#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/47/2214795.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214795_Fobs loop_ _publ_author_name 'Thiruvalluvar, A.' 'Gunaseelan, A. Thomas' 'Martin, A. Ebenezer' 'Prasad, K. J. Rajendra' 'Butcher, R. J.' _publ_section_title ; 3,9-Dimethyl-10H-isoxazolo[5,4-a]carbazole ; _journal_coeditor_code LH2462 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3631 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-I 2ya' _symmetry_space_group_name_H-M 'I 1 2/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.974 _cell_angle_gamma 90.000 _cell_length_a 23.6402 _cell_length_b 5.0840 _cell_length_c 19.2139 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high 0.6612 _[local]_cod_data_source_file lh2462Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ooacha in I2/a z=8 c15h12n2o' _shelx_refln_list_code 4 _shelx_f_calc_maximum 323.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 0.00 6.19 37.39 o 8 0 0 12810.86 12783.95 300.49 o 10 0 0 8675.83 9961.92 196.77 o 12 0 0 38.59 6.02 18.11 o 14 0 0 7582.77 8972.17 343.43 o 16 0 0 102.75 74.99 26.05 o 18 0 0 255.79 259.18 27.67 o 20 0 0 1465.00 1443.05 39.55 o 22 0 0 1059.22 1051.59 65.79 o 24 0 0 93.58 57.98 77.39 o 26 0 0 86.02 17.76 55.53 o 28 0 0 69.35 65.87 107.86 o 30 0 0 90.10 88.78 112.13 o 32 0 0 64.95 119.81 125.42 o 34 0 0 23.18 90.39 181.35 o 5 1 0 296.04 239.13 18.34 o 7 1 0 1361.83 1285.50 25.64 o 9 1 0 3168.48 3053.93 34.52 o 11 1 0 2894.33 3278.22 23.97 o 13 1 0 214.50 184.20 10.63 o 15 1 0 1290.01 1226.02 20.93 o 17 1 0 2905.15 2928.54 36.42 o 19 1 0 1034.00 1071.73 22.48 o 21 1 0 137.92 117.29 22.25 o 23 1 0 76.61 69.37 31.13 o 25 1 0 0.48 1.51 17.37 o 27 1 0 1.09 24.84 152.11 o 29 1 0 1.88 0.05 15.61 o 31 1 0 9.19 48.71 76.36 o 33 1 0 41.23 26.85 157.76 o 0 2 0 3086.36 3286.16 47.07 o 2 2 0 6955.91 6746.67 91.60 o 4 2 0 244.50 215.35 8.97 o 6 2 0 256.75 241.15 8.69 o 8 2 0 1506.69 1569.56 27.78 o 10 2 0 33.10 23.02 14.05 o 12 2 0 91.62 75.59 30.06 o 14 2 0 56.02 56.84 20.26 o 16 2 0 99.24 71.09 24.88 o 18 2 0 269.72 273.17 30.33 o 20 2 0 19.60 42.12 34.06 o 22 2 0 14.87 0.73 4.45 o 24 2 0 0.72 29.48 34.83 o 26 2 0 8.92 -2.86 90.97 o 28 2 0 1.97 35.97 72.13 o 30 2 0 0.13 11.54 128.53 o 32 2 0 1.82 45.84 112.11 o 1 3 0 425.46 439.67 12.52 