#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214751.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214751_Fobs loop_ _publ_author_name 'Gowda, B. Thimme' 'Babitha, K. S.' 'Svoboda, Ingrid' 'Fuess, Hartmut' _publ_section_title ; Potassium 4-chlorobenzenesulfonate ; _journal_coeditor_code IM2021 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2222 _journal_volume 63 _journal_year 2007 _space_group_IT_number 11 _symmetry_space_group_name_Hall '-P 2yb' _symmetry_space_group_name_H-M 'P 1 21/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.236 _cell_angle_gamma 90.000 _cell_length_a 6.1688 _cell_length_b 6.8130 _cell_length_c 9.8040 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high 0.8009 _[local]_cod_data_source_file im2021Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TG1 NEW: P21/M' _shelx_refln_list_code 4 _shelx_f_calc_maximum 118.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 99.02 111.61 1.52 o 2 0 0 3495.04 3597.65 12.15 o 3 0 0 557.59 606.30 3.50 o 4 0 0 922.96 925.09 7.29 o 5 0 0 193.90 199.07 2.58 o 6 0 0 2.41 3.15 1.18 o 7 0 0 7.00 7.86 1.75 o 1 1 0 4022.77 3984.49 38.60 o 2 1 0 357.22 363.49 3.91 o 3 1 0 153.93 148.81 1.14 o 4 1 0 1202.00 1169.72 5.15 o 5 1 0 128.18 132.62 1.08 o 6 1 0 739.40 727.86 6.35 o 7 1 0 18.16 17.94 1.36 o 0 2 0 13926.61 13252.02 359.00 o 1 2 0 610.29 692.69 5.90 o 2 2 0 1422.34 1385.55 16.78 o 3 2 0 1.03 0.54 0.19 o 4 2 0 960.43 932.00 5.05 o 5 2 0 260.24 279.69 2.84 o 6 2 0 21.96 21.47 0.93 o 7 2 0 5.14 9.61 1.74 o 1 3 0 116.33 110.12 1.04 o 2 3 0 1207.49 1250.47 5.13 o 3 3 0 121.91 121.88 1.78 o 4 3 0 1253.82 1221.62 6.55 o 5 3 0 155.12 161.38 1.76 o 6 3 0 471.41 461.41 3.83 o 7 3 0 23.38 21.65 1.80 o 0 4 0 2995.41 3248.89 16.52 o 1 4 0 147.32 185.36 3.43 o 2 4 0 1126.42 1104.81 7.35 o 3 4 0 2.69 3.95 0.76 o 4 4 0 507.11 509.02 5.79 o 5 4 0 56.07 68.26 1.33 o 6 4 0 1.55 3.80 2.01 o 1 5 0 264.28 265.60 2.78 o 2 5 0 177.49 193.22 1.76 o 3 5 0 155.41 158.70 2.47 o 4 5 0 267.31 258.61 2.19 o 5 5 0 12.50 9.75 1.67 o 6 5 0 158.48 160.52 2.32 o 0 6 0 1043.10 1107.96 9.64 o 1 6 0 2.91 3.81 1.31 o 2 6 0 714.75 698.10 9.23 o 3 6 0 2.43 3.67 1.97 o 4 6 0 154.31 148.94 2.30 o 5 6 0 0.14 3.76 2.01 o 1 7 0 22.37 21.81 1.75 o 2 7 0 102.65 104.25 4.46 o 3 7 0 67.63 64.24 2.38 o 4 7 0 127.41 124.11 3.11 o 0 8 0 95.54 98.28 3.47 o 1 8 0 4.61 0.04 1.84 o 2 8 0 167.67 174.52 4.42 o -7 0 1 0.09 1.07 1.48 o -6 0 1 13.76 11.36 1.26 o -5 0 1 51.28 53.17 0.83 o -4 0 1 187.65 193.95 1.03 o -3 0 1 383.23 431.93 3.36 o -2 0 1 1858.17 1828.41 14.22 o -1 0 1 780.40 833.91 11.15 o 1 0 1 32.68 34.47 0.69 o 2 0 1 4173.88 4251.90 33.45 o 3 0 1 129.11 120.03 2.94 o 4 0 1 90.59 92.90 1.84 o 5 0 1 601.23 609.05 4.91 o 6 0 1 30.39 34.88 1.12 o 7 0 1 31.01 26.73 2.44 o -7 1 1 31.16 35.32 1.73 o -6 1 1 149.50 148.54 1.37 o -5 1 1 0.57 0.74 0.42 o -4 1 1 286.24 266.22 1.61 o -3 1 1 0.55 0.40 0.10 o -2 1 1 461.47 465.97 3.72 o -1 1 1 345.68 348.74 3.03 o 0 1 1 329.20 357.19 4.09 o 1 1 1 847.30 930.32 8.92 o 2 1 1 287.82 262.24 1.77 o 3 1 1 100.44 118.54 1.49 o 4 1 1 270.73 276.30 1.50 