#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:33:48 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181068 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/48/2214802.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214802_Fobs loop_ _publ_author_name 'Rutt, Oliver J.' 'Cowley, Andrew R.' 'Clarke, Simon J.' _publ_section_title ; Bis(ethylamino)tetrafluorosilicon ; _journal_coeditor_code MG2025 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3406 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _audit_creation_date 07-05-23 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 99.655(2) _cell_angle_gamma 90 _cell_length_a 8.4788(4) _cell_length_b 6.9602(3) _cell_length_c 7.2206(4) _cod_data_source_file mg2025Isup2.hkl _cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 3 0 0 288.30 327.89 6.70 o 4 0 0 311.90 315.87 9.70 o 5 0 0 38.40 42.85 2.30 o 6 0 0 526.80 509.71 12.60 o 7 0 0 397.10 412.63 10.80 o 8 0 0 78.80 85.83 4.20 o 9 0 0 12.00 8.93 3.00 o 10 0 0 -2.60 0.53 5.40 < 2 1 0 16.70 9.37 1.36 o 3 1 0 129.45 104.03 3.60 o 4 1 0 685.65 698.25 14.65 o 5 1 0 560.10 550.30 11.50 o 6 1 0 164.90 147.19 4.05 o 7 1 0 44.00 44.26 2.66 o 8 1 0 5.85 2.38 2.36 < 9 1 0 4.05 0.45 4.58 < 10 1 0 -4.30 0.01 3.30 < 0 2 0 5153.70 5488.42 157.00 o 1 2 0 4.70 3.63 1.60 < 2 2 0 290.45 262.42 7.55 o 3 2 0 122.00 111.32 3.15 o 4 2 0 382.40 347.51 10.14 o 5 2 0 48.95 54.83 2.21 o 6 2 0 549.70 519.20 13.52 o 7 2 0 575.05 559.88 16.85 o 8 2 0 268.85 251.53 10.46 o 9 2 0 26.85 26.06 4.48 o 10 2 0 42.85 40.75 6.28 o 1 3 0 737.65 732.65 25.14 o 2 3 0 1276.05 1218.20 45.66 o 3 3 0 635.10 671.01 17.24 o 4 3 0 1.15 1.53 2.38 < 5 3 0 8.00 18.03 3.11 < 6 3 0 15.75 16.38 2.22 o 7 3 0 33.55 35.99 2.72 o 8 3 0 53.65 55.73 3.55 o 9 3 0 36.60 34.75 4.33 o 10 3 0 4.00 1.18 5.42 < 0 4 0 3227.10 3188.02 90.90 o 1 4 0 1101.20 1039.19 22.70 o 2 4 0 576.05 596.29 17.23 o 3 4 0 381.10 363.26 10.85 o 4 4 0 28.95 29.41 2.41 o 5 4 0 90.25 92.97 3.71 o 6 4 0 93.00 93.73 5.88 o 7 4 0 62.65 72.63 4.18 o 8 4 0 34.35 37.17 4.30 o 9 4 0 -3.55 1.17 5.26 < 1 5 0 91.60 103.46 2.70 o 2 5 0 94.30 78.45 4.75 o 3 5 0 2.40 0.01 2.94 < 4 5 0 257.15 247.17 8.22 o 5 5 0 344.35 329.42 11.22 o 6 5 0 72.75 81.74 5.35 o 7 5 0 10.30 11.63 2.30 o 8 5 0 2.45 3.32 3.62 < 9 5 0 3.60 10.13 5.60 < 0 6 0 29.70 34.13 3.50 o 1 6 0 2.00 0.20 1.90 < 2 6 0 24.10 20.96 2.10 o 3 6 0 71.65 70.77 3.67 o 4 6 0 13.90 14.55 2.73 o 5 6 0 47.45 47.26 3.87 o 6 6 0 34.40 32.41 3.69 o 7 6 0 24.90 39.13 5.06 o 8 6 0 60.70 57.61 7.79 o 1 7 0 76.40 75.46 3.90 o 2 7 0 96.10 100.01 4.40 o 3 7 0 78.90 72.08 4.53 o 4 7 0 0.30 0.28 2.86 < 5 7 0 3.00 5.80 4.06 < 6 7 0 2.15 0.14 4.54 < 0 8 0 67.90 79.99 8.00 o 1 8 0 50.90 58.80 4.10 o 2 8 0 130.15 120.38 9.65 o 3 8 0 142.65 142.01 8.52 o 4 8 0 46.50 57.69 5.80 o 5 8 0 39.30 31.40 5.40 o -10 1 1 1.70 1.93 4.09 < -9 1 1 40.50 44.56 3.58 o -8 1 1 72.25 73.49 4.04 o -7 1 1 755.60 740.78 20.22 o -6 1 1 497.15 487.56 10.73 o -5 1 1 21.30 23.84 1.87 o -4 1 1 75.65 50.95 2.52 o -3 1 1 37.35 34.29 