#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214881.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214881_Fobs loop_ _publ_author_name 'Mohamed, Sharmarke' 'Barnett, Sarah A.' 'Tocher, Derek A.' _publ_section_title ; 5-Fluoro-3-hydroxy-3-(nitromethyl)-1H-indol-2(3H)-one ; _journal_coeditor_code TK2184 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3577 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.536 _cell_angle_gamma 90.000 _cell_length_a 7.9400 _cell_length_b 15.7867 _cell_length_c 7.2980 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.7507 _[local]_cod_data_source_file tk2184Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sadmerge in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 122.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 50.28 49.13 1.28 o 2 0 0 1523.05 1365.38 18.67 o 3 0 0 1790.82 1732.51 23.69 o 4 0 0 23.99 33.85 0.76 o 5 0 0 175.56 185.21 2.92 o 6 0 0 79.35 82.71 2.07 o 7 0 0 25.56 26.61 1.17 o 8 0 0 113.47 107.80 2.79 o 9 0 0 424.07 455.68 12.87 o 1 1 0 1597.32 1320.53 21.99 o 2 1 0 2456.69 2410.97 28.52 o 3 1 0 687.83 717.80 7.03 o 4 1 0 1.44 4.66 0.22 o 5 1 0 263.82 265.57 2.89 o 6 1 0 54.00 53.37 1.11 o 7 1 0 59.43 61.58 1.30 o 8 1 0 270.58 272.18 3.94 o 9 1 0 0.74 0.55 0.42 o 1 2 0 532.01 513.87 5.47 o 2 2 0 1911.83 1984.59 23.12 o 3 2 0 881.76 894.29 9.53 o 4 2 0 671.34 711.27 7.03 o 5 2 0 1575.87 1610.60 17.13 o 6 2 0 60.86 64.99 1.09 o 7 2 0 29.04 32.74 0.92 o 8 2 0 126.58 119.46 2.51 o 9 2 0 40.38 43.08 1.43 o 1 3 0 2578.49 2526.55 25.21 o 2 3 0 132.25 122.96 1.46 o 3 3 0 11.79 16.00 0.38 o 4 3 0 136.71 151.32 2.28 o 5 3 0 1198.25 1259.96 13.50 o 6 3 0 140.51 133.24 1.84 o 7 3 0 708.06 673.71 9.90 o 8 3 0 0.51 0.29 0.39 o 9 3 0 16.00 20.72 1.21 o 10 3 0 71.00 90.90 3.79 o 0 4 0 2266.33 2157.73 29.45 o 1 4 0 2960.37 3040.85 29.64 o 2 4 0 25.87 26.69 0.44 o 3 4 0 1670.46 1727.59 18.23 o 4 4 0 759.25 738.27 8.01 o 5 4 0 114.02 108.06 1.82 o 6 4 0 42.09 37.22 0.79 o 7 4 0 61.13 62.63 1.59 o 8 4 0 46.56 45.46 1.40 o 9 4 0 0.18 0.83 0.44 o 1 5 0 526.12 553.24 5.46 o 2 5 0 12.11 16.97 0.32 o 3 5 0 1.18 1.08 0.18 o 4 5 0 1025.75 1158.79 12.41 o 5 5 0 112.60 99.70 1.43 o 6 5 0 631.17 633.31 9.24 o 7 5 0 358.71 335.56 4.64 o 8 5 0 7.77 10.71 0.76 o 9 5 0 6.16 8.57 0.77 o 0 6 0 3865.15 3602.79 49.01 o 1 6 0 118.91 107.15 1.33 o 2 6 0 97.52 92.69 1.08 o 3 6 0 753.63 808.80 8.73 o 4 6 0 906.92 932.72 10.07 o 5 6 0 0.03 0.69 0.25 o 6 6 0 670.68 652.24 8.26 o 7 6 0 34.75 30.88 1.11 o 8 