#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:33:27 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181067 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/47/2214759.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214759_Fobs loop_ _publ_author_name 'Pospieszna-Markiewicz, Izabela' 'Radecka-Paryzek, Wanda' 'Kubicki, Maciej' _publ_section_title ; Putrescinium dichloride: a redetermination at 100 K ; _journal_coeditor_code IS2183 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3650 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.472 _cell_angle_gamma 90.000 _cell_length_a 4.5625 _cell_length_b 8.3514 _cell_length_c 10.6957 _exptl_crystal_F_000 172.00 _reflns_d_resolution_high 0.7570 _cod_data_source_file is2183Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wrp10 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 65.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 233.73 183.19 8.03 o 2 0 0 13.72 20.55 2.15 o 3 0 0 183.90 182.58 6.88 o 4 0 0 1320.75 1390.75 47.43 o 5 0 0 4.83 2.41 9.23 o 6 0 0 49.81 16.51 11.24 o 1 1 0 1254.34 1202.57 11.21 o 2 1 0 316.37 315.81 4.19 o 3 1 0 216.84 216.13 5.52 o 4 1 0 5.28 2.85 2.45 o 5 1 0 168.09 181.17 8.76 o 0 2 0 0.65 2.67 1.13 o 1 2 0 466.31 455.30 4.41 o 2 2 0 2.12 2.61 1.35 o 3 2 0 70.23 65.70 3.97 o 4 2 0 26.28 18.68 6.49 o 5 2 0 29.92 21.95 7.49 o 1 3 0 2027.89 2123.10 23.60 o 2 3 0 398.01 359.13 5.36 o 3 3 0 813.20 833.30 13.97 o 4 3 0 38.72 37.54 7.98 o 5 3 0 104.00 104.20 11.65 o 0 4 0 1284.70 1294.51 9.58 o 1 4 0 483.78 477.15 12.21 o 2 4 0 1.47 2.38 1.34 o 3 4 0 209.43 205.65 6.83 o 4 4 0 356.35 357.24 11.11 o 5 4 0 90.54 91.85 13.26 o 1 5 0 11.42 10.49 2.53 o 2 5 0 1.97 2.52 1.75 o 3 5 0 1.42 7.19 3.59 o 4 5 0 1.76 12.93 6.76 o 5 5 0 3.11 4.17 5.89 o 0 6 0 359.20 402.23 14.76 o 1 6 0 327.96 343.44 8.86 o 2 6 0 0.76 2.94 3.60 o 3 6 0 225.76 238.95 11.43 o 4 6 0 154.98 142.78 21.63 o 5 6 0 73.47 56.41 16.04 o 1 7 0 160.61 149.99 7.71 o 2 7 0 795.05 878.84 19.26 o 3 7 0 93.45 78.15 11.77 o 4 7 0 0.03 1.36 5.44 o 0 8 0 11.54 11.65 8.22 o 1 8 0 221.44 221.47 9.20 o 2 8 0 12.64 6.45 5.05 o 3 8 0 43.57 24.74 15.95 o 4 8 0 0.12 0.00 6.82 o 1 9 0 51.49 45.38 9.72 o 2 9 0 99.79 82.70 15.83 o 3 9 0 22.13 5.14 6.55 o 0 10 0 278.25 