#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:33:27 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181067 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/47/2214785.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214785_Fobs loop_ _publ_author_name 'Curran, Louise A.' 'Jenkinson, Sarah F.' 'Jones, Nigel A.' 'Watkin, David J.' 'Fleet, George W. J.' _publ_section_title ; 2,6-Anhydro-1-deoxy-3,4-O-isopropylidene-3-C-methyl-\b-D-ribo-hex-2-ulofuranose ; _journal_coeditor_code LH2449 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3388 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _audit_creation_date 07-05-17 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 6.6307(2) _cell_length_b 11.1029(4) _cell_length_c 14.1409(5) _cod_data_source_file lh2449Isup2.hkl _cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 0 1760.20 1961.57 82.70 o 4 0 0 504.00 528.32 19.60 o 6 0 0 51.70 49.97 3.10 o 8 0 0 104.70 111.89 6.40 o 2 1 0 1018.20 1085.00 28.60 o 3 1 0 167.30 163.37 6.60 o 4 1 0 48.80 48.96 2.30 o 5 1 0 0.80 0.35 1.79 o 6 1 0 37.80 35.37 2.00 o 7 1 0 0.40 1.70 2.15 o 8 1 0 21.00 21.51 3.20 o 2 2 0 104.10 116.27 2.80 o 3 2 0 24.20 23.77 1.40 o 4 2 0 226.60 224.27 9.00 o 5 2 0 85.20 92.43 2.70 o 6 2 0 24.50 26.72 1.50 o 7 2 0 29.40 27.20 1.90 o 8 2 0 9.20 8.99 2.70 o 1 3 0 204.90 215.12 4.30 o 2 3 0 9.20 8.61 0.40 o 3 3 0 170.00 187.43 4.40 o 4 3 0 580.20 564.59 15.30 o 5 3 0 34.80 36.50 1.20 o 6 3 0 81.80 82.75 2.10 o 7 3 0 5.10 8.74 2.20 o 8 3 0 118.70 108.92 6.30 o 0 4 0 115.50 138.50 3.30 o 1 4 0 315.10 300.07 7.50 o 2 4 0 198.40 196.98 4.80 o 3 4 0 1.40 0.12 1.20 o 4 4 0 28.60 32.64 2.10 o 5 4 0 99.30 98.55 4.10 o 6 4 0 5.80 7.77 1.70 o 7 4 0 52.40 48.73 3.30 o 8 4 0 13.30 16.29 2.80 o 1 5 0 76.00 67.52 1.80 o 2 5 0 0.40 0.08 0.51 o 3 5 0 35.40 33.18 2.00 o 4 5 0 59.10 56.05 3.10 o 5 5 0 70.50 70.61 3.70 o 6 5 0 5.00 2.57 1.50 o 7 5 0 5.80 5.05 2.20 o 8 5 0 26.90 25.21 4.20 o 0 6 0 1343.60 1375.22 38.50 o 1 6 0 548.80 539.51 10.30 o 2 6 0 923.80 917.49 18.00 o 3 6 0 50.80 48.10 1.70 o 4 6 0 28.10 27.29 2.00 o 5 6 0 1.60 0.07 1.90 o 6 6 0 16.90 13.34 2.10 o 7 6 0 48.00 45.17 3.90 o 1 7 0 338.80 324.43 6.40 o 2 7 0 302.90 278.05 6.10 o 3 7 0 2.50 2.15 0.50 o 4 7 0 106.30 101.79 3.70 o 5 7 0 0.40 3.11 2.91 o 6 7 0 10.40 5.29 3.10 o 7 7 0 3.40 1.48 3.10 o 0 8 0 480.80 462.22 14.70 o 1 8 0 -0.30 0.79 1.10 o 2 8 0 331.40 317.69 7.30 o 3 8 0 68.40 67.22 2.40 o 4 8 0 5.90 7.57 1.90 o 5 8 0 6.60 8.38 2.60 o 6 8 0 31.60 25.94 4.90 o 7 8 0 22.50 26.18 3.30 o 1 9 0 681.70 675.59 16.50 o 2 9 0 291.60 278.45 6.30 o 3 9 0 139.60 136.82 4.30 o 4 9 0 8.70 12.88 1.90 o 5 9 0 44.80 44.90 3.40 o 6 9 0 18.20 23.67 4.30 o 0 10 0 74.20 80.55 3.90 o 1 10 0 70.80 77.85 2.60 o 2 10 0 49.80 45.61 2.10 o 3 10 0 4.40 6.76 0.90 o 4 10 0 5.90 6.77 0.60 o 6 10 0 2.00 8.77 4.20 o 1 11 0 181.40 178.92 5.60 o 2 11 0 12.20 10.94 1.50 o 3 11 0 79.00 82.15 2.80 o 4 11 0 79.20 79.51 5.00 o 5 11 0 56.80 44.21 6.30 o 0 12 