#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/47/2214788.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214788_Fobs loop_ _publ_author_name 'Sarojini, B. K.' 'Yathirajan, H. S.' 'Mayekar, A. N.' 'Narayana, B.' 'Bolte, Michael' _publ_section_title ; (2E)-1-(2,4-Dichlorophenyl)-3-(quinolin-8-yl)prop-2-en-1-one ; _journal_coeditor_code LH2452 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3488 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.181 _cell_angle_gamma 90.000 _cell_length_a 11.9121 _cell_length_b 10.7112 _cell_length_c 12.7824 _exptl_crystal_F_000 672.00 _reflns_d_resolution_high 0.8213 _[local]_cod_data_source_file lh2452Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yat96 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 166.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10236.47 11952.66 691.18 o 3 0 0 1334.21 1172.50 116.42 o 4 0 0 3182.34 3135.17 255.82 o 5 0 0 58.44 50.62 3.75 o 6 0 0 1523.06 1829.43 105.55 o 7 0 0 407.17 463.09 9.14 o 8 0 0 1110.18 1180.48 244.16 o 9 0 0 301.49 311.36 60.11 o 10 0 0 739.51 747.29 294.10 o 11 0 0 762.76 679.18 352.84 o 12 0 0 15.73 9.46 9.44 o 13 0 0 119.04 94.91 50.14 o 2 1 0 2159.52 1662.05 145.89 o 3 1 0 3998.16 3098.46 225.09 o 4 1 0 1764.52 1665.42 92.76 o 5 1 0 436.74 429.19 39.95 o 6 1 0 279.39 270.01 38.24 o 7 1 0 604.41 526.37 64.79 o 8 1 0 235.21 221.21 23.27 o 9 1 0 329.31 285.85 29.44 o 10 1 0 284.36 265.26 29.28 o 11 1 0 0.95 -5.67 5.67 o 12 1 0 165.54 135.43 35.14 o 13 1 0 0.96 3.74 5.55 o 0 2 0 1197.10 897.11 64.79 o 1 2 0 5128.69 5678.79 146.48 o 2 2 0 337.48 315.78 13.90 o 3 2 0 3628.24 3686.58 152.42 o 4 2 0 1640.02 1588.31 222.68 o 5 2 0 10.03 24.69 5.15 o 6 2 0 593.70 608.62 44.00 o 7 2 0 1663.15 1731.03 253.02 o 8 2 0 119.94 117.08 16.19 o 9 2 0 751.05 686.13 95.94 o 10 2 0 398.55 362.08 43.74 o 11 2 0 9.01 6.49 4.87 o 12 2 0 41.67 34.56 7.57 o 13 2 0 0.09 0.18 6.47 o 1 3 0 1023.94 912.47 73.72 o 2 3 0 116.37 121.58 5.08 o 3 3 0 7.11 11.27 1.57 o 4 3 0 381.51 398.92 29.64 o 5 3 0 35.17 33.05 2.69 o 6 3 0 516.91 505.39 67.60 o 7 3 0 14.29 21.77 3.27 o 8 3 0 174.60 150.81 26.10 o 9 3 0 115.50 97.81 4.84 o 10 3 0 42.24 30.45 6.10 o 11 3 0 81.35 81.40 9.56 o 12 3 0 32.67 16.04 6.04 o 0 4 0 0.45 1.77 1.27 o 1 4 0 1226.58 1226.28 85.63 o 2 4 0 442.49 418.84 31.92 o 3 4 0 1537.05 1663.99 51.19 o 4 4 0 1052.42 994.35 61.78 o 5 4 0 51.72 62.25 6.26 o 6 4 0 101.48 90.60 8.47 o 7 4 0 631.72 659.31 36.92 o 8 4 0 