o 5 1 1 86.65 100.60 0.86 o 6 1 1 0.08 1.15 0.71 o 7 1 1 3.03 2.91 1.73 o -7 2 1 8.94 7.72 1.61 o -6 2 1 2.40 1.04 0.57 o -5 2 1 55.64 55.81 0.70 o -4 2 1 552.54 553.57 3.85 o -3 2 1 20.83 22.50 0.41 o -2 2 1 1674.85 1624.32 7.72 o -1 2 1 80.58 99.60 1.74 o 0 2 1 167.23 141.54 2.33 o 1 2 1 172.15 225.77 2.90 o 2 2 1 451.37 409.00 2.83 o 3 2 1 6.13 5.97 0.29 o 4 2 1 0.24 0.34 0.32 o 5 2 1 174.83 199.32 1.56 o 6 2 1 12.20 12.28 1.07 o 7 2 1 13.39 14.47 2.21 o -7 3 1 39.18 46.63 1.70 o -6 3 1 81.46 75.14 1.31 o -5 3 1 63.14 66.01 1.32 o -4 3 1 260.89 261.94 2.47 o -3 3 1 61.47 66.17 1.02 o -2 3 1 771.95 749.49 7.89 o -1 3 1 152.21 141.73 1.36 o 0 3 1 44.19 56.04 0.67 o 1 3 1 1368.38 1475.77 17.79 o 2 3 1 104.32 87.86 1.11 o 3 3 1 125.47 135.64 2.09 o 4 3 1 444.15 455.45 3.85 o 5 3 1 63.95 75.16 1.73 o 6 3 1 34.45 35.96 1.26 o 7 3 1 8.65 8.14 1.83 o -6 4 1 9.59 10.36 2.28 o -5 4 1 21.83 18.10 1.29 o -4 4 1 199.16 190.49 2.26 o -3 4 1 59.26 58.40 1.52 o -2 4 1 442.07 464.55 3.26 o -1 4 1 16.21 25.26 0.83 o 0 4 1 486.87 477.48 4.65 o 1 4 1 18.55 31.77 0.53 o 2 4 1 129.03 113.98 1.51 o 3 4 1 12.95 13.46 0.88 o 4 4 1 1.69 0.63 0.93 o 5 4 1 59.74 68.27 1.97 o 6 4 1 4.64 2.01 1.68 o -6 5 1 89.06 91.35 2.13 o -5 5 1 7.59 8.68 1.63 o -4 5 1 77.05 77.38 1.62 o -3 5 1 32.72 33.66 1.40 o -2 5 1 0.50 2.84 0.66 o -1 5 1 10.00 8.22 0.81 o 0 5 1 151.46 160.49 2.46 o 1 5 1 29.78 33.75 1.05 o 2 5 1 52.34 42.99 0.80 o 3 5 1 19.73 26.79 1.57 o 4 5 1 87.96 90.99 1.44 o 5 5 1 15.74 19.38 1.66 o 6 5 1 14.60 13.30 2.77 o -5 6 1 3.34 -0.78 1.99 o -4 6 1 21.25 20.31 2.14 o -3 6 1 116.97 114.29 1.49 o -2 6 1 73.13 100.38 3.21 o -1 6 1 159.44 166.67 1.62 o 0 6 1 435.00 449.43 5.10 o 1 6 1 9.21 7.81 1.21 o 2 6 1 94.90 92.44 1.75 o 3 6 1 35.08 34.74 1.38 o 4 6 1 0.09 1.60 0.94 o 5 6 1 27.92 34.09 2.75 o -4 7 1 24.69 22.73 3.11 o -3 7 1 14.12 20.51 3.01 o -2 7 1 0.09 0.28 1.51 o -1 7 1 1.91 -0.54 1.55 o 0 7 1 31.68 31.53 1.79 o 1 7 1 25.86 24.33 1.82 o 2 7 1 23.21 19.50 2.10 o 3 7 1 65.64 62.91 2.60 o 4 7 1 46.09 44.55 2.29 o -2 8 1 37.02 39.91 3.16 o -1 8 1 5.10 6.30 3.10 o 0 8 1 78.62 77.75 2.41 o 1 8 1 0.40 2.68 2.11 o 2 8 1 1.88 -2.72 2.72 o -7 0 2 95.81 104.62 3.53 o -6 0 2 1.24 0.94 1.27 o -5 0 2 138.98 151.42 2.27 o -4 0 2 229.61 272.99 3.99 o -3 0 2 275.49 263.75 2.76 o -2 0 2 826.34 877.97 8.95 o -1 0 2 800.97 844.20 8.89 o 0 0 2 11.24 12.14 0.23 o 1 0 2 181.60 163.38 2.83 o 2 0 2 20.22 23.83 0.34 o 3 0 2 880.30 896.14 6.49 o 4 0 2 0.11 0.00 0.25 o 5 0 2 574.19 564.37 4.70 o 6 0 2 0.52 0.03 0.95 o 7 0 2 234.86 239.71 8.36 o -7 1 2 0.32 -0.34 1.25 o -6 1 2 101.28 89.67 0.89 o -5 1 2 5.34 12.97 0.63 o -4 1 2 17.24 14.17 0.39 o -3 1 2 3108.77 3241.99 9.54 o -2 1 2 345.72 385.43 2.90 o -1 1 2 2505.87 2459.41 10.51 o 0 1 2 240.25 281.72 2.44 o 1 1 2 3844.37 3680.76 12.35 o 2 1 2 156.83 167.05 1.39 o 3 1 2 533.32 539.81 3.30 o 4 1 2 0.12 -0.19 0.23 o 5 1 2 7.28 17.12 0.66 o 6 1 2 2.40 2.64 1.00 o 7 1 2 11.76 16.72 1.77 o -7 2 2 119.73 125.79 1.86 o -6 2 2 3.91 5.02 0.92 o -5 2 2 351.48 374.63 1.76 o -4 2 2 9.36 11.44 0.53 o -3 2 2 384.17 369.79 3.86 o -2 2 