6 0 0.01 0.28 0.38 o 9 6 0 56.91 57.66 1.72 o 1 7 0 144.73 129.57 1.61 o 2 7 0 555.51 566.74 5.65 o 3 7 0 75.43 77.38 0.98 o 4 7 0 15.01 14.57 0.53 o 5 7 0 799.86 799.91 9.92 o 6 7 0 205.46 201.10 3.01 o 7 7 0 13.89 16.07 0.69 o 8 7 0 0.46 0.32 0.38 o 9 7 0 1.52 1.94 0.50 o 0 8 0 846.81 897.15 12.48 o 2 8 0 49.14 39.76 0.60 o 3 8 0 133.15 153.97 2.25 o 4 8 0 184.73 171.27 2.71 o 5 8 0 153.56 164.86 2.51 o 6 8 0 947.36 924.68 11.53 o 7 8 0 58.45 64.07 1.42 o 8 8 0 25.81 22.84 1.02 o 9 8 0 63.35 60.54 1.80 o 1 9 0 431.14 450.77 5.06 o 2 9 0 79.36 81.38 1.12 o 3 9 0 366.57 390.63 5.49 o 4 9 0 310.38 354.91 4.71 o 5 9 0 191.79 184.78 2.79 o 6 9 0 17.39 17.60 0.72 o 7 9 0 25.74 25.38 0.88 o 8 9 0 0.37 -0.25 0.29 o 9 9 0 29.10 29.19 2.32 o 0 10 0 2.45 5.88 0.35 o 1 10 0 5.04 5.97 0.26 o 2 10 0 211.59 213.32 2.66 o 3 10 0 458.54 437.72 5.68 o 4 10 0 146.79 138.77 2.20 o 5 10 0 272.73 274.63 3.90 o 6 10 0 28.20 25.73 0.85 o 7 10 0 34.27 29.57 0.95 o 8 10 0 0.99 1.17 0.35 o 1 11 0 70.55 77.44 1.07 o 2 11 0 36.61 29.83 0.67 o 3 11 0 60.39 54.60 1.14 o 4 11 0 125.57 132.80 2.17 o 5 11 0 38.25 33.96 0.95 o 6 11 0 61.20 63.88 1.42 o 7 11 0 15.93 15.00 0.72 o 8 11 0 0.92 0.85 0.36 o 0 12 0 368.17 422.46 6.26 o 1 12 0 45.18 54.19 0.98 o 2 12 0 246.03 267.14 3.74 o 3 12 0 6.62 6.16 0.44 o 4 12 0 70.45 68.11 1.40 o 5 12 0 1.07 1.71 0.34 o 6 12 0 14.19 15.82 0.72 o 7 12 0 4.92 4.26 0.48 o 8 12 0 43.19 45.78 1.90 o 1 13 0 3.51 3.52 0.32 o 2 13 0 360.69 361.74 5.78 o 3 13 0 25.56 19.45 0.72 o 4 13 0 32.47 32.34 0.93 o 5 13 0 257.67 262.98 3.88 o 6 13 0 81.12 83.23 1.74 o 7 13 0 73.13 76.10 1.72 o 0 14 0 71.30 67.14 1.96 o 1 14 0 84.70 80.96 1.36 o 2 14 0 15.37 13.98 0.79 o 3 14 0 355.94 346.80 4.79 o 4 14 0 41.21 33.14 0.98 o 5 14 0 2.04 1.87 0.38 o 6 14 0 100.90 92.92 1.91 o 7 14 0 3.56 5.05 0.54 o 1 15 0 47.64 51.13 1.21 o 2 15 0 5.58 6.49 0.64 o 3 15 0 28.14 28.04 0.89 o 4 15 0 45.86 42.13 1.14 o 5 15 0 65.62 64.74 1.50 o 6 15 0 68.91 65.53 1.58 o 7 15 0 1.56 2.26 1.04 o 0 16 0 486.70 464.02 8.95 o 1 16 0 263.41 246.04 4.36 o 2 16 0 8.87 8.89 0.72 o 3 16 0 15.56 17.21 0.73 o 4 16 0 13.78 16.11 0.73 o 5 16 0 8.64 9.44 0.63 o 6 16 0 16.20 14.38 0.79 o 1 17 0 7.73 6.48 0.67 o 2 17 0 11.84 11.24 0.96 o 3 17 0 38.12 36.24 1.53 o 4 17 0 48.99 46.32 1.26 o 5 17 0 2.40 1.77 0.41 o 0 18 0 0.79 1.52 1.09 o 1 18 0 59.62 56.67 1.71 o 2 18 0 1.79 1.71 0.44 o 3 18 0 42.82 38.87 1.39 o 4 18 0 47.55 49.30 1.61 o 5 18 0 0.04 0.45 0.48 o 1 19 0 4.73 3.88 0.63 o 2 19 0 84.69 77.57 2.06 