#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214725.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214725_Fobs loop_ _publ_author_name 'Lu, Jilin' 'Zhang, Dashun' 'Li, Lin' 'Liu, Beiping' _publ_section_title ; Poly[tetrabromidohexakis(\m~2~-isonicotinato)bis(\m~2~-pyridinium-4-carboxylato)pentazinc(II)] ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2147 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.528 _cell_angle_gamma 90.000 _cell_length_a 14.0960 _cell_length_b 13.6139 _cell_length_c 14.7811 _exptl_crystal_F_000 1592.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file hk2280Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' c in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 477.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 56154.74 55765.48 2540.32 o 3 0 0 4658.51 4032.79 127.30 o 4 0 0 8451.91 8280.81 196.88 o 5 0 0 3.87 42.13 17.21 o 6 0 0 7201.05 7688.79 159.16 o 7 0 0 155.87 190.81 24.05 o 8 0 0 323.29 425.98 28.46 o 9 0 0 3486.72 3442.92 68.79 o 10 0 0 326.78 353.66 26.10 o 11 0 0 10343.40 10173.27 295.92 o 12 0 0 4782.99 4935.59 127.95 o 13 0 0 4472.65 4237.30 117.68 o 14 0 0 5945.53 5917.63 253.33 o 15 0 0 1416.60 1222.46 65.60 o 16 0 0 367.95 418.03 279.18 o 2 1 0 1433.57 1320.87 27.22 o 3 1 0 160.53 213.99 17.31 o 4 1 0 565.55 488.21 10.91 o 5 1 0 337.34 360.22 15.91 o 6 1 0 1439.49 1712.84 29.41 o 7 1 0 237.95 249.13 13.68 o 8 1 0 2.15 18.26 10.12 o 9 1 0 337.90 357.45 17.14 o 10 1 0 941.56 982.72 35.22 o 11 1 0 3620.17 3742.71 106.79 o 12 1 0 571.55 533.68 27.34 o 13 1 0 648.14 756.24 55.05 o 14 1 0 531.54 540.69 45.94 o 15 1 0 225.97 300.14 56.39 o 16 1 0 0.81 82.49 83.28 o 1 2 0 116.17 291.72 10.56 o 2 2 0 185590.58 172959.63 11318.00 o 3 2 0 3.07 36.07 6.19 o 4 2 0 30365.77 30037.87 626.43 o 5 2 0 2398.37 2113.09 37.79 o 6 2 0 2712.05 2479.75 36.59 o 7 2 0 593.60 457.56 30.19 o 8 2 0 2136.34 2065.03 66.86 o 9 2 0 52.55 86.92 13.37 o 10 2 0 5013.52 5042.38 114.82 o 11 2 0 8901.46 9330.14 184.99 o 12 2 0 3744.28 3730.42 103.80 o 13 2 0 1883.66 1787.11 82.85 o 14 2 0 2717.08 2328.17 182.32 o 15 2 0 1148.98 1148.35 62.60 o 16 2 0 1694.50 1738.13 104.10 o 1 3 0 46.40 88.71 5.21 o 2 3 0 396.07 437.35 18.75 o 3 3 0 1371.41 1548.66 49.36 o 4 3 0 1677.78 1672.24 27.52 o 5 3 0 5.03 45.20 7.90 o 6 3 0 6572.08 7190.58 138.27 o 7 3 0 16.14 40.80 10.86 o 8 3 0 897.83 916.68 50.62 o 9 3 0 2665.28 