2 29.26 24.27 0.84 o -1 2 2 0.05 4.05 0.52 o 0 2 2 45.47 58.82 0.83 o 1 2 2 1675.51 1649.53 10.39 o 2 2 2 63.96 62.53 0.74 o 3 2 2 1108.77 1158.87 7.68 o 4 2 2 107.93 99.81 0.76 o 5 2 2 391.67 395.62 2.98 o 6 2 2 7.36 7.59 1.16 o 7 2 2 134.45 131.33 2.32 o -7 3 2 0.08 2.11 1.52 o -6 3 2 12.52 8.72 1.22 o -5 3 2 1.86 10.96 0.99 o -4 3 2 12.56 15.48 0.74 o -3 3 2 530.93 541.61 5.86 o -2 3 2 267.00 284.82 2.86 o -1 3 2 421.56 437.53 3.56 o 0 3 2 206.21 225.68 3.09 o 1 3 2 2218.54 2072.21 21.25 o 2 3 2 337.03 341.44 3.26 o 3 3 2 757.24 754.21 3.83 o 4 3 2 0.23 1.24 0.51 o 5 3 2 61.18 68.81 1.52 o 6 3 2 0.11 -0.94 1.00 o -6 4 2 6.24 7.82 1.69 o -5 4 2 237.68 231.70 1.96 o -4 4 2 3.36 1.68 0.85 o -3 4 2 204.57 199.46 1.99 o -2 4 2 12.10 6.87 0.56 o -1 4 2 4.20 6.43 0.46 o 0 4 2 8.41 8.28 0.53 o 1 4 2 338.41 312.60 2.99 o 2 4 2 9.85 9.93 0.61 o 3 4 2 357.72 376.22 3.74 o 4 4 2 25.68 19.53 0.96 o 5 4 2 273.37 290.10 6.06 o 6 4 2 7.45 4.42 1.88 o -6 5 2 14.24 15.22 2.49 o -5 5 2 15.80 12.03 1.76 o -4 5 2 3.20 3.88 1.35 o -3 5 2 383.94 368.75 1.99 o -2 5 2 27.38 27.39 0.84 o -1 5 2 752.71 777.99 6.77 o 0 5 2 34.63 27.95 0.90 o 1 5 2 782.11 766.82 5.63 o 2 5 2 11.30 12.90 0.87 o 3 5 2 74.75 84.91 2.97 o 4 5 2 0.32 0.56 1.02 o 5 5 2 5.79 6.73 1.78 o -5 6 2 85.61 79.25 3.68 o -4 6 2 6.50 3.98 2.08 o -3 6 2 65.76 71.93 1.86 o -2 6 2 7.63 9.76 1.45 o -1 6 2 48.04 40.84 1.48 o 0 6 2 44.20 42.99 1.31 o 1 6 2 1.78 1.28 1.03 o 2 6 2 8.10 7.43 1.41 o 3 6 2 65.08 69.84 1.43 o 4 6 2 0.39 -0.55 1.02 o 5 6 2 176.21 196.18 6.18 o -4 7 2 0.43 1.78 3.59 o -3 7 2 55.61 47.39 2.25 o -2 7 2 4.78 3.06 2.48 o -1 7 2 233.29 238.64 6.30 o 0 7 2 1.87 0.05 0.77 o 1 7 2 238.48 237.72 4.80 o 2 7 2 2.57 0.35 1.89 o 3 7 2 32.76 41.68 2.29 o 4 7 2 0.01 2.98 2.35 o -2 8 2 12.25 16.11 3.59 o -1 8 2 2.11 0.62 3.25 o 0 8 2 3.45 1.47 2.51 o 1 8 2 27.16 23.67 3.10 o 2 8 2 0.03 -0.61 4.88 o -7 0 3 106.53 109.82 4.43 o -6 0 3 19.44 18.43 1.34 o -5 0 3 385.72 402.37 5.75 o -4 0 3 195.45 190.38 3.04 o -3 0 3 8.35 13.89 0.50 o -2 0 3 121.75 111.87 0.72 o -1 0 3 1.73 5.12 0.22 o 0 0 3 1648.18 1718.14 12.83 o 1 0 3 640.45 611.35 4.99 o 2 0 3 20.78 26.83 0.68 o 3 0 3 122.64 103.91 1.19 o 4 0 3 2.09 2.35 0.66 o 5 0 3 490.15 501.28 2.63 o 6 0 3 11.97 6.48 1.58 o 7 0 3 61.46 66.39 3.53 o -7 1 3 1.50 2.23 1.47 o -6 1 3 7.06 5.08 1.08 o -5 1 3 202.36 213.38 1.91 o -4 1 3 130.98 132.73 1.14 o -3 1 3 1162.02 1074.57 8.13 o -2 1 3 296.10 291.04 2.47 o -1 1 3 5298.93 5093.63 22.25 o 0 1 3 253.80 266.82 3.62 o 1 1 3 2450.90 2437.21 7.66 o 2 1 3 85.25 101.10 0.88 o 3 1 3 393.53 361.46 2.23 o 4 1 3 7.82 6.85 0.59 o 5 1 3 9.53 14.53 0.73 o 6 1 3 2.30 0.67 1.12 o 7 1 3 19.44 21.67 2.17 o -7 2 3 97.86 98.03 1.61 o -6 2 3 56.24 57.53 1.17 o -5 2 3 519.45 514.19 3.14 o -4 2 3 180.94 185.65 2.41 o -3 2 3 211.49 219.42 2.13 o -2 2 3 58.84 83.68 1.01 o -1 2 3 68.45 77.83 1.10 o 0 2 3 0.06 0.62 0.20 o 1 2 3 1345.55 1323.58 12.14 o 2 2 3 164.63 190.49 1.72 o 3 2 3 765.16 726.83 5.39 o 4 2 3 11.97 11.29 0.72 o 5 2 3 523.07 523.34 3.52 o 6 2 3 0.30 0.52 1.20 o -7 3 3 8.40 8.04 2.00 o -6 3 3 1.01 0.07 