o 3 3 0 2756.40 3005.00 43.24 o 5 3 0 155.22 140.50 13.57 o 7 3 0 401.22 390.27 26.38 o 9 3 0 54.79 49.98 16.83 o 11 3 0 890.13 904.05 19.19 o 13 3 0 312.54 335.51 24.04 o 15 3 0 7.56 -6.99 19.20 o 17 3 0 60.45 59.25 46.04 o 19 3 0 721.98 765.76 62.69 o 21 3 0 392.08 414.71 66.72 o 23 3 0 80.02 112.57 60.13 o 25 3 0 21.28 -18.61 80.22 o 27 3 0 2.40 15.81 74.97 o 29 3 0 108.07 169.92 96.04 o 0 4 0 10.94 26.64 21.34 o 2 4 0 2.34 0.09 4.20 o 4 4 0 120.56 109.47 18.15 o 6 4 0 324.21 323.02 22.32 o 8 4 0 677.99 755.93 28.61 o 10 4 0 43.75 42.42 28.49 o 12 4 0 1875.81 2009.96 45.04 o 14 4 0 534.42 485.38 49.41 o 16 4 0 53.56 59.13 52.68 o 18 4 0 0.64 24.40 40.46 o 20 4 0 11.36 45.95 58.96 o 22 4 0 53.80 83.86 107.62 o 24 4 0 1.52 40.36 113.11 o 26 4 0 32.57 -17.78 951.33 o 28 4 0 19.29 42.99 167.56 o 1 5 0 40.03 2.57 12.75 o 3 5 0 19.62 21.62 24.06 o 5 5 0 0.52 -1.90 4.20 o 7 5 0 379.24 441.53 35.26 o 9 5 0 2.07 -16.12 22.46 o 11 5 0 47.26 33.65 55.57 o 13 5 0 18.25 52.67 59.33 o 15 5 0 1.40 51.70 69.89 o 17 5 0 13.35 42.77 71.47 o 19 5 0 12.27 25.19 64.41 o 21 5 0 0.18 14.45 97.95 o 23 5 0 1.49 70.23 88.74 o 0 6 0 17.95 -24.22 48.75 o 2 6 0 76.16 60.67 57.25 o 4 6 0 0.34 8.67 51.36 o 6 6 0 22.56 29.30 39.42 o 8 6 0 9.97 7.71 19.98 o 10 6 0 51.39 74.70 97.75 o 12 6 0 66.36 82.65 93.34 o 14 6 0 8.36 65.67 85.99 o 16 6 0 0.60 -5.65 77.38 o 18 6 0 2.92 20.31 83.94 o 1 7 0 6.82 53.52 133.96 o 3 7 0 34.75 8.31 29.90 o 5 7 0 58.49 94.20 102.08 o 7 7 0 31.75 7.18 78.63 o 9 7 0 2.05 -18.28 64.42 o 11 7 0 12.24 68.41 129.25 o -34 1 1 69.35 124.64 166.52 o -32 1 1 25.50 168.14 134.31 o -30 1 1 3.84 21.34 76.52 o -28 1 1 42.33 61.40 42.42 o -26 1 1 16.36 17.90 35.36 o -24 1 1 36.28 66.52 41.07 o -22 1 1 109.75 87.11 38.50 o -20 1 1 612.20 599.56 17.87 o -18 1 1 144.26 158.50 14.45 o -16 1 1 322.57 314.57 12.07 o -14 1 1 815.86 863.10 17.61 o -12 1 1 384.49 413.17 9.19 o -10 1 1 269.16 273.24 13.07 o -8 1 1 214.95 246.13 10.98 o -6 1 1 240.86 224.93 13.36 o -4 1 1 1404.76 1348.61 40.04 o 4 1 1 890.10 845.32 37.90 o 6 1 1 300.67 268.73 12.86 o 8 1 1 352.96 325.94 9.30 o 10 1 1 990.90 1166.30 22.94 o 12 1 1 2900.93 3227.05 52.83 o 14 1 1 22.82 22.12 15.46 o 16 1 1 8.27 3.15 7.72 o 18 1 1 139.18 128.96 18.11 o 20 1 1 2393.26 2481.48 33.46 o 22 1 1 637.60 601.42 23.60 o 24 1 1 35.51 