2437.05 81.91 o 10 3 0 3115.58 3334.62 57.66 o 11 3 0 234.62 252.62 19.77 o 12 3 0 3760.71 3505.13 130.10 o 13 3 0 4735.98 5005.27 179.62 o 14 3 0 1980.53 1933.64 80.45 o 15 3 0 2383.19 2398.31 112.50 o 16 3 0 31.80 43.48 52.46 o 0 4 0 19854.32 19583.54 450.51 o 1 4 0 17614.74 19006.99 332.46 o 2 4 0 28033.49 27486.71 581.84 o 3 4 0 2095.42 2646.34 40.30 o 4 4 0 3001.82 2572.52 44.68 o 5 4 0 32697.63 34777.47 696.43 o 6 4 0 8862.11 8711.28 215.38 o 7 4 0 20446.62 21122.45 455.23 o 8 4 0 9156.89 9021.84 171.43 o 9 4 0 108.91 154.57 30.80 o 10 4 0 2291.17 2529.97 91.60 o 11 4 0 1673.38 1659.28 85.67 o 12 4 0 6093.86 6407.08 164.04 o 13 4 0 3423.49 3375.18 133.03 o 14 4 0 1887.58 1936.00 114.94 o 15 4 0 1882.08 1885.80 125.10 o 16 4 0 1.21 -67.21 81.82 o 1 5 0 1706.92 1839.14 64.84 o 2 5 0 3.27 37.19 13.78 o 3 5 0 15427.53 15553.78 336.12 o 4 5 0 218.51 418.07 34.91 o 5 5 0 7439.85 7324.74 158.25 o 6 5 0 1496.29 1375.18 121.87 o 7 5 0 3760.11 4020.72 322.81 o 8 5 0 1832.51 1902.00 88.80 o 9 5 0 1579.02 1877.05 82.99 o 10 5 0 1237.45 1415.34 130.91 o 11 5 0 1895.11 1923.15 84.51 o 12 5 0 1495.01 1504.97 86.88 o 13 5 0 51.74 37.47 48.75 o 14 5 0 95.56 130.15 46.60 o 15 5 0 1179.48 1248.47 151.57 o 0 6 0 4034.22 3924.58 117.06 o 1 6 0 11695.75 12603.38 257.26 o 2 6 0 3233.36 2897.34 58.35 o 3 6 0 421.96 425.26 20.58 o 4 6 0 746.17 688.61 30.87 o 5 6 0 7453.39 7308.42 147.77 o 6 6 0 732.62 691.67 41.40 o 7 6 0 24997.22 26177.21 789.09 o 8 6 0 2115.56 2367.75 149.70 o 9 6 0 2563.94 2981.24 145.35 o 10 6 0 1263.39 1339.62 108.00 o 11 6 0 451.93 566.25 61.65 o 12 6 0 2209.95 2363.63 109.91 o 13 6 0 206.73 233.78 66.92 o 14 6 0 1511.08 1657.50 130.46 o 15 6 0 1684.89 1763.68 154.62 o 1 7 0 6240.03 6726.33 155.43 o 2 7 0 803.44 868.94 23.12 o 3 7 0 31044.28 32352.37 943.31 o 4 7 0 4854.29 4837.78 117.26 o 5 7 0 26718.64 27708.09 804.04 o 6 7 0 6621.81 6555.68 161.50 o 7 7 0 6163.55 5719.09 285.41 o 8 7 0 5064.11 5488.31 189.39 o 9 7 0 3298.91 3390.78 148.92 o 10 7 0 707.44 835.06 64.98 o 11 7 0 288.98 242.69 53.68 o 12 7 0 88.82 59.38 66.02 o 13 7 0 4.17 67.73 59.31 o 14 7 0 1683.89 1702.38 127.12 o 15 7 0 260.32 322.02 91.42 o 0 8 0 1826.43 2039.41 159.90 o 1 8 0 63.04 158.97 36.19 o 2 8 0 3.65 0.39 16.74 o 3 8 0 491.78 485.07 41.46 o 4 8 0 6.47 3.66 24.45 o 5 8 0 3045.07 3078.23 92.16 o 6 8 0 412.36 495.20 35.43 o 7 8 0 122.81 105.69 14.44 o 8 8 0 1886.05 1995.67 