307.96 16.47 o 1 10 0 128.57 123.42 14.42 o 2 10 0 1.32 2.32 7.74 o -6 1 1 190.47 197.77 16.87 o -5 1 1 0.23 0.00 5.07 o -4 1 1 81.27 74.47 6.53 o -3 1 1 550.98 550.30 7.55 o -2 1 1 1230.63 1267.73 10.17 o -1 1 1 58.49 54.10 3.30 o 0 1 1 88.49 60.26 6.70 o 1 1 1 2332.74 2403.51 37.73 o 2 1 1 968.49 952.44 7.76 o 3 1 1 3.08 2.91 1.57 o 4 1 1 62.81 59.91 5.46 o 5 1 1 326.67 353.03 14.18 o -5 2 1 338.01 362.67 10.85 o -4 2 1 307.32 313.91 12.50 o -3 2 1 37.16 34.45 3.60 o -2 2 1 241.06 244.36 4.05 o -1 2 1 3496.04 3400.28 58.83 o 0 2 1 1207.78 1236.96 43.99 o 1 2 1 90.93 100.04 2.93 o 2 2 1 216.20 208.20 4.20 o 3 2 1 1125.77 1157.59 29.96 o 4 2 1 238.94 247.08 6.97 o 5 2 1 19.90 13.69 5.60 o -5 3 1 7.16 4.29 5.29 o -4 3 1 118.21 101.35 9.76 o -3 3 1 5.27 6.10 3.51 o -2 3 1 643.25 656.30 14.68 o -1 3 1 51.79 61.46 3.19 o 0 3 1 377.05 363.43 15.14 o 1 3 1 36.72 37.22 3.04 o 2 3 1 394.59 404.84 6.63 o 3 3 1 0.97 2.38 2.02 o 4 3 1 39.25 37.66 7.92 o 5 3 1 9.38 10.34 5.68 o -5 4 1 70.01 82.62 24.76 o -4 4 1 52.56 64.64 8.82 o -3 4 1 162.45 152.98 8.84 o -2 4 1 762.16 782.18 18.39 o -1 4 1 0.10 2.80 2.19 o 0 4 1 634.54 627.41 14.04 o 1 4 1 359.46 383.68 4.88 o 2 4 1 968.66 976.45 34.31 o 3 4 1 8.02 8.49 3.08 o 4 4 1 425.41 442.69 12.49 o 5 4 1 1.11 5.62 6.24 o -5 5 1 7.19 8.39 6.79 o -4 5 1 39.31 35.39 8.88 o -3 5 1 1003.37 1030.22 19.35 o -2 5 1 218.17 210.94 5.07 o -1 5 1 185.85 185.59 5.62 o 0 5 1 374.88 375.43 9.19 o 1 5 1 1276.66 1259.70 40.61 o 2 5 1 401.14 395.87 8.60 o 3 5 1 42.63 32.53 6.36 o 4 5 1 126.77 130.71 11.56 o 5 5 1 244.07 219.36 18.05 o -5 6 1 150.71 149.17 21.53 o -4 6 1 45.11 48.78 15.44 o -3 6 1 14.92 10.01 5.73 o -2 6 1 66.85 64.36 6.58 o -1 6 1 395.48 369.83 18.15 o 0 6 1 130.32 132.28 4.63 o 1 6 1 48.30 47.91 6.28 o 2 6 1 125.33 129.50 6.49 o 3 6 1 129.69 133.09 16.75 o 4 6 1 115.56 100.67 14.74 o 5 6 1 1.45 2.24 7.78 o -4 7 1 4.85 0.69 5.78 o -3 7 1 46.20 40.69 9.18 o -2 7 1 73.88 67.24 9.61 o -1 7 1 57.41 53.27 6.84 o 0 7 1 70.89 54.09 10.80 o 1 7 1 268.31 274.02 8.27 o 2 7 1 0.52 2.20 3.63 o 3 7 1 1.14 6.36 5.80 o 4 7 1 13.43 6.36 5.79 o -4 8 1 275.81 233.33 39.64 o -3 8 1 0.94 0.02 5.04 o -2 8 1 134.26 125.74 17.27 o -1 8 1 236.92 241.86 8.66 o 0 8 1 488.83 554.24 13.10 o 1 8 1 1.63 1.26 3.48 