71.37 51.52 o 26 1 1 13.85 0.40 29.49 o 28 1 1 21.70 20.13 39.66 o 30 1 1 39.55 79.13 72.44 o 32 1 1 0.22 56.21 137.49 o 34 1 1 31.18 166.93 155.69 o -33 2 1 20.61 43.96 167.04 o -31 2 1 30.69 -30.06 137.48 o -29 2 1 1.68 44.58 83.18 o -27 2 1 6.84 -0.10 67.21 o -25 2 1 9.49 6.67 38.03 o -23 2 1 39.67 45.26 39.60 o -21 2 1 0.00 -17.70 32.12 o -19 2 1 17.79 7.02 13.57 o -17 2 1 684.06 648.52 30.40 o -15 2 1 123.05 155.05 22.14 o -13 2 1 258.81 269.26 17.70 o -11 2 1 182.41 171.67 27.70 o -9 2 1 2251.73 2303.26 45.21 o -7 2 1 1282.98 1296.77 30.25 o -5 2 1 1438.78 1490.45 28.55 o -3 2 1 813.62 739.18 16.18 o -1 2 1 340.15 275.92 8.87 o 1 2 1 480.82 500.24 11.83 o 3 2 1 340.51 299.50 9.58 o 5 2 1 90.42 69.40 7.15 o 7 2 1 68.65 95.06 11.19 o 9 2 1 267.76 311.96 12.13 o 11 2 1 0.11 11.95 7.16 o 13 2 1 290.49 271.23 13.51 o 15 2 1 161.72 163.89 16.48 o 17 2 1 245.10 237.17 16.18 o 19 2 1 109.77 96.68 16.63 o 21 2 1 7.61 -2.07 19.21 o 23 2 1 321.90 338.31 36.43 o 25 2 1 9.52 -5.92 11.95 o 27 2 1 5.47 28.67 129.22 o 29 2 1 10.61 9.09 48.07 o 31 2 1 47.09 10.53 49.46 o -30 3 1 31.02 93.19 106.57 o -28 3 1 79.29 145.53 144.43 o -26 3 1 21.85 81.24 91.47 o -24 3 1 1.23 23.96 77.36 o -22 3 1 236.10 366.30 74.11 o -20 3 1 419.19 420.49 62.34 o -18 3 1 46.76 48.09 58.76 o -16 3 1 430.43 421.87 47.38 o -14 3 1 351.44 372.42 42.27 o -12 3 1 551.73 536.40 27.50 o -10 3 1 2.98 -1.21 5.76 o -8 3 1 1181.48 1286.07 30.94 o -6 3 1 1524.12 1700.34 39.81 o -4 3 1 1579.47 1704.22 23.36 o -2 3 1 1400.25 1493.72 16.89 o 0 3 1 199.59 173.61 10.97 o 2 3 1 351.95 350.70 12.91 o 4 3 1 91.16 72.81 13.29 o 6 3 1 141.78 105.77 12.41 o 8 3 1 1074.98 1167.95 20.99 o 10 3 1 378.09 445.30 17.51 o 12 3 1 60.16 50.52 23.64 o 14 3 1 75.17 58.43 39.70 o 16 3 1 99.05 118.48 43.75 o 18 3 1 1.69 1.39 15.06 o 20 3 1 1.46 -43.19 75.11 o 22 3 1 691.96 917.84 67.26 o 24 3 1 176.44 267.82 75.72 o 26 3 1 0.39 46.25 64.96 o 28 3 1 69.60 66.85 222.04 o 30 3 1 1.53 10.61 86.36 o -27 4 1 3.81 73.21 86.85 o -25 4 1 3.61 20.20 129.48 o -23 4 1 16.25 24.67 82.89 o -21 4 1 0.66 5.86 39.31 o -19 4 1 122.32 167.76 69.03 o -17 4 1 429.20 429.40 61.13 o -15 4 1 720.43 810.13 57.30 o -13 4 1 0.86 3.51 7.84 o -11 4 1 336.79 306.41 43.70 o -9 4 1 26.98 6.77 21.15 o -7 4 1 4.65 3.33 8.08 o -5 4 1 330.66 361.19 21.78 o -3 4 1 