126.50 o 9 8 0 2820.27 2913.78 129.34 o 10 8 0 61.67 64.91 41.31 o 11 8 0 6.29 33.96 50.29 o 12 8 0 1337.49 1531.56 211.89 o 13 8 0 30.26 -62.80 67.41 o 14 8 0 1228.03 1300.94 124.26 o 1 9 0 4168.43 5130.85 438.35 o 2 9 0 382.89 605.38 38.44 o 3 9 0 12022.96 12726.62 346.89 o 4 9 0 1209.69 1138.20 66.16 o 5 9 0 9086.62 9651.08 228.25 o 6 9 0 888.13 964.63 47.96 o 7 9 0 5044.05 5027.96 244.43 o 8 9 0 841.20 758.70 66.80 o 9 9 0 65.23 116.04 56.13 o 10 9 0 2445.03 2559.07 162.00 o 11 9 0 98.41 26.22 64.79 o 12 9 0 19.40 14.76 56.82 o 13 9 0 202.83 166.75 74.71 o 14 9 0 284.90 266.92 98.97 o 0 10 0 8573.16 9724.24 788.24 o 1 10 0 3367.80 3636.14 127.50 o 2 10 0 1479.72 1487.11 95.48 o 3 10 0 172.41 211.24 40.37 o 4 10 0 2295.20 2588.62 129.06 o 5 10 0 1734.73 1812.61 71.85 o 6 10 0 5814.52 6175.07 187.50 o 7 10 0 772.85 721.17 76.31 o 8 10 0 3268.44 2953.61 246.33 o 9 10 0 281.09 228.84 79.70 o 10 10 0 1429.18 1612.21 160.47 o 11 10 0 144.25 172.99 85.87 o 12 10 0 167.01 211.92 82.46 o 13 10 0 957.00 1305.14 193.21 o 1 11 0 530.46 831.11 132.29 o 2 11 0 25846.72 27560.26 1182.68 o 3 11 0 155.89 193.80 35.33 o 4 11 0 744.10 870.92 69.17 o 5 11 0 117.52 143.54 32.69 o 6 11 0 64.56 131.68 22.42 o 7 11 0 68.79 79.55 15.79 o 9 11 0 55.73 -3.85 74.63 o 10 11 0 1464.91 1847.49 175.80 o 11 11 0 24.31 29.99 66.11 o 12 11 0 725.72 784.64 125.81 o 13 11 0 364.66 295.97 122.31 o 0 12 0 145.36 178.13 28.88 o 1 12 0 637.30 751.97 76.97 o 2 12 0 1913.19 2062.14 181.06 o 3 12 0 537.93 712.99 103.96 o 4 12 0 1487.85 1728.31 103.01 o 5 12 0 1140.09 1106.76 85.45 o 6 12 0 2154.62 2110.66 144.19 o 7 12 0 1704.21 1721.36 90.68 o 8 12 0 576.85 430.68 65.61 o 9 12 0 1625.09 1957.39 182.92 o 10 12 0 180.56 171.81 80.27 o 11 12 0 552.67 900.21 153.93 o 12 12 0 140.76 297.54 124.64 o 1 13 0 49.04 93.56 26.81 o 2 13 0 726.06 799.98 59.64 o 3 13 0 425.42 407.97 35.71 o 4 13 0 9678.44 9719.83 390.81 o 5 13 0 7.32 17.19 37.54 o 6 13 0 787.51 812.26 71.40 o 7 13 0 547.63 514.56 41.68 o 8 13 0 506.80 682.72 103.92 o 9 13 0 1157.19 1374.17 169.61 o 10 13 0 831.95 992.11 160.80 o 11 13 0 128.07 160.04 121.20 o 0 14 0 3854.17 3607.99 218.43 o 1 14 0 39.64 16.94 24.81 o 2 14 0 4563.60 4869.99 213.07 o 3 14 0 119.37 121.72 29.30 o 4 14 0 5023.57 5125.14 176.27 o 5 14 0 1339.40 1429.37 60.16 o 6 14 0 64.51 70.97 40.58 o 7 14 0 4937.88 4809.97 309.60 o 8 14 0 27.01 48.18 74.57 o 9 14 0 3512.96 