0.82 o -5 3 3 180.31 192.62 2.32 o -4 3 3 1.14 1.12 0.76 o -3 3 3 561.60 523.59 8.54 o -2 3 3 1.32 0.85 0.34 o -1 3 3 952.97 845.45 8.93 o 0 3 3 227.13 234.21 8.14 o 1 3 3 333.24 322.57 2.67 o 2 3 3 109.13 104.14 1.11 o 3 3 3 279.15 260.28 2.37 o 4 3 3 68.54 57.95 0.81 o 5 3 3 2.82 2.93 0.95 o 6 3 3 3.68 1.85 1.52 o -6 4 3 24.46 22.60 1.98 o -5 4 3 224.70 234.16 4.04 o -4 4 3 72.10 88.85 1.40 o -3 4 3 83.30 86.95 1.32 o -2 4 3 1.20 4.03 0.59 o -1 4 3 4.65 8.53 0.52 o 0 4 3 0.37 0.18 0.25 o 1 4 3 431.65 462.45 2.52 o 2 4 3 31.06 30.30 0.70 o 3 4 3 411.96 381.24 3.48 o 4 4 3 2.26 0.67 1.00 o 5 4 3 223.89 219.65 3.95 o 6 4 3 0.22 1.85 1.56 o -6 5 3 7.69 3.89 1.97 o -5 5 3 33.57 35.89 1.53 o -4 5 3 57.45 54.79 1.43 o -3 5 3 386.78 384.64 2.19 o -2 5 3 83.52 83.09 1.14 o -1 5 3 949.60 881.32 12.16 o 0 5 3 38.89 39.87 0.93 o 1 5 3 463.45 468.14 2.62 o 2 5 3 4.65 1.53 0.95 o 3 5 3 113.50 108.24 2.74 o 4 5 3 0.48 -0.27 1.08 o 5 5 3 8.03 10.08 2.03 o -5 6 3 47.58 61.52 3.00 o -4 6 3 13.39 22.78 2.08 o -3 6 3 5.55 6.83 1.46 o -2 6 3 22.49 17.01 1.50 o -1 6 3 2.05 -0.40 1.08 o 0 6 3 19.88 18.68 1.45 o 1 6 3 52.82 53.27 1.13 o 2 6 3 0.62 -0.78 1.46 o 3 6 3 82.53 74.92 1.55 o 4 6 3 5.82 7.77 2.08 o -4 7 3 10.62 9.67 7.98 o -3 7 3 120.28 132.84 3.05 o -2 7 3 14.22 16.61 2.39 o -1 7 3 189.54 191.25 3.52 o 0 7 3 13.03 11.67 1.97 o 1 7 3 100.88 97.35 4.00 o 2 7 3 0.48 5.58 2.47 o 3 7 3 29.36 28.91 4.30 o -2 8 3 1.21 3.99 3.35 o -1 8 3 0.00 -1.66 2.90 o 0 8 3 18.60 13.27 2.52 o 1 8 3 49.17 40.13 3.34 o -7 0 4 118.10 109.20 1.98 o -6 0 4 55.48 47.34 1.93 o -5 0 4 254.06 277.49 3.75 o -4 0 4 3.27 2.98 0.72 o -3 0 4 0.75 0.27 0.32 o -2 0 4 73.17 69.08 0.70 o -1 0 4 541.75 530.70 3.36 o 0 0 4 115.92 170.11 3.10 o 1 0 4 456.91 450.73 4.76 o 2 0 4 12.61 21.17 1.14 o 3 0 4 200.06 198.32 2.98 o 4 0 4 16.40 10.54 0.87 o 5 0 4 43.54 43.00 1.29 o 6 0 4 1.29 0.14 2.09 o -7 1 4 8.26 6.53 1.50 o -6 1 4 5.27 5.24 1.14 o -5 1 4 234.48 223.59 1.52 o -4 1 4 290.24 290.33 1.86 o -3 1 4 308.89 301.83 1.67 o -2 1 4 139.81 130.45 1.05 o -1 1 4 3199.65 3219.90 24.68 o 0 1 4 750.28 809.10 4.14 o 1 1 4 724.50 757.23 3.49 o 2 1 4 167.89 160.42 1.31 o 3 1 4 266.40 257.71 4.53 o 4 1 4 45.38 52.56 0.76 o 5 1 4 22.68 28.23 0.92 o 6 1 4 57.36 51.24 1.52 o -7 2 4 62.07 56.28 1.81 o -6 2 4 102.14 98.61 2.62 o -5 2 4 189.95 213.69 3.39 o -4 2 4 119.80 107.77 0.97 o -3 2 4 155.36 149.75 1.25 o -2 2 4 10.22 4.85 0.42 o -1 2 4 25.98 29.30 0.72 o 0 2 4 171.96 175.51 2.30 o 1 2 4 182.27 165.03 1.08 o 2 2 4 263.09 252.62 1.73 o 3 2 4 397.44 389.56 3.99 o 4 2 4 65.93 56.64 0.76 o 5 2 4 141.87 134.47 1.55 o 6 2 4 0.06 -0.44 1.03 o -7 3 4 9.17 14.67 2.92 o -6 3 4 20.91 20.01 1.40 o -5 3 4 328.17 317.66 1.87 o -4 3 4 117.70 115.20 1.80 o -3 3 4 473.63 469.89 6.17 o -2 3 4 11.90 10.49 0.58 o -1 3 4 918.63 932.34 8.46 o 0 3 4 26.76 21.68 0.47 o 1 3 4 19.64 14.44 0.49 o 2 3 4 19.13 20.04 0.54 o 3 3 4 10.01 9.08 0.70 o 4 3 4 0.33 0.40 0.55 o 5 3 4 14.91 20.58 1.10 o 6 3 4 15.45 16.02 1.56 o -6 4 4 46.67 45.95 1.68 o -5 4 4 86.51 97.28 1.42 o -4 4 4 52.73 47.44 1.20 o -3 4 4 34.37 36.69 2.05 