o 2 8 1 86.84 82.93 11.01 o 3 8 1 247.42 279.38 19.30 o 4 8 1 146.89 121.31 14.34 o -3 9 1 196.68 184.85 44.88 o -2 9 1 119.56 128.88 13.60 o -1 9 1 10.33 11.58 7.42 o 0 9 1 47.67 45.37 10.11 o 1 9 1 348.13 382.38 14.00 o 2 9 1 107.72 95.03 13.93 o 3 9 1 7.16 3.92 8.52 o -2 10 1 0.37 5.09 7.53 o -1 10 1 1.34 6.43 9.38 o 0 10 1 15.49 9.58 6.67 o 1 10 1 5.07 0.61 7.35 o 2 10 1 0.68 2.48 6.91 o 0 11 1 77.90 55.01 13.94 o -5 0 2 365.24 386.38 22.36 o -4 0 2 48.22 36.23 13.27 o -3 0 2 26.42 25.01 4.78 o -2 0 2 2127.20 2168.66 60.33 o -1 0 2 3401.43 2981.61 17.46 o 0 0 2 119.71 102.86 5.17 o 1 0 2 217.06 201.02 6.74 o 2 0 2 2776.34 2933.40 30.82 o 3 0 2 740.80 727.62 10.81 o 4 0 2 4.30 2.80 3.63 o 5 0 2 13.99 14.05 8.57 o -5 1 2 139.66 128.60 15.49 o -4 1 2 23.11 14.39 5.19 o -3 1 2 603.52 620.14 7.73 o -2 1 2 110.07 114.55 2.96 o -1 1 2 1454.23 1434.81 21.00 o 1 1 2 3484.25 3466.19 102.70 o 2 1 2 3.13 2.08 1.39 o 3 1 2 90.61 85.36 4.51 o 4 1 2 54.29 54.41 5.66 o 5 1 2 226.26 245.33 17.26 o -5 2 2 99.79 78.16 14.52 o -4 2 2 5.40 6.63 4.03 o -3 2 2 1.88 2.85 2.52 o -2 2 2 198.62 191.35 2.74 o -1 2 2 149.18 144.73 3.47 o 0 2 2 9.76 18.25 4.44 o 1 2 2 6.08 4.59 1.59 o 2 2 2 112.98 109.73 3.90 o 3 2 2 56.18 51.02 5.05 o 4 2 2 17.25 16.96 4.55 o 5 2 2 16.15 2.81 4.86 o -5 3 2 16.95 18.28 13.63 o -4 3 2 571.28 550.21 18.71 o -3 3 2 323.49 309.41 8.38 o -2 3 2 608.91 604.14 23.45 o -1 3 2 664.45 721.06 19.86 o 0 3 2 1823.94 1922.02 39.52 o 1 3 2 497.47 450.00 8.05 o 2 3 2 603.80 635.09 8.28 o 3 3 2 286.78 293.58 7.88 o 4 3 2 242.05 239.34 8.70 o 5 3 2 238.09 239.84 11.31 o -5 4 2 145.25 139.15 14.79 o -4 4 2 31.01 33.30 9.87 o -3 4 2 8.21 6.17 3.38 o -2 4 2 1043.27 1086.07 9.61 o -1 4 2 435.29 419.91 15.42 o 0 4 2 238.35 242.18 8.76 o 1 4 2 102.37 95.79 5.33 o 2 4 2 790.06 795.44 19.45 o 3 4 2 202.21 201.30 7.01 o 4 4 2 95.84 51.97 67.70 o 5 4 2 30.15 16.07 6.67 o -5 5 2 1.53 6.82 6.64 o -4 5 2 14.84 10.22 5.25 o -3 5 2 62.29 71.79 6.50 o -2 5 2 32.41 29.16 4.85 o -1 5 2 1.69 5.78 3.16 o 0 5 2 19.90 17.74 3.16 o 1 5 2 33.93 36.97 4.66 o 2 5 2 8.03 10.22 2.83 o 3 5 2 1.93 2.35 2.28 o 4 5 2 0.02 2.78 5.89 o 5 5 2 3.56 0.00 7.37 o -5 6 2 238.23 281.47 28.02 o -4 6 2 10.50 9.00 5.60 o -3 6 2 49.96 31.49 5.90 o -2 6 2 157.90 162.40 