#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214869.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214869_Fobs loop_ _publ_author_name 'Shustova, Natalia B.' 'Peryshkov, Dimitry V.' 'Kareev, Ivan E.' 'Boltalina, Olga V.' 'Strauss, Steven H.' _publ_section_title ; 1,6,11,16,18,24,27,36-Octakis(trifluoromethyl)-1,6,11,16,18,24,27,36-octahydro(C~60~--I~h~)[5,6]fullerene deuterochloroform solvate ; _journal_coeditor_code TK2170 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3398 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.821 _cell_angle_gamma 90.000 _cell_length_a 14.5346 _cell_length_b 15.5805 _cell_length_c 20.1746 _exptl_crystal_F_000 2728.00 _reflns_d_resolution_high 0.6600 _[local]_cod_data_source_file tk2170Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ss182r_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 387.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1555.36 1508.58 26.59 o 3 0 0 1709.81 1632.24 28.11 o 4 0 0 15771.76 14691.22 166.41 o 5 0 0 69065.82 67146.31 727.31 o 6 0 0 9747.19 10183.73 122.93 o 7 0 0 2970.72 2174.90 44.03 o 8 0 0 4070.34 4080.50 74.96 o 9 0 0 1769.40 2132.27 53.35 o 10 0 0 5951.14 5804.87 103.31 o 11 0 0 275.60 280.09 29.18 o 12 0 0 9719.84 9312.83 253.18 o 13 0 0 9310.31 9694.39 212.78 o 14 0 0 4257.88 4010.41 122.07 o 15 0 0 1496.18 1382.09 79.60 o 16 0 0 3075.56 3013.06 114.73 o 17 0 0 3801.02 4349.17 141.57 o 18 0 0 1254.99 1048.46 107.26 o 19 0 0 1192.07 1262.05 122.47 o 20 0 0 569.10 423.22 142.03 o 1 1 0 3878.52 4936.90 45.70 o 2 1 0 1603.43 1697.72 22.24 o 3 1 0 17250.65 19371.32 155.19 o 4 1 0 7986.16 7745.66 66.44 o 5 1 0 31958.49 32463.73 254.66 o 6 1 0 64110.50 62221.91 480.60 o 7 1 0 202.82 183.57 9.66 o 8 1 0 58.51 52.46 10.32 o 9 1 0 507.54 570.71 19.57 o 10 1 0 1024.76 1004.75 26.67 o 11 1 0 4024.95 3935.76 55.00 o 12 1 0 3433.41 3269.41 65.73 o 13 1 0 11.45 -5.16 23.92 o 14 1 0 218.62 251.37 31.09 o 15 1 0 730.09 697.31 42.87 o 16 1 0 3.44 75.02 37.88 o 17 1 0 11.65 15.03 37.75 o 18 1 0 159.58 209.81 46.87 o 19 1 0 91.62 80.60 64.03 o 20 1 0 124.55 76.16 69.94 o 21 1 0 72.04 -23.81 120.30 o 0 2 0 6985.16 6545.03 79.35 o 1 2 0 2365.84 2215.11 21.95 o 2 2 0 27478.88 30466.34 224.00 o 3 2 0 39025.55 40743.35 357.81 o 4 2 0 3.41 24.08 11.21 o 5 2 0 55840.71 56450.99 473.91 o 6 2 0 4778.06 5012.49 56.85 o 7 2 0 2949.91 3784.79 42.25 o 8 2 0 828.67 877.34 18.75 o 9 2 0 21.41 