2612.04 2628.65 183.83 o 9 4 0 122.18 134.10 8.68 o 10 4 0 12.41 15.04 5.14 o 11 4 0 50.49 37.77 6.26 o 12 4 0 0.04 -1.21 4.72 o 1 5 0 590.13 673.84 59.25 o 2 5 0 1087.82 1211.03 72.27 o 3 5 0 3441.60 3099.04 654.24 o 4 5 0 10.49 8.29 2.61 o 5 5 0 189.39 224.55 15.60 o 6 5 0 301.72 289.36 23.40 o 7 5 0 6.73 7.96 3.00 o 8 5 0 0.07 11.97 4.37 o 9 5 0 123.27 119.54 14.13 o 10 5 0 149.06 142.24 14.57 o 11 5 0 21.77 21.77 5.38 o 12 5 0 187.40 190.83 11.59 o 0 6 0 8037.57 7964.92 294.91 o 1 6 0 1813.41 1780.64 173.11 o 2 6 0 103.63 96.10 10.38 o 3 6 0 3.72 7.36 2.38 o 4 6 0 381.20 417.90 30.64 o 5 6 0 1650.08 1710.32 147.29 o 6 6 0 693.30 735.54 56.08 o 7 6 0 149.29 169.02 16.13 o 8 6 0 30.46 32.80 4.54 o 9 6 0 253.28 226.56 20.56 o 10 6 0 329.78 329.09 21.30 o 11 6 0 452.64 395.77 60.25 o 1 7 0 34.81 36.83 3.31 o 2 7 0 1358.31 1326.27 104.96 o 3 7 0 201.93 222.44 25.17 o 4 7 0 136.79 145.02 7.86 o 5 7 0 332.36 389.40 44.61 o 6 7 0 226.91 248.15 41.09 o 7 7 0 97.58 109.06 8.60 o 8 7 0 14.55 12.16 4.72 o 9 7 0 407.22 409.55 48.80 o 10 7 0 53.94 51.34 10.07 o 11 7 0 114.15 100.54 15.74 o 0 8 0 11.76 9.67 4.73 o 1 8 0 4.15 11.65 4.80 o 2 8 0 677.25 783.84 28.98 o 3 8 0 351.61 341.62 19.84 o 4 8 0 0.33 4.36 3.35 o 5 8 0 970.21 975.28 90.86 o 6 8 0 394.43 420.60 60.46 o 7 8 0 608.00 654.72 68.22 o 8 8 0 269.29 309.23 29.93 o 9 8 0 57.89 46.26 11.07 o 10 8 0 8.57 1.17 4.38 o 1 9 0 6.23 11.72 3.49 o 2 9 0 143.52 160.71 6.41 o 3 9 0 0.51 0.43 4.16 o 4 9 0 605.92 654.78 31.07 o 5 9 0 12.49 6.00 4.25 o 6 9 0 57.57 61.74 6.44 o 7 9 0 0.87 0.42 4.49 o 8 9 0 49.77 48.88 5.37 o 9 9 0 191.22 191.76 22.24 o 0 10 0 74.61 101.82 10.69 o 1 10 0 5.11 4.78 4.19 o 2 10 0 45.51 50.63 5.07 o 3 10 0 541.24 603.84 89.57 o 4 10 0 12.16 12.24 5.32 o 5 10 0 2.35 -1.76 4.29 o 6 10 0 88.42 91.03 12.46 o 7 10 0 452.16 430.59 33.95 o 8 10 0 536.78 608.62 70.54 o 1 11 0 490.51 611.52 83.77 o 2 11 0 291.29 365.97 26.29 o 3 11 0 209.11 224.32 41.99 o 4 11 0 27.97 26.46 5.38 o 5 11 0 2.03 8.09 5.59 o 6 11 0 25.99 17.88 5.31 o 7 11 0 11.68 3.78 7.55 o 0 12 0 238.09 402.00 221.72 o 1 12 0 422.06 578.84 89.81 o 2 12 0 50.24 42.84 14.06 o 3 12 0 204.94 192.82 50.75 o 4 12 0 66.16 69.27 10.72 o 5 12 0 59.22 77.83 11.16 o -13 1 1 125.01 102.59 21.93 o -12 1 1 4.15 3.96 5.49 o -11 1 1 117.33 100.28 16.23 o -10 1 1 8.19 6.96 4.70 o -9 1 1 852.50 966.20 42.47 o -8 1 1 130.27 124.82 5.89 o -7 1 1 11.49 17.30 5.07 o -6 1 1 1440.94 1487.47 104.64 o -5 1 1 1863.34 1885.13 