0 13.30 12.45 2.80 o 1 12 0 -1.20 0.02 1.50 o 2 12 0 41.30 39.71 2.40 o 3 12 0 -1.40 0.01 1.00 o 4 12 0 33.50 35.56 5.90 o 1 13 0 2.40 2.91 1.80 o 2 13 0 1.10 1.16 1.50 o 1 14 0 3.70 0.40 2.70 o 2 0 1 381.30 423.59 7.50 o 3 0 1 756.20 804.71 16.00 o 4 0 1 880.00 869.71 21.30 o 5 0 1 51.30 47.74 2.00 o 6 0 1 19.40 18.18 1.80 o 7 0 1 21.00 21.59 1.80 o 8 0 1 2.10 0.50 2.40 o 2 1 1 37.50 34.92 1.27 o 3 1 1 342.65 375.59 8.77 o 4 1 1 122.05 105.29 3.68 o 5 1 1 33.05 36.24 1.65 o 6 1 1 98.75 98.48 3.45 o 7 1 1 22.60 22.65 1.80 o 8 1 1 8.05 9.19 2.90 o 2 2 1 210.95 226.20 5.07 o 3 2 1 272.60 281.59 9.37 o 4 2 1 121.15 122.97 3.17 o 5 2 1 60.95 59.44 2.15 o 6 2 1 50.50 46.88 2.41 o 7 2 1 32.50 30.72 1.67 o 8 2 1 70.30 70.48 4.40 o 0 3 1 0.90 0.55 0.57 o 1 3 1 707.15 782.75 13.84 o 2 3 1 313.00 323.40 7.10 o 3 3 1 275.50 265.79 8.57 o 4 3 1 270.05 263.92 9.46 o 5 3 1 43.05 36.68 2.89 o 6 3 1 8.00 7.30 1.61 o 7 3 1 53.15 48.90 2.69 o 8 3 1 5.75 7.88 2.55 o 0 4 1 72.80 70.77 1.90 o 1 4 1 128.90 131.91 2.83 o 2 4 1 653.45 658.48 14.47 o 3 4 1 0.70 0.27 1.59 o 4 4 1 43.35 43.90 2.47 o 5 4 1 125.80 132.27 5.00 o 6 4 1 32.55 33.93 2.45 o 7 4 1 130.80 131.13 5.65 o 8 4 1 36.15 35.84 4.00 o 0 5 1 249.00 256.77 6.20 o 1 5 1 511.35 525.13 10.21 o 2 5 1 104.45 103.70 2.71 o 3 5 1 6.40 6.91 0.98 o 4 5 1 289.10 284.52 8.23 o 5 5 1 18.80 18.02 2.50 o 6 5 1 47.65 47.23 3.26 o 7 5 1 19.30 17.36 2.60 o 8 5 1 5.20 1.37 3.01 o 0 6 1 328.40 322.59 7.90 o 1 6 1 11.15 11.43 0.75 o 2 6 1 257.00 243.90 5.51 o 3 6 1 58.05 54.72 1.90 o 4 6 1 135.15 140.07 4.76 o 5 6 1 112.00 107.30 5.95 o 6 6 1 1.60 5.30 2.18 o 7 6 1 3.75 2.09 2.75 o 0 7 1 128.70 123.88 3.00 o 1 7 1 138.70 139.00 3.28 o 2 7 1 148.05 135.38 3.61 o 3 7 1 260.80 249.44 6.63 o 4 7 1 49.15 47.71 2.81 o 5 7 1 20.70 18.65 2.67 o 6 7 1 14.85 10.85 3.42 o 7 7 1 4.75 7.14 2.91 o 0 8 1 63.70 63.96 2.00 o 1 8 1 59.65 62.66 1.95 o 2 8 1 3.35 4.38 0.85 o 3 8 1 94.75 99.89 2.90 o 4 8 1 61.10 67.84 3.25 o 5 8 1 29.40 33.45 3.01 o 6 8 1 -1.30 1.76 2.92 o 7 8 1 7.70 7.87 3.15 o 0 9 1 10.00 10.99 1.10 o 1 9 1 11.40 10.14 1.15 o 2 9 1 193.75 196.43 5.19 o 3 9 1 67.90 66.27 2.50 o 4 9 1 48.35 54.25 3.21 o 5 9 1 7.40 12.54 2.66 o 6 9 1 69.20 57.68 5.90 o 0 10 1 -0.30 0.00 0.99 o 1 10 1 129.55 127.72 3.90 o 2 10 1 72.20 71.95 2.36 o 3 10 1 87.25 88.42 2.91 o 4 10 1 6.55 6.86 1.43 o 5 10 1 65.75 62.58 6.91 o 6 10 1 2.80 0.39 3.69 o 0 11 1 8.00 8.73 1.50 o 1 11 1 3.30 2.60 1.25 o 2 11 1 138.40 134.08 4.85 o 3 11 1 3.55 4.34 0.95 o 4 11 1 17.45 23.07 4.02 o 5 11 1 13.10 15.24 4.40 o 0 12 1 5.30 5.03 1.40 o 1 12 1 37.25 38.18 2.35 o 2 12 1 3.20 3.19 1.70 o 3 12 1 46.10 40.45 3.86 o 4 12 1 0.80 2.32 7.51 o 0 13 1 12.40 14.90 2.00 o 1 13 1 18.40 18.16 2.06 o 2 13 1 9.50 9.42 2.36 o 3 13 1 19.00 18.54 4.60 o 0 14 1 6.80 1.83 7.00 o 1 14 1 0.30 2.24 3.01 o 2 0 2 2.50 2.78 0.50 o 3 0 2 39.50 44.93 1.40 o 4 0 2 112.10 110.66 2.80 o 5 0 2 204.40 192.57 5.60 o 6 0 2 18.80 20.48 1.80 o 7 0 2 26.40 26.84 2.30 o 8 0 2 42.50 