3.09 10.72 o 10 2 0 130.05 143.61 13.31 o 11 2 0 3954.16 4038.63 52.78 o 12 2 0 1469.22 1382.70 35.17 o 13 2 0 648.28 646.01 46.62 o 14 2 0 4303.55 4265.98 98.65 o 15 2 0 94.49 51.21 27.75 o 16 2 0 173.24 151.77 39.04 o 17 2 0 77.72 114.40 41.02 o 18 2 0 221.52 217.70 54.45 o 19 2 0 14.52 30.15 52.41 o 20 2 0 0.34 -36.30 74.59 o 21 2 0 271.65 198.48 88.53 o 1 3 0 43315.71 46052.09 345.11 o 2 3 0 1357.77 1487.97 20.73 o 3 3 0 7552.65 8410.43 70.26 o 4 3 0 4147.71 4762.51 56.04 o 5 3 0 13.87 17.85 13.24 o 6 3 0 3029.54 3526.95 69.30 o 7 3 0 2249.71 1885.27 42.53 o 8 3 0 1382.81 1438.02 33.59 o 9 3 0 711.34 745.59 22.42 o 10 3 0 1436.88 1492.03 29.95 o 11 3 0 2351.29 2245.17 38.63 o 12 3 0 3888.34 3967.46 61.56 o 13 3 0 2105.47 2046.65 60.17 o 14 3 0 1.26 -18.67 26.12 o 15 3 0 200.81 207.07 37.16 o 16 3 0 185.34 168.80 38.70 o 17 3 0 4704.94 4621.50 227.85 o 18 3 0 1032.97 1107.00 80.32 o 19 3 0 8.41 -53.45 68.63 o 20 3 0 42.95 101.48 66.35 o 21 3 0 60.81 -14.02 79.63 o 0 4 0 26267.59 27358.29 308.62 o 1 4 0 3572.05 3110.58 35.64 o 2 4 0 2325.24 2105.65 25.83 o 3 4 0 1778.70 1865.34 22.87 o 4 4 0 2952.25 2876.50 29.58 o 5 4 0 13458.02 13483.66 140.99 o 6 4 0 14954.73 15934.98 173.70 o 7 4 0 198.61 76.59 18.61 o 8 4 0 5070.23 5353.76 84.20 o 9 4 0 208.66 220.29 24.40 o 10 4 0 1902.53 1904.20 39.31 o 11 4 0 2735.39 2749.16 57.23 o 12 4 0 3088.71 3230.36 107.98 o 13 4 0 1334.30 1291.20 61.57 o 14 4 0 1.68 -20.03 32.66 o 15 4 0 905.13 876.01 51.95 o 16 4 0 41.55 -34.41 39.42 o 17 4 0 508.93 430.37 57.98 o 18 4 0 1038.25 1261.86 95.10 o 19 4 0 512.93 581.26 76.85 o 20 4 0 7.97 27.46 84.60 o 21 4 0 39.29 150.33 84.80 o 1 5 0 40093.20 42263.91 333.82 o 2 5 0 1678.96 1410.08 23.81 o 3 5 0 790.97 537.69 16.61 o 4 5 0 10.05 -8.59 9.00 o 5 5 0 27149.24 30469.78 246.51 o 6 5 0 19704.55 21794.99 219.97 o 7 5 0 434.51 646.22 27.15 o 8 5 0 201.44 125.19 23.37 o 9 5 0 320.74 380.76 29.48 o 10 5 0 84.24 61.28 24.59 o 11 5 0 502.18 456.69 28.76 o 12 5 0 4897.32 4958.06 92.28 o 13 5 0 0.10 8.92 29.96 o 14 5 0 983.83 1007.68 61.72 o 15 5 0 1160.51 1156.41 68.52 o 16 5 0 77.65 5.36 43.66 o 17 5 0 1.03 -34.34 45.46 o 18 5 0 21.81 67.98 54.24 o 19 5 0 18.53 53.36 63.75 o 20 5 0 28.58 -62.42 71.49 o 21 5 0 147.10 133.98 155.93 o 0 6 0 2654.59 2536.57 50.21 o 1 6 0 35.61 19.57 10.64 o 2 6 0 726.97 655.89 19.33 o 3 6 0 3105.99 3768.29 41.86 o 4 6 0 30.80 -9.26 9.26 o 5 6 0 6529.60 6026.66 64.00 o 6 