#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/47/2214724.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214724_Fobs loop_ _publ_author_name 'Ali, Basem Fares' 'Al-Far, Rawhi' 'Ng, Seik Weng' _publ_section_title ; 2,3-Dimethylquinoxalinediium hexabromidostannate(IV) trihydrate ; _journal_coeditor_code HK2278 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2102 _journal_page_last m2103 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.599 _cell_angle_gamma 90.000 _cell_length_a 9.8979 _cell_length_b 13.6201 _cell_length_c 16.0983 _exptl_crystal_F_000 1504.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file hk2278Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 513.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1450.23 1728.42 82.00 o 2 0 0 21351.92 20335.83 349.04 o 3 0 0 2161.22 1757.07 80.52 o 4 0 0 56297.65 53068.90 682.43 o 5 0 0 45910.30 46414.47 967.82 o 7 0 0 3904.32 3766.61 473.63 o 8 0 0 9258.90 8778.46 484.56 o 9 0 0 756.84 579.70 144.70 o 10 0 0 587.84 633.10 121.19 o 11 0 0 1813.35 1982.38 313.75 o 12 0 0 0.18 60.24 59.53 o 2 1 0 1415.07 1546.55 48.20 o 3 1 0 40.26 108.32 24.43 o 4 1 0 11686.59 11516.32 138.27 o 5 1 0 61415.28 60617.52 749.77 o 6 1 0 4446.74 4639.34 102.63 o 7 1 0 624.48 599.17 58.64 o 8 1 0 6497.78 6521.83 195.68 o 9 1 0 193.68 148.59 47.95 o 10 1 0 2588.18 2977.82 228.59 o 11 1 0 103.70 118.76 73.42 o 12 1 0 10.18 129.73 89.16 o 1 2 0 1634.81 2025.38 50.54 o 2 2 0 69516.95 66798.59 2989.01 o 3 2 0 7680.95 7687.67 120.70 o 4 2 0 20260.12 20542.05 264.50 o 5 2 0 3543.43 3524.32 78.70 o 6 2 0 785.34 779.94 43.36 o 7 2 0 409.79 546.86 52.90 o 8 2 0 222.77 185.64 39.95 o 9 2 0 485.98 508.80 80.27 o 10 2 0 10.32 72.46 51.89 o 11 2 0 437.23 553.87 121.83 o 12 2 0 3.32 117.80 126.42 o 1 3 0 34979.98 34759.47 369.89 o 2 3 0 6312.71 7444.28 133.32 o 4 3 0 707.85 866.31 34.93 o 5 3 0 6380.58 5975.35 104.62 o 6 3 0 72.43 138.23 24.61 o 7 3 0 8543.41 7775.74 192.46 o 8 3 0 7888.48 8009.13 219.66 o 9 3 0 137.38 152.11 36.61 o 10 3 0 282.58 219.10 59.94 o 11 3 0 27.08 64.70 113.13 o 0 4 0 50326.37 54905.58 696.10 o 1 4 0 584.58 627.38 25.59 o 3 4 0 13315.11 13895.95 167.44 o 4 4 0 4440.34 4331.65 83.55 o 5 4 0 8442.79 7918.09 142.30 o 6 4 0 34.37 93.00 21.24 o 7 4 0 14682.96 15267.97 323.88 o 8 4 0 7856.84 7620.74 210.22 o 9 4 0 1043.58 1091.14 106.88 o 10 4 0 191.27 226.54 66.77 o 11 4 0 