4219.21 334.48 o 10 14 0 633.33 887.82 167.62 o 1 15 0 313.14 231.88 69.36 o 2 15 0 987.13 1032.56 90.89 o 3 15 0 2120.15 2198.21 147.91 o 4 15 0 1405.67 1480.19 84.70 o 5 15 0 388.62 380.96 43.34 o 6 15 0 197.66 163.27 33.24 o 7 15 0 2254.75 2554.50 209.91 o 8 15 0 4.57 115.75 77.12 o 0 16 0 1516.79 1601.10 135.16 o 1 16 0 35.04 18.82 38.72 o 2 16 0 1692.89 1695.41 92.44 o 3 16 0 585.70 657.60 53.58 o 4 16 0 262.14 241.94 56.31 o 5 16 0 887.83 920.99 83.05 o 6 16 0 1.35 -1.91 31.09 o 7 16 0 3528.61 4252.24 293.15 o 1 17 0 343.17 240.70 51.53 o 2 17 0 29.66 26.83 62.36 o 3 17 0 2374.41 2239.07 148.98 o 4 17 0 1.66 -24.49 29.80 o -17 1 1 68.94 179.84 143.28 o -16 1 1 1816.04 1960.30 86.91 o -15 1 1 2087.88 2096.03 59.90 o -14 1 1 3855.38 3862.21 80.76 o -13 1 1 12715.46 13109.18 250.20 o -12 1 1 4000.49 4047.81 75.75 o -11 1 1 38359.37 38387.32 1008.46 o -10 1 1 1353.15 1272.78 42.28 o -9 1 1 12229.01 12560.67 271.08 o -8 1 1 2427.68 2379.61 42.13 o -7 1 1 2592.51 3006.40 43.74 o -6 1 1 4778.19 4230.71 53.76 o -5 1 1 25276.30 26933.43 488.62 o -4 1 1 6932.97 6164.16 73.51 o -3 1 1 46612.87 49779.06 1104.98 o -2 1 1 1549.37 1210.02 16.01 o 1 1 1 24113.64 23828.86 516.48 o 2 1 1 134.68 285.47 13.26 o 3 1 1 2249.17 2721.27 35.71 o 4 1 1 5.07 66.63 8.56 o 5 1 1 5552.58 6179.37 117.05 o 6 1 1 1174.30 987.67 18.49 o 7 1 1 2962.76 3118.53 55.19 o 8 1 1 14002.42 13836.64 268.41 o 9 1 1 13957.80 14506.62 311.88 o 10 1 1 7414.43 7277.40 177.36 o 11 1 1 14135.13 14748.19 317.57 o 12 1 1 40.63 77.30 13.69 o 13 1 1 555.52 561.98 34.17 o 14 1 1 107.57 158.26 28.81 o 15 1 1 264.95 197.79 29.06 o 16 1 1 103.18 163.26 118.42 o -16 2 1 405.51 325.39 82.68 o -15 2 1 3.35 0.31 29.32 o -14 2 1 4.03 17.71 15.23 o -13 2 1 3369.27 3180.73 84.34 o -12 2 1 187.16 199.92 17.40 o -11 2 1 205.79 191.32 25.47 o -10 2 1 991.43 983.82 38.57 o -9 2 1 6895.14 7199.56 136.31 o -8 2 1 698.42 810.83 24.01 o -7 2 1 4325.69 4181.64 87.49 o -6 2 1 697.07 627.59 15.47 o -5 2 1 190.73 202.32 18.37 o -4 2 1 10064.17 9939.97 128.24 o -3 2 1 2558.33 2556.10 36.73 o -2 2 1 50719.26 52643.16 1383.53 o -1 2 1 16848.29 17877.38 264.12 o 0 2 1 11440.01 11591.90 364.58 o 1 2 1 22761.12 24450.54 519.41 o 2 2 1 20547.89 22121.52 740.75 o 3 2 1 8991.33 8938.37 147.57 o 4 2 1 1891.58 1860.55 46.00 o 5 2 1 8301.99 8431.74 121.53 o 6 2 1 2802.63 2751.36 53.01 o 7 2 1 3553.81 3067.80 58.29 o 8 2 1 5159.12 5005.29 