89.11 o -4 1 1 4585.30 4841.87 358.72 o -3 1 1 238.95 241.13 12.02 o -2 1 1 143.27 134.01 7.20 o 1 1 1 2982.06 2172.55 52.30 o 2 1 1 9469.96 8388.97 497.25 o 3 1 1 2565.27 1904.47 90.89 o 4 1 1 853.74 693.69 49.07 o 5 1 1 0.58 3.72 1.97 o 6 1 1 113.95 79.53 5.85 o 7 1 1 1596.08 1364.15 147.52 o 8 1 1 23.24 18.33 3.07 o 9 1 1 224.42 180.79 14.58 o 10 1 1 789.81 786.35 116.29 o 11 1 1 51.29 47.11 11.12 o 12 1 1 123.57 99.00 24.76 o -13 2 1 777.96 710.02 96.23 o -12 2 1 160.44 159.91 17.65 o -11 2 1 68.60 69.94 6.47 o -10 2 1 272.03 268.09 23.03 o -9 2 1 216.35 226.21 13.36 o -8 2 1 725.50 615.57 124.85 o -7 2 1 301.46 270.29 16.18 o -6 2 1 226.44 354.67 11.49 o -5 2 1 5547.14 6678.70 362.06 o -4 2 1 937.78 1054.19 60.43 o -3 2 1 4644.89 5146.06 181.00 o -2 2 1 0.21 2.80 1.57 o -1 2 1 962.23 820.86 71.16 o 0 2 1 3192.75 2529.78 130.17 o 1 2 1 6347.00 5633.90 452.46 o 2 2 1 1701.88 1284.63 56.07 o 3 2 1 231.62 155.87 14.11 o 4 2 1 1451.91 1206.92 70.46 o 5 2 1 239.57 212.61 30.40 o 6 2 1 1353.52 1308.12 109.18 o 7 2 1 443.20 463.05 44.01 o 8 2 1 89.55 86.85 10.22 o 9 2 1 123.66 108.38 10.58 o 10 2 1 0.47 2.12 4.42 o 11 2 1 235.94 235.17 34.86 o 12 2 1 13.50 7.66 5.35 o -13 3 1 288.53 272.58 36.38 o -12 3 1 27.48 18.38 5.56 o -11 3 1 455.18 408.28 31.64 o -10 3 1 169.34 167.27 18.13 o -9 3 1 207.21 180.74 28.34 o -8 3 1 2607.34 2496.66 115.93 o -7 3 1 1535.37 1585.42 63.26 o -6 3 1 1265.97 1397.22 49.08 o -5 3 1 2471.32 2820.10 152.79 o -4 3 1 1464.27 1592.21 76.64 o -3 3 1 33.41 43.34 2.92 o -2 3 1 782.89 754.43 63.44 o -1 3 1 778.72 670.37 43.30 o 0 3 1 334.98 265.48 24.12 o 1 3 1 291.17 257.02 12.49 o 2 3 1 3997.32 3308.96 347.30 o 3 3 1 4175.66 3953.76 282.52 o 4 3 1 1835.08 1547.20 93.93 o 5 3 1 993.58 954.52 52.80 o 6 3 1 129.56 121.42 13.34 o 7 3 1 277.39 268.22 14.95 o 8 3 1 265.60 293.04 15.24 o 9 3 1 49.27 47.62 9.16 o 10 3 1 3.01 1.92 4.13 o 11 3 1 90.73 81.60 14.29 o 12 3 1 169.67 142.57 25.82 o -13 4 1 447.45 438.15 17.02 o -12 4 1 148.54 144.20 18.59 o -11 4 1 129.13 126.20 14.29 o -10 4 1 305.92 315.18 32.21 o -9 4 1 772.12 761.36 59.59 o -8 4 1 113.74 123.28 14.59 o -7 4 1 1389.76 1231.27 136.25 o -6 4 1 944.93 980.76 86.58 o -5 4 1 286.82 328.90 18.88 o -4 4 1 24.88 25.24 2.65 o -3 4 1 1281.03 1381.97 35.64 o -2 4 1 2210.16 2296.28 97.43 o -1 4 1 152.60 116.53 6.85 o 0 4 1 556.10 507.82 33.69 o 1 4 1 664.02 592.72 40.99 o 2 4 1 894.61 861.97 72.17 o 3 4 1 111.85 121.73 14.13 o 4 4 1 1462.78 1320.45 