.08 o 5 9 0 791.46 922.88 46.88 o 7 9 0 1746.85 1866.33 45.44 o 9 9 0 259.98 258.52 42.53 o 11 9 0 194.89 251.12 43.14 o 13 9 0 173.81 195.84 43.45 o 15 9 0 138.50 105.83 45.69 o 17 9 0 53.41 47.30 49.14 o 0 10 0 5574.68 5486.20 109.47 o 2 10 0 2.24 45.48 55.78 o 4 10 0 120.35 112.85 45.65 o 6 10 0 36.20 49.14 42.62 o 8 10 0 344.16 365.97 40.75 o 10 10 0 0.88 52.60 41.50 o 12 10 0 428.45 442.99 45.20 o 14 10 0 28.01 35.47 42.12 o 16 10 0 158.57 170.34 48.03 o 18 10 0 51.51 82.78 51.71 o 1 11 0 587.97 539.20 51.11 o 3 11 0 4588.03 4401.86 99.39 o 5 11 0 2833.51 2901.88 66.97 o 7 11 0 157.65 153.64 41.95 o 9 11 0 247.21 219.61 41.63 o 11 11 0 114.35 162.01 42.99 o 13 11 0 786.21 725.65 45.65 o 15 11 0 119.67 130.63 44.05 o 17 11 0 215.09 227.99 47.11 o 0 12 0 41573.10 40515.23 657.30 o 2 12 0 2422.87 2541.92 56.41 o 4 12 0 254.87 330.68 48.37 o 6 12 0 319.50 417.13 44.27 o 8 12 0 457.46 537.93 44.04 o 10 12 0 325.31 314.36 42.34 o 12 12 0 237.62 242.86 44.83 o 14 12 0 577.43 529.49 47.99 o 16 12 0 208.35 202.03 44.94 o 18 12 0 78.14 97.51 50.85 o 1 13 0 2449.26 2804.76 57.12 o 3 13 0 4298.76 5218.92 86.62 o 5 13 0 363.40 298.63 46.58 o 7 13 0 49.06 87.22 43.77 o 9 13 0 233.56 197.05 41.97 o 11 13 0 50.48 67.18 43.53 o 13 13 0 281.76 325.07 42.85 o 15 13 0 1.23 29.10 44.19 o 17 13 0 14.28 -16.44 48.76 o 0 14 0 245.74 169.65 77.91 o 2 14 0 153.80 196.06 48.54 o 4 14 0 7.31 72.77 46.20 o 6 14 0 513.82 493.61 46.16 o 8 14 0 30.75 71.26 41.98 o 10 14 0 1597.48 1555.09 45.71 o 12 14 0 29.41 52.86 41.57 o 14 14 0 961.39 932.18 49.33 o 16 14 0 157.61 158.32 48.30 o 1 15 0 277.90 389.69 48.96 o 3 15 0 1523.16 1302.69 51.01 o 5 15 0 1291.23 1279.34 51.34 o 7 15 0 365.58 291.28 43.96 o 9 15 0 3602.13 3579.82 99.37 o 11 15 0 157.47 148.29 41.85 o 13 15 0 90.62 143.58 44.25 o 15 15 0 175.62 194.46 48.15 o 17 15 0 37.05 27.52 49.35 o 0 16 0 6.78 128.64 67.95 o 2 16 0 1164.82 1092.64 50.91 o 4 16 0 218.95 313.27 48.70 o 6 16 0 330.70 348.66 47.09 o 8 16 0 624.39 639.04 40.76 o 10 16 0 2118.13 1979.49 74.12 o 12 16 0 213.98 182.19 42.51 o 14 16 0 493.72 529.54 44.71 o 16 16 0 16.75 18.14 47.35 o 1 17 0 868.78 763.31 53.60 o 3 17 0 2909.73 2928.59 77.40 o 5 17 0 