o 3 19 0 12.02 14.71 0.95 o 4 19 0 113.16 120.00 5.12 o 0 20 0 94.62 100.40 4.57 o 1 20 0 2.95 3.12 0.70 o 2 20 0 4.18 4.25 0.63 o 3 20 0 2.02 1.65 1.08 o -10 1 1 140.92 140.44 3.05 o -9 1 1 160.67 158.92 2.71 o -8 1 1 214.34 215.90 3.28 o -7 1 1 340.04 304.11 4.19 o -6 1 1 53.24 52.28 0.93 o -5 1 1 166.84 213.78 2.35 o -4 1 1 55.14 39.97 0.61 o -3 1 1 2248.55 2344.76 22.59 o -2 1 1 142.28 154.32 1.80 o 0 1 1 69.05 60.09 0.95 o 1 1 1 0.38 0.74 0.09 o 2 1 1 369.67 413.38 4.48 o 3 1 1 4.49 10.54 0.29 o 5 1 1 849.34 901.22 8.93 o 6 1 1 197.59 199.83 2.88 o 7 1 1 465.66 433.78 5.76 o 8 1 1 33.46 29.54 1.09 o 9 1 1 61.40 56.50 2.16 o -10 2 1 12.03 19.73 1.07 o -9 2 1 2.59 3.59 0.55 o -8 2 1 104.02 97.71 1.85 o -7 2 1 50.77 50.24 1.15 o -6 2 1 17.06 16.73 0.54 o -5 2 1 49.53 50.16 0.86 o -4 2 1 126.36 167.53 1.85 o -3 2 1 6270.82 6334.24 77.13 o -2 2 1 492.86 429.93 4.25 o -1 2 1 2696.75 2342.01 34.28 o 0 2 1 1881.40 1833.14 19.82 o 1 2 1 3648.76 3413.89 36.25 o 2 2 1 13.48 10.03 0.25 o 3 2 1 3.61 2.64 0.18 o 4 2 1 203.25 189.73 2.07 o 5 2 1 1400.99 1342.82 14.38 o 6 2 1 861.77 853.16 9.54 o 7 2 1 10.23 9.68 0.67 o 8 2 1 120.65 112.19 2.42 o 9 2 1 124.18 123.76 3.49 o -10 3 1 0.07 1.20 0.47 o -9 3 1 1.72 2.34 0.51 o -8 3 1 44.69 39.68 1.28 o -7 3 1 686.12 698.04 8.76 o -6 3 1 6.29 5.97 0.38 o -5 3 1 461.94 483.07 6.04 o -4 3 1 2233.48 2365.99 24.94 o -3 3 1 687.18 701.09 6.90 o -2 3 1 274.55 286.51 3.18 o -1 3 1 590.97 589.50 7.14 o 0 3 1 2146.96 2271.90 21.94 o 1 3 1 6965.20 6493.53 85.15 o 2 3 1 2998.49 3101.14 29.89 o 3 3 1 798.69 769.04 7.56 o 4 3 1 10.96 13.25 0.36 o 5 3 1 1.35 0.89 0.20 o 6 3 1 620.27 606.21 8.11 o 7 3 1 225.39 229.69 3.96 o 8 3 1 0.00 0.23 0.35 o 9 3 1 95.97 97.24 2.35 o -10 4 1 1.41 2.36 0.66 o -9 4 1 30.17 27.53 1.15 o -8 4 1 43.29 35.54 1.23 o -7 4 1 0.32 0.25 0.25 o -6 4 1 143.57 127.00 2.01 o -5 4 1 0.08 0.39 0.16 o -4 4 1 26.35 28.56 0.58 o -3 4 1 97.60 98.32 1.15 o -2 4 1 296.10 296.91 3.01 o -1 4 1 4353.47 4014.34 47.99 o 0 4 1 6145.89 5651.89 56.20 o 1 4 1 9784.79 8889.24 126.32 o 2 4 1 307.92 331.94 3.36 o 3 4 1 242.19 270.16 2.82 o 4 4 1 13.55 10.60 0.36 o 5 4 1 46.93 42.79 0.90 o 6 4 1 100.65 87.52 1.88 o 7 4 1 17.66 18.99 0.88 o 8 4 1 0.98 2.89 0.53 o 9 4 1 0.11 1.53 0.47 o -10 5 1 17.47 23.95 2.04 o -9 5 1 199.44 218.53 4.06 o -8 5 1 10.11 13.81 0.82 o -7 5 1 0.07 0.36 0.26 o -6 5 1 43.11 44.59 1.01 o -5 5 1 57.27 66.41 1.08 o -4 5 1 271.61 326.13 3.75 o -3 5 1 626.16 651.30 6.45 o -2 5 1 18.39 23.23 0.42 o -1 5 1 