42.57 3.50 o 2 1 2 341.50 363.63 6.88 o 3 1 2 891.70 909.48 20.25 o 4 1 2 69.15 65.65 2.26 o 5 1 2 26.25 30.32 1.67 o 6 1 2 243.35 243.56 7.10 o 7 1 2 47.30 43.43 2.75 o 8 1 2 3.80 5.48 2.32 o 1 2 2 2675.85 3001.79 53.20 o 2 2 2 572.10 587.27 9.80 o 3 2 2 148.30 137.06 3.81 o 4 2 2 55.75 51.57 1.94 o 5 2 2 314.00 317.77 9.34 o 6 2 2 134.80 138.86 4.25 o 7 2 2 54.85 55.29 2.30 o 8 2 2 14.20 14.39 3.15 o 0 3 2 876.70 957.56 16.10 o 1 3 2 643.25 689.66 11.76 o 2 3 2 1155.40 1185.82 34.60 o 3 3 2 38.60 37.45 2.26 o 4 3 2 625.15 622.55 19.76 o 5 3 2 213.70 215.72 7.94 o 6 3 2 68.70 75.84 3.06 o 7 3 2 8.00 9.85 1.72 o 8 3 2 12.35 12.11 3.06 o 0 4 2 511.80 511.13 9.10 o 1 4 2 1052.35 1086.75 19.05 o 2 4 2 1681.55 1696.89 33.78 o 3 4 2 324.00 312.78 10.63 o 4 4 2 65.40 61.57 2.82 o 5 4 2 353.30 348.62 12.49 o 6 4 2 206.00 201.85 9.46 o 7 4 2 33.20 34.12 2.53 o 8 4 2 3.55 3.92 3.20 o 0 5 2 238.60 250.89 4.80 o 1 5 2 115.00 114.74 2.57 o 2 5 2 270.50 278.69 5.69 o 3 5 2 159.35 155.98 3.89 o 4 5 2 642.20 634.56 23.60 o 5 5 2 237.85 244.94 9.95 o 6 5 2 74.65 76.68 5.54 o 7 5 2 5.35 6.53 2.55 o 8 5 2 12.55 9.61 3.31 o 0 6 2 148.10 145.23 3.80 o 1 6 2 442.00 443.28 10.45 o 2 6 2 473.75 456.67 10.39 o 3 6 2 148.40 144.08 3.77 o 4 6 2 50.65 50.94 3.13 o 5 6 2 156.30 153.66 7.08 o 6 6 2 42.30 45.01 3.83 o 7 6 2 7.75 10.74 2.61 o 0 7 2 335.90 346.77 8.00 o 1 7 2 78.95 77.55 2.45 o 2 7 2 101.50 91.94 2.85 o 3 7 2 119.40 115.38 3.58 o 4 7 2 104.05 106.86 4.98 o 5 7 2 75.30 82.54 4.24 o 6 7 2 34.05 34.98 3.18 o 7 7 2 9.25 6.48 3.39 o 0 8 2 35.10 35.29 1.50 o 1 8 2 183.05 183.88 4.42 o 2 8 2 173.25 169.01 4.34 o 3 8 2 67.10 63.51 2.46 o 4 8 2 8.20 8.95 1.80 o 5 8 2 38.05 37.27 3.94 o 6 8 2 9.60 7.94 3.22 o 7 8 2 4.55 1.05 3.61 o 0 9 2 227.60 219.95 6.00 o 1 9 2 51.70 57.53 2.00 o 2 9 2 31.55 31.96 1.56 o 3 9 2 21.60 24.42 1.30 o 4 9 2 10.70 10.85 1.95 o 5 9 2 12.70 9.31 3.30 o 6 9 2 -0.15 1.03 3.46 o 0 10 2 9.90 11.25 1.20 o 1 10 2 211.80 206.54 6.10 o 2 10 2 173.45 172.68 4.76 o 3 10 2 89.10 78.14 2.97 o 4 10 2 2.90 3.35 1.50 o 5 10 2 24.45 19.94 5.00 o 6 10 2 0.05 1.37 4.15 o 0 11 2 4.20 3.81 1.20 o 1 11 2 17.45 20.09 1.65 o 2 11 2 2.95 1.77 1.20 o 3 11 2 45.95 47.24 2.21 o 4 11 2 27.90 29.98 2.89 o 5 11 2 6.90 5.96 3.96 o 0 12 2 21.10 23.02 2.00 o 1 12 2 1.45 2.27 1.56 o 2 12 2 1.85 5.61 1.96 o 3 12 2 47.55 41.96 3.86 o 4 12 2 20.20 17.55 4.30 o 0 13 2 0.90 2.79 3.42 o 1 13 2 5.35 6.17 1.95 o 2 13 2 15.45 13.65 3.62 o 3 13 2 6.20 6.46 4.20 o 0 14 2 2.20 3.36 3.00 o 1 14 2 5.50 8.59 3.50 o 1 0 3 162.90 184.42 3.30 o 2 0 3 308.50 311.49 5.70 o 3 0 3 3.50 2.00 0.70 o 4 0 3 239.20 225.18 8.00 o 5 0 3 3.30 0.58 1.20 o 6 0 3 0.00 0.36 0.01 o 7 0 3 80.50 81.62 4.60 o 8 0 3 5.70 5.12 2.90 o 1 1 3 736.00 821.89 16.34 o 2 1 3 400.90 419.17 7.92 o 3 1 3 175.15 179.58 4.81 o 4 1 3 95.95 86.54 3.00 o 5 1 3 103.70 103.81 3.68 o 6 1 3 10.90 12.83 1.40 o 7 1 3 152.60 153.38 5.56 o 8 1 3 6.90 5.63 2.42 o 0 2 3 5.20 8.15 0.60 o 1 2 3 191.65 183.51 3.70 o 2 2 