2142.66 2369.85 86.30 o 7 17 0 117.36 140.01 46.19 o 9 17 0 2549.87 2700.90 94.02 o 11 17 0 44.73 65.40 42.97 o 13 17 0 171.84 199.67 43.17 o 15 17 0 59.02 18.80 49.85 o 0 18 0 17.03 38.95 68.26 o 2 18 0 350.38 279.73 48.38 o 4 18 0 12.32 36.28 48.65 o 6 18 0 1038.17 1060.00 47.29 o 8 18 0 195.78 228.10 44.16 o 10 18 0 17.58 61.72 45.94 o 12 18 0 26.35 20.52 41.76 o 14 18 0 141.87 133.22 45.35 o 16 18 0 23.14 37.12 51.83 o 1 19 0 95.25 99.19 49.40 o 3 19 0 66.35 85.33 47.06 o 5 19 0 213.08 268.55 47.56 o 7 19 0 342.45 327.33 46.88 o 9 19 0 671.45 632.47 45.94 o 11 19 0 140.56 134.87 47.56 o 13 19 0 17.49 47.87 44.57 o 15 19 0 0.10 63.22 47.24 o 0 20 0 254.41 423.13 70.08 o 2 20 0 45.44 50.97 48.27 o 4 20 0 48.61 42.36 44.49 o 6 20 0 898.17 894.63 48.64 o 8 20 0 62.44 44.05 44.18 o 10 20 0 23.07 49.01 46.65 o 12 20 0 16.41 -9.13 47.34 o 14 20 0 14.41 25.25 52.08 o 1 21 0 84.57 120.09 47.13 o 3 21 0 138.95 193.44 47.44 o 5 21 0 840.05 902.31 49.34 o 7 21 0 33.84 1.85 47.26 o 9 21 0 4.06 65.75 46.40 o 11 21 0 141.40 114.87 49.13 o 13 21 0 30.92 71.99 51.35 o 0 22 0 462.02 598.27 74.58 o 2 22 0 1081.53 1139.25 52.01 o 4 22 0 16.61 -13.92 48.94 o 6 22 0 1277.98 1204.89 50.42 o 8 22 0 544.42 491.35 45.55 o 10 22 0 136.48 113.25 46.16 o 12 22 0 23.41 76.51 48.83 o 14 22 0 169.42 205.76 50.82 o 1 23 0 30.11 94.19 50.75 o 3 23 0 116.96 77.57 48.59 o 5 23 0 329.39 367.13 47.78 o 7 23 0 1.16 61.38 45.87 o 9 23 0 174.55 153.06 48.16 o 11 23 0 3.89 8.72 47.41 o 13 23 0 21.49 61.06 52.76 o 0 24 0 649.98 625.94 115.66 o 2 24 0 6.07 17.31 51.29 o 4 24 0 0.59 44.86 45.87 o 6 24 0 263.24 308.22 46.28 o 8 24 0 17.94 39.61 45.78 o 10 24 0 19.18 27.12 48.84 o 12 24 0 153.87 182.62 54.38 o 1 25 0 142.19 15.67 53.90 o 3 25 0 592.24 559.20 50.33 o 5 25 0 13.62 -26.34 48.64 o 7 25 0 67.81 59.19 48.13 o 9 25 0 55.61 62.24 49.99 o 11 25 0 0.51 48.76 52.07 o 0 26 0 676.65 664.18 79.26 o 2 26 0 20.36 -36.12 59.75 o 4 26 0 76.07 61.04 48.76 o 6 26 0 41.24 56.78 49.61 o 8 26 0 17.30 21.90 49.23 o 10 26 0 6.45 58.49 50.76 o 1 27 0 1.14 116.19 54.22 o 3 27 0 9.78 -9.23 50.32 o 5 27 0 108.58 124.75 52.99 o 7 27 0 57.59 44.52 48.12 o 9 27 0 56.37 93.88 51.45 o 0 28 0 166.46 136.33 