1.76 o -2 1 1 1184.10 1250.87 29.48 o 2 1 1 240.15 209.69 6.65 o 3 1 1 306.30 305.14 7.36 o 4 1 1 649.50 673.27 14.28 o 5 1 1 61.05 64.78 2.40 o 6 1 1 225.40 214.64 5.72 o 7 1 1 70.15 65.88 3.15 o 8 1 1 10.50 15.78 3.04 o 9 1 1 8.50 11.26 4.23 < 10 1 1 16.60 23.09 7.10 < -10 2 1 6.50 3.59 3.50 < -9 2 1 18.10 19.59 3.41 o -8 2 1 10.40 8.09 2.49 o -7 2 1 14.75 13.82 2.16 o -6 2 1 89.40 90.77 3.01 o -5 2 1 79.20 79.87 2.77 o -4 2 1 87.30 84.97 2.81 o -3 2 1 48.10 46.82 1.90 o -2 2 1 313.15 292.97 8.26 o -1 2 1 1.95 5.16 1.91 < 0 2 1 70.65 72.61 3.32 o 1 2 1 67.10 68.60 2.90 o 2 2 1 -0.40 0.01 2.44 < 3 2 1 44.80 41.48 1.95 o 4 2 1 57.20 42.37 2.28 o 5 2 1 55.10 69.00 2.35 o 6 2 1 -1.10 1.54 2.46 < 7 2 1 10.80 14.04 2.36 o 8 2 1 0.25 0.69 2.50 < 9 2 1 0.60 1.76 3.87 < 10 2 1 -0.10 0.51 5.98 < -10 3 1 13.10 10.41 3.50 o -9 3 1 46.30 48.88 5.85 o -8 3 1 59.45 58.47 3.75 o -7 3 1 408.20 393.56 14.67 o -6 3 1 291.90 289.14 11.73 o -5 3 1 81.15 82.17 4.02 o -4 3 1 -0.30 5.57 2.15 < -3 3 1 4.10 5.33 1.56 < -2 3 1 199.10 202.58 6.57 o -1 3 1 58.85 56.72 2.51 o 0 3 1 427.15 425.87 19.55 o 1 3 1 851.95 845.98 30.75 o 2 3 1 -0.25 1.83 1.88 < 3 3 1 176.15 182.55 5.26 o 4 3 1 269.45 253.21 7.61 o 5 3 1 42.80 49.13 2.30 o 6 3 1 161.45 153.75 4.87 o 7 3 1 75.00 74.88 3.71 o 8 3 1 40.50 45.95 3.22 o 9 3 1 32.75 36.74 4.80 o -9 4 1 34.80 36.32 4.00 o -8 4 1 31.10 30.87 3.71 o -7 4 1 1.60 0.01 1.90 < -6 4 1 22.30 23.57 3.23 o -5 4 1 7.80 11.78 1.76 o -4 4 1 -1.30 0.95 2.57 < -3 4 1 225.85 230.35 6.45 o -2 4 1 404.95 337.48 11.12 o -1 4 1 23.40 40.35 1.70 o 0 4 1 100.40 101.07 2.90 o 1 4 1 212.35 249.21 8.70 o 2 4 1 86.45 67.02 3.48 o 3 4 1 5.15 2.82 1.94 < 4 4 1 0.45 0.23 2.59 < 5 4 1 3.60 3.38 1.60 < 6 4 1 26.10 24.79 2.62 o 7 4 1 34.45 33.77 3.53 o 8 4 1 -1.50 0.01 3.07 < 9 4 1 0.50 2.02 4.67 < -9 5 1 6.50 8.45 6.31 < -8 5 1 1.15 2.82 4.56 < -7 5 1 69.55 73.02 6.05 o -6 5 1 83.10 88.68 5.38 o -5 5 1 140.75 134.27 5.87 o -4 5 1 171.60 175.21 5.86 o -3 5 1 87.15 88.87 3.61 o -2 5 1 267.80 257.02 7.96 o -1 5 1 162.10 154.31 4.20 o 0 5 1 426.10 395.24 9.50 o 1 5 1 873.50 812.98 29.31 o 2 5 1 272.15 245.99 9.00 o 3 5 1 339.60 329.83 10.79 o 4 5 1 123.05 120.07 4.69 o 5 5 1 -0.15 1.61 2.63 < 6 5 1 25.70 24.89 3.14 o 7 5 1 11.20 13.10 3.49 o 8 5 1 20.80 18.62 4.32 o -8 6 1 7.95 8.10 6.10 < -7 6 1 -0.75 5.60 4.90 < -6 6 1 54.35 59.76 3.96 o -5 6 1 59.15 68.68 3.91 o -4 6 1 68.70 68.57 3.75 o -3 6 1 -1.20 0.11 2.09 < -2 6 1 37.05 31.41 3.76 o -1 6 1 3.10 3.64 2.24 < 0 6 1 2.40 0.41 1.80 < 1 6 1 3.00 4.70 1.90 < 2 6 1 -0.80 0.51 3.22 < 3 6 1 20.70 20.75 2.71 o 4 6 1 17.20 17.81 2.92 o 5 6 1 21.50 30.29 3.51 o 6 6 1 4.95 1.95 3.46 < 7 6 1 0.10 0.02 3.29 < -6 7 1 38.45 40.15 5.85 o -5 7 1 87.35 78.86 5.73 o -4 7 1 85.70 84.04 5.76 o -3 7 1 6.00 9.81 4.24 < -2 7 1 6.20 4.22 3.14 < -1 7 1 1.60 4.37 4.67 < 0 7 1 -3.30 1.56 2.00 < 1 7 1 76.80 80.28 3.80 o 2 7 1 62.30 55.71 3.60 o 3 7 1 111.95 93.98 6.33 o 4 7 1 29.45 33.93 3.89 o 5 7 1 1.55 2.73 3.46 < 6 7 1 27.55 22.42 7.46 o -5 8 1 0.50 0.30 4.30 < -4 8 