o -2 4 4 7.66 2.62 0.70 o -1 4 4 0.13 0.18 0.36 o 0 4 4 110.37 126.95 1.26 o 1 4 4 203.62 165.64 2.31 o 2 4 4 101.47 105.47 2.34 o 3 4 4 195.68 199.52 1.48 o 4 4 4 29.41 26.76 1.11 o 5 4 4 70.24 65.96 1.37 o -5 5 4 70.65 61.70 2.31 o -4 5 4 128.23 131.00 1.59 o -3 5 4 123.60 127.01 2.32 o -2 5 4 128.55 128.97 1.67 o -1 5 4 375.98 382.09 7.98 o 0 5 4 139.90 140.31 1.64 o 1 5 4 203.66 180.66 4.49 o 2 5 4 2.14 1.46 1.01 o 3 5 4 47.38 43.70 1.26 o 4 5 4 27.78 25.69 1.62 o 5 5 4 7.80 13.64 2.01 o -5 6 4 29.37 38.24 4.63 o -4 6 4 4.30 0.36 0.73 o -3 6 4 2.65 1.92 1.78 o -2 6 4 7.39 2.73 1.59 o -1 6 4 51.03 55.35 1.35 o 0 6 4 6.45 9.46 1.50 o 1 6 4 123.10 100.71 3.59 o 2 6 4 8.06 11.27 2.18 o 3 6 4 46.78 46.77 1.90 o 4 6 4 9.27 7.98 2.53 o -3 7 4 75.67 73.94 2.75 o -2 7 4 45.52 46.87 2.53 o -1 7 4 101.36 102.92 2.86 o 0 7 4 19.36 23.29 2.04 o 1 7 4 34.35 30.45 3.28 o 2 7 4 0.05 -1.76 3.03 o 3 7 4 1.54 -1.77 3.29 o -1 8 4 0.00 4.41 4.13 o 0 8 4 28.43 36.69 3.25 o -7 0 5 13.71 16.22 2.80 o -6 0 5 116.00 108.45 2.69 o -5 0 5 87.02 105.59 1.80 o -4 0 5 805.98 807.55 3.55 o -3 0 5 339.12 317.32 1.99 o -2 0 5 1983.72 1902.21 11.84 o -1 0 5 110.28 109.34 1.56 o 0 0 5 3605.20 3860.68 16.42 o 1 0 5 80.12 92.82 2.07 o 2 0 5 39.93 46.41 1.06 o 3 0 5 2.37 6.81 0.99 o 4 0 5 0.04 -0.75 0.75 o 5 0 5 194.40 179.44 2.32 o 6 0 5 71.93 70.27 3.08 o -7 1 5 71.49 64.42 2.31 o -6 1 5 99.97 94.04 1.60 o -5 1 5 92.93 93.17 0.92 o -4 1 5 175.43 175.65 1.91 o -3 1 5 94.03 99.70 1.06 o -2 1 5 9.21 9.37 0.48 o -1 1 5 153.51 168.27 1.24 o 0 1 5 585.89 655.74 6.33 o 1 1 5 7.40 5.44 0.36 o 2 1 5 653.06 686.44 7.41 o 3 1 5 42.69 42.51 0.67 o 4 1 5 917.77 890.49 10.60 o 5 1 5 26.87 25.45 1.08 o 6 1 5 280.95 267.74 6.01 o -7 2 5 1.76 4.71 1.77 o -6 2 5 70.24 72.84 2.22 o -5 2 5 14.15 44.70 0.99 o -4 2 5 330.88 320.18 3.23 o -3 2 5 225.10 223.59 0.99 o -2 2 5 606.17 604.17 5.03 o -1 2 5 516.49 503.83 6.47 o 0 2 5 1985.49 2144.97 16.26 o 1 2 5 771.42 794.53 4.58 o 2 2 5 325.36 317.73 3.73 o 3 2 5 33.73 36.05 0.74 o 4 2 5 70.79 62.38 0.85 o 5 2 5 76.59 69.03 2.36 o 6 2 5 37.82 42.95 1.62 o -6 3 5 137.56 143.03 2.55 o -5 3 5 29.04 24.44 1.10 o -4 3 5 192.18 189.76 1.99 o -3 3 5 0.14 0.35 0.45 o -2 3 5 32.48 31.96 0.58 o -1 3 5 4.32 3.11 0.52 o 0 3 5 953.89 1003.58 10.78 o 1 3 5 10.26 7.33 0.56 o 2 3 5 950.88 949.78 7.25 o 3 3 5 21.50 16.26 0.82 o 4 3 5 527.85 526.91 2.88 o 5 3 5 0.22 -0.17 1.11 o 6 3 5 126.93 120.82 2.93 o -6 4 5 18.40 17.86 1.98 o -5 4 5 13.68 27.96 1.25 o -4 4 5 250.42 229.69 3.96 o -3 4 5 103.09 98.06 1.60 o -2 4 5 494.95 518.89 5.52 o -1 4 5 108.26 113.97 1.81 o 0 4 5 856.61 883.18 11.62 o 1 4 5 283.97 275.02 2.70 o 2 4 5 217.04 204.67 3.89 o 3 4 5 16.44 19.51 1.08 o 4 4 5 34.48 27.04 1.23 o 5 4 5 20.83 22.52 1.69 o -5 5 5 25.85 23.37 1.85 o -4 5 5 45.93 45.24 1.85 o -3 5 5 85.07 94.14 1.59 o -2 5 5 6.29 5.57 1.17 o -1 5 5 19.35 22.37 1.07 o 0 5 5 35.68 34.50 1.47 o 1 5 5 0.04 1.79 1.11 o 2 5 5 257.10 251.03 4.08 o 3 5 5 5.20 4.64 1.57 o 4 5 5 245.65 268.61 4.12 o -4 6 5 187.23 179.35 2.80 o -3 6 5 34.32 33.70 1.75 o -2 6 5 379.27 399.18 8.46 o -1 