3 126.15 123.04 3.28 o 3 2 3 63.00 52.32 1.94 o 4 2 3 12.55 13.60 0.71 o 5 2 3 42.15 44.24 1.78 o 6 2 3 5.35 7.56 0.80 o 7 2 3 34.75 33.71 1.95 o 8 2 3 1.70 0.33 2.61 o 0 3 3 632.40 693.90 13.30 o 1 3 3 3606.25 3787.24 74.05 o 2 3 3 20.50 23.53 0.76 o 3 3 3 320.30 318.96 9.78 o 4 3 3 195.70 197.53 6.97 o 5 3 3 1.15 1.70 2.03 o 6 3 3 36.05 35.86 2.91 o 7 3 3 37.05 40.26 2.97 o 8 3 3 11.20 10.63 2.70 o 0 4 3 346.40 325.48 6.60 o 1 4 3 1422.35 1483.63 32.69 o 2 4 3 213.10 216.12 5.45 o 3 4 3 7.65 5.69 1.39 o 4 4 3 58.05 56.99 2.94 o 5 4 3 242.95 238.90 9.69 o 6 4 3 8.70 11.57 2.08 o 7 4 3 19.50 19.58 2.18 o 8 4 3 -1.80 0.39 4.59 o 0 5 3 145.10 145.83 2.80 o 1 5 3 959.40 999.89 18.92 o 2 5 3 290.65 288.19 7.67 o 3 5 3 117.80 111.20 3.49 o 4 5 3 140.85 148.64 5.57 o 5 5 3 89.90 86.32 4.53 o 6 5 3 46.80 50.29 3.80 o 7 5 3 12.45 17.63 3.34 o 0 6 3 365.20 349.36 7.30 o 1 6 3 304.65 304.38 7.44 o 2 6 3 277.55 270.74 6.38 o 3 6 3 66.75 65.72 2.28 o 4 6 3 223.35 237.29 8.70 o 5 6 3 395.85 369.98 17.14 o 6 6 3 10.35 10.81 2.53 o 7 6 3 35.35 34.96 4.54 o 0 7 3 15.10 18.24 1.00 o 1 7 3 2.70 2.62 0.73 o 2 7 3 25.40 21.93 1.08 o 3 7 3 38.90 40.05 1.75 o 4 7 3 335.95 330.74 14.04 o 5 7 3 41.90 45.83 3.38 o 6 7 3 5.25 1.82 3.23 o 7 7 3 3.30 3.88 3.61 o 0 8 3 54.90 61.76 2.00 o 1 8 3 1.80 2.42 0.76 o 2 8 3 44.90 47.99 1.96 o 3 8 3 18.85 18.18 1.20 o 4 8 3 181.55 174.66 8.48 o 5 8 3 73.75 71.24 4.65 o 6 8 3 8.40 6.53 3.14 o 7 8 3 4.10 2.67 4.50 o 0 9 3 6.00 7.23 1.10 o 1 9 3 37.20 40.14 1.70 o 2 9 3 82.95 85.81 2.89 o 3 9 3 33.50 36.26 1.51 o 4 9 3 95.90 87.41 4.60 o 5 9 3 21.25 25.58 3.06 o 6 9 3 14.90 14.38 4.68 o 0 10 3 308.00 299.65 8.30 o 1 10 3 11.75 10.71 1.30 o 2 10 3 15.45 17.39 1.37 o 3 10 3 32.55 35.88 1.88 o 4 10 3 58.70 53.83 3.71 o 5 10 3 6.65 7.25 3.04 o 6 10 3 2.95 2.73 4.15 o 0 11 3 16.80 18.29 1.50 o 1 11 3 58.80 54.55 2.55 o 2 11 3 8.55 6.81 1.35 o 3 11 3 2.00 1.78 1.12 o 4 11 3 9.00 5.10 2.90 o 5 11 3 22.20 19.84 4.42 o 0 12 3 12.20 13.32 1.60 o 1 12 3 36.50 35.09 2.30 o 2 12 3 1.35 3.30 1.38 o 3 12 3 51.70 45.15 4.11 o 4 12 3 45.30 41.04 4.50 o 0 13 3 9.40 6.44 2.10 o 1 13 3 6.25 9.75 3.16 o 2 13 3 19.80 17.62 2.20 o 3 13 3 29.10 18.00 5.40 o 1 14 3 13.30 9.90 4.90 o 0 0 4 3566.30 3867.10 189.40 o 1 0 4 132.00 127.29 2.70 o 2 0 4 214.10 204.89 4.30 o 3 0 4 272.10 264.11 5.50 o 4 0 4 163.70 173.11 4.40 o 5 0 4 72.20 70.25 3.00 o 6 0 4 145.10 154.37 4.70 o 7 0 4 1.70 2.05 1.60 o 8 0 4 67.20 57.61 5.90 o 0 1 4 14.50 14.26 0.50 o 1 1 4 96.70 100.32 3.01 o 2 1 4 1174.65 1184.04 22.61 o 3 1 4 61.85 52.69 1.60 o 4 1 4 14.25 13.11 1.05 o 5 1 4 8.05 5.69 1.15 o 6 1 4 773.30 764.03 22.65 o 7 1 4 7.10 6.07 1.41 o 8 1 4 8.30 7.80 2.72 o 0 2 4 22.30 34.23 1.10 o 1 2 4 61.25 63.29 1.45 o 2 2 4 696.25 716.31 14.86 o 3 2 4 658.90 638.20 13.94 o 4 2 4 112.30 113.76 3.34 o 5 2 4 21.80 19.84 1.16 o 6 2 4 288.95 285.94 9.89 o 7 2 4 17.90 17.88 1.20 o 8 2 4 61.30 59.66 4.63 o 0 3 4 279.30 290.62 6.90 o 1 3 4 144.05 152.53 3.65 o 2 3 4 203.15 