105.21 138.37 186.29 o 1 5 0 1414.76 1735.59 45.72 o 2 5 0 4091.91 4232.29 86.14 o 3 5 0 60905.63 61325.53 961.85 o 4 5 0 11.31 85.81 15.69 o 5 5 0 124.42 180.71 33.74 o 6 5 0 16.00 107.44 20.61 o 7 5 0 11009.89 10981.23 249.60 o 8 5 0 12054.46 12851.63 447.42 o 9 5 0 128.44 160.50 40.70 o 10 5 0 59.28 162.84 70.10 o 11 5 0 6.17 122.31 82.68 o 0 6 0 644.73 777.35 46.45 o 1 6 0 15.82 52.27 13.06 o 2 6 0 657.02 687.16 26.09 o 3 6 0 10.79 82.85 23.24 o 4 6 0 2326.12 1853.35 76.40 o 5 6 0 1025.54 1429.20 49.25 o 6 6 0 7948.31 7949.49 225.80 o 7 6 0 6670.33 6710.99 168.70 o 8 6 0 638.40 571.88 58.23 o 9 6 0 2305.46 2295.93 173.27 o 10 6 0 1149.41 1189.78 145.01 o 11 6 0 1196.37 1011.05 156.63 o 1 7 0 11550.99 12380.33 145.50 o 2 7 0 1077.51 1110.44 37.33 o 3 7 0 6468.86 6666.75 129.39 o 4 7 0 58.27 143.21 41.57 o 5 7 0 38143.70 41083.31 925.98 o 6 7 0 5261.47 5344.22 133.18 o 7 7 0 78.86 94.71 28.58 o 8 7 0 268.63 198.03 55.14 o 9 7 0 493.98 460.93 85.99 o 10 7 0 5246.73 5276.37 247.61 o 11 7 0 7.82 132.67 63.88 o 0 8 0 38238.21 41219.45 587.86 o 1 8 0 551.84 594.21 33.56 o 2 8 0 18867.14 19228.79 235.33 o 3 8 0 4400.70 4052.54 116.27 o 4 8 0 7781.48 8029.67 224.82 o 5 8 0 12076.83 12311.49 353.69 o 6 8 0 7522.79 7631.21 212.74 o 7 8 0 159.17 176.87 56.02 o 8 8 0 178.20 220.25 77.30 o 9 8 0 3173.26 2934.82 213.78 o 10 8 0 747.72 712.79 102.32 o 1 9 0 294.03 246.80 28.19 o 2 9 0 461.17 392.59 30.99 o 3 9 0 1151.72 1008.31 68.56 o 4 9 0 1071.12 1089.64 80.87 o 5 9 0 8996.45 9278.14 307.36 o 6 9 0 4741.26 4647.05 202.67 o 7 9 0 481.00 476.56 79.73 o 8 9 0 240.74 221.98 74.57 o 9 9 0 1110.99 1142.16 151.30 o 10 9 0 4031.93 4483.08 250.20 o 0 10 0 611.93 638.97 66.36 o 1 10 0 0.16 63.01 20.52 o 2 10 0 583.08 660.24 55.19 o 3 10 0 49.34 93.13 32.89 o 4 10 0 1008.28 1061.48 82.78 o 5 10 0 1801.39 1510.17 196.91 o 6 10 0 167.95 234.87 61.78 o 7 10 0 696.08 544.88 84.07 o 8 10 0 1932.61 1936.06 184.83 o 9 10 0 1873.72 1776.91 174.89 o 10 10 0 31.40 174.23 91.56 o 1 11 0 534.44 486.12 51.46 o 2 11 0 446.83 488.44 58.36 o 3 11 0 6042.38 6244.45 202.38 o 4 11 0 1679.20 1765.05 113.07 o 5 11 0 1284.60 1444.45 122.77 o 6 11 0 225.13 176.54 42.84 o 7 11 0 2021.98 2033.59 185.92 o 8 11 0 2541.42 2402.99 199.17 o 9 11 0 18.85 174.86 65.06 o 0 12 0 5069.52 5152.03 211.23 o 1 12 0 240.86 216.21 47.30 o 2 12 0 5246.92 5191.29 178.69 o 3 12 0 2059.01 1946.73 115.38 o 4 