6 5 0.48 -1.22 1.22 o 0 6 5 311.33 316.01 4.81 o 1 6 5 17.13 11.83 1.66 o 2 6 5 47.97 46.50 2.95 o 3 6 5 9.67 14.41 8.06 o 4 6 5 2.71 -2.61 2.61 o -3 7 5 23.43 23.33 2.41 o -2 7 5 5.02 4.82 1.96 o -1 7 5 0.33 -1.09 2.17 o 0 7 5 11.34 15.67 1.86 o 1 7 5 0.01 0.44 0.93 o 2 7 5 151.58 133.41 4.56 o -7 0 6 20.48 15.63 3.47 o -6 0 6 20.18 18.45 1.81 o -5 0 6 97.69 97.45 2.60 o -4 0 6 1551.88 1447.39 4.97 o -3 0 6 1324.20 1243.08 9.81 o -2 0 6 2073.94 1978.59 11.76 o -1 0 6 136.87 114.59 1.13 o 0 0 6 2087.14 2178.25 20.64 o 1 0 6 325.92 270.62 3.03 o 2 0 6 204.70 205.29 3.96 o 3 0 6 24.29 21.56 0.96 o 4 0 6 10.96 10.20 1.31 o 5 0 6 16.41 15.72 1.75 o 6 0 6 73.60 71.33 2.72 o -7 1 6 90.24 98.78 3.12 o -6 1 6 86.53 77.97 1.92 o -5 1 6 173.89 154.49 2.50 o -4 1 6 0.07 -0.13 0.34 o -3 1 6 504.75 480.72 3.71 o -2 1 6 113.23 99.13 0.70 o -1 1 6 54.97 51.25 0.67 o 0 1 6 452.71 395.11 3.24 o 1 1 6 13.29 12.72 0.49 o 2 1 6 1104.32 1040.68 9.71 o 3 1 6 35.69 38.01 0.86 o 4 1 6 342.78 339.03 8.07 o 5 1 6 32.94 38.39 1.29 o 6 1 6 64.79 68.47 1.71 o -6 2 6 63.36 66.38 1.58 o -5 2 6 18.38 27.04 1.22 o -4 2 6 1100.12 1071.57 7.83 o -3 2 6 484.01 464.69 2.79 o -2 2 6 750.23 711.67 5.63 o -1 2 6 146.66 126.81 1.51 o 0 2 6 615.20 629.45 6.06 o 1 2 6 689.21 603.64 6.42 o 2 2 6 83.35 85.01 1.28 o 3 2 6 172.28 157.00 3.05 o 4 2 6 0.27 -1.08 1.34 o 5 2 6 1.19 2.50 1.02 o -6 3 6 89.45 79.88 1.92 o -5 3 6 163.17 170.32 3.04 o -4 3 6 59.14 57.05 1.12 o -3 3 6 99.67 90.33 1.46 o -2 3 6 22.77 25.04 0.95 o -1 3 6 33.53 36.85 0.77 o 0 3 6 604.27 594.72 4.68 o 1 3 6 100.21 93.82 0.97 o 2 3 6 1112.69 1064.28 12.35 o 3 3 6 20.43 22.33 1.12 o 4 3 6 399.61 379.09 2.51 o 5 3 6 4.12 7.63 1.96 o -6 4 6 70.68 84.25 2.98 o -5 4 6 18.16 22.09 1.53 o -4 4 6 457.48 466.79 6.43 o -3 4 6 256.21 252.43 3.56 o -2 4 6 421.60 396.17 7.01 o -1 4 6 224.75 221.87 4.13 o 0 4 6 452.29 486.59 7.35 o 1 4 6 234.91 223.38 2.82 o 2 4 6 52.09 55.89 1.09 o 3 4 6 39.92 31.08 1.43 o 4 4 6 2.07 2.77 1.46 o 5 4 6 0.01 -0.07 1.31 o -5 5 6 64.47 77.22 1.96 o -4 5 6 3.32 4.45 2.35 o -3 5 6 40.99 38.89 1.92 o -2 5 6 82.60 83.97 3.09 o -1 5 6 37.51 30.41 1.20 o 0 5 6 227.48 242.28 3.90 o 1 5 6 1.04 -0.63 0.66 o 2 5 6 144.17 138.23 4.33 o 3 5 6 38.61 40.09 2.84 o 4 5 6 128.80 122.18 3.77 o -4 6 6 136.46 150.55 5.21 o -3 6 6 138.80 146.35 3.22 o -2 6 6 275.53 256.59 5.11 o -1 6 6 156.35 159.29 2.26 o 0 6 6 313.58 336.57 4.12 o 1 6 6 15.80 17.12 1.80 o 2 6 6 17.27 9.70 2.69 o 3 6 6 0.86 -2.51 2.51 o -2 7 6 17.93 19.89 2.84 o -1 7 6 2.48 6.13 2.49 o 0 7 6 105.80 108.98 2.10 o 1 7 6 11.74 12.94 2.77 o -6 0 7 9.64 12.30 1.87 o -5 0 7 84.39 93.40 2.08 o -4 0 7 33.86 31.42 1.24 o -3 0 7 23.59 17.32 0.98 o -2 0 7 116.92 100.38 2.04 o -1 0 7 179.62 189.75 3.07 o 0 0 7 400.12 419.26 4.28 o 1 0 7 466.08 403.66 7.26 o 2 0 7 301.13 293.26 8.47 o 3 0 7 562.95 553.52 10.84 o 4 0 7 0.46 -1.07 1.47 o 5 0 7 153.61 149.56 3.16 o -6 1 7 71.10 58.84 1.89 o -5 1 7 0.28 1.93 1.02 o -4 1 7 63.08 53.83 1.48 o -3 1 7 584.19 581.02 4.80 o -2 1 7 118.66 111.57 1.32 o -1 1 7 31.45 33.76 0.84 o 0 1 7 52.49 61.44 1.19 o 1 1 7 198.84 