189.14 4.30 o 3 3 4 439.10 419.08 17.90 o 4 3 4 202.20 195.01 7.12 o 5 3 4 88.90 87.92 4.32 o 6 3 4 49.80 53.95 3.62 o 7 3 4 29.00 32.22 2.57 o 8 3 4 36.45 35.72 3.95 o 0 4 4 128.80 122.78 3.00 o 1 4 4 69.45 62.05 2.10 o 2 4 4 886.15 900.20 18.87 o 3 4 4 522.25 519.48 14.83 o 4 4 4 166.70 162.52 6.23 o 5 4 4 41.45 40.60 2.94 o 6 4 4 225.10 221.03 10.56 o 7 4 4 5.05 3.23 3.38 o 8 4 4 53.15 60.93 4.51 o 0 5 4 3.80 3.48 0.40 o 1 5 4 106.90 108.52 3.16 o 2 5 4 104.40 106.12 2.59 o 3 5 4 169.90 171.64 4.90 o 4 5 4 542.50 544.60 19.23 o 5 5 4 223.50 236.71 8.57 o 6 5 4 30.90 30.41 3.01 o 7 5 4 15.50 18.09 3.31 o 0 6 4 72.60 70.18 1.90 o 1 6 4 145.40 137.06 4.02 o 2 6 4 36.00 36.41 1.57 o 3 6 4 85.05 71.90 3.01 o 4 6 4 223.50 213.03 9.63 o 5 6 4 44.65 41.14 3.10 o 6 6 4 73.50 84.08 5.16 o 7 6 4 36.10 36.64 4.84 o 0 7 4 176.50 190.53 3.90 o 1 7 4 1.85 1.99 0.63 o 2 7 4 26.45 25.82 1.62 o 3 7 4 77.40 68.03 2.50 o 4 7 4 358.75 348.98 15.88 o 5 7 4 119.15 125.02 5.76 o 6 7 4 66.70 57.92 5.21 o 7 7 4 -4.70 2.34 4.32 o 0 8 4 0.00 0.15 0.01 o 1 8 4 95.85 90.07 2.92 o 2 8 4 45.75 47.72 2.28 o 3 8 4 35.55 37.89 1.58 o 4 8 4 33.85 39.17 2.53 o 5 8 4 58.35 44.76 4.43 o 6 8 4 -5.55 0.98 3.73 o 0 9 4 123.70 130.57 4.00 o 1 9 4 19.80 20.80 1.22 o 2 9 4 22.85 21.82 1.90 o 3 9 4 11.75 10.16 1.14 o 4 9 4 48.70 48.68 2.59 o 5 9 4 14.00 14.83 2.69 o 6 9 4 4.00 5.74 4.48 o 0 10 4 33.40 32.78 1.90 o 1 10 4 96.90 99.62 3.41 o 2 10 4 13.40 12.41 1.55 o 3 10 4 33.90 31.51 2.19 o 4 10 4 0.85 1.39 0.94 o 5 10 4 22.95 22.51 5.58 o 0 11 4 4.70 4.64 1.30 o 1 11 4 11.15 14.10 1.51 o 2 11 4 27.20 26.54 1.81 o 3 11 4 5.75 4.92 1.37 o 4 11 4 20.90 21.14 4.10 o 5 11 4 2.15 5.00 4.90 o 0 12 4 6.80 6.07 1.60 o 1 12 4 34.75 34.82 2.10 o 2 12 4 3.35 3.14 1.97 o 3 12 4 4.25 5.38 1.90 o 4 12 4 5.40 3.09 3.10 o 0 13 4 3.80 2.20 2.80 o 1 13 4 11.90 13.18 3.65 o 2 13 4 72.70 65.45 4.60 o 1 0 5 2.00 1.67 0.30 o 2 0 5 66.40 67.14 1.60 o 3 0 5 2.00 1.32 0.50 o 4 0 5 157.10 149.02 4.60 o 5 0 5 153.10 147.12 5.80 o 6 0 5 60.80 68.97 2.70 o 7 0 5 10.10 11.86 1.40 o 8 0 5 13.40 13.59 4.00 o 0 1 5 49.60 45.51 1.90 o 1 1 5 251.00 260.57 7.37 o 2 1 5 16.35 16.40 0.55 o 3 1 5 1024.90 1008.81 18.96 o 4 1 5 51.95 50.85 1.61 o 5 1 5 323.05 341.66 11.39 o 6 1 5 44.40 46.94 2.51 o 7 1 5 38.80 40.02 2.06 o 8 1 5 1.60 0.82 2.59 o 0 2 5 906.40 910.85 27.80 o 1 2 5 399.20 388.72 10.65 o 2 2 5 823.25 808.97 16.46 o 3 2 5 181.45 169.27 3.60 o 4 2 5 68.40 63.99 2.29 o 5 2 5 46.70 45.82 2.22 o 6 2 5 1.50 1.28 1.02 o 7 2 5 20.00 17.99 1.35 o 8 2 5 -0.30 2.01 3.86 o 0 3 5 202.60 218.61 6.40 o 1 3 5 112.30 115.78 2.91 o 2 3 5 264.90 254.55 5.81 o 3 3 5 385.15 367.89 8.75 o 4 3 5 8.85 9.20 1.97 o 5 3 5 10.50 12.58 1.72 o 6 3 5 55.95 56.27 3.81 o 7 3 5 6.65 6.25 2.64 o 8 3 5 8.15 10.30 3.45 o 0 4 5 88.30 94.28 2.30 o 1 4 5 55.25 50.64 1.90 o 2 4 5 1202.05 1177.83 24.43 o 3 4 5 76.50 77.28 2.32 o 4 4 5 14.40 12.92 1.88 o 5 4 5 -0.65 2.28 1.59 o 6 4 5 24.80 24.22 3.54 o 7 4 5 13.15 9.78 2.84 o 0 5 5 