1 2.15 0.54 3.73 < -3 8 1 6.20 6.78 3.63 < -2 8 1 25.95 26.98 5.13 o -1 8 1 9.00 10.27 5.06 < 0 8 1 6.80 5.27 3.20 < 1 8 1 8.90 3.47 3.40 < 2 8 1 21.40 21.31 3.70 o 3 8 1 18.15 22.96 4.47 o 4 8 1 29.30 29.69 4.50 o -10 0 2 4.10 2.36 5.90 < -9 0 2 89.70 100.15 5.30 o -8 0 2 13.50 14.12 2.70 o -7 0 2 -3.80 1.22 3.30 < -6 0 2 310.10 308.79 7.90 o -5 0 2 122.70 111.45 3.70 o -4 0 2 769.70 777.12 25.70 o -3 0 2 5119.70 5126.96 125.70 o -2 0 2 3407.10 3380.49 97.50 o -1 0 2 2037.80 2049.77 65.90 o 0 0 2 5.60 4.85 1.60 o 1 0 2 728.30 776.47 23.00 o 2 0 2 1231.80 1204.69 39.50 o 3 0 2 944.20 893.46 23.80 o 4 0 2 2754.40 2762.96 57.00 o 5 0 2 522.70 544.43 12.10 o 6 0 2 30.00 35.18 2.20 o 7 0 2 12.90 15.02 2.90 o 8 0 2 20.80 23.03 3.80 o 9 0 2 -0.20 2.09 3.85 < 10 0 2 65.30 37.58 11.30 o -10 1 2 -2.25 0.42 4.52 < -9 1 2 10.05 2.87 2.84 o -8 1 2 30.80 32.51 2.84 o -7 1 2 106.05 104.38 3.66 o -6 1 2 156.80 155.92 4.58 o -5 1 2 119.25 122.57 4.18 o -4 1 2 116.10 109.93 3.73 o -3 1 2 303.80 299.33 8.10 o -2 1 2 158.35 154.17 4.95 o -1 1 2 92.95 86.28 3.36 o 0 1 2 12.80 20.40 1.06 o 1 1 2 359.65 398.03 10.05 o 2 1 2 826.00 836.62 21.80 o 3 1 2 590.75 554.04 13.76 o 4 1 2 203.00 217.65 5.35 o 5 1 2 43.50 42.26 2.40 o 6 1 2 16.15 14.81 2.45 o 7 1 2 6.70 4.83 2.35 < 8 1 2 8.90 9.48 2.95 o 9 1 2 15.45 10.17 5.47 < 10 1 2 7.40 0.38 10.20 < -10 2 2 20.95 17.78 4.97 o -9 2 2 228.05 211.61 10.69 o -8 2 2 111.25 102.08 4.53 o -7 2 2 34.55 33.29 2.83 o -6 2 2 272.75 270.86 7.97 o -5 2 2 23.55 22.41 2.34 o -4 2 2 48.20 54.99 3.36 o -3 2 2 392.15 426.54 10.13 o -2 2 2 1.25 3.04 1.18 < -1 2 2 125.65 98.70 3.65 o 0 2 2 1663.15 1685.38 55.23 o 1 2 2 220.40 185.75 7.77 o 2 2 2 12.00 12.57 1.55 o 3 2 2 141.30 143.86 4.47 o 4 2 2 1391.70 1316.98 32.76 o 5 2 2 443.25 448.26 11.36 o 6 2 2 10.95 11.70 2.30 o 7 2 2 39.05 37.40 2.75 o 8 2 2 17.40 15.80 2.96 o 9 2 2 44.60 52.60 6.17 o -10 3 2 11.60 2.52 5.80 < -9 3 2 20.60 14.97 2.60 o -8 3 2 5.10 6.01 2.75 < -7 3 2 8.70 4.20 3.42 < -6 3 2 44.40 47.80 2.84 o -5 3 2 291.40 280.17 7.54 o -4 3 2 487.15 468.28 12.03 o -3 3 2 128.70 140.65 3.58 o -2 3 2 6.60 4.41 1.51 o -1 3 2 155.10 149.52 5.23 o 0 3 2 331.65 292.48 9.76 o 1 3 2 8.35 10.65 2.30 o 2 3 2 20.45 23.73 2.45 o 3 3 2 0.30 0.47 1.37 < 4 3 2 153.45 161.47 4.88 o 5 3 2 335.75 318.67 7.96 o 6 3 2 171.55 162.57 5.42 o 7 3 2 48.65 53.03 3.06 o 8 3 2 6.35 1.05 5.43 < 9 3 2 21.85 27.21 7.26 o -9 4 2 20.20 16.76 3.20 o -8 4 2 0.00 4.08 0.01 < -7 4 2 8.70 6.51 2.00 o -6 4 2 210.50 204.82 9.65 o -5 4 2 179.05 185.09 5.60 o -4 4 2 460.65 439.45 12.01 o -3 4 2 772.05 786.08 21.31 o -2 4 2 596.10 567.23 15.88 o -1 4 2 723.70 744.04 24.38 o 0 4 2 277.30 280.03 8.49 o 1 4 2 731.55 721.30 18.68 o 2 4 2 752.85 700.96 21.60 o 3 4 2 314.25 309.78 9.03 o 4 4 2 499.60 480.83 13.00 o 5 4 2 74.05 80.71 3.48 o 6 4 2 0.80 0.05 1.61 < 7 4 2 6.60 7.26 2.77 < 8 4 2 6.90 0.06 4.77 < 9 4 2 -6.70 4.47 6.75 < -9 5 2 -5.30 0.14 6.50 < -8 5 2 9.80 14.15 5.16 < -7 5 2 36.45 38.97 4.33 o -6 5 2 39.10 41.68 3.52 o -5 5 2 3.10 7.20 2.15 < -4 