115.48 o 5 4 1 0.54 1.73 2.37 o 6 4 1 140.36 130.35 8.54 o 7 4 1 308.69 307.06 28.60 o 8 4 1 889.28 834.02 59.89 o 9 4 1 2.47 -0.73 3.74 o 10 4 1 36.11 26.87 4.97 o 11 4 1 46.36 63.17 12.90 o 12 4 1 119.58 125.88 20.29 o -12 5 1 5.28 2.56 5.18 o -11 5 1 211.67 180.89 30.79 o -10 5 1 235.68 218.35 40.56 o -9 5 1 19.56 15.72 4.19 o -8 5 1 1.93 2.74 3.70 o -7 5 1 586.42 602.15 58.70 o -6 5 1 386.77 387.50 13.19 o -5 5 1 1637.74 1769.72 112.27 o -4 5 1 1422.50 1506.38 101.51 o -3 5 1 120.77 121.27 5.62 o -2 5 1 169.76 185.18 14.84 o -1 5 1 1140.71 1090.92 52.00 o 0 5 1 304.98 267.59 26.93 o 1 5 1 1365.56 1317.97 81.41 o 2 5 1 124.84 118.22 7.16 o 3 5 1 343.55 352.07 26.25 o 4 5 1 660.18 715.27 42.99 o 5 5 1 1051.74 1165.57 117.77 o 6 5 1 126.94 135.69 7.45 o 7 5 1 13.84 17.49 3.42 o 8 5 1 101.07 95.07 11.67 o 9 5 1 18.44 21.34 4.48 o 10 5 1 119.08 120.50 15.05 o 11 5 1 126.70 126.86 12.20 o -12 6 1 35.32 22.22 6.77 o -11 6 1 5.95 4.71 5.46 o -10 6 1 60.30 50.62 7.18 o -9 6 1 87.38 93.46 9.62 o -8 6 1 0.72 7.56 4.08 o -7 6 1 100.98 103.24 8.53 o -6 6 1 425.02 397.01 51.74 o -5 6 1 399.43 381.23 56.26 o -4 6 1 112.94 130.15 8.02 o -3 6 1 315.02 318.03 21.64 o -2 6 1 323.05 309.97 27.26 o -1 6 1 1989.58 2020.26 99.24 o 0 6 1 773.09 882.08 52.79 o 1 6 1 164.34 178.65 11.38 o 2 6 1 48.06 67.44 8.24 o 3 6 1 98.45 132.67 10.36 o 4 6 1 18.73 15.62 3.21 o 5 6 1 12.45 9.39 3.40 o 6 6 1 1224.34 1269.04 125.84 o 7 6 1 483.96 582.24 72.82 o 8 6 1 884.84 864.43 85.52 o 9 6 1 58.61 59.39 9.49 o 10 6 1 94.76 101.39 12.55 o 11 6 1 31.08 19.46 7.80 o -11 7 1 124.53 116.38 9.53 o -10 7 1 124.72 114.26 10.75 o -9 7 1 117.39 118.90 14.53 o -8 7 1 13.63 8.43 4.64 o -7 7 1 189.87 221.84 18.32 o -6 7 1 1593.62 1690.62 107.23 o -5 7 1 960.27 1032.82 74.68 o -4 7 1 75.09 77.94 7.45 o -3 7 1 455.70 506.72 25.42 o -2 7 1 16.73 11.55 2.93 o -1 7 1 925.37 947.39 69.43 o 0 7 1 140.65 114.39 4.31 o 1 7 1 1.82 4.97 3.00 o 2 7 1 908.22 1050.79 142.56 o 3 7 1 79.06 66.25 4.55 o 4 7 1 597.36 686.47 57.49 o 5 7 1 565.74 500.74 45.73 o 6 7 1 42.47 47.00 4.02 o 7 7 1 250.89 242.94 19.11 o 8 7 1 1.93 7.67 4.67 o 9 7 1 29.65 26.40 7.17 o 10 7 1 152.72 143.09 26.76 o -10 8 1 298.29 348.80 42.20 o -9 8 1 156.58 145.31 18.06 o -8 8 1 702.01 682.38 72.98 o -7 8 1 76.54 80.02 5.97 o -6 8 1 476.21 490.80 42.53 o -5 8 1 2001.88 1995.91 192.34 o -4 8 1 120.56 111.19 8.50 o -3 8 1 121.82 113.69 7.11 o -2 8 1 233.08 228.96 18.03 o -1 8 1 1.55 6.70 3.00 o 0 8 1 645.44 