12 0 47.63 156.74 54.19 o 5 12 0 391.56 305.87 61.76 o 6 12 0 121.81 179.94 58.49 o 7 12 0 1197.49 982.97 187.63 o 8 12 0 195.68 206.44 69.77 o 9 12 0 347.14 188.59 70.47 o 1 13 0 248.20 211.56 45.13 o 2 13 0 915.87 869.17 79.78 o 3 13 0 869.06 687.07 95.63 o 4 13 0 1021.37 1087.80 115.81 o 5 13 0 6.86 96.40 46.67 o 6 13 0 223.71 181.07 54.50 o 7 13 0 224.02 203.99 57.00 o 8 13 0 1229.66 1043.43 165.41 o 0 14 0 1204.31 1000.88 140.44 o 1 14 0 50.89 118.56 33.91 o 2 14 0 69.52 168.05 44.52 o 3 14 0 381.86 465.57 76.55 o 4 14 0 38.92 122.02 55.46 o 5 14 0 29.58 74.73 41.67 o 6 14 0 113.86 114.21 85.68 o 7 14 0 326.27 268.33 74.42 o 1 15 0 557.59 299.49 67.22 o 2 15 0 186.76 247.95 57.46 o 3 15 0 118.64 148.46 45.14 o 4 15 0 27.96 115.15 45.99 o 5 15 0 472.96 265.30 58.13 o 6 15 0 339.93 166.41 56.24 o 0 16 0 1286.52 443.29 177.03 o 1 16 0 226.20 317.93 85.45 o 2 16 0 62.69 136.17 41.24 o 3 16 0 24.35 102.21 53.56 o 4 16 0 170.63 198.93 71.58 o 5 16 0 376.61 256.75 107.69 o 1 17 0 185.76 115.02 50.95 o 2 17 0 3.56 209.41 66.74 o 3 17 0 36.14 258.72 90.24 o -12 1 1 1.09 99.76 70.80 o -11 1 1 1996.58 2182.46 220.05 o -10 1 1 2271.10 2356.70 253.45 o -9 1 1 6.74 60.60 28.58 o -8 1 1 5280.08 5467.70 179.27 o -7 1 1 16.86 42.03 20.54 o -6 1 1 5865.96 6504.40 126.38 o -5 1 1 2.67 59.09 19.01 o -4 1 1 5461.59 4691.85 100.24 o -3 1 1 651.43 598.23 32.19 o -2 1 1 3160.73 2440.59 93.24 o -1 1 1 37.35 114.66 23.10 o 2 1 1 53.94 136.85 30.83 o 3 1 1 1630.56 1347.20 43.95 o 4 1 1 420.28 409.82 29.90 o 5 1 1 63.30 94.21 23.33 o 6 1 1 144.63 129.99 29.32 o 7 1 1 5793.25 5771.91 182.11 o 8 1 1 80.21 104.15 33.82 o 9 1 1 0.02 164.34 66.94 o 10 1 1 50.98 99.68 55.98 o 11 1 1 50.10 110.02 58.71 o -12 2 1 109.51 125.23 88.14 o -11 2 1 3144.77 3167.34 242.24 o -10 2 1 2364.72 2580.22 173.14 o -9 2 1 43.81 86.96 42.17 o -8 2 1 530.45 594.07 51.19 o -7 2 1 1434.70 1466.99 59.10 o -6 2 1 252.59 236.11 30.37 o -5 2 1 10230.78 9575.22 228.52 o -4 2 1 513.70 666.69 32.38 o -3 2 1 94209.38 90140.48 7619.30 o -2 2 1 7891.95 8081.95 101.26 o -1 2 1 1336.77 1446.30 34.81 o 0 2 1 4859.01 4498.35 95.98 o 1 2 1 257.64 464.66 32.72 o 2 2 1 1456.37 1212.12 41.78 o 3 2 1 1659.14 1411.78 59.16 o 4 2 1 28.96 96.65 48.43 o 5 2 1 1335.15 1228.40 51.19 o 6 2 1 1674.71 1590.94 72.74 o 7 2 1 1016.71 864.99 65.26 o 8 2 1 7719.09 8205.96 246.26 o 9 2 1 1.88 119.11 43.72 o 10 2 1 1286.10 1570.80 