405.50 442.81 9.50 o 1 5 5 403.50 403.00 10.41 o 2 5 5 35.00 32.69 1.53 o 3 5 5 11.75 9.74 0.79 o 4 5 5 111.45 114.39 5.00 o 5 5 5 86.45 90.61 4.40 o 6 5 5 14.90 17.77 2.84 o 7 5 5 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1.90 o 3 9 10 26.80 29.22 2.29 o 4 9 10 3.60 4.67 2.50 o 0 10 10 5.70 18.58 5.00 o 1 10 10 32.50 32.41 4.08 o 2 10 10 30.75 31.80 2.41 o 3 10 10 21.15 19.68 2.55 o 4 10 10 7.40 9.01 2.40 o 0 11 10 7.40 0.45 4.60 o 1 11 10 6.90 3.42 4.62 o 2 11 10 10.50 12.99 2.10 o 1 0 11 15.40 14.71 1.00 o 2 0 11 1.00 0.93 1.40 o 3 0 11 58.60 58.78 2.00 o 4 0 11 13.10 11.99 1.10 o 5 0 11 19.20 18.03 1.40 o 6 0 11 0.10 0.34 0.70 o 0 1 11 102.10 96.62 3.60 o 1 1 11 41.80 45.60 1.35 o 2 1 11 63.90 65.28 2.10 o 3 1 11 96.10 98.67 2.80 o 4 1 11 45.30 47.52 1.85 o 5 1 11 86.90 80.34 3.15 o 6 1 11 -0.20 0.14 1.95 o 0 2 11 2.90 3.30 0.70 o 1 2 11 34.65 35.67 1.30 o 2 2 11 20.70 21.41 1.15 o 3 2 11 61.50 62.76 2.21 o 4 2 11 44.70 45.60 2.10 o 5 2 11 11.50 9.16 1.36 o 6 2 11 17.95 17.02 2.62 o 0 3 11 402.00 398.76 11.30 o 1 3 11 182.90 181.24 4.71 o 2 3 11 29.50 28.90 1.30 o 3 3 11 169.75 170.59 5.21 o 4 3 11 36.30 37.42 2.10 o 5 3 11 1.30 0.17 2.99 o 6 3 11 5.30 5.70 1.80 o 0 4 11 101.70 100.21 3.40 o 1 4 11 136.40 128.73 3.40 o 2 4 11 58.05 56.09 2.15 o 3 4 11 30.80 33.31 1.60 o 4 4 11 16.70 13.53 2.80 o 5 4 11 29.40 30.56 3.60 o 6 4 11 -0.70 1.46 2.18 o 0 5 11 315.50 297.53 9.70 o 1 5 11 69.80 69.01 2.25 o 2 5 11 5.85 7.83 1.08 o 3 5 11 45.50 46.82 3.67 o 4 5 11 16.05 16.78 2.91 o 5 5 11 86.25 86.15 6.65 o 6 5 11 10.00 11.14 2.00 o 0 6 11 96.20 92.85 2.60 o 1 6 11 111.25 110.73 4.43 o 2 6 11 3.60 3.37 1.08 o 3 6 11 14.60 14.84 3.77 o 4 6 11 55.80 50.51 4.57 o 5 6 11 51.90 51.05 3.90 o 0 7 11 1.70 0.29 1.50 o 1 7 11 5.25 5.80 1.14 o 2 7 11 9.25 10.88 1.61 o 3 7 11 4.60 4.49 2.68 o 4 7 11 11.90 10.92 3.67 o 5 7 11 29.30 29.72 5.10 o 0 8 11 4.70 5.46 1.60 o 1 8 11 27.55 27.56 2.06 o 2 8 11 6.65 6.51 1.62 o 3 8 11 48.75 41.68 2.96 o 4 8 11 94.50 86.19 5.80 o 0 9 11 15.00 20.89 2.60 o 1 9 11 18.70 19.31 2.04 o 2 9 11 7.15 6.35 1.52 o 3 9 11 4.25 4.01 1.61 o 4 9 11 -0.50 1.89 2.83 o 0 10 11 3.20 2.23 5.80 o 1 10 11 1.35 0.69 4.40 o 2 10 11 5.30 5.64 3.56 o 3 10 11 -0.40 0.45 4.55 o 0 11 11 4.40 0.07 7.10 o 1 11 11 25.25 20.95 6.63 o 2 11 11 -2.70 1.85 6.70 o 0 0 12 -2.50 0.03 1.10 o 1 0 12 216.40 221.81 6.30 o 2 0 12 20.30 23.78 1.10 o 3 0 12 83.60 87.21 2.50 o 4 0 12 6.20 5.97 0.90 o 5 0 12 6.60 9.52 1.00 o 6 0 12 5.10 4.26 1.40 o 0 1 12 5.10 6.99 1.00 o 1 1 12 56.15 53.65 1.95 o 2 1 12 311.60 299.25 8.15 o 3 1 12 29.90 34.91 1.60 o 4 1 12 30.35 30.78 1.60 o 5 1 12 0.85 2.36 1.75 o 6 1 12 12.10 13.26 1.73 o 0 2 12 19.20 16.46 1.10 o 1 2 12 265.80 272.15 6.70 o 2 2 12 0.45 0.13 0.99 o 3 2 12 81.05 85.90 2.95 o 4 2 12 20.40 19.27 1.45 o 5 2 12 5.50 5.15 1.30 o 6 2 12 35.55 35.57 3.86 o 0 3 12 233.60 218.86 6.50 o 1 3 12 42.15 44.63 1.85 o 2 3 12 351.65 334.97 9.75 o 3 3 12 112.10 115.24 3.75 o 4 3 12 18.45 23.32 1.50 o 