78.22 o 2 28 0 12.47 85.32 54.25 o 4 28 0 23.52 29.35 52.15 o 6 28 0 6.28 47.84 52.71 o 8 28 0 21.17 72.54 49.35 o 10 28 0 10.30 70.51 55.80 o 1 29 0 4.29 -8.67 82.85 o 3 29 0 36.30 76.46 54.59 o 5 29 0 55.40 73.68 54.82 o 7 29 0 17.35 108.47 54.40 o 0 30 0 26.69 -34.84 79.86 o 2 30 0 41.76 149.93 56.31 o 4 30 0 0.14 0.34 57.88 o 6 30 0 9.15 42.59 56.10 o 1 31 0 2.45 44.76 57.66 o 3 31 0 2.30 -53.75 60.03 o 5 31 0 57.54 40.82 58.51 o 0 32 0 18.62 122.72 85.77 o 2 32 0 1.94 3.47 57.59 o -19 1 1 4.25 7.69 48.96 o -17 1 1 39.29 5.51 45.21 o -15 1 1 476.92 541.71 43.19 o -13 1 1 567.10 533.29 42.91 o -11 1 1 579.38 514.22 44.76 o -9 1 1 102.72 77.41 43.51 o -7 1 1 55.32 70.21 44.49 o -5 1 1 10731.66 9548.89 421.22 o -3 1 1 124792.38 135440.08 5510.39 o -1 1 1 3079.87 3247.99 90.85 o 1 1 1 2112.47 2842.37 169.43 o 3 1 1 20.23 108.48 74.27 o 5 1 1 51459.87 48513.62 1166.91 o 7 1 1 64.71 72.02 49.17 o 9 1 1 120.86 126.07 46.71 o 11 1 1 1285.48 1368.78 48.15 o 13 1 1 750.61 626.98 50.09 o 15 1 1 1112.86 1111.36 50.41 o 17 1 1 197.11 153.70 51.37 o 19 1 1 27.35 60.06 60.89 o -18 2 1 123.23 119.67 46.50 o -16 2 1 5.63 -16.01 43.27 o -14 2 1 73.59 87.73 43.85 o -12 2 1 735.79 793.91 42.73 o -10 2 1 2548.80 2410.63 67.33 o -8 2 1 605.38 847.28 48.50 o -6 2 1 492.73 357.64 47.14 o -4 2 1 6754.92 5925.24 201.52 o -2 2 1 12202.48 12555.92 342.48 o 0 2 1 62.92 70.87 81.37 o 2 2 1 24518.88 24310.55 163.36 o 4 2 1 72431.48 67740.09 6446.44 o 6 2 1 143.37 147.68 53.89 o 8 2 1 4673.33 4212.51 108.06 o 10 2 1 1564.59 1460.66 48.76 o 12 2 1 1252.34 1202.43 48.74 o 14 2 1 8.33 8.35 46.33 o 16 2 1 108.29 125.17 50.28 o 18 2 1 20.64 68.70 57.16 o -19 3 1 2.65 -4.16 50.01 o -17 3 1 49.09 91.39 45.64 o -15 3 1 209.92 160.80 42.41 o -13 3 1 254.20 270.83 43.62 o -11 3 1 8.05 18.17 42.71 o -9 3 1 919.15 953.98 48.86 o -7 3 1 10406.17 8976.77 356.30 o -5 3 1 3608.49 3508.84 125.06 o -3 3 1 12083.12 9213.33 646.30 o -1 3 1 2217.28 1808.86 74.78 o 1 3 1 3419.44 3155.20 105.09 o 3 3 1 89002.87 90876.55 1414.58 o 5 3 1 12.76 30.79 58.00 o 7 3 1 7963.72 8179.93 250.93 o 9 3 1 392.84 361.81 46.82 o 11 3 1 281.94 274.39 46.55 o 13 3 1 423.28 433.26 47.32 o 15 3 1 740.99 658.29 49.39 o 