714.83 754.67 28.19 o -1 4 1 834.76 907.26 17.55 o 1 4 1 391.04 397.08 18.75 o 3 4 1 678.79 688.28 18.97 o 5 4 1 1.44 -5.47 15.27 o 7 4 1 17.19 12.65 21.95 o 9 4 1 0.92 2.39 12.82 o 11 4 1 141.62 148.90 36.44 o 13 4 1 50.56 32.31 24.21 o 15 4 1 39.12 38.52 44.34 o 17 4 1 5.41 -20.80 74.48 o 19 4 1 5.49 -13.20 56.48 o 21 4 1 9.29 17.15 41.22 o 23 4 1 69.25 166.41 79.10 o 27 4 1 14.34 83.29 175.72 o -24 5 1 5.63 60.59 138.46 o -22 5 1 0.85 9.50 53.53 o -20 5 1 28.20 93.64 84.11 o -18 5 1 75.37 119.88 89.61 o -16 5 1 375.20 438.92 69.14 o -14 5 1 182.90 203.93 64.77 o -12 5 1 51.29 9.55 21.06 o -10 5 1 263.19 313.78 48.68 o -8 5 1 17.03 18.35 29.45 o -6 5 1 694.10 763.23 40.55 o -4 5 1 111.05 108.16 46.54 o -2 5 1 20.09 -1.83 48.87 o 0 5 1 2.16 -0.03 6.22 o 2 5 1 53.75 41.85 28.21 o 4 5 1 12.90 1.21 20.13 o 6 5 1 301.26 287.35 32.59 o 8 5 1 279.78 270.30 41.35 o 10 5 1 0.56 14.34 33.80 o 12 5 1 124.03 137.09 69.86 o 14 5 1 29.86 0.30 24.29 o 16 5 1 7.19 -0.43 3.57 o 18 5 1 11.83 61.94 87.31 o 20 5 1 26.21 98.61 109.33 o 22 5 1 0.15 68.97 132.22 o 24 5 1 1.24 20.30 1308.77 o -19 6 1 55.61 126.49 113.11 o -17 6 1 10.13 51.77 106.78 o -15 6 1 11.87 2.59 6.05 o -13 6 1 6.45 -2.25 30.15 o -11 6 1 28.76 26.33 44.79 o -9 6 1 27.60 0.19 11.08 o -7 6 1 1.04 -14.91 36.43 o -5 6 1 24.05 -14.53 66.53 o -3 6 1 75.55 67.49 58.44 o -1 6 1 297.93 258.64 68.67 o 1 6 1 243.50 247.60 75.73 o 3 6 1 52.52 99.38 65.35 o 5 6 1 65.45 66.36 73.65 o 7 6 1 89.13 172.46 64.83 o 9 6 1 43.93 58.03 46.31 o 11 6 1 0.79 4.13 54.64 o 13 6 1 4.81 42.18 182.64 o 15 6 1 5.45 25.22 188.88 o 17 6 1 54.70 103.56 138.36 o -12 7 1 3.31 -37.98 96.09 o -10 7 1 0.23 -14.40 88.94 o -8 7 1 0.02 0.00 0.03 o -6 7 1 0.71 -10.90 84.66 o -4 7 1 6.84 24.01 64.02 o -2 7 1 2.95 -10.66 65.75 o 0 7 1 23.04 -0.45 148.10 o 2 7 1 5.39 8.51 182.81 o 4 7 1 0.14 -7.40 29.56 o 6 7 1 18.31 -29.83 147.79 o 8 7 1 1.47 -29.56 128.76 o 10 7 1 45.39 105.00 132.74 o -34 0 2 25.87 4.19 60.73 o -32 0 2 7.42 8.15 83.05 o -30 0 2 27.73 47.34 144.56 o -28 0 2 179.69 186.10 94.80 o -26 0 2 58.36 44.68 44.62 o -24 0 2 204.16 180.44 45.53 o -22 0 2 550.02 488.00 37.44 o -20 0 2 538.30 557.15 44.77 o -18 0 2 186.06 191.76 35.13 o -16 0 2 1375.97 1443.22 44.23 o -14 0 2 1401.90 1623.68 55.32 o -12 0 2 4823.74 5262.85 60.11 o -10 0 2 627.08 609.31 