130.21 o 11 2 1 63.21 215.95 615.82 o -12 3 1 19.91 184.99 118.81 o -11 3 1 1786.25 1758.29 186.15 o -10 3 1 4468.99 4514.26 186.73 o -9 3 1 413.92 418.70 60.89 o -8 3 1 1934.87 1928.14 86.73 o -7 3 1 220.16 186.68 30.36 o -6 3 1 1739.17 1705.56 62.34 o -5 3 1 219.76 251.03 28.57 o -4 3 1 13597.88 14369.94 176.85 o -3 3 1 24966.41 23223.85 231.37 o -2 3 1 28848.88 32045.26 300.76 o -1 3 1 10028.69 9623.54 98.03 o 0 3 1 12297.64 13212.20 140.22 o 1 3 1 13481.41 11730.98 131.23 o 2 3 1 7308.27 5663.93 97.83 o 3 3 1 3682.34 3219.55 78.76 o 4 3 1 735.14 696.71 36.18 o 5 3 1 5007.46 4551.36 93.04 o 6 3 1 1639.95 1450.14 68.83 o 7 3 1 10774.63 10575.71 246.90 o 8 3 1 570.57 690.71 67.14 o 9 3 1 138.23 182.55 41.99 o 10 3 1 1.41 88.44 60.29 o 11 3 1 14.25 100.96 80.17 o -12 4 1 258.91 197.76 135.45 o -11 4 1 165.39 159.18 117.42 o -10 4 1 730.64 662.50 113.43 o -9 4 1 1965.39 2002.40 128.51 o -8 4 1 3527.87 3375.08 92.13 o -7 4 1 572.97 584.96 45.14 o -6 4 1 402.81 334.12 36.37 o -5 4 1 4596.52 4261.68 98.80 o -4 4 1 3296.60 2848.71 68.75 o -3 4 1 19506.78 19274.53 213.94 o -2 4 1 18999.84 17111.96 167.11 o -1 4 1 38750.09 36871.70 311.16 o 0 4 1 4202.26 4979.47 111.77 o 1 4 1 284.39 468.90 25.25 o 2 4 1 7881.94 7429.96 129.65 o 3 4 1 4101.70 3597.90 69.72 o 4 4 1 3256.12 2879.36 77.30 o 5 4 1 273.98 352.50 35.79 o 6 4 1 10133.45 10372.34 252.04 o 7 4 1 3488.08 3418.51 127.42 o 8 4 1 1423.15 1534.98 97.02 o 9 4 1 1.65 110.18 43.39 o 10 4 1 492.76 541.70 99.96 o 11 4 1 1.14 117.27 100.18 o -11 5 1 2.17 143.12 109.42 o -10 5 1 304.42 185.58 51.12 o -9 5 1 3415.41 3444.23 176.92 o -8 5 1 6185.78 6930.36 246.66 o -7 5 1 1640.68 1456.47 65.80 o -6 5 1 11267.72 11594.63 251.26 o -5 5 1 116.04 154.47 29.39 o -4 5 1 839.18 817.22 36.60 o -3 5 1 12321.06 11347.15 168.68 o -2 5 1 6464.77 6609.68 108.91 o -1 5 1 8896.99 9855.60 109.15 o 0 5 1 26519.60 24910.43 205.90 o 1 5 1 1671.48 1522.60 43.46 o 2 5 1 4216.71 3835.97 88.31 o 3 5 1 1628.49 1386.02 57.77 o 4 5 1 987.87 977.77 46.59 o 5 5 1 12822.80 13073.26 242.29 o 6 5 1 2795.55 2683.37 88.21 o 7 5 1 77.36 102.73 28.78 o 8 5 1 1425.96 1354.44 92.30 o 9 5 1 952.18 760.16 98.84 o 10 5 1 84.11 111.79 55.13 o 11 5 1 416.07 290.02 93.51 o -11 6 1 243.21 257.56 75.35 o -10 6 1 21.22 88.38 44.14 o -9 6 1 2569.66 2438.10 173.44 o -8 6 1 3530.29 3291.62 139.54 o -7 6 1 1738.39 1798.03 73.98 o -6 6 1 1125.46 1071.88 