5 2 1.95 0.49 2.07 < -3 5 2 41.20 38.43 2.65 o -2 5 2 55.60 64.45 2.75 o -1 5 2 92.50 97.99 4.30 o 0 5 2 23.75 17.56 2.00 o 1 5 2 117.45 108.77 4.10 o 2 5 2 351.40 333.10 9.43 o 3 5 2 225.75 229.97 7.74 o 4 5 2 25.45 21.72 2.82 o 5 5 2 7.80 6.28 2.14 o 6 5 2 0.55 3.03 2.34 < 7 5 2 1.45 0.05 3.44 < 8 5 2 15.40 17.96 5.99 < -8 6 2 18.25 14.80 6.76 < -7 6 2 27.30 24.40 5.45 o -6 6 2 110.90 128.65 6.30 o -5 6 2 76.70 74.45 4.47 o -4 6 2 65.55 61.76 3.70 o -3 6 2 8.55 10.73 2.65 o -2 6 2 12.95 13.85 2.69 o -1 6 2 1.00 0.12 2.33 < 0 6 2 -1.90 0.20 2.28 < 1 6 2 52.35 55.59 3.00 o 2 6 2 100.45 93.21 4.00 o 3 6 2 23.40 21.57 2.97 o 4 6 2 73.35 70.36 4.56 o 5 6 2 18.75 24.07 2.67 o 6 6 2 19.90 19.59 3.37 o 7 6 2 68.15 63.07 8.04 o -6 7 2 17.00 15.78 3.90 o -5 7 2 28.25 27.54 3.46 o -4 7 2 24.15 27.47 3.36 o -3 7 2 1.60 0.05 4.39 < -2 7 2 2.50 0.94 3.17 < -1 7 2 8.00 6.56 2.65 o 0 7 2 6.10 6.27 2.36 < 1 7 2 6.60 8.37 2.36 < 2 7 2 3.80 4.85 1.91 < 3 7 2 1.45 1.34 2.91 < 4 7 2 30.45 31.21 3.41 o 5 7 2 68.90 68.80 9.21 o 6 7 2 19.60 28.98 7.42 < -4 8 2 75.90 72.46 5.76 o -3 8 2 45.45 47.50 5.66 o -2 8 2 23.40 28.27 4.56 o -1 8 2 98.50 91.63 7.51 o 0 8 2 126.35 113.46 8.59 o 1 8 2 166.10 165.91 10.50 o 2 8 2 126.40 127.06 8.10 o 3 8 2 36.20 30.47 4.70 o 4 8 2 17.30 18.65 10.50 < -10 1 3 87.45 76.22 10.15 o -9 1 3 71.85 70.94 5.06 o -8 1 3 102.20 96.99 4.43 o -7 1 3 132.30 129.40 4.50 o -6 1 3 16.05 17.88 1.58 o -5 1 3 656.45 655.60 16.36 o -4 1 3 561.10 557.67 14.97 o -3 1 3 2722.05 2720.11 78.29 o -2 1 3 2570.65 2594.79 69.51 o -1 1 3 25.10 21.51 2.94 o 0 1 3 226.15 197.50 7.15 o 1 1 3 130.25 117.14 4.04 o 2 1 3 664.25 631.43 17.75 o 3 1 3 903.65 858.59 20.12 o 4 1 3 637.25 610.10 13.70 o 5 1 3 516.90 509.21 12.42 o 6 1 3 4.80 0.12 2.30 < 7 1 3 1.75 6.94 3.16 < 8 1 3 29.00 30.54 3.55 o 9 1 3 16.40 15.92 6.79 < -10 2 3 6.35 1.33 6.84 < -9 2 3 12.75 15.52 3.29 o -8 2 3 25.55 21.13 2.20 o -7 2 3 15.30 19.81 2.97 o -6 2 3 4.25 5.56 2.35 < -5 2 3 72.45 75.74 3.17 o -4 2 3 70.45 73.41 3.11 o -3 2 3 43.10 43.65 2.32 o -2 2 3 442.75 454.85 14.32 o -1 2 3 152.65 124.74 4.75 o 0 2 3 3.35 4.29 2.35 < 1 2 3 124.15 85.96 4.65 o 2 2 3 423.85 509.94 12.52 o 3 2 3 89.80 82.72 3.22 o 4 2 3 7.60 7.73 2.18 o 5 2 3 34.75 30.90 2.46 o 6 2 3 8.05 8.11 2.33 o 7 2 3 0.85 1.01 2.41 < 8 2 3 -2.80 3.37 3.26 < 9 2 3 4.80 4.60 5.40 < -10 3 3 53.30 56.83 7.23 o -9 3 3 46.35 48.30 5.97 o -8 3 3 94.80 94.33 5.76 o -7 3 3 6.60 6.77 2.95 < -6 3 3 6.65 4.39 2.50 < -5 3 3 303.65 304.26 9.59 o -4 3 3 210.85 198.30 5.55 o -3 3 3 718.65 725.34 18.83 o -2 3 3 444.20 454.03 12.56 o -1 3 3 2.45 2.94 1.92 < 0 3 3 32.05 22.90 2.16 o 1 3 3 21.60 25.62 3.01 o 2 3 3 278.30 270.83 8.44 o 3 3 3 358.35 348.43 9.55 o 4 3 3 305.65 300.65 9.89 o 5 3 3 388.85 346.71 10.43 o 6 3 3 15.85 18.40 2.62 o 7 3 3 9.90 6.86 2.96 o 8 3 3 37.30 40.19 6.39 o 9 3 3 17.70 12.22 6.73 < -9 4 3 11.40 12.52 6.97 < -8 4 3 10.45 10.55 4.44 < -7 4 3 -0.95 0.56 3.49 < -6 4 3 68.20 74.10 5.02 o -5 4 3 234.55 233.53 14.04 o -4 4 3 198.25 202.88 5.95 o -3 4 3 