27.93 o -8 0 2 140.04 161.61 27.01 o -6 0 2 4277.64 4608.35 59.41 o 6 0 2 1477.39 1447.16 39.23 o 8 0 2 4855.79 4768.16 67.78 o 10 0 2 315.78 281.01 36.80 o 12 0 2 244.07 280.46 35.85 o 14 0 2 488.90 381.61 34.06 o 16 0 2 161.63 179.35 32.08 o 18 0 2 497.06 515.35 44.31 o 20 0 2 226.60 215.39 55.73 o 22 0 2 124.88 110.80 58.12 o 24 0 2 246.68 300.88 76.16 o 26 0 2 265.21 265.49 85.51 o 28 0 2 62.29 85.51 83.67 o 30 0 2 1.93 -8.54 296.27 o 32 0 2 24.12 32.34 759.48 o 34 0 2 183.01 320.78 157.20 o -33 1 2 68.07 44.12 116.11 o -31 1 2 82.84 77.54 163.45 o -29 1 2 8.47 -2.10 78.31 o -27 1 2 22.01 1.31 10.83 o -25 1 2 123.82 133.27 50.80 o -23 1 2 100.56 112.26 43.79 o -21 1 2 539.90 492.86 19.60 o -19 1 2 30.21 40.15 12.36 o -17 1 2 81.62 56.52 9.98 o -15 1 2 154.82 142.34 7.68 o -13 1 2 1905.22 1962.67 30.01 o -11 1 2 1212.08 1289.95 19.08 o -9 1 2 561.54 608.94 17.88 o -7 1 2 1526.65 1546.80 19.28 o -5 1 2 3408.35 3615.04 48.65 o -3 1 2 10173.43 9273.31 49.38 o 1 1 2 7127.29 6394.26 60.82 o 3 1 2 337.69 294.73 10.61 o 5 1 2 4119.61 3761.92 49.25 o 7 1 2 43.83 42.51 6.63 o 9 1 2 1005.67 1155.39 28.91 o 11 1 2 2105.11 2468.04 43.10 o 13 1 2 408.21 385.15 22.96 o 15 1 2 785.86 837.15 20.35 o 17 1 2 834.96 844.96 20.59 o 19 1 2 769.66 764.80 20.79 o 21 1 2 41.54 31.83 20.45 o 23 1 2 88.73 82.80 30.58 o 25 1 2 154.66 123.72 48.45 o 27 1 2 0.98 -15.18 82.34 o 29 1 2 1.19 13.23 37.49 o 31 1 2 0.08 25.99 65.29 o 33 1 2 2.72 5.99 105.58 o -32 2 2 23.39 73.39 199.40 o -30 2 2 41.62 97.23 80.35 o -28 2 2 30.47 47.12 124.26 o -26 2 2 15.30 56.15 80.42 o -24 2 2 10.73 13.20 55.35 o -22 2 2 1084.45 1133.20 37.54 o -20 2 2 0.14 8.17 22.33 o -18 2 2 1977.93 1886.46 40.90 o -16 2 2 103.78 75.91 21.43 o -14 2 2 101.98 96.18 18.46 o -12 2 2 507.46 506.89 16.12 o -10 2 2 2565.49 2853.97 60.38 o -8 2 2 0.00 0.47 11.07 o -6 2 2 135.67 142.09 14.77 o -4 2 2 512.30 514.69 10.72 o -2 2 2 35.11 42.01 6.67 o 0 2 2 17.66 3.57 6.35 o 2 2 2 3352.10 3396.69 41.93 o 4 2 2 260.56 234.75 10.41 o 6 2 2 6330.02 6757.28 71.94 o 8 2 2 433.30 464.58 10.74 o 10 2 2 2292.50 2538.37 29.90 o 12 2 2 624.04 673.02 17.01 o 14 2 2 127.28 97.51 16.69 o 16 2 2 2064.44 2179.69 32.80 o 18 2 2 34.00 6.31 9.71 o 20 2 2 481.64 427.26 35.56 o 22 2 2 61.82 56.31 41.40 o 24 2 2 5.88 15.16 62.66 o 26 2 2 6.70 7.64 43.17 