6 0 114.60 217.78 13.89 o 7 6 0 721.36 810.73 23.47 o 8 6 0 4263.45 4175.40 83.91 o 9 6 0 60.16 60.44 26.64 o 10 6 0 122.88 137.88 29.66 o 11 6 0 584.66 643.27 41.32 o 12 6 0 507.05 488.92 50.33 o 13 6 0 3387.65 3291.71 89.40 o 14 6 0 35.16 -36.96 53.76 o 15 6 0 3703.98 3827.71 125.42 o 16 6 0 23.32 32.26 41.53 o 17 6 0 761.28 776.37 72.84 o 18 6 0 0.08 29.44 52.81 o 19 6 0 110.50 32.83 65.31 o 20 6 0 33.31 2.22 73.95 o 1 7 0 9389.96 10419.04 106.32 o 2 7 0 2918.55 3514.99 47.31 o 3 7 0 2257.49 2619.09 40.37 o 4 7 0 109.81 103.60 13.24 o 5 7 0 88.03 82.91 19.61 o 6 7 0 1527.02 1508.08 26.35 o 7 7 0 99.15 72.31 12.70 o 8 7 0 2589.67 2644.42 45.88 o 9 7 0 1483.98 1613.36 67.58 o 10 7 0 1317.00 1476.37 68.19 o 11 7 0 47.65 51.49 35.44 o 12 7 0 850.90 875.54 69.70 o 13 7 0 1407.05 1260.03 117.03 o 14 7 0 35.60 -49.55 59.23 o 15 7 0 800.55 670.19 101.03 o 16 7 0 0.33 18.18 71.94 o 17 7 0 9.75 29.56 43.90 o 18 7 0 12.79 31.39 51.14 o 19 7 0 66.43 31.23 75.25 o 20 7 0 41.47 4.39 68.40 o 0 8 0 1980.03 1476.23 46.58 o 1 8 0 7677.95 8554.58 93.91 o 2 8 0 2542.80 2542.97 42.71 o 3 8 0 6.16 1.92 12.10 o 4 8 0 2794.71 2992.56 46.10 o 5 8 0 150.84 205.25 18.18 o 6 8 0 2637.67 2668.45 44.05 o 7 8 0 553.99 606.18 23.90 o 8 8 0 3489.93 3375.74 59.36 o 9 8 0 73.11 9.99 17.96 o 10 8 0 482.83 534.89 39.93 o 11 8 0 4404.45 4068.60 118.91 o 12 8 0 26.49 -19.60 40.67 o 13 8 0 155.89 84.20 85.08 o 14 8 0 202.41 242.93 81.26 o 15 8 0 646.10 350.07 167.19 o 16 8 0 310.31 254.47 90.35 o 17 8 0 109.09 8.00 81.28 o 18 8 0 145.00 186.03 58.08 o 19 8 0 560.48 611.00 120.86 o 20 8 0 354.31 305.93 137.40 o 1 9 0 47.27 16.11 14.30 o 2 9 0 1047.13 1283.45 34.83 o 3 9 0 197.24 196.53 17.58 o 4 9 0 189.04 92.91 16.87 o 5 9 0 6.89 11.06 15.22 o 6 9 0 2913.80 2837.96 52.37 o 7 9 0 1044.04 1118.61 30.69 o 8 9 0 1060.13 1075.67 32.74 o 9 9 0 0.27 -8.99 20.23 o 10 9 0 272.23 192.80 34.31 o 11 9 0 827.41 854.89 48.77 o 12 9 0 392.41 377.04 59.87 o 13 9 0 1281.41 1151.22 123.13 o 14 9 0 6.70 44.22 74.24 o 15 9 0 270.28 349.56 213.29 o 16 9 0 68.05 -24.76 73.66 o 17 9 0 13.15 89.31 127.81 o 18 9 0 79.91 35.79 127.81 o 19 9 0 1124.14 1325.58 220.48 o 20 9 0 74.63 -123.02 141.23 o 0 10 0 6563.60 6232.90 122.69 o 1 10 0 504.59 447.32 23.90 o 2 10 0 3202.28 3356.39 57.64 o 3 10 0 110.27 121.71 18.05 o 4 10 0 227.92 219.80 23.74 o 5 10 0 420.40 435.02 30.75 o 6 10 0 347.79 312.92 24.53 o 7 10 0 1050.37 891.76 35.35 o 