5 3 12 11.20 11.00 1.84 o 6 3 12 7.35 8.89 2.20 o 0 4 12 34.70 35.15 1.80 o 1 4 12 333.00 335.20 9.07 o 2 4 12 31.95 31.63 1.50 o 3 4 12 38.15 42.09 1.91 o 4 4 12 17.50 14.70 3.81 o 5 4 12 20.85 19.72 3.69 o 6 4 12 9.60 7.00 2.20 o 0 5 12 570.80 570.17 19.70 o 1 5 12 7.70 8.05 0.92 o 2 5 12 52.55 49.72 2.65 o 3 5 12 29.40 33.88 3.26 o 4 5 12 29.70 27.99 4.53 o 5 5 12 16.60 17.96 3.96 o 0 6 12 1.10 1.28 0.60 o 1 6 12 269.00 260.44 9.14 o 2 6 12 6.40 8.06 1.22 o 3 6 12 3.10 3.24 2.92 o 4 6 12 19.95 21.48 3.87 o 5 6 12 64.80 69.33 6.61 o 0 7 12 80.90 81.28 3.00 o 1 7 12 5.35 5.90 1.55 o 2 7 12 0.30 0.95 1.43 o 3 7 12 -0.20 2.75 4.16 o 4 7 12 6.05 5.48 5.49 o 0 8 12 0.80 1.60 3.22 o 1 8 12 75.65 71.53 4.04 o 2 8 12 3.30 4.41 1.52 o 3 8 12 30.55 28.97 4.72 o 4 8 12 11.00 17.01 4.75 o 0 9 12 5.00 0.66 5.80 o 1 9 12 14.05 14.57 5.10 o 2 9 12 0.40 0.76 5.48 o 3 9 12 3.70 1.51 4.28 o 0 10 12 22.90 29.51 6.10 o 1 10 12 18.85 16.00 5.92 o 2 10 12 3.10 1.16 3.96 o 1 0 13 233.40 226.46 7.10 o 2 0 13 24.80 24.72 1.60 o 3 0 13 2.40 2.12 0.90 o 4 0 13 2.50 1.85 1.10 o 5 0 13 3.90 4.45 1.10 o 6 0 13 54.90 53.36 4.30 o 0 1 13 10.60 12.82 1.20 o 1 1 13 66.30 65.38 2.30 o 2 1 13 67.00 66.68 2.50 o 3 1 13 28.10 28.87 1.55 o 4 1 13 31.30 32.47 1.95 o 5 1 13 1.60 3.76 1.55 o 6 1 13 35.00 33.88 3.25 o 0 2 13 22.20 20.75 1.60 o 1 2 13 88.70 86.36 2.75 o 2 2 13 116.75 114.35 4.15 o 3 2 13 0.45 1.67 1.43 o 4 2 13 24.80 25.26 1.77 o 5 2 13 10.10 10.11 1.78 o 0 3 13 32.30 35.06 1.90 o 1 3 13 251.60 243.64 7.25 o 2 3 13 31.00 31.21 1.60 o 3 3 13 65.25 60.98 2.75 o 4 3 13 7.95 9.16 1.46 o 5 3 13 7.40 6.10 2.06 o 0 4 13 35.60 34.49 1.80 o 1 4 13 6.40 6.68 0.95 o 2 4 13 7.55 8.09 1.10 o 3 4 13 1.55 1.40 1.08 o 4 4 13 7.80 8.43 1.69 o 5 4 13 6.50 5.51 2.00 o 0 5 13 0.70 1.08 1.51 o 1 5 13 109.20 107.90 3.81 o 2 5 13 29.25 32.83 2.35 o 3 5 13 14.00 12.62 3.16 o 4 5 13 11.30 9.62 3.26 o 5 5 13 3.60 4.59 5.08 o 0 6 13 117.50 111.32 3.70 o 1 6 13 11.00 12.32 1.16 o 2 6 13 47.30 49.61 2.95 o 3 6 13 0.60 0.53 3.59 o 4 6 13 28.65 24.59 5.85 o 0 7 13 22.60 23.32 1.80 o 1 7 13 44.35 46.37 2.36 o 2 7 13 5.55 6.72 1.65 o 3 7 13 16.90 14.63 4.12 o 4 7 13 5.50 2.53 3.99 o 0 8 13 151.20 133.37 8.50 o 1 8 13 2.50 3.55 3.02 o 2 8 13 17.85 20.12 4.12 o 3 8 13 6.60 5.67 5.31 o 0 9 13 0.20 3.13 1.43 o 1 9 13 19.70 24.65 4.94 o 2 9 13 62.00 53.02 6.58 o 0 10 13 15.60 17.06 2.60 o 1 10 13 5.70 5.91 4.02 o 0 0 14 445.20 418.87 22.50 o 1 0 14 90.60 96.87 3.60 o 2 0 14 61.00 59.20 2.80 o 3 0 14 4.00 5.90 1.40 o 4 0 14 58.30 59.56 2.90 o 5 0 14 69.50 65.11 3.50 o 0 1 14 23.20 24.49 1.80 o 1 1 14 28.05 26.27 1.65 o 2 1 14 19.75 19.53 1.40 o 3 1 14 43.55 42.51 2.25 o 4 1 14 11.75 12.72 1.71 o 5 1 14 35.45 37.79 2.94 o 0 2 14 246.70 239.28 9.20 o 1 2 14 87.05 89.14 3.26 o 2 2 14 13.40 13.23 1.30 o 3 2 14 55.65 58.09 2.75 o 4 2 14 53.10 57.10 3.01 o 5 2 14 99.15 90.16 5.64 o 0 3 14 52.60 53.56 2.50 o 1 3 14 12.00 13.54 1.25 o 2 3 14 19.90 21.75 1.60 o 3 3 14 5.80 6.51 1.10 o 4 3 14 