51.80 o -5 6 1 21454.22 22006.26 329.77 o -4 6 1 2787.09 2635.16 68.99 o -3 6 1 8.29 68.53 19.25 o -2 6 1 2464.72 2231.31 50.85 o -1 6 1 10428.43 11061.32 159.20 o 0 6 1 19260.99 18237.32 172.63 o 1 6 1 1108.69 813.39 40.52 o 2 6 1 2695.79 2794.03 68.10 o 3 6 1 2207.94 2267.32 73.15 o 4 6 1 1666.85 1543.18 95.80 o 5 6 1 5179.60 4794.39 67.80 o 6 6 1 5064.42 4943.66 166.20 o 7 6 1 338.64 362.53 50.19 o 8 6 1 529.07 475.49 59.91 o 9 6 1 207.16 231.96 69.15 o 10 6 1 3599.12 3588.15 213.38 o 11 6 1 115.08 203.27 75.59 o -11 7 1 333.67 278.37 77.77 o -10 7 1 1757.05 1564.41 157.72 o -9 7 1 762.68 816.44 115.89 o -8 7 1 1672.48 1757.36 106.25 o -7 7 1 2254.51 2092.61 61.88 o -6 7 1 1944.32 1895.51 75.40 o -5 7 1 13050.08 13378.08 281.92 o -4 7 1 1614.72 1455.52 52.72 o -3 7 1 56.54 113.96 20.60 o -2 7 1 757.05 824.51 35.95 o -1 7 1 21966.40 21899.23 244.69 o 0 7 1 936.19 1391.62 50.40 o 1 7 1 3055.71 2822.07 62.87 o 2 7 1 5609.22 5149.94 93.08 o 3 7 1 2211.75 2147.63 79.26 o 4 7 1 4567.37 4422.27 142.85 o 5 7 1 14.43 118.75 36.62 o 6 7 1 2502.87 2493.21 123.62 o 7 7 1 26.40 76.59 23.54 o 8 7 1 160.39 173.20 49.94 o 9 7 1 848.07 698.90 123.52 o 10 7 1 1472.09 1725.76 160.73 o -11 8 1 2.85 129.34 182.41 o -10 8 1 991.80 1045.26 136.01 o -9 8 1 648.79 543.35 97.04 o -8 8 1 9.81 108.64 71.65 o -7 8 1 289.37 261.96 46.03 o -6 8 1 10916.79 11492.99 388.29 o -5 8 1 344.70 356.56 61.62 o -4 8 1 2917.68 2897.45 112.86 o -3 8 1 3000.53 2973.70 68.61 o -2 8 1 112.53 274.97 48.88 o -1 8 1 2185.74 2204.26 60.67 o 0 8 1 14421.51 14089.55 174.10 o 1 8 1 765.35 813.88 42.34 o 2 8 1 2233.22 2182.78 63.56 o 3 8 1 106.28 157.34 30.35 o 4 8 1 55.93 177.97 46.13 o 5 8 1 7063.14 6725.41 231.12 o 6 8 1 252.66 174.14 51.06 o 7 8 1 221.86 256.28 57.88 o 8 8 1 1345.03 1359.21 149.57 o 9 8 1 1248.53 1406.50 159.27 o 10 8 1 22.12 130.57 66.73 o -10 9 1 5.09 164.33 62.58 o -9 9 1 146.86 91.25 51.87 o -8 9 1 2711.63 2702.60 187.21 o -7 9 1 1537.76 1740.18 108.67 o -6 9 1 2582.21 2375.47 109.81 o -5 9 1 8784.66 9273.58 272.31 o -4 9 1 718.90 655.25 65.91 o -3 9 1 368.25 334.87 34.39 o -2 9 1 35.58 69.21 19.21 o -1 9 1 2344.50 2306.11 67.36 o 0 9 1 4961.20 4855.53 101.08 o 1 9 1 866.17 888.68 51.63 o 2 9 1 856.50 872.28 49.83 o 3 9 1 529.09 566.43 64.13 o 4 9 1 2565.27 2450.93 125.86 o 5 9 1 3321.89 3316.46 178.95 o 6 9 1 387.47 416.11 70.34 o 7 9 1 610.80 524.69 88.16 o 8 9 1 