8 10 0 11866.98 11538.12 132.42 o 9 10 0 842.23 795.26 48.56 o 10 10 0 6.72 -20.63 28.81 o 11 10 0 102.80 70.61 35.48 o 12 10 0 394.57 444.86 65.27 o 13 10 0 165.57 167.21 101.21 o 14 10 0 16.06 -71.47 71.47 o 15 10 0 70.05 106.29 86.80 o 16 10 0 165.88 2.85 82.75 o 17 10 0 27.13 86.91 136.12 o 18 10 0 8.39 4.79 133.40 o 19 10 0 554.23 539.37 186.13 o 1 11 0 91.98 106.82 19.35 o 2 11 0 3169.41 3066.58 52.30 o 3 11 0 224.56 209.00 21.28 o 4 11 0 455.46 486.77 28.54 o 5 11 0 10.46 15.46 24.61 o 6 11 0 55.50 1.10 22.69 o 7 11 0 735.54 662.49 37.90 o 8 11 0 3.10 -4.22 22.40 o 9 11 0 2270.61 2191.82 57.31 o 10 11 0 9.35 2.73 27.14 o 11 11 0 66.72 104.25 39.25 o 12 11 0 73.36 108.68 54.35 o 13 11 0 1009.04 970.14 205.54 o 14 11 0 750.96 767.96 119.19 o 15 11 0 19.09 88.36 104.73 o 16 11 0 1455.41 1517.13 220.00 o 17 11 0 80.80 -74.77 126.85 o 18 11 0 213.26 75.41 150.34 o 19 11 0 15.96 56.72 153.06 o 0 12 0 2017.91 2254.61 69.22 o 1 12 0 1884.05 1868.35 48.78 o 2 12 0 141.39 146.78 19.03 o 3 12 0 3310.46 3300.54 57.17 o 4 12 0 584.94 443.08 33.09 o 5 12 0 5531.35 5229.35 90.43 o 6 12 0 6511.75 6098.02 107.39 o 7 12 0 1.05 26.09 25.71 o 8 12 0 1542.49 1420.52 62.30 o 9 12 0 59.43 10.93 26.58 o 10 12 0 1404.75 1313.68 63.34 o 11 12 0 166.89 130.91 65.69 o 12 12 0 290.66 293.07 64.34 o 13 12 0 541.46 504.51 61.78 o 14 12 0 18.81 -19.58 44.07 o 15 12 0 70.96 42.91 81.68 o 16 12 0 1136.38 1428.94 233.42 o 17 12 0 2.80 41.70 148.26 o 18 12 0 6.12 225.11 172.39 o 1 13 0 786.21 802.77 34.39 o 2 13 0 3797.47 3369.43 65.58 o 3 13 0 264.94 372.95 31.96 o 4 13 0 622.99 639.78 44.30 o 5 13 0 1338.71 1373.78 58.00 o 6 13 0 693.71 589.74 44.46 o 7 13 0 386.24 291.44 37.99 o 8 13 0 1422.67 1456.97 59.68 o 9 13 0 14.88 -28.49 28.49 o 10 13 0 2609.83 2724.14 87.65 o 11 13 0 121.25 199.12 48.67 o 12 13 0 115.82 188.47 61.47 o 13 13 0 85.92 7.17 48.16 o 14 13 0 822.90 911.39 122.93 o 15 13 0 711.64 645.18 124.14 o 16 13 0 59.95 120.94 186.29 o 17 13 0 3.21 -90.43 151.14 o 18 13 0 542.46 258.18 178.94 o 0 14 0 2585.96 2435.72 74.94 o 1 14 0 33.94 9.35 24.81 o 2 14 0 570.35 626.14 42.66 o 3 14 0 412.32 430.53 45.60 o 4 14 0 339.08 288.35 43.37 o 5 14 0 158.24 180.54 51.75 o 6 14 0 396.81 409.12 45.00 o 7 14 0 887.17 829.64 55.74 o 8 14 0 1706.37 1830.73 76.00 o 9 14 0 719.59 779.42 51.62 o 10 14 0 1505.60 1455.91 80.60 o 11 14 0 21.47 -2.30 40.04 o 12 14 0 81.48 45.06 45.31 o 13 14 0 6.97 41.40 