1.85 0.96 1.57 o 5 3 14 9.05 12.75 2.16 o 0 4 14 21.60 26.83 1.70 o 1 4 14 27.05 29.95 1.70 o 2 4 14 4.80 5.45 1.10 o 3 4 14 2.60 3.05 1.78 o 4 4 14 7.60 8.13 2.00 o 5 4 14 12.55 13.64 2.71 o 0 5 14 30.40 28.16 1.70 o 1 5 14 15.20 15.65 1.32 o 2 5 14 9.55 11.28 1.96 o 3 5 14 3.25 3.64 1.51 o 4 5 14 14.80 16.03 2.55 o 0 6 14 0.60 0.56 0.93 o 1 6 14 8.15 9.70 1.90 o 2 6 14 4.90 6.04 1.51 o 3 6 14 22.25 26.68 2.38 o 4 6 14 5.45 6.66 4.18 o 0 7 14 57.70 59.03 3.90 o 1 7 14 37.20 40.39 5.94 o 2 7 14 8.95 9.99 1.84 o 3 7 14 -0.95 1.52 5.20 o 0 8 14 -1.40 0.18 1.70 o 1 8 14 14.05 16.09 2.49 o 2 8 14 3.85 2.77 4.24 o 0 9 14 31.30 34.54 3.00 o 1 9 14 53.45 52.97 4.26 o 1 0 15 213.60 200.21 8.60 o 2 0 15 11.50 11.32 1.50 o 3 0 15 14.30 15.19 1.90 o 4 0 15 15.60 17.44 1.90 o 0 1 15 68.60 68.43 3.60 o 1 1 15 2.35 2.06 1.05 o 2 1 15 11.60 12.19 1.55 o 3 1 15 26.60 26.61 2.15 o 4 1 15 7.90 8.79 1.71 o 0 2 15 60.80 57.75 3.40 o 1 2 15 75.30 76.90 3.45 o 2 2 15 10.45 11.55 1.30 o 3 2 15 13.25 13.64 1.65 o 4 2 15 31.30 31.55 2.93 o 0 3 15 2.30 2.85 1.20 o 1 3 15 0.15 1.11 1.45 o 2 3 15 17.70 15.81 1.85 o 3 3 15 7.05 10.62 1.71 o 4 3 15 2.25 2.02 4.09 o 0 4 15 4.30 5.22 1.20 o 1 4 15 27.85 26.54 1.95 o 2 4 15 1.40 3.74 2.28 o 3 4 15 2.10 2.72 1.90 o 4 4 15 7.40 10.19 2.20 o 0 5 15 7.00 5.58 1.60 o 1 5 15 6.75 11.57 2.16 o 2 5 15 9.95 10.83 1.95 o 3 5 15 3.35 6.91 2.03 o 0 6 15 21.20 20.62 2.90 o 1 6 15 39.15 37.79 2.86 o 2 6 15 4.20 4.56 1.96 o 3 6 15 19.50 22.35 2.85 o 0 7 15 0.80 0.00 4.47 o 1 7 15 12.45 15.53 2.30 o 2 7 15 18.90 18.13 2.83 o 0 8 15 13.90 10.70 3.10 o 1 8 15 2.20 4.53 2.25 o 0 0 16 48.80 49.36 4.40 o 1 0 16 2.30 0.88 1.70 o 2 0 16 9.20 8.10 1.50 o 3 0 16 1.70 4.31 2.10 o 4 0 16 2.30 0.95 2.10 o 0 1 16 15.30 14.45 2.00 o 1 1 16 18.50 21.02 1.75 o 2 1 16 23.20 25.36 2.31 o 3 1 16 9.85 10.73 2.00 o 4 1 16 3.05 6.12 2.43 o 0 2 16 0.50 1.70 2.83 o 1 2 16 20.50 20.43 2.26 o 2 2 16 11.30 12.42 1.75 o 3 2 16 3.55 2.36 2.00 o 4 2 16 8.25 8.53 2.47 o 0 3 16 5.70 3.49 1.80 o 1 3 16 2.50 2.87 1.45 o 2 3 16 32.10 30.54 3.00 o 3 3 16 1.05 0.99 3.67 o 0 4 16 85.60 75.46 5.20 o 1 4 16 0.65 1.48 2.24 o 2 4 16 5.90 6.90 2.32 o 3 4 16 2.65 2.30 1.98 o 0 5 16 25.20 28.77 2.80 o 1 5 16 9.25 12.66 2.16 o 2 5 16 5.85 4.23 2.10 o 0 6 16 9.20 9.14 2.00 o 1 6 16 3.55 5.73 2.06 o 2 6 16 -0.60 0.94 3.41 o 0 7 16 2.50 4.87 2.30 o 1 0 17 5.30 8.82 1.60 o 2 0 17 0.80 0.09 2.86 o 3 0 17 0.30 0.49 2.30 o 0 1 17 57.10 64.76 3.50 o 1 1 17 6.60 8.28 1.70 o 2 1 17 11.95 14.88 2.11 o 3 1 17 -0.30 0.50 3.33 o 0 2 17 13.70 15.38 2.00 o 1 2 17 15.60 18.33 2.36 o 2 2 17 3.15 1.68 2.37 o 3 2 17 2.80 3.43 4.16 o 0 3 17 2.50 0.00 1.80 o 1 3 17 11.30 14.59 2.20 o 2 3 17 14.50 12.90 2.45 o 0 4 17 3.80 1.00 2.50 o 1 4 17 21.45 20.65 3.11 o 2 4 17 0.50 1.70 2.82 o 0 5 17 -1.80 0.07 2.40 o 1 5 17 -0.60 0.08 2.87 o 0 0 18 188.50 178.99 11.00 o 1 0 18 46.70 45.60 4.20 o 0 1 18 5.60 6.98 2.10 o 1 1 18 11.55 11.53 2.90 o 0 2 18 170.10 158.49 10.00 o 1 2 18 24.60 35.46 4.45 o