17 3 1 5.27 109.55 52.84 o 19 3 1 14.36 -2.40 57.98 o -18 4 1 67.57 55.30 46.87 o -16 4 1 40.19 20.82 43.72 o -14 4 1 76.97 133.29 44.08 o -12 4 1 57.06 121.44 61.75 o -10 4 1 767.14 838.00 46.05 o -8 4 1 903.12 1020.09 44.51 o -6 4 1 1.78 0.33 51.51 o -4 4 1 1837.17 2086.88 68.49 o -2 4 1 7978.87 7254.32 197.83 o 0 4 1 158.62 251.57 71.62 o 2 4 1 2456.80 2172.96 75.92 o 4 4 1 20761.37 19960.30 364.71 o 6 4 1 91.03 95.78 48.68 o 8 4 1 13087.61 12841.62 372.00 o 10 4 1 15.76 56.97 48.06 o 12 4 1 211.43 166.84 46.28 o 14 4 1 38.10 86.52 46.53 o 16 4 1 5.02 44.31 49.11 o 18 4 1 1.21 -4.31 55.60 o -19 5 1 7.56 55.97 50.06 o -17 5 1 205.03 265.81 47.14 o -15 5 1 233.08 284.80 43.84 o -13 5 1 162.30 213.99 46.39 o -11 5 1 6.12 56.52 43.28 o -9 5 1 241.36 165.03 40.99 o -7 5 1 239.77 142.15 48.10 o -5 5 1 3361.03 3554.14 105.58 o -3 5 1 11.62 64.83 59.87 o -1 5 1 4367.27 4324.90 98.25 o 1 5 1 33.77 125.44 82.27 o 3 5 1 16279.21 15537.02 249.70 o 5 5 1 76.16 128.13 53.57 o 7 5 1 2506.20 2567.89 75.93 o 9 5 1 496.58 405.79 47.95 o 11 5 1 51.38 70.24 45.20 o 13 5 1 37.78 102.05 46.63 o 15 5 1 60.33 105.99 46.69 o 17 5 1 13.32 80.77 50.83 o 19 5 1 7.45 36.15 55.89 o -18 6 1 1.52 52.40 47.64 o -16 6 1 79.01 87.87 43.86 o -14 6 1 100.68 124.09 44.33 o -12 6 1 55.47 54.88 41.12 o -10 6 1 87.52 78.41 43.67 o -8 6 1 231.68 192.23 45.96 o -6 6 1 627.89 551.51 45.51 o -4 6 1 96.79 170.57 54.06 o -2 6 1 514.07 563.39 61.30 o 0 6 1 2.62 60.14 69.63 o 2 6 1 2230.44 2452.37 231.91 o 4 6 1 8638.95 7802.47 144.24 o 6 6 1 185.15 285.50 45.96 o 8 6 1 8684.64 8316.36 243.97 o 10 6 1 37.81 102.82 45.83 o 12 6 1 0.00 6.50 46.19 o 14 6 1 74.39 105.80 46.04 o 16 6 1 0.55 32.36 51.46 o 18 6 1 7.16 -13.25 52.81 o -19 7 1 8.29 41.64 50.35 o -17 7 1 108.34 106.80 45.51 o -15 7 1 34.59 32.44 45.16 o -13 7 1 147.80 109.49 42.58 o -11 7 1 206.59 250.68 43.59 o -9 7 1 61.91 98.10 46.06 o -7 7 1 1503.53 1526.16 44.56 o -5 7 1 17.83 42.77 46.32 o -3 7 1 2030.37 2252.00 60.29 o -1 7 1 929.86 1035.92 64.40 o 1 7 1 202.28 221.42 79.63 o 3 7 1 1312.87 1176.74 64.14 o 5 7 1 2377.93 2296.43 51.53 o 7 7 1 62.03 162.73 44.21 o 9 7 1 764.47 727.82 46.00 o 11 7 1 41.28 80.82 51.21 o 13 7 1 28.11 