54.75 o 14 14 0 917.94 770.31 90.44 o 15 14 0 1098.89 1272.71 325.52 o 16 14 0 4.61 45.17 61.92 o 17 14 0 712.96 894.50 103.82 o 1 15 0 764.59 846.24 44.66 o 2 15 0 114.22 -5.71 30.17 o 3 15 0 1665.35 1549.99 71.10 o 4 15 0 1936.31 1904.00 76.09 o 5 15 0 3.25 -32.88 32.88 o 6 15 0 1608.25 1552.03 71.99 o 7 15 0 386.96 425.61 69.52 o 8 15 0 412.58 398.57 48.33 o 9 15 0 827.55 958.20 62.89 o 10 15 0 44.49 45.68 39.44 o 11 15 0 281.00 385.32 49.68 o 12 15 0 317.39 208.87 56.10 o 13 15 0 241.28 256.00 85.47 o 14 15 0 104.05 6.29 67.72 o 15 15 0 340.31 298.06 79.20 o 16 15 0 238.09 156.46 102.65 o 0 16 0 492.51 630.97 94.34 o 1 16 0 447.25 495.86 51.11 o 2 16 0 17.60 4.79 33.04 o 3 16 0 679.90 641.66 58.57 o 4 16 0 55.52 -14.61 34.00 o 5 16 0 167.02 152.85 39.97 o 6 16 0 190.11 162.95 41.35 o 7 16 0 472.99 577.30 49.83 o 8 16 0 473.52 348.37 45.55 o 9 16 0 18.49 20.94 35.98 o 10 16 0 1.09 11.57 39.73 o 11 16 0 232.85 205.19 56.82 o 12 16 0 1915.04 2112.59 129.04 o 13 16 0 210.74 106.39 73.57 o 14 16 0 0.07 16.99 73.50 o 15 16 0 354.58 478.62 92.79 o 1 17 0 174.45 110.56 68.63 o 2 17 0 37.79 -27.81 35.48 o 3 17 0 373.87 281.63 50.05 o 4 17 0 139.88 120.90 43.37 o 5 17 0 233.62 249.87 45.20 o 6 17 0 209.73 195.80 42.96 o 7 17 0 47.01 -37.62 37.62 o 8 17 0 172.91 101.02 43.06 o 9 17 0 108.98 137.20 43.02 o 10 17 0 51.44 82.76 45.09 o 11 17 0 111.42 55.83 54.60 o 12 17 0 129.68 179.34 77.44 o 13 17 0 143.70 148.07 85.17 o 14 17 0 50.74 147.36 116.15 o 15 17 0 3.87 43.07 81.41 o 0 18 0 13.87 -51.55 70.17 o 1 18 0 339.63 354.94 72.66 o 2 18 0 4.82 -0.37 47.95 o 3 18 0 113.74 -11.54 74.18 o 4 18 0 2.83 -36.36 39.38 o 5 18 0 100.01 108.18 45.11 o 6 18 0 350.67 266.24 53.73 o 7 18 0 0.01 51.92 42.07 o 8 18 0 1319.93 1361.24 73.40 o 9 18 0 137.77 175.82 53.46 o 10 18 0 30.74 -6.07 53.61 o 11 18 0 554.66 610.22 88.20 o 12 18 0 26.59 150.23 77.55 o 13 18 0 29.26 -80.56 80.73 o 14 18 0 395.47 412.66 104.66 o 1 19 0 219.54 168.33 108.15 o 2 19 0 15.46 13.79 73.54 o 3 19 0 0.24 -51.49 51.49 o 4 19 0 308.33 314.63 68.06 o 5 19 0 39.06 18.25 50.87 o 6 19 0 67.69 78.35 49.64 o 7 19 0 497.36 524.23 63.99 o 8 19 0 48.81 47.22 50.45 o 9 19 0 87.00 98.82 55.89 o 10 19 0 41.20 69.10 57.83 o 11 19 0 10.31 45.17 73.16 o 12 19 0 7.66 39.76 150.34 o 0 20 0 186.52 360.93 99.82 o 1 20 0 0.64 101.90 62.21 o 2 20 0 495.43 424.17 75.70 o 3 20 0 174.02 87.01 61.87 o 4 20 0 31.71 30.53 60.70 o 5 20 0 1.15 