734.94 28.45 o 1 8 1 680.03 771.21 50.51 o 2 8 1 124.37 123.24 17.72 o 3 8 1 83.86 83.64 6.71 o 4 8 1 366.59 387.71 42.10 o 5 8 1 187.65 198.25 20.03 o 6 8 1 24.91 15.50 3.97 o 7 8 1 5.43 8.63 4.25 o 8 8 1 2.23 0.87 4.92 o 9 8 1 20.39 21.84 5.49 o 10 8 1 47.32 46.24 8.62 o -9 9 1 280.31 272.46 31.97 o -8 9 1 48.70 57.92 7.71 o -7 9 1 250.43 243.79 20.78 o -6 9 1 773.42 794.31 65.13 o -5 9 1 88.94 91.71 9.18 o -4 9 1 7.86 10.94 4.01 o -3 9 1 220.36 207.49 22.59 o -2 9 1 5.94 13.40 3.50 o -1 9 1 81.10 99.39 4.95 o 0 9 1 145.54 143.68 12.75 o 1 9 1 0.63 2.09 3.77 o 2 9 1 848.29 923.38 53.30 o 3 9 1 295.99 308.65 35.15 o 4 9 1 656.30 603.07 13.70 o 5 9 1 11.63 17.82 4.75 o 6 9 1 42.22 42.64 6.40 o 7 9 1 60.33 54.58 11.46 o 8 9 1 0.57 0.95 5.14 o 9 9 1 0.78 4.43 4.75 o -8 10 1 68.93 68.85 10.95 o -7 10 1 19.77 12.80 4.64 o -6 10 1 258.26 235.50 24.98 o -5 10 1 284.21 271.20 23.06 o -4 10 1 1.80 3.88 4.52 o -3 10 1 17.14 30.31 5.34 o -2 10 1 1923.59 2171.10 266.53 o -1 10 1 56.46 78.38 12.89 o 0 10 1 39.91 44.93 5.94 o 1 10 1 105.03 109.86 21.42 o 2 10 1 77.12 90.88 7.89 o 3 10 1 3.88 8.79 4.63 o 4 10 1 14.96 14.93 4.71 o 5 10 1 23.40 32.34 6.55 o 6 10 1 0.28 2.72 4.41 o 7 10 1 64.99 72.99 11.81 o 8 10 1 274.53 280.45 20.81 o -7 11 1 119.87 108.82 17.26 o -6 11 1 33.71 30.90 6.99 o -5 11 1 26.21 25.74 5.81 o -4 11 1 121.38 127.67 7.68 o -3 11 1 207.53 236.21 24.95 o -2 11 1 89.27 88.87 15.14 o -1 11 1 10.21 15.41 5.42 o 0 11 1 2.94 9.39 4.86 o 1 11 1 194.47 197.35 50.80 o 2 11 1 15.94 17.56 5.60 o 3 11 1 212.21 267.30 33.42 o 4 11 1 19.10 23.90 5.21 o 5 11 1 104.02 127.31 11.03 o 6 11 1 23.97 25.25 5.54 o -5 12 1 13.30 8.05 6.96 o -4 12 1 14.10 7.58 6.41 o -3 12 1 26.18 31.79 6.42 o -2 12 1 5.22 5.54 6.31 o -1 12 1 49.01 31.61 17.43 o 0 12 1 3.91 -1.17 7.12 o 1 12 1 268.93 314.61 45.33 o 2 12 1 1.59 -1.48 5.90 o 3 12 1 243.43 250.04 44.36 o 4 12 1 8.28 5.88 6.44 o -1 13 1 64.34 -15.75 15.75 o -13 0 2 697.56 530.73 168.31 o -12 0 2 92.94 92.89 21.59 o -11 0 2 300.72 281.80 36.07 o -10 0 2 134.33 158.53 25.76 o -9 0 2 26.77 39.25 12.47 o -8 0 2 1091.07 1180.12 206.48 o -7 0 2 1.13 2.05 4.36 o -6 0 2 330.84 376.90 14.22 o -5 0 2 5727.54 6373.00 118.86 o -4 0 2 10400.51 14561.49 279.97 o -2 0 2 685.34 588.14 27.29 o 1 0 2 330.79 208.86 7.50 o 2 0 2 23466.57 21107.42 1226.75 o 3 0 2 63.67 53.08 6.00 o 4 0 2 6424.10 6277.76 1695.49 o 5 0 2 1746.12 1465.66 266.19 o 6 0 2 4417.83 3046.99 570.48 o 7 0 2 469.21 369.30 73.48 o 8 