369.91 329.92 91.71 o 9 9 1 0.36 150.13 67.04 o 10 9 1 1876.12 1837.73 184.86 o -10 10 1 847.10 837.52 150.06 o -9 10 1 744.63 579.84 112.09 o -8 10 1 438.71 622.87 137.21 o -7 10 1 897.40 732.57 91.00 o -6 10 1 2423.33 2673.60 138.21 o -5 10 1 3228.42 3092.99 155.15 o -4 10 1 3507.63 3717.68 140.35 o -3 10 1 121.93 123.49 25.74 o -2 10 1 3183.51 3274.22 95.26 o -1 10 1 2964.93 3086.13 92.31 o 0 10 1 94.09 107.22 27.32 o 1 10 1 381.88 388.12 43.98 o 2 10 1 751.96 786.98 74.91 o 3 10 1 1370.00 1317.75 106.87 o 4 10 1 1079.50 1050.23 98.41 o 5 10 1 15.91 166.24 65.66 o 6 10 1 278.67 279.57 76.77 o 7 10 1 1382.39 1450.19 130.50 o 8 10 1 102.99 217.11 104.53 o 9 10 1 1193.13 1015.17 150.64 o -9 11 1 878.57 754.99 135.07 o -8 11 1 1325.34 1226.55 174.71 o -7 11 1 1561.38 1846.91 184.80 o -6 11 1 362.84 264.76 65.04 o -5 11 1 285.35 283.89 57.69 o -4 11 1 2680.67 2490.06 124.90 o -3 11 1 12001.63 13846.02 280.12 o -2 11 1 1121.81 1085.40 64.41 o -1 11 1 328.44 366.29 38.04 o 0 11 1 7.41 80.86 23.49 o 1 11 1 64.32 91.98 27.43 o 2 11 1 2715.72 2665.78 114.74 o 3 11 1 1069.88 1154.77 98.81 o 4 11 1 286.52 319.48 65.16 o 5 11 1 12.50 71.80 36.66 o 6 11 1 222.15 209.11 66.25 o 7 11 1 39.93 101.73 60.36 o 8 11 1 2466.78 2766.78 216.11 o 9 11 1 457.27 320.49 91.77 o -9 12 1 19.33 50.34 56.03 o -8 12 1 2735.40 2923.09 228.54 o -7 12 1 1077.17 876.10 152.11 o -6 12 1 105.31 116.98 39.53 o -5 12 1 15.30 59.58 39.35 o -4 12 1 1977.90 2385.95 134.77 o -3 12 1 2457.76 2368.79 100.27 o -2 12 1 3090.20 3562.66 111.16 o -1 12 1 7.59 111.36 41.92 o 0 12 1 1649.71 1774.42 90.09 o 1 12 1 3095.96 3136.24 128.39 o 2 12 1 5400.60 6187.54 195.79 o 3 12 1 1844.28 1860.90 127.17 o 4 12 1 1024.67 962.03 112.30 o 5 12 1 580.61 631.67 94.81 o 6 12 1 131.68 108.55 58.58 o 7 12 1 2827.21 3368.01 239.84 o 8 12 1 736.41 621.76 143.32 o -8 13 1 76.97 138.79 74.41 o -7 13 1 729.46 671.43 117.46 o -6 13 1 336.18 252.15 69.66 o -5 13 1 101.10 97.26 34.65 o -4 13 1 2028.02 2035.06 134.67 o -3 13 1 2596.90 3144.58 154.59 o -2 13 1 1600.01 1557.11 96.38 o -1 13 1 134.90 133.73 44.00 o 0 13 1 133.90 110.51 40.90 o 1 13 1 137.22 188.05 44.29 o 2 13 1 2066.45 2637.95 145.92 o 3 13 1 1012.22 1242.20 125.46 o 4 13 1 5.73 114.16 67.46 o 5 13 1 31.94 104.60 48.88 o 6 13 1 934.12 873.16 126.93 o 7 13 1 806.70 623.21 115.64 o 8 13 1 659.01 526.06 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