o 28 2 2 26.97 42.32 175.80 o 30 2 2 191.65 434.74 145.97 o 32 2 2 5.94 -22.51 293.27 o -31 3 2 2.07 36.36 241.30 o -29 3 2 99.18 113.66 136.15 o -27 3 2 116.56 206.96 107.87 o -25 3 2 45.25 81.22 85.22 o -23 3 2 157.71 172.62 75.64 o -21 3 2 4.33 5.38 14.87 o -19 3 2 132.94 180.03 72.41 o -17 3 2 8.22 14.68 23.61 o -15 3 2 1046.88 1041.80 48.18 o -13 3 2 0.47 -33.28 33.28 o -11 3 2 307.77 310.63 20.51 o -9 3 2 1079.68 1118.79 27.13 o -7 3 2 420.12 429.50 28.35 o -5 3 2 620.42 610.41 18.55 o -3 3 2 138.32 140.71 12.29 o -1 3 2 23.36 12.52 6.69 o 1 3 2 9.31 2.17 7.90 o 3 3 2 6.84 4.04 5.76 o 5 3 2 440.67 401.55 12.44 o 7 3 2 92.97 77.47 11.87 o 9 3 2 777.07 789.14 18.54 o 11 3 2 28.44 22.64 14.12 o 13 3 2 2365.74 2395.54 38.75 o 15 3 2 71.54 62.04 41.93 o 17 3 2 98.93 67.54 49.30 o 19 3 2 170.01 158.63 56.02 o 21 3 2 91.77 22.20 45.60 o 23 3 2 676.54 794.67 60.44 o 25 3 2 67.45 125.67 116.78 o 27 3 2 46.42 18.53 102.92 o 29 3 2 1.53 16.76 747.58 o -28 4 2 2.31 -6.65 45.02 o -26 4 2 68.93 58.65 99.88 o -24 4 2 5.32 32.78 76.15 o -22 4 2 29.16 117.81 81.48 o -20 4 2 30.72 60.00 64.99 o -18 4 2 47.22 71.30 60.79 o -16 4 2 98.63 141.75 55.17 o -14 4 2 27.18 7.72 17.83 o -12 4 2 435.76 458.44 46.76 o -10 4 2 300.04 274.26 45.62 o -8 4 2 66.40 58.31 26.08 o -6 4 2 16.71 12.77 12.10 o -4 4 2 134.95 129.20 16.64 o -2 4 2 351.22 375.09 17.18 o 0 4 2 5.87 0.08 11.85 o 2 4 2 544.59 563.93 19.43 o 4 4 2 352.53 348.93 16.76 o 6 4 2 162.03 148.31 16.69 o 8 4 2 368.73 360.08 17.36 o 10 4 2 11.65 -8.08 23.27 o 12 4 2 76.26 79.88 36.35 o 14 4 2 92.65 103.58 40.84 o 16 4 2 0.04 -3.78 19.52 o 18 4 2 32.97 4.30 32.15 o 20 4 2 91.76 128.80 54.18 o 22 4 2 56.00 97.26 72.21 o 24 4 2 20.18 28.30 48.43 o 26 4 2 14.25 -8.11 34.92 o 28 4 2 26.41 35.47 117.56 o -23 5 2 0.03 -16.82 555.85 o -21 5 2 3.77 76.90 158.86 o -19 5 2 11.06 36.28 59.98 o -17 5 2 39.25 45.00 67.51 o -15 5 2 255.58 259.81 62.98 o -13 5 2 133.25 85.05 70.04 o -11 5 2 84.86 4.04 33.95 o -9 5 2 91.98 56.20 44.09 o -7 5 2 32.68 20.66 20.40 o -5 5 2 80.53 122.05 39.37 o -3 5 2 260.37 277.94 40.28 o -1 5 2 352.91 375.68 31.84 o 1 5 2 576.31 560.07 31.22 o 3 5 2 1063.45 1192.67 29.48 o 5 5 2 356.88 348.81 32.22 o 7 5 2 399.78 435.70 33.70 o 9 5 2 87.73 72.96 35.24 o 11 5 2 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