3.20 3.84 1.56 < -2 4 3 295.85 307.68 8.20 o -1 4 3 173.60 182.32 5.16 o 0 4 3 24.65 19.78 1.46 o 1 4 3 47.00 39.21 3.54 o 2 4 3 180.90 187.61 6.40 o 3 4 3 4.80 7.03 2.33 < 4 4 3 69.10 70.65 3.88 o 5 4 3 118.60 127.50 5.82 o 6 4 3 31.35 36.54 3.46 o 7 4 3 10.75 0.02 6.06 < 8 4 3 3.35 3.83 5.40 < -8 5 3 28.20 30.79 4.60 o -7 5 3 5.85 3.72 4.21 < -6 5 3 34.80 37.39 3.61 o -5 5 3 183.70 193.45 7.25 o -4 5 3 116.50 116.11 4.61 o -3 5 3 374.65 360.32 11.80 o -2 5 3 359.95 361.18 12.63 o -1 5 3 210.85 201.89 8.16 o 0 5 3 250.35 264.13 8.20 o 1 5 3 103.45 99.79 5.66 o 2 5 3 172.90 171.23 7.91 o 3 5 3 99.30 100.49 4.55 o 4 5 3 66.40 64.08 4.26 o 5 5 3 120.65 116.84 7.28 o 6 5 3 18.50 16.07 4.87 o 7 5 3 4.00 8.90 5.11 < -7 6 3 17.90 16.27 5.05 o -6 6 3 2.45 2.87 2.81 < -5 6 3 18.00 17.47 2.76 o -4 6 3 7.55 9.93 2.16 o -3 6 3 21.05 24.96 3.75 o -2 6 3 159.45 162.71 8.21 o -1 6 3 47.30 55.42 3.03 o 0 6 3 -1.20 0.01 1.79 < 1 6 3 68.45 72.35 5.25 o 2 6 3 204.05 216.41 10.39 o 3 6 3 70.85 63.24 5.71 o 4 6 3 2.15 0.66 4.15 < 5 6 3 5.70 9.12 6.05 < 6 6 3 14.40 5.31 6.42 < -6 7 3 32.65 41.51 6.24 o -5 7 3 40.10 45.82 5.46 o -4 7 3 5.30 2.04 3.31 < -3 7 3 9.20 8.94 3.16 < -2 7 3 6.50 8.31 2.95 < -1 7 3 11.75 15.82 2.75 o 0 7 3 65.40 59.26 4.46 o 1 7 3 14.80 15.94 1.87 o 2 7 3 13.15 17.36 4.40 o 3 7 3 8.15 10.82 4.66 < 4 7 3 18.00 15.70 4.81 o 5 7 3 58.50 65.72 9.56 o -4 8 3 13.25 28.28 4.30 o -3 8 3 3.00 1.43 3.20 < -2 8 3 14.50 19.35 3.00 o -1 8 3 11.60 14.79 2.90 o 0 8 3 26.20 9.00 7.20 o 1 8 3 8.70 0.30 6.70 < 2 8 3 -2.50 5.43 6.50 < 3 8 3 -3.25 0.17 7.36 < -10 0 4 72.30 59.06 8.80 o -9 0 4 19.90 21.01 1.80 o -8 0 4 8.90 8.41 1.50 o -7 0 4 8.20 6.82 1.30 o -6 0 4 20.70 18.44 1.40 o -5 0 4 746.50 701.50 19.00 o -4 0 4 1800.00 1840.17 40.70 o -3 0 4 550.40 530.82 16.70 o -2 0 4 2121.90 2192.16 61.50 o -1 0 4 950.00 988.82 32.40 o 0 0 4 337.70 327.34 9.10 o 1 0 4 974.70 1078.60 27.40 o 2 0 4 821.90 860.04 19.70 o 3 0 4 491.20 429.47 12.90 o 4 0 4 9.70 9.93 1.60 o 5 0 4 5.70 4.35 1.90 o 6 0 4 48.70 47.88 2.80 o 7 0 4 5.00 2.27 2.20 < 8 0 4 42.10 43.23 4.10 o 9 0 4 14.70 27.44 5.00 < -10 1 4 3.70 3.93 6.30 < -9 1 4 33.10 32.80 3.76 o -8 1 4 38.90 41.88 3.00 o -7 1 4 38.95 42.38 2.96 o -6 1 4 58.30 58.79 3.05 o -5 1 4 53.90 53.24 2.70 o -4 1 4 84.25 85.42 3.26 o -3 1 4 92.50 99.74 2.91 o -2 1 4 67.80 69.56 2.80 o -1 1 4 -2.35 1.36 2.79 < 0 1 4 171.55 178.17 6.00 o 1 1 4 185.05 162.01 6.97 o 2 1 4 143.15 142.02 4.70 o 3 1 4 120.00 133.85 3.55 o 4 1 4 51.65 40.98 2.45 o 5 1 4 36.95 34.81 2.40 o 6 1 4 25.80 33.94 2.85 o 7 1 4 13.90 13.76 3.36 o 8 1 4 5.65 0.81 4.06 < -10 2 4 138.95 137.85 16.56 o -9 2 4 90.50 91.63 7.20 o -8 2 4 64.00 59.51 4.56 o -7 2 4 31.90 32.73 2.85 o -6 2 4 23.90 25.21 2.50 o -5 2 4 136.30 135.92 5.26 o -4 2 4 249.55 259.98 7.95 o -3 2 4 11.30 14.45 1.10 o -2 2 4 50.20 64.10 2.31 o -1 2 4 31.65 27.48 1.55 o 0 2 4 96.65 91.62 5.47 o 1 2 4 21.40 24.53 2.86 o 2 2 4 94.95 100.59 3.52 o 3 2 4 189.60 178.65 5.89 o 4 2 4 35.35 36.03 2.85 o 5 2 4 84.90 82.89 3.71 o 6 2 4 200.30 