40.78 66.29 o 6 20 0 1.92 -38.74 59.30 o 7 20 0 233.73 122.73 64.08 o 8 20 0 642.64 746.52 78.08 o 9 20 0 41.46 -56.78 56.78 o 10 20 0 87.56 118.43 70.10 o 11 20 0 15.70 89.92 81.01 o 1 21 0 653.82 669.99 117.47 o 2 21 0 242.32 291.53 94.27 o 3 21 0 480.40 399.18 105.12 o 4 21 0 68.71 61.71 77.56 o 5 21 0 0.39 9.76 116.07 o 6 21 0 406.66 320.68 153.53 o 7 21 0 66.79 -4.02 153.53 o 8 21 0 55.61 -12.31 78.10 o 9 21 0 127.54 97.32 80.43 o 0 22 0 461.24 596.88 161.36 o 1 22 0 64.16 -48.60 105.45 o 2 22 0 55.33 131.38 89.08 o 3 22 0 19.84 -10.00 75.00 o 4 22 0 181.22 107.63 88.65 o 5 22 0 41.64 8.53 78.46 o 6 22 0 130.73 139.86 118.79 o 7 22 0 274.42 380.21 107.32 o 1 23 0 468.24 606.96 135.16 o 2 23 0 54.54 70.25 90.39 o 3 23 0 157.49 193.51 96.82 o 4 23 0 27.25 -68.14 80.29 o -20 1 1 520.09 537.18 99.24 o -19 1 1 603.07 603.06 80.09 o -18 1 1 219.59 237.65 47.14 o -17 1 1 1401.89 1425.57 70.77 o -16 1 1 821.03 872.85 70.34 o -15 1 1 64.67 96.62 30.69 o -14 1 1 130.51 153.77 29.06 o -13 1 1 2035.04 2105.33 54.40 o -12 1 1 49.83 49.78 18.25 o -11 1 1 108.81 69.41 15.29 o -10 1 1 434.54 442.44 18.29 o -9 1 1 3398.87 3816.57 42.67 o -8 1 1 2685.72 2467.05 30.92 o -7 1 1 355.84 444.91 15.97 o -6 1 1 1778.42 1611.74 22.42 o -5 1 1 1522.14 1597.60 20.77 o -4 1 1 8826.57 8914.62 81.84 o -3 1 1 16284.02 16558.10 133.80 o -2 1 1 2918.14 2867.08 25.05 o -1 1 1 11733.75 11573.89 82.76 o 0 1 1 917.30 891.99 14.93 o 1 1 1 2157.35 2181.98 19.29 o 2 1 1 217.03 179.20 6.20 o 3 1 1 5335.20 5180.82 44.77 o 4 1 1 17072.60 17350.11 139.77 o 5 1 1 7354.48 6997.65 65.39 o 6 1 1 11.59 27.00 8.11 o 7 1 1 18565.19 19845.37 161.83 o 8 1 1 2046.70 2259.38 33.63 o 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108.56 o -6 6 28 132.84 120.92 83.13 o -5 6 28 16.39 9.60 79.73 o -4 6 28 8.73 6.96 74.47 o -3 6 28 12.90 -13.34 72.81 o -2 6 28 353.50 259.75 91.60 o -1 6 28 675.57 847.50 144.37 o 0 6 28 368.24 275.07 91.77 o 1 6 28 10.42 -26.33 74.24 o 2 6 28 58.68 14.23 74.56 o 3 6 28 32.08 115.84 113.31 o -9 7 28 0.33 135.80 116.03 o -8 7 28 892.98 413.17 133.76 o -7 7 28 3.36 7.84 109.43 o -6 7 28 383.05 236.67 118.76 o -5 7 28 19.67 -77.18 77.18 o -4 7 28 518.84 487.50 105.10 o -3 7 28 250.06 286.00 96.53 o -2 7 28 175.06 400.79 100.48 o -1 7 28 238.68 315.02 113.83 o 0 7 28 814.52 715.75 188.92 o 1 7 28 118.96 53.25 81.39 o 2 7 28 22.97 -53.76 69.70 o -8 8 28 33.86 79.73 112.79 o -7 8 28 226.25 