189.85 3.98 o 2 1 7 260.29 239.52 3.23 o 3 1 7 0.15 -0.28 1.25 o 4 1 7 8.66 7.45 1.48 o 5 1 7 2.81 10.21 1.79 o -6 2 7 17.40 16.61 1.63 o -5 2 7 71.58 74.40 2.16 o -4 2 7 1.34 2.09 0.82 o -3 2 7 5.93 6.95 0.84 o -2 2 7 82.17 72.95 1.41 o -1 2 7 3.02 2.87 0.69 o 0 2 7 20.24 18.85 0.74 o 1 2 7 388.16 356.31 5.22 o 2 2 7 22.39 20.77 1.13 o 3 2 7 220.06 219.85 5.07 o 4 2 7 0.17 -0.67 0.79 o 5 2 7 75.84 74.33 2.71 o -6 3 7 36.48 32.82 2.92 o -5 3 7 2.43 3.39 1.14 o -4 3 7 59.05 52.92 1.42 o -3 3 7 202.86 196.95 2.76 o -2 3 7 307.22 314.71 4.83 o -1 3 7 185.42 180.57 3.10 o 0 3 7 5.45 3.92 0.95 o 1 3 7 528.74 526.07 4.91 o 2 3 7 27.96 24.08 1.24 o 3 3 7 18.85 14.91 1.42 o 4 3 7 28.86 32.43 2.36 o 5 3 7 0.04 2.07 2.18 o -5 4 7 65.04 77.10 2.17 o -4 4 7 3.73 7.88 1.77 o -3 4 7 5.90 6.89 1.85 o -2 4 7 30.66 32.51 1.30 o -1 4 7 6.08 4.52 1.09 o 0 4 7 1.69 1.08 1.07 o 1 4 7 124.08 121.45 1.82 o 2 4 7 13.23 10.62 1.40 o 3 4 7 107.43 97.57 2.29 o 4 4 7 1.95 1.42 1.82 o -4 5 7 0.56 -2.65 2.65 o -3 5 7 100.84 97.51 1.86 o -2 5 7 17.03 17.77 1.80 o -1 5 7 94.09 87.90 3.19 o 0 5 7 0.37 -1.20 1.20 o 1 5 7 96.12 98.29 2.45 o 2 5 7 2.09 0.19 1.68 o 3 5 7 0.31 0.82 2.57 o -3 6 7 55.36 62.31 4.96 o -2 6 7 10.68 13.00 2.67 o -1 6 7 0.05 -0.23 2.00 o 0 6 7 8.78 7.71 2.71 o 1 6 7 34.31 33.96 3.14 o 2 6 7 17.42 20.46 3.39 o -6 0 8 116.39 106.96 3.02 o -5 0 8 16.93 14.62 2.17 o -4 0 8 53.05 52.39 1.75 o -3 0 8 0.73 1.33 0.64 o -2 0 8 7.30 4.94 1.21 o -1 0 8 167.82 147.66 3.32 o 0 0 8 3.57 4.45 0.99 o 1 0 8 265.87 264.61 5.15 o 2 0 8 198.59 194.30 4.14 o 3 0 8 233.32 223.41 8.42 o 4 0 8 114.65 119.30 7.49 o 5 0 8 271.65 293.63 12.63 o -6 1 8 92.95 94.52 1.91 o -5 1 8 158.97 160.83 2.56 o -4 1 8 93.58 75.62 1.18 o -3 1 8 366.82 341.98 3.58 o -2 1 8 319.72 283.45 2.56 o -1 1 8 557.25 540.17 3.89 o 0 1 8 294.84 302.41 2.17 o 1 1 8 77.11 74.05 1.52 o 2 1 8 0.16 0.60 0.71 o 3 1 8 0.11 0.00 1.06 o 4 1 8 55.29 47.79 2.95 o 5 1 8 84.57 93.72 3.32 o -6 2 8 64.09 68.26 2.83 o -5 2 8 41.71 37.34 1.42 o -4 2 8 4.09 4.12 1.19 o -3 2 8 4.33 3.38 0.82 o -2 2 8 22.58 21.92 0.93 o -1 2 8 388.09 340.38 2.81 o 0 2 8 7.59 9.15 1.00 o 1 2 8 566.72 529.81 8.45 o 2 2 8 35.24 35.49 1.50 o 3 2 8 251.08 243.20 2.90 o 4 2 8 18.96 20.30 2.89 o -5 3 8 56.60 58.12 2.07 o -4 3 8 70.37 68.77 1.58 o -3 3 8 138.69 130.15 1.50 o -2 3 8 305.22 274.49 4.95 o -1 3 8 238.16 231.94 4.92 o 0 3 8 396.53 411.67 5.66 o 1 3 8 118.04 107.28 1.77 o 2 3 8 35.83 27.12 1.49 o 3 3 8 30.60 30.88 3.12 o 4 3 8 8.54 5.58 2.63 o -5 4 8 21.70 13.09 3.03 o -4 4 8 10.88 6.96 2.61 o -3 4 8 5.13 2.82 1.79 o -2 4 8 1.75 1.49 1.30 o -1 4 8 106.63 93.01 1.57 o 0 4 8 8.82 9.22 1.86 o 1 4 8 265.67 263.28 6.17 o 2 4 8 26.20 23.69 1.70 o 3 4 8 156.74 153.67 4.16 o -4 5 8 70.66 80.11 4.28 o -3 5 8 219.95 214.68 3.18 o -2 5 8 50.42 43.83 2.46 o -1 5 8 172.79 180.37 2.40 o 0 5 8 15.26 15.46 2.80 o 1 5 8 22.13 17.68 1.99 o 2 5 8 9.59 8.64 2.66 o 3 5 8 0.09 0.74 4.39 o -2 6 8 2.50 6.34 2.64 o -1 6 8 0.02 0.25 2.60 o 0 6 8 14.71 20.37 2.75 o 1 6 8 61.45 56.11 3.86 o -5 0 9 3.54 14.42 2.40 o -4 0 9 111.99 96.21 6.13 o -3 0 