6.06 o -1 6 2 824.38 882.50 16.31 o 0 6 2 15.80 17.32 4.11 o 1 6 2 88.86 87.44 5.47 o 2 6 2 172.43 172.51 7.52 o 3 6 2 408.28 405.51 9.88 o 4 6 2 9.49 6.52 4.25 o -4 7 2 360.95 311.16 56.32 o -3 7 2 231.57 226.80 17.75 o -2 7 2 48.91 66.51 10.09 o -1 7 2 2.50 3.76 3.51 o 0 7 2 1030.73 1107.77 17.16 o 1 7 2 254.54 258.16 17.33 o 2 7 2 70.49 59.65 9.77 o 3 7 2 12.96 8.68 6.90 o 4 7 2 336.39 311.94 22.54 o -4 8 2 18.19 5.71 6.92 o -3 8 2 23.89 18.36 8.56 o -2 8 2 44.75 34.63 11.99 o -1 8 2 15.87 8.95 5.12 o 0 8 2 71.49 74.60 14.14 o 1 8 2 89.79 89.01 13.31 o 2 8 2 1.70 1.85 5.38 o 3 8 2 45.27 34.37 24.09 o 4 8 2 30.64 14.00 7.25 o -3 9 2 68.62 54.92 12.43 o -2 9 2 36.67 26.95 17.52 o -1 9 2 52.39 40.87 8.40 o 0 9 2 27.92 24.58 8.74 o 1 9 2 170.53 169.80 10.45 o 2 9 2 1.93 3.41 6.48 o 3 9 2 6.62 9.66 7.34 o -2 10 2 80.04 46.98 35.11 o -1 10 2 319.42 312.69 18.46 o 0 10 2 48.22 36.95 10.79 o 1 10 2 79.41 55.04 12.12 o 2 10 2 97.29 104.34 21.34 o -5 1 3 53.28 37.37 11.44 o -4 1 3 580.70 596.70 27.76 o -3 1 3 146.03 128.91 9.89 o -2 1 3 122.78 129.26 4.23 o -1 1 3 160.98 160.53 4.24 o 0 1 3 4340.58 4181.50 113.64 o 1 1 3 73.07 66.88 2.15 o 2 1 3 6.59 4.29 2.04 o 3 1 3 245.24 264.57 5.07 o 4 1 3 594.94 610.38 8.49 o 5 1 3 9.74 5.69 5.87 o -5 2 3 161.46 169.52 10.24 o -4 2 3 0.88 3.48 5.00 o -3 2 3 1021.58 893.34 87.50 o -2 2 3 278.55 244.76 5.62 o -1 2 3 1781.47 1727.14 115.02 o 0 2 3 60.08 60.52 1.96 o 1 2 3 2141.47 2153.99 25.18 o 2 2 3 590.49 594.59 9.11 o 3 2 3 397.34 403.43 6.71 o 4 2 3 28.09 23.26 4.52 o 5 2 3 212.54 230.54 14.10 o -5 3 3 14.80 15.99 8.77 o -4 3 3 32.07 43.25 12.33 o -3 3 3 127.86 153.26 10.02 o -2 3 3 287.66 315.71 11.30 o -1 3 3 96.46 105.94 5.26 o 0 3 3 520.15 508.19 4.97 o 1 3 3 242.04 247.71 4.23 o 2 3 3 234.20 247.15 5.11 o 3 3 3 18.19 13.63 4.23 o 4 3 3 207.22 204.28 8.33 o 5 3 3 0.76 3.00 6.83 o -5 4 3 30.46 18.12 10.55 o -4 4 3 7.00 3.62 4.81 o -3 4 3 98.40 87.02 7.24 o -2 4 3 361.44 351.89 10.70 o -1 4 3 131.53 135.81 5.34 o 0 4 3 40.11 40.25 3.14 o 1 4 3 175.66 176.85 4.34 o 2 4 3 207.78 210.31 5.56 o 3 4 3 213.84 209.97 5.96 o 4 4 3 73.70 65.44 11.28 o 5 4 3 19.04 13.11 11.07 o -5 5 3 137.08 148.39 14.03 o -4 5 3 531.91 601.36 14.80 o -3 5 3 39.06 29.46 6.01 o -2 5 3 23.97 21.94 4.29 o -1 5 3 988.05 1027.77 14.81 o 0 5 3 941.52 969.15 24.18 o 1 5 3 181.12 187.39 4.71 o 2 5 3 15.12 12.31 3.66 o 3 5 3 815.57 855.49 10.32 o 4 5 3 152.01 159.34 11.24 o 5 5 3 111.66 92.55 19.45 o -4 6 3 0.72 3.57 5.33 o -3 6 3 74.65 93.43 8.99 o -2 6 3 448.80 430.00 12.72 o -1 6 3 0.06 3.38 2.39 o 0 6 3 45.08 40.75 4.85 o 1 6 3 337.27 341.49 7.04 o 2 6 3 229.93 253.12 5.66 o 3 6 3 27.07 21.87 6.72 o 4 6 3 1.17 3.72 4.84 o -4 7 3 11.83 5.08 10.78 o -3 7 3 20.97 12.69 9.38 o -2 7 3 4.69 3.88 4.59 o -1 7 3 5.41 4.43 2.73 o 0 7 3 113.29 112.28 13.81 o 1 7 3 0.02 2.13 2.94 o 2 7 3 0.03 6.39 5.39 o 3 7 3 8.00 3.46 6.16 o 4 7 3 55.86 45.81 13.16 o -4 8 3 34.75 17.11 9.62 o -3 8 3 85.91 58.86 12.40 o -2 8 3 362.84 389.41 14.29 o -1 8 3 222.51 227.04 8.81 o 0 8 3 103.24 98.51 10.98 o 1 8 3 72.19 65.70 15.05 o 2 8 3 532.94 606.45 16.67 o 3 8 3 58.78 42.33 19.07 o -3 9 3 132.18 135.72 22.93 o -2 9 3 4.49 3.30 7.15 o -1 9 3 304.28 332.21 15.32 o 0 9 3 92.24 80.65 14.55 o 1 9 3 181.99 196.32 14.32 o 2 9 3 18.72 7.11 7.16 o 3 9 3 124.98 100.45 15.28 o -2 10 3 27.42 25.55 11.01 o -1 10 3 1.10 0.00 6.62 o 0 10 3 9.82 10.72 8.51 o 1 10 3 21.21 11.06 6.82 o 2 10 3 38.78 10.09 8.98 o -5 0 4 22.39 20.86 12.62 o -4 0 4 458.93 485.48 18.57 o -3 0 4 548.26 529.71 11.19 o -2 0 4 840.57 795.22 44.25 o -1 0 4 80.09 88.23 6.11 o 0 0 4 2218.52 2206.44 96.65 o 1 0 4 1110.57 1149.38 10.77 o 2 0 4 843.77 821.30 8.45 o 3 0 4 0.10 1.51 2.01 o 4 0 4 229.63 245.08 13.98 o 5 0 4 353.18 401.16 17.01 o -5 1 4 101.44 86.85 13.37 o -4 1 4 127.20 96.66 8.52 o -3 1 4 1.19 8.75 9.62 o -2 1 4 212.40 197.09 11.02 o -1 1 4 418.50 382.23 6.01 o 0 1 4 1058.26 1060.06 5.86 o 1 1 4 218.55 221.54 3.68 o 2 1 4 7.38 4.39 2.18 o 3 1 4 368.96 379.07 6.29 o 4 1 4 190.26 191.95 11.27 o 5 1 4 42.82 38.90 9.40 o -5 2 4 49.42 39.39 8.45 o -4 2 4 42.52 43.91 8.10 o -3 2 4 375.63 377.10 9.77 o -2 2 4 0.48 2.50 1.82 o -1 2 4 5.38 4.09 1.07 o 0 2 4 47.61 49.98 2.47 o 1 2 4 1015.22 1055.46 22.12 o 2 2 4 43.05 42.30 3.74 o 3 2 4 26.32 28.46 4.32 o 4 2 4 12.85 11.87 5.80 o 5 2 4 67.96 49.32 10.26 o -5 3 4 224.63 211.57 12.47 o -4 3 4 246.61 230.59 14.42 o -3 3 4 3.49 6.84 3.17 o -2 3 4 524.61 532.67 11.65 o -1 3 4 1026.28 964.47 19.44 o 0 3 4 677.04 692.05 9.72 o 1 3 4 48.81 49.10 