25.06 44.31 o 15 7 1 2.68 28.42 45.61 o 17 7 1 2.40 -9.00 50.32 o -18 8 1 4.39 -8.66 46.02 o -16 8 1 78.01 21.87 46.66 o -14 8 1 87.05 44.07 43.39 o -12 8 1 128.46 211.28 42.24 o -10 8 1 1149.41 1191.05 49.95 o -8 8 1 1144.83 1023.20 40.64 o -6 8 1 2518.64 2196.66 63.57 o -4 8 1 5.62 47.08 47.82 o -2 8 1 53.85 49.42 55.99 o 0 8 1 133.28 99.32 68.48 o 2 8 1 914.28 941.44 63.59 o 4 8 1 7.61 24.01 51.24 o 6 8 1 547.45 600.43 45.41 o 8 8 1 25.15 70.81 44.15 o 10 8 1 465.37 477.98 44.28 o 12 8 1 0.51 48.66 45.83 o 14 8 1 74.91 98.27 46.87 o 16 8 1 1.05 -47.42 48.01 o 18 8 1 3.19 29.19 53.97 o -17 9 1 19.55 79.47 47.92 o -15 9 1 161.94 135.89 43.23 o -13 9 1 5.77 99.17 42.38 o -11 9 1 713.23 742.77 45.37 o -9 9 1 470.24 471.78 41.07 o -7 9 1 530.45 431.82 41.18 o -5 9 1 3589.74 3160.13 86.01 o -3 9 1 795.11 785.06 50.73 o -1 9 1 1.99 31.63 57.85 o 1 9 1 26.34 137.26 64.29 o 3 9 1 9221.13 8926.06 136.66 o 5 9 1 7.32 21.44 45.34 o 7 9 1 621.14 618.94 44.39 o 9 9 1 30.76 53.20 43.56 o 11 9 1 530.91 538.55 43.67 o 13 9 1 82.90 50.15 46.27 o 15 9 1 100.32 115.43 45.63 o 17 9 1 89.52 138.47 52.01 o -18 10 1 63.59 109.37 48.20 o -16 10 1 45.57 7.71 43.09 o -14 10 1 0.00 17.74 40.20 o -12 10 1 536.26 487.45 44.00 o -10 10 1 0.05 -4.69 42.85 o -8 10 1 373.18 440.62 41.83 o -6 10 1 1840.19 1839.77 73.82 o -4 10 1 219.50 137.75 44.07 o -2 10 1 794.36 823.69 50.84 o 0 10 1 3569.62 3507.80 72.09 o 2 10 1 327.16 325.46 54.49 o 4 10 1 4913.11 4618.59 84.59 o 6 10 1 1640.80 1659.02 46.96 o 8 10 1 88.56 108.41 42.73 o 10 10 1 293.14 347.56 44.05 o 12 10 1 44.46 35.84 42.35 o 14 10 1 136.56 92.04 48.17 o 16 10 1 17.41 51.30 50.66 o 18 10 1 41.72 121.05 54.77 o -17 11 1 0.38 38.03 49.03 o -15 11 1 140.48 170.18 42.53 o -13 11 1 152.61 195.17 41.24 o -11 11 1 489.33 504.94 41.72 o -9 11 1 619.42 670.50 41.71 o -7 11 1 3083.81 3152.44 88.94 o -5 11 1 1141.45 1303.15 45.68 o -3 11 1 6265.69 5834.29 122.82 o -1 11 1 4583.05 4536.11 92.30 o 1 11 1 751.56 996.95 57.33 o 3 11 1 469.25 331.11 52.54 o 5 11 1 2520.73 2309.48 69.67 o 7 11 1 2570.95 2735.05 77.78 o 9 11 1 19.99 -22.28 43.33 o 11 11 1 291.38 275.79 42.64 o 13 11 1 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