9 184.31 200.80 2.26 o -2 0 9 0.73 1.59 1.21 o -1 0 9 36.92 50.47 1.95 o 0 0 9 2.30 3.28 1.29 o 1 0 9 224.66 243.83 4.30 o 2 0 9 132.03 137.68 4.02 o 3 0 9 83.95 90.98 3.53 o 4 0 9 29.38 29.04 7.06 o -5 1 9 141.83 133.25 4.19 o -4 1 9 370.67 371.40 7.09 o -3 1 9 303.67 303.76 5.01 o -2 1 9 173.48 185.94 2.53 o -1 1 9 350.70 351.35 2.79 o 0 1 9 91.08 112.07 1.07 o 1 1 9 18.40 20.30 1.13 o 2 1 9 10.61 11.81 1.34 o 3 1 9 1.13 1.28 2.48 o 4 1 9 12.13 11.79 2.26 o -5 2 9 22.93 23.63 2.03 o -4 2 9 56.31 53.53 2.15 o -3 2 9 47.82 52.95 1.06 o -2 2 9 47.10 40.16 1.42 o -1 2 9 56.29 60.81 1.16 o 0 2 9 82.23 84.41 1.46 o 1 2 9 415.42 419.34 4.90 o 2 2 9 113.26 113.10 2.02 o 3 2 9 164.31 174.53 5.31 o 4 2 9 5.97 4.26 4.83 o -5 3 9 111.61 115.70 6.68 o -4 3 9 127.02 125.35 4.66 o -3 3 9 95.24 85.56 1.41 o -2 3 9 100.96 110.44 1.50 o -1 3 9 64.06 61.03 1.29 o 0 3 9 171.64 176.70 3.02 o 1 3 9 1.50 1.99 1.30 o 2 3 9 39.36 37.72 1.82 o 3 3 9 0.71 1.98 4.16 o -4 4 9 13.73 11.08 2.35 o -3 4 9 20.24 25.00 1.74 o -2 4 9 29.66 26.77 1.67 o -1 4 9 71.68 73.28 2.04 o 0 4 9 37.79 38.82 2.35 o 1 4 9 191.08 177.42 2.29 o 2 4 9 52.80 51.02 2.65 o 3 4 9 61.24 79.85 4.99 o -3 5 9 66.90 70.38 3.55 o -2 5 9 94.98 106.75 4.23 o -1 5 9 111.15 105.18 4.78 o 0 5 9 47.98 49.70 3.13 o 1 5 9 14.30 12.30 2.98 o -5 0 10 9.43 32.31 4.12 o -4 0 10 50.62 47.69 3.78 o -3 0 10 13.07 13.38 2.02 o -2 0 10 33.41 37.09 1.79 o -1 0 10 16.89 10.94 2.45 o 0 0 10 31.56 32.41 2.22 o 1 0 10 12.05 8.81 2.59 o 2 0 10 3.42 3.94 1.71 o 3 0 10 0.14 4.50 3.93 o -5 1 10 18.14 16.96 2.52 o -4 1 10 68.55 64.27 2.34 o -3 1 10 9.71 9.38 1.40 o -2 1 10 2.02 1.18 1.09 o -1 1 10 119.94 116.85 1.75 o 0 1 10 4.84 7.58 1.62 o 1 1 10 51.88 56.65 1.82 o 2 1 10 150.71 156.24 3.26 o 3 1 10 19.98 16.47 3.62 o -4 2 10 17.26 17.79 2.08 o -3 2 10 54.28 55.44 1.43 o -2 2 10 50.52 51.98 1.46 o -1 2 10 3.27 6.39 1.28 o 0 2 10 142.28 151.16 1.60 o 1 2 10 6.39 6.70 1.75 o 2 2 10 15.81 12.73 1.73 o 3 2 10 13.52 13.59 2.79 o -4 3 10 28.48 28.24 2.33 o -3 3 10 12.02 11.14 1.90 o -2 3 10 6.82 4.63 1.69 o -1 3 10 19.79 15.73 1.73 o 0 3 10 19.50 20.03 1.90 o 1 3 10 0.06 -1.23 1.84 o 2 3 10 46.06 50.16 4.60 o -3 4 10 12.78 11.69 2.24 o -2 4 10 47.96 47.29 2.10 o -1 4 10 0.65 3.07 2.87 o 0 4 10 88.57 94.64 4.98 o 1 4 10 0.40 1.50 1.63 o -4 0 11 244.18 258.01 4.33 o -3 0 11 462.82 526.36 7.58 o -2 0 11 86.29 92.82 2.23 o -1 0 11 178.78 183.95 2.96 o 0 0 11 6.21 6.07 3.88 o 1 0 11 148.57 152.46 3.91 o 2 0 11 114.10 125.53 4.87 o -4 1 11 86.91 89.82 2.50 o -3 1 11 1.46 1.17 1.32 o -2 1 11 205.82 218.71 1.76 o -1 1 11 47.99 45.07 1.56 o 0 1 11 360.91 399.73 3.76 o 1 1 11 223.93 243.24 4.32 o 2 1 11 239.97 273.33 4.12 o -3 2 11 439.58 460.04 8.90 o -2 2 11 28.66 31.92 1.67 o -1 2 11 309.46 312.48 3.97 o 0 2 11 12.20 18.18 2.46 o 1 2 11 221.28 226.89 2.31 o -2 3 11 237.95 234.14 3.39 o -1 3 11 44.54 41.91 2.22 o 0 3 11 393.96 450.60 6.33 o 1 3 11 84.12 86.07 2.85 o -2 0 12 62.85 65.61 3.98 o -1 0 12 53.70 67.26 4.15 o 0 0 12 24.37 25.36 4.27 o -2 1 12 28.31 24.77 2.89 o -1 1 12 22.54 25.34 2.90 o 0 1 12 48.04 55.39 3.56 o