185.82 9.26 o 7 2 4 63.80 63.05 4.30 o 8 2 4 130.30 112.85 10.94 o -9 3 4 10.15 7.34 4.98 < -8 3 4 2.75 1.78 3.36 < -7 3 4 50.70 56.39 4.02 o -6 3 4 138.30 146.50 5.71 o -5 3 4 237.05 229.73 8.01 o -4 3 4 83.25 84.84 3.57 o -3 3 4 2.55 1.68 3.16 < -2 3 4 61.65 70.77 2.53 o -1 3 4 27.85 29.36 2.89 o 0 3 4 -1.05 9.81 3.18 < 1 3 4 21.50 19.97 3.57 o 2 3 4 82.40 94.66 3.63 o 3 3 4 106.90 96.15 4.66 o 4 3 4 140.85 152.07 6.72 o 5 3 4 44.15 45.38 2.89 o 6 3 4 -2.90 0.12 2.49 < 7 3 4 1.65 1.92 4.65 < 8 3 4 -5.20 0.33 5.53 < -9 4 4 9.10 15.22 6.35 < -8 4 4 16.45 20.02 4.30 o -7 4 4 44.00 46.10 4.50 o -6 4 4 -0.10 3.46 3.64 < -5 4 4 186.90 180.81 7.92 o -4 4 4 413.35 412.08 12.70 o -3 4 4 310.30 300.51 10.19 o -2 4 4 924.50 949.43 36.54 o -1 4 4 593.75 598.94 20.79 o 0 4 4 353.05 363.60 13.41 o 1 4 4 343.70 358.19 13.91 o 2 4 4 140.75 141.31 6.95 o 3 4 4 125.75 119.47 5.26 o 4 4 4 37.00 38.54 3.55 o 5 4 4 48.10 45.01 4.60 o 6 4 4 52.00 57.51 6.34 o 7 4 4 2.30 5.23 5.25 < -8 5 4 24.60 36.09 4.90 o -7 5 4 9.95 14.04 4.89 < -6 5 4 6.25 2.16 4.11 < -5 5 4 3.05 0.85 2.20 < -4 5 4 7.90 8.59 2.15 o -3 5 4 32.25 33.23 2.66 o -2 5 4 62.60 73.69 3.92 o -1 5 4 6.80 5.94 2.60 < 0 5 4 57.90 63.82 5.19 o 1 5 4 48.35 49.83 4.77 o 2 5 4 36.70 35.37 5.08 o 3 5 4 24.40 31.30 4.15 o 4 5 4 1.65 4.19 2.91 < 5 5 4 12.15 12.07 4.97 < 6 5 4 17.30 22.77 7.14 < -7 6 4 48.40 60.20 4.90 o -6 6 4 6.70 3.45 3.10 < -5 6 4 5.70 6.37 2.35 < -4 6 4 0.65 5.54 3.64 < -3 6 4 0.90 0.18 2.80 < -2 6 4 83.80 79.11 5.98 o -1 6 4 42.35 42.39 3.26 o 0 6 4 15.10 15.43 4.43 o 1 6 4 11.50 13.58 4.67 < 2 6 4 2.95 0.20 4.90 < 3 6 4 3.10 10.96 4.76 < 4 6 4 33.85 36.27 5.63 o 5 6 4 79.60 72.71 10.80 o -5 7 4 33.00 44.70 4.80 o -4 7 4 14.15 23.03 6.20 < -3 7 4 5.20 7.84 3.65 < -2 7 4 2.70 1.20 3.71 < -1 7 4 7.75 10.22 3.34 < 0 7 4 21.80 2.29 5.70 o 1 7 4 9.80 13.87 6.67 < 2 7 4 14.20 11.26 6.45 < 3 7 4 5.25 3.21 7.15 < 4 7 4 7.05 7.08 9.14 < -2 8 4 144.30 132.69 14.50 o -1 8 4 111.90 127.89 8.30 o 0 8 4 103.90 93.90 11.50 o 1 8 4 73.00 52.70 9.30 o -10 1 5 7.50 2.95 7.96 < -9 1 5 10.50 15.67 6.17 < -8 1 5 47.85 44.91 3.77 o -7 1 5 194.75 183.26 8.32 o -6 1 5 266.35 260.65 9.96 o -5 1 5 126.60 103.75 4.86 o -4 1 5 262.55 264.29 11.83 o -3 1 5 1.75 2.13 1.57 < -2 1 5 31.50 39.17 2.33 o -1 1 5 734.00 774.70 21.26 o 0 1 5 717.10 687.95 20.31 o 1 1 5 752.40 726.26 28.81 o 2 1 5 400.00 444.24 10.54 o 3 1 5 5.75 4.63 1.71 o 4 1 5 13.10 16.45 2.01 o 5 1 5 0.45 0.85 2.05 < 6 1 5 103.00 98.53 5.60 o 7 1 5 164.95 155.70 8.03 o 8 1 5 56.05 54.13 8.02 o -9 2 5 2.55 0.67 4.45 < -8 2 5 0.70 0.04 3.65 < -7 2 5 3.90 8.08 2.55 < -6 2 5 3.85 0.86 2.12 < -5 2 5 45.75 45.59 2.85 o -4 2 5 44.95 43.76 2.82 o -3 2 5 11.25 11.37 1.53 o -2 2 5 18.05 17.74 2.40 o -1 2 5 82.15 92.16 2.77 o 0 2 5 69.40 77.20 4.49 o 1 2 5 6.55 2.97 3.15 < 2 2 5 61.50 65.15 3.94 o 3 2 5 24.65 27.53 2.28 o 4 2 5 0.40 2.02 2.60 < 5 2 5 15.35 14.49 2.51 o 6 2 5 21.60 23.49 3.06 o 7 2 5 7.00 6.81 4.24 < -9 3 5 40.50 38.95 8.17 o -8 3 5 48.85 54.09 6.36 o -7 3 5 121.80 120.50 6.86 o -6 