95.71 o 9 2 1 11853.79 11734.26 295.78 o 10 2 1 2677.76 2619.18 80.78 o 11 2 1 312.87 339.89 20.48 o 12 2 1 1988.66 1803.61 73.63 o 13 2 1 332.80 297.73 25.13 o 14 2 1 134.13 115.81 40.46 o 15 2 1 8.32 81.73 61.38 o 16 2 1 693.50 509.58 202.18 o -16 3 1 1872.54 2007.83 100.65 o -15 3 1 128.31 105.04 41.02 o -14 3 1 1484.77 1329.75 59.71 o -13 3 1 3313.51 3235.81 127.18 o -12 3 1 134.75 200.95 17.78 o -11 3 1 3954.22 3898.33 90.03 o -10 3 1 1189.76 1416.44 88.20 o -9 3 1 8680.85 8466.42 144.14 o -8 3 1 2314.00 2141.01 35.89 o -7 3 1 1618.55 1441.29 47.75 o -6 3 1 50987.31 52674.86 1390.68 o -5 3 1 1605.00 2026.86 35.33 o -4 3 1 19123.87 18142.26 312.11 o -3 3 1 8397.99 9584.82 123.42 o -2 3 1 1257.07 1073.83 22.32 o -1 3 1 4178.73 4947.39 88.64 o 0 3 1 6.41 80.18 15.47 o 1 3 1 2139.79 2610.59 92.80 o 2 3 1 957.90 1161.70 21.21 o 3 3 1 3184.23 3671.67 57.00 o 4 3 1 2199.22 2343.74 43.08 o 5 3 1 2411.83 2529.63 71.64 o 6 3 1 2396.75 2318.24 66.47 o 7 3 1 4959.26 5499.70 159.19 o 8 3 1 10780.89 10688.69 228.11 o 9 3 1 6250.37 6559.98 192.99 o 10 3 1 4740.98 4921.15 177.37 o 11 3 1 137.34 225.00 31.31 o 12 3 1 5536.85 6032.11 200.66 o 13 3 1 106.60 113.44 30.09 o 14 3 1 1458.16 1703.21 102.86 o 15 3 1 1467.96 1408.89 76.11 o -16 4 1 160.93 154.50 44.49 o -15 4 1 18.21 -8.80 75.62 o -14 4 1 101.05 108.04 37.11 o -13 4 1 15.12 62.71 35.10 o -12 4 1 815.50 735.05 37.29 o -11 4 1 2777.61 2621.26 103.83 o -10 4 1 6022.77 6155.15 111.33 o -9 4 1 629.87 712.84 41.94 o -8 4 1 9455.71 8730.50 191.31 o -7 4 1 3113.01 3073.19 78.94 o -6 4 1 33838.09 35061.74 818.91 o -5 4 1 230.98 243.68 16.24 o -4 4 1 1051.39 872.11 23.39 o -3 4 1 4041.10 4483.62 83.25 o -2 4 1 19427.71 19555.49 366.01 o -1 4 1 4713.57 5016.45 110.07 o 0 4 1 5962.62 6272.87 100.91 o 1 4 1 4479.61 4760.85 98.30 o 2 4 1 16608.47 16845.38 583.98 o 3 4 1 13.19 92.63 19.26 o 4 4 1 7605.47 7734.65 130.22 o 5 4 1 22216.26 23883.74 643.09 o 6 4 1 12.95 14.25 20.24 o 7 4 1 16693.40 17193.13 426.64 o 8 4 1 373.83 426.47 34.98 o 9 4 1 4527.50 4689.34 109.25 o 10 4 1 3877.74 4297.98 130.41 o 11 4 1 2974.52 2869.01 114.20 o 12 4 1 1561.82 1454.91 72.70 o 13 4 1 53.66 92.82 37.90 o 14 4 1 177.15 138.56 69.19 o 15 4 1 21.21 -9.32 28.96 o -16 5 1 392.47 472.53 76.41 o -15 5 1 293.29 233.96 66.71 o -14 5 1 748.75 696.30 71.21 o -13 5 1 25.39 27.57 39.97 o -12 5 1 1224.53 1331.89 75.25 o -11 5 1 1429.07 1570.06 62.07 o -10 5 1 168.83 197.88 34.42 o -9 5 1 1967.22 1766.09 108.04 o -8 5 1 3529.73 3539.33 102.35 o -7 5 1 5058.02 4642.30 128.13 o -6 5 1 43082.52 43677.46 1148.10 o -5 5 1 2398.29 2283.92 73.93 o -4 5 1 128358.07 137984.36 6693.92 o -3 5 1 431.88 491.06 37.86 o -2 5 1 14847.52 14306.54 273.46 o -1 5 1 186.90 169.21 17.59 o 0 5 1 1342.29 1533.10 23.51 o 1 5 1 7.14 145.73 23.14 o 2 5 1 7079.34 7498.15 226.09 o 3 5 1 141.03 218.05 15.90 o 4 5 1 11158.04 11705.91 165.93 o 5 5 1 4352.89 4755.67 103.41 o 6 5 1 7.12 88.03 19.63 o 7 5 1 5369.57 5799.15 145.51 o 8 5 1 5153.39 5273.40 134.49 o 9 5 1 1769.73 1839.81 74.25 o 10 5 1 13215.62 14014.27 429.97 o 11 5 1 53.18 57.14 33.11 o 12 5 1 7769.69 8283.58 243.85 o 13 5 1 3638.98 3762.69 130.69 o 14 5 1 296.55 251.87 58.05 o 15 5 1 2984.60 3317.14 186.38 o -16 6 1 54.17 122.97 55.96 o -15 6 1 574.28 824.14 135.79 o -14 6 1 10.65 50.20 45.09 o -13 6 1 53.42 107.45 57.21 o -12 6 1 1550.67 1784.63 104.00 o -11 6 1 16.01 48.91 36.14 o -10 6 1 11499.08 12149.67 408.58 o -9 6 1 19.74 16.63 16.56 o -8 6 1 16436.55 16302.04 473.80 o -7 6 1 169.55 160.90 12.99 o -6 6 1 49470.23 50330.82 1406.69 o -5 6 1 119.86 136.42 16.90 o -4 6 1 36823.66 39192.75 964.84 o -3 6 1 0.70 816.10 47.73 o -2 6 1 140.11 121.77 10.36 o -1 6 1 482.56 475.93 16.72 o 0 6 1 18467.45 20695.36 440.66 o 1 6 1 2048.89 1752.12 128.07 o 2 6 1 845.58 694.51 40.61 o 3 6 1 4410.88 4561.27 171.00 o 4 6 1 8433.69 8323.36 216.18 o 5 6 1 7441.73 7456.20 129.40 o 6 6 1 6121.74 6342.44 200.93 o 7 6 1 4148.30 4344.73 146.87 o 8 6 1 2519.84 2663.95 94.02 o 9 6 1 1146.52 1155.53 101.48 o 10 6 1 286.27 253.64 78.94 o 11 6 1 176.54 114.47 48.34 o 12 6 1 1185.72 1234.46 89.57 o 13 6 1 492.95 424.10 71.29 o 14 6 1 2090.81 2127.30 131.61 o 15 6 1 2196.23 2258.69 165.70 o -15 7 1 241.03 266.86 68.62 o -14 7 1 25.22 9.99 52.36 o -13 7 1 376.24 410.13 61.44 o -12 7 1 213.68 239.84 65.75 o -11 7 1 615.44 754.29 73.70 o -10 7 1 883.10 846.18 75.70 o -9 7 1 1491.39 1494.49 87.00 o -7 7 1 2049.13 1789.06 79.73 o -6 7 1 12924.63 13476.78 321.33 o -5 7 1 41.57 5.23 22.96 o -4 7 1 17813.46 18169.94 351.71 o -3 7 1 202.78 194.91 10.99 o -2 7 1 2451.54 1994.38 35.18 o -1 7 1 319.46 279.13 22.48 o 0 7 1 1044.11 1046.03 50.37 o 1 7 1 3314.41 3023.49 71.18 o 2 7 1 109.49 344.32 132.39 o 3 7 1 8835.73 8691.87 289.85 o 4 7 1 2.70 56.83 21.96 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