0 2 48.94 49.57 9.00 o 9 0 2 155.29 129.43 33.36 o 10 0 2 161.65 141.81 20.49 o 11 0 2 78.77 53.98 16.36 o 12 0 2 5.48 -6.35 7.91 o -13 1 2 0.28 -4.99 5.67 o -12 1 2 37.81 29.31 5.87 o -11 1 2 233.84 234.80 11.24 o -10 1 2 48.15 54.73 5.95 o -9 1 2 214.12 213.91 18.38 o -8 1 2 99.76 120.30 8.48 o -7 1 2 1448.63 1787.67 103.43 o -6 1 2 30.49 79.86 25.31 o -5 1 2 4.78 0.54 2.89 o -4 1 2 366.19 416.41 11.47 o -3 1 2 859.06 1058.94 22.51 o -2 1 2 0.16 0.42 1.38 o -1 1 2 4095.46 4051.01 264.57 o 0 1 2 2784.14 2397.87 179.48 o 1 1 2 16734.07 16098.03 1014.44 o 2 1 2 19281.65 20577.90 932.42 o 3 1 2 1267.66 1021.07 81.03 o 4 1 2 1418.68 1196.20 73.32 o 5 1 2 3.81 0.32 1.79 o 6 1 2 35.44 35.06 5.91 o 7 1 2 0.30 3.82 3.08 o 8 1 2 230.89 192.49 22.24 o 9 1 2 773.73 674.48 86.62 o 10 1 2 112.63 100.03 23.67 o 11 1 2 389.44 355.24 60.50 o 12 1 2 46.25 41.74 9.74 o -13 2 2 28.06 25.64 7.04 o -12 2 2 576.88 449.82 73.70 o -11 2 2 318.48 318.47 41.18 o -10 2 2 797.91 882.23 122.78 o -9 2 2 243.75 241.73 34.73 o -8 2 2 338.65 426.32 15.86 o -7 2 2 1969.85 2280.50 102.76 o -6 2 2 780.85 985.35 28.84 o -5 2 2 1214.06 1478.68 33.56 o -4 2 2 570.49 625.99 22.21 o -3 2 2 2306.13 2571.26 111.78 o -2 2 2 5481.27 5691.97 464.78 o -1 2 2 27587.43 39740.54 980.12 o 0 2 2 189.54 154.72 8.70 o 1 2 2 10835.54 8305.52 596.38 o 2 2 2 740.66 578.48 21.25 o 3 2 2 118.47 132.77 6.16 o 4 2 2 982.81 872.84 40.98 o 5 2 2 485.41 491.29 19.50 o 6 2 2 131.71 107.00 4.36 o 7 2 2 195.92 174.84 17.91 o 8 2 2 294.37 254.33 30.40 o 9 2 2 257.30 222.05 28.89 o 10 2 2 258.19 234.80 44.30 o 11 2 2 0.20 0.01 5.26 o 12 2 2 20.12 7.14 5.40 o -13 3 2 42.52 40.82 7.50 o -12 3 2 73.39 74.99 12.06 o -11 3 2 3.28 -7.82 9.18 o -10 3 2 72.31 68.25 9.57 o -9 3 2 120.84 126.88 8.49 o -8 3 2 55.77 77.23 6.68 o -7 3 2 388.30 521.99 25.18 o -6 3 2 441.41 562.07 34.58 o -5 3 2 330.70 394.63 19.94 o -4 3 2 1063.19 1360.74 58.73 o -3 3 2 191.66 226.37 6.37 o -2 3 2 1288.51 1104.97 111.43 o -1 3 2 170.36 130.99 10.09 o 0 3 2 2161.81 1628.90 132.53 o 1 3 2 275.82 221.64 10.46 o 2 3 2 329.48 269.87 15.42 o 3 3 2 1.32 -0.09 2.04 o 4 3 2 1.36 2.70 2.40 o 5 3 2 12.77 15.22 2.70 o 6 3 2 49.99 46.69 3.04 o 7 3 2 20.39 16.83 3.04 o 8 3 2 25.96 23.61 4.25 o 9 3 2 137.08 147.65 16.52 o 10 3 2 19.97 9.18 4.59 o 11 3 2 8.05 7.15 4.73 o 12 3 2 1.32 -3.64 6.25 o -13 4 2 55.21 67.02 7.31 o -12 4 2 643.95 661.77 189.33 o -11 4 2 707.98 610.71 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