3 5 124.70 123.41 6.07 o -5 3 5 17.35 18.85 2.45 o -4 3 5 86.40 91.60 4.24 o -3 3 5 -0.10 0.01 1.57 < -2 3 5 -1.30 1.73 2.92 < -1 3 5 349.15 350.45 16.41 o 0 3 5 228.20 220.33 9.42 o 1 3 5 237.80 253.10 13.24 o 2 3 5 183.95 175.65 10.20 o 3 3 5 8.30 10.51 2.62 o 4 3 5 0.40 3.80 2.92 < 5 3 5 11.45 14.09 3.81 o 6 3 5 94.80 93.67 9.52 o 7 3 5 94.60 102.58 11.75 o -8 4 5 1.20 5.21 6.96 < -7 4 5 35.35 37.83 4.10 o -6 4 5 4.55 5.63 2.96 < -5 4 5 10.80 8.35 2.56 o -4 4 5 10.65 12.63 1.59 o -3 4 5 3.45 0.58 1.50 < -2 4 5 29.70 34.84 2.50 o -1 4 5 54.05 54.52 4.60 o 0 4 5 17.50 19.97 4.67 o 1 4 5 19.90 18.76 4.71 o 2 4 5 215.30 215.24 10.71 o 3 4 5 95.20 101.53 8.45 o 4 4 5 1.25 1.83 3.01 < 5 4 5 12.90 8.95 4.93 < 6 4 5 31.60 26.02 7.40 o -7 5 5 43.25 52.02 6.03 o -6 5 5 61.00 59.58 8.01 o -5 5 5 14.15 16.18 4.49 o -4 5 5 102.05 112.76 5.54 o -3 5 5 103.95 106.77 7.05 o 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20.80 25.48 2.60 o 4 0 6 9.00 14.08 1.90 o 5 0 6 0.20 1.74 1.79 < 6 0 6 24.50 29.15 2.50 o 7 0 6 45.10 45.06 6.50 o -9 1 6 0.10 2.27 7.41 < -8 1 6 9.30 7.31 5.18 < -7 1 6 21.80 21.75 2.89 o -6 1 6 37.10 45.08 3.39 o -5 1 6 110.00 112.31 5.55 o -4 1 6 76.85 77.95 5.90 o -3 1 6 -1.40 1.55 2.02 < -2 1 6 21.95 17.87 1.95 o -1 1 6 62.35 60.56 2.80 o 0 1 6 57.05 63.57 2.80 o 1 1 6 30.75 30.32 2.66 o 2 1 6 16.55 18.11 2.61 o 3 1 6 19.35 18.95 2.25 o 4 1 6 39.70 39.55 2.62 o 5 1 6 27.35 29.81 2.70 o 6 1 6 3.10 6.77 4.00 < 7 1 6 3.35 0.60 5.66 < -9 2 6 3.70 0.11 7.21 < -8 2 6 96.90 96.85 8.98 o -7 2 6 210.20 200.96 10.90 o -6 2 6 217.00 202.76 10.16 o -5 2 6 40.80 32.32 3.10 o -4 2 6 29.90 36.07 2.80 o -3 2 6 22.00 29.66 2.01 o -2 2 6 136.25 137.15 3.87 o -1 2 6 21.25 22.11 1.60 o 0 2 6 459.90 444.30 15.11 o 1 2 6 91.80 93.59 3.91 o 2 2 6 74.00 79.02 5.10 o 3 2 6 30.25 34.83 3.73 o 4 2 6 2.45 1.20 3.05 < 5 2 6 36.05 37.43 3.95 o 6 2 6 84.60 82.44 6.75 o -8 3 6 70.05 62.84 7.86 o -7 3 6 48.00 48.21 4.51 o -6 3 6 12.85 16.50 3.32 o -5 3 6 18.80 17.62 2.73 o -4 3 6 13.15 14.42 2.55 o -3 3 6 14.60 17.69 1.65 o -2 3 6 55.95 62.93 4.71 o -1 3 6 37.25 35.10 4.21 o 0 3 6 10.35 4.68 3.56 < 1 3 6 94.65 103.83 7.85 o 2 3 6 170.40 183.66 11.80 o 3 3 6 111.50 112.92 10.46 o 4 3 6 4.75 2.67 3.32 < 5 3 6 7.55 2.19 6.37 < 6 3 6 -0.95 0.00 9.75 < -7 4 6 79.50 83.14 6.15 o -6 4 6 161.45 156.50 9.15 o -5 4 6 155.75 151.94 7.73 o -4 4 6 90.45 88.75 4.94 o -3 4 6 202.95 193.44 9.04 o -2 4 6 82.85 96.49 6.26 o -1 4 6 260.55 252.02 15.61 o 0 4 6 496.50 469.17 26.14 o 1 4 6 145.60 157.96 9.11 o 2 4 6 146.00 143.32 11.42 o 3 4 6 70.25 59.27 8.39 o 4 4 6 -0.85 2.20 7.18 < 5 4 6 2.95 5.26 6.91 < -6 5 6 29.25 25.56 6.08 o -5 5 6 157.25 139.23 12.34 o -4 5 6 82.15 85.29 8.14 o -3 5 6 0.90 0.03 4.55 < -2 5 6 59.95 53.29 6.55 o -1 5 6 101.50 100.77 8.12 o 0 5 6 35.65 32.05 5.73 o 1 5 6 0.20 0.30 6.01 < 2 5 6 4.20 5.94 6.40 < 3 5 6 1.70 1.74 6.46 < 4 5 6 16.05 22.76 7.07 < -5 6 6 14.30 15.72 7.40 < -4 6 6 8.90 4.46 6.91 < -3 6 6 35.20 18.93 8.80 o -2 6 6 5.00 0.44 7.00 < -1 6 6 4.10 1.07 6.35 < 0 6 6 