371.11 133.45 o -6 8 28 161.17 33.83 129.83 o -5 8 28 156.81 236.32 97.17 o -4 8 28 763.70 752.70 117.62 o -3 8 28 205.74 259.48 111.42 o -2 8 28 122.13 147.70 105.29 o -1 8 28 270.31 320.02 238.45 o 0 8 28 1.00 -10.52 133.80 o 1 8 28 18.48 -87.38 87.38 o -6 9 28 80.73 86.59 87.54 o -5 9 28 845.23 888.02 124.54 o -4 9 28 270.67 438.99 140.38 o -3 9 28 0.10 -23.82 103.05 o -2 9 28 108.91 186.04 106.57 o -1 9 28 20.61 114.84 109.59 o -10 1 29 1.47 -89.10 96.79 o -9 1 29 187.58 190.23 113.52 o -8 1 29 49.16 -84.88 149.38 o -7 1 29 144.23 -18.15 104.56 o -6 1 29 338.58 114.00 174.86 o -5 1 29 344.67 311.44 127.93 o -4 1 29 3145.83 3543.17 185.28 o -3 1 29 320.38 298.39 62.80 o -2 1 29 191.42 267.06 61.51 o -1 1 29 292.82 357.11 67.23 o 0 1 29 398.02 453.54 70.40 o 1 1 29 176.54 166.81 81.31 o 2 1 29 90.11 43.00 95.24 o 3 1 29 0.00 17.79 76.34 o -10 2 29 0.99 -103.24 103.24 o -9 2 29 45.70 -154.65 154.65 o -8 2 29 160.44 480.30 425.22 o -7 2 29 2.18 5.02 100.17 o -6 2 29 0.05 84.46 109.07 o -5 2 29 164.97 429.44 132.92 o -4 2 29 6.01 -4.44 78.85 o -3 2 29 1001.82 852.43 117.51 o -2 2 29 80.03 276.44 80.35 o -1 2 29 233.18 263.67 81.12 o 0 2 29 62.66 21.37 68.20 o 1 2 29 36.15 75.00 66.96 o 2 2 29 168.71 158.77 71.94 o 3 2 29 226.65 303.15 91.35 o -9 3 29 265.87 221.63 121.63 o -8 3 29 44.58 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110.66 o -5 6 29 1294.65 1390.90 141.99 o -4 6 29 11.38 39.13 106.87 o -3 6 29 978.34 916.58 203.99 o -2 6 29 95.02 57.18 87.44 o -1 6 29 35.66 56.21 103.71 o 0 6 29 80.30 159.17 109.91 o -5 7 29 90.16 37.77 85.94 o -4 7 29 227.61 217.54 92.38 o -3 7 29 32.52 43.82 83.98 o -2 7 29 174.90 124.64 109.45 o -7 0 30 30.98 -37.39 159.93 o -6 0 30 135.65 -88.51 152.58 o -5 0 30 147.93 74.13 158.33 o -3 0 30 57.09 4.88 78.71 o -2 0 30 5.26 40.20 109.42 o -1 0 30 107.13 148.88 86.05 o 0 0 30 1661.43 1600.58 297.78 o -7 1 30 105.09 54.41 142.83 o -6 1 30 6.43 -95.83 106.94 o -5 1 30 384.46 451.82 139.28 o -4 1 30 29.16 71.13 139.40 o -3 1 30 0.22 -52.31 64.84 o -2 1 30 528.10 629.90 85.60 o -1 1 30 201.05 167.18 68.29 o 0 1 30 1872.25 2524.80 132.44 o -7 2 30 255.15 159.56 174.38 o -6 2 30 1684.93 2111.14 305.79 o -5 2 30 0.05 -69.17 114.19 o -4 2 30 233.60 -110.17 110.17 o -3 2 30 39.30 -32.85 79.69 o -2 2 30 1039.27 1365.70 152.52 o -1 2 30 75.68 63.26 64.18 o 0 2 30 2.45 102.62 71.17 o -6 3 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