3.68 o 2 3 4 728.05 727.18 9.61 o 3 3 4 372.01 381.41 7.24 o 4 3 4 271.15 264.17 10.05 o 5 3 4 0.32 1.52 7.30 o -5 4 4 0.13 5.73 8.44 o -4 4 4 140.32 167.83 14.54 o -3 4 4 429.64 458.99 10.87 o -2 4 4 228.97 234.27 8.66 o -1 4 4 34.15 38.64 4.47 o 0 4 4 583.39 577.47 7.48 o 1 4 4 654.03 671.88 7.81 o 2 4 4 218.13 216.49 6.51 o 3 4 4 20.23 12.19 3.66 o 4 4 4 217.08 234.04 9.98 o 5 4 4 119.96 100.37 22.43 o -5 5 4 25.78 20.05 8.58 o -4 5 4 0.04 9.85 7.04 o -3 5 4 49.05 41.53 6.89 o -2 5 4 115.68 117.44 5.41 o -1 5 4 152.20 147.65 5.11 o 0 5 4 26.15 23.55 4.56 o 1 5 4 5.37 4.68 2.27 o 2 5 4 56.80 46.09 5.60 o 3 5 4 96.77 90.39 6.56 o 4 5 4 25.91 17.61 10.42 o -4 6 4 2.30 3.91 5.67 o -3 6 4 590.18 680.91 27.10 o -2 6 4 131.06 128.46 9.48 o -1 6 4 40.38 39.20 4.71 o 0 6 4 2.70 3.42 2.39 o 1 6 4 868.12 934.13 18.66 o 2 6 4 107.33 118.28 6.41 o 3 6 4 1.37 2.96 3.10 o 4 6 4 23.08 14.85 7.43 o -4 7 4 119.45 98.61 19.45 o -3 7 4 4.05 6.64 4.56 o -2 7 4 249.34 237.85 8.29 o -1 7 4 506.61 535.34 15.08 o 0 7 4 187.77 193.67 7.91 o 1 7 4 29.96 25.58 5.59 o 2 7 4 339.87 328.25 9.00 o 3 7 4 239.43 247.00 19.67 o 4 7 4 94.17 70.48 12.32 o -3 8 4 44.60 28.66 8.88 o -2 8 4 21.79 28.99 8.70 o -1 8 4 0.83 5.80 5.14 o 0 8 4 17.79 12.71 5.76 o 1 8 4 58.37 50.34 11.87 o 2 8 4 28.05 22.76 9.82 o 3 8 4 0.06 4.99 6.72 o -3 9 4 4.95 3.93 7.29 o -2 9 4 91.39 64.69 11.24 o -1 9 4 25.92 16.12 9.04 o 0 9 4 119.22 122.05 12.55 o 1 9 4 2.63 1.97 7.45 o 2 9 4 28.66 6.68 10.00 o -1 10 4 0.17 4.35 5.43 o 0 10 4 153.82 154.80 15.53 o 1 10 4 126.83 102.95 14.65 o -5 1 5 199.24 213.69 10.06 o -4 1 5 1.30 4.90 3.43 o -3 1 5 8.08 9.32 5.45 o -2 1 5 1125.69 1107.14 18.96 o -1 1 5 715.84 692.37 5.65 o 0 1 5 0.02 0.66 0.89 o 1 1 5 22.58 19.16 2.83 o 2 1 5 1184.04 1230.73 39.56 o 3 1 5 219.61 220.82 12.06 o 4 1 5 1.83 6.03 5.12 o 5 1 5 6.66 4.75 5.48 o -5 2 5 201.71 204.07 11.49 o -4 2 5 298.72 302.23 18.66 o -3 2 5 287.64 291.77 13.94 o -2 2 5 620.46 646.74 9.05 o -1 2 5 1800.87 1803.17 29.88 o 0 2 5 401.67 384.02 4.82 o 1 2 5 1142.97 1121.46 17.69 o 2 2 5 131.87 121.99 4.14 o 3 2 5 551.96 548.37 14.28 o 4 2 5 87.66 100.41 9.81 o 5 2 5 331.01 350.48 12.48 o -5 3 5 1.37 8.01 5.82 o -4 3 5 7.42 12.73 7.80 o 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