7.00 14.32 6.71 < 1 6 6 6.10 5.09 10.57 < 2 6 6 45.25 45.74 8.60 o 3 6 6 63.30 53.91 9.50 o -8 1 7 11.15 9.19 6.26 < -7 1 7 214.10 198.99 13.85 o -6 1 7 110.80 114.83 8.01 o -5 1 7 42.60 54.26 5.92 o -4 1 7 43.35 41.73 3.32 o -3 1 7 72.20 75.29 4.54 o -2 1 7 200.30 185.50 7.05 o -1 1 7 57.25 61.36 3.11 o 0 1 7 189.40 198.76 7.62 o 1 1 7 88.95 90.91 4.20 o 2 1 7 -2.10 0.38 2.42 < 3 1 7 88.80 91.23 5.31 o 4 1 7 105.15 104.52 6.71 o 5 1 7 43.65 40.71 4.65 o -8 2 7 -2.80 1.69 7.35 < -7 2 7 2.15 3.17 5.22 < -6 2 7 7.75 7.94 3.28 < -5 2 7 0.00 4.48 5.42 < -4 2 7 5.10 4.80 2.16 < -3 2 7 5.80 5.33 1.45 o -2 2 7 16.60 17.79 1.78 o -1 2 7 -0.85 0.00 3.17 < 0 2 7 2.50 3.09 3.17 < 1 2 7 -2.05 0.42 3.84 < 2 2 7 0.95 2.93 4.56 < 3 2 7 6.70 7.30 4.14 < 4 2 7 4.35 5.82 10.32 < 5 2 7 8.00 1.42 6.85 < -7 3 7 103.40 100.18 10.86 o -6 3 7 43.15 55.91 6.16 o -5 3 7 42.85 48.23 4.07 o -4 3 7 31.65 32.38 3.27 o -3 3 7 26.00 26.21 1.80 o -2 3 7 51.50 56.77 4.41 o -1 3 7 3.60 8.19 3.62 < 0 3 7 70.95 77.90 5.85 o 1 3 7 77.20 66.65 7.98 o 2 3 7 9.15 14.96 5.31 < 3 3 7 103.70 107.72 10.32 o 4 3 7 87.85 80.32 10.35 o -6 4 7 1.50 0.14 4.54 < -5 4 7 2.60 0.12 3.30 < -4 4 7 -2.20 2.54 4.72 < -3 4 7 9.25 5.65 3.48 < -2 4 7 7.65 9.46 4.97 < -1 4 7 6.05 3.48 5.85 < 0 4 7 13.05 18.70 5.37 < 1 4 7 17.80 13.50 5.67 o 2 4 7 0.00 0.52 6.35 < 3 4 7 5.80 0.15 6.65 < 4 4 7 2.40 0.30 6.70 < -5 5 7 113.30 97.06 11.30 o -4 5 7 120.05 114.02 13.10 o -3 5 7 67.55 74.84 9.94 o -2 5 7 76.85 72.23 9.80 o -1 5 7 17.35 18.90 6.50 < 0 5 7 51.30 50.84 8.97 o 1 5 7 54.55 62.56 9.35 o 2 5 7 25.70 35.81 7.52 o -7 0 8 3.20 6.09 4.40 < -6 0 8 72.10 70.64 8.80 o -5 0 8 17.40 30.28 6.30 < -4 0 8 236.00 234.90 11.80 o -3 0 8 601.10 565.53 23.50 o -2 0 8 548.30 503.27 20.40 o -1 0 8 173.40 178.59 7.50 o 0 0 8 4.40 3.56 2.10 < 1 0 8 9.60 9.35 2.20 o 2 0 8 4.40 5.21 3.30 < 3 0 8 38.00 41.38 4.70 o 4 0 8 205.70 180.10 17.90 o -7 1 8 24.10 25.36 8.62 < -6 1 8 18.45 18.72 5.55 o -5 1 8 2.70 2.00 5.41 < -4 1 8 0.55 0.22 3.34 < -3 1 8 -1.80 0.16 3.81 < -2 1 8 -2.25 1.04 2.49 < -1 1 8 1.70 1.07 2.87 < 0 1 8 1.70 2.88 3.64 < 1 1 8 19.80 22.36 2.71 o 2 1 8 40.75 43.50 3.60 o 3 1 8 29.20 31.22 5.61 o -6 2 8 21.40 9.38 8.38 < -5 2 8 16.60 2.80 8.40 < -4 2 8 18.05 22.16 3.26 o -3 2 8 98.15 90.35 4.45 o -2 2 8 64.05 66.55 3.54 o -1 2 8 4.60 7.52 4.45 < 0 2 8 16.80 14.61 4.91 o 1 2 8 -2.55 0.39 5.39 < 2 2 8 1.45 6.14 5.43 < 3 2 8 56.55 58.41 8.39 o -5 3 8 42.15 43.79 7.84 o -4 3 8 48.00 42.70 7.76 o -3 3 8 0.90 1.01 3.34 < -2 3 8 8.35 10.22 3.58 < -1 3 8 55.40 61.55 6.39 o 0 3 8 75.60 78.19 7.90 o 1 3 8 7.85 10.19 5.59 < 2 3 8 1.10 2.60 8.02 < -4 4 8 178.80 162.38 13.30 o -3 4 8 213.05 202.67 14.34 o -2 4 8 143.45 143.45 12.40 o -1 4 8 78.95 81.50 7.92 o 0 4 8 21.50 19.49 6.08 o 1 4 8 25.95 32.74 9.00 < -4 1 9 26.10 39.76 5.83 o -3 1 9 243.95 230.96 12.87 o -2 1 9 187.40 177.42 9.97 o -1 1 9 28.60 31.61 4.10 o 0 1 9 -0.60 0.89 3.78 < 1 1 9 -4.00 0.71 5.81 < -3 2 9 3.95 0.05 4.32 < -2 2 9 6.05 8.01 5.41 < -1 2 9 3.70 3.70 4.35 < 0 2 9 8.50 0.33 4.14 <