2705.39 2709.86 65.87 o 0 5 1 7580.61 6903.43 77.76 o 1 5 1 412.91 425.42 5.27 o 2 5 1 3734.34 4016.01 42.47 o 3 5 1 466.99 491.00 4.93 o 4 5 1 2.29 1.62 0.20 o 5 5 1 242.14 229.76 3.23 o 6 5 1 0.21 -0.03 0.22 o 7 5 1 226.15 224.96 3.93 o 8 5 1 44.39 39.97 1.33 o 9 5 1 0.01 -0.16 0.39 o -9 6 1 91.75 96.16 2.32 o -8 6 1 0.32 1.26 0.45 o -7 6 1 9.43 7.78 0.57 o -6 6 1 84.06 79.40 1.49 o -5 6 1 54.34 62.45 1.04 o -4 6 1 124.22 127.08 1.85 o -3 6 1 288.05 354.08 3.63 o -2 6 1 290.04 273.08 2.83 o -1 6 1 2319.34 2429.58 23.42 o 0 6 1 26.18 23.59 0.53 o 1 6 1 1.15 1.59 0.18 o 2 6 1 332.21 361.70 4.10 o 3 6 1 695.82 766.51 8.38 o 4 6 1 468.31 496.13 9.18 o 5 6 1 8.01 8.09 0.47 o 6 6 1 88.20 92.76 1.68 o 7 6 1 99.77 91.36 2.07 o 8 6 1 56.67 53.90 1.59 o 9 6 1 8.57 7.60 0.76 o -9 7 1 203.24 217.36 4.09 o -8 7 1 196.11 188.81 3.53 o -7 7 1 14.74 17.19 0.70 o -6 7 1 131.02 134.91 2.19 o -5 7 1 12.88 14.23 0.48 o -4 7 1 2142.00 2245.27 23.73 o -3 7 1 464.19 511.62 5.17 o -2 7 1 102.93 97.16 1.17 o -1 7 1 42.23 51.84 0.73 o 0 7 1 1.99 1.31 0.19 o 1 7 1 1276.13 1416.10 16.99 o 2 7 1 0.61 1.30 0.22 o 3 7 1 158.51 168.45 2.12 o 4 7 1 89.09 92.85 1.58 o 5 7 1 723.76 715.61 8.99 o 6 7 1 196.70 182.05 2.80 o 7 7 1 62.00 65.59 1.44 o 8 7 1 0.54 1.46 0.45 o 9 7 1 50.67 55.52 2.83 o -9 8 1 27.01 26.50 1.17 o -8 8 1 0.93 0.18 0.31 o -7 8 1 74.29 68.80 1.47 o -6 8 1 657.59 658.88 8.41 o -5 8 1 146.68 148.25 2.31 o -4 8 1 28.47 28.96 0.64 o -3 8 1 7.67 11.21 0.34 o -2 8 1 13.48 14.48 0.36 o -1 8 1 280.83 298.52 3.12 o 0 8 1 0.68 1.98 0.20 o 1 8 1 2935.63 3124.42 30.12 o 2 8 1 179.20 197.90 2.44 o 3 8 1 57.08 63.75 1.18 o 4 8 1 35.58 38.71 0.92 o 5 8 1 0.55 2.06 0.34 o 6 8 1 1.81 3.15 0.39 o 7 8 1 15.75 14.26 0.67 o 8 8 1 0.21 0.28 0.39 o -9 9 1 2.24 2.00 0.53 o -8 9 1 52.20 47.54 1.27 o -7 9 1 6.42 6.47 0.53 o -6 9 1 220.21 220.56 3.28 o -5 9 1 26.29 19.56 0.69 o -4 9 1 807.81 791.97 9.82 o -3 9 1 448.11 457.18 5.36 o -2 9 1 7.21 11.06 0.36 o -1 9 1 105.35 113.27 1.37 o 0 9 1 270.79 292.90 3.42 o 1 9 1 39.00 40.05 0.63 o 2 9 1 165.67 162.73 2.10 o 3 9 1 388.84 432.70 5.59 o 4 9 1 381.12 399.91 5.28 o 5 9 1 12.31 13.21 0.61 o 6 9 1 446.92 441.02 5.94 o 7 9 1 55.10 52.12 1.28 o 8 9 1 15.96 17.12 0.96 o -9 10 1 208.97 207.92 7.24 o -8 10 1 16.03 15.54 0.76 o -7 10 1 0.42 0.19 0.31 o -6 10 1 19.79 18.36 0.74 o -5 10 1 31.93 33.95 0.92 o -4 10 1 678.35 692.78 8.70 o -3 10 1 37.02 34.79 0.85 o -2 10 1 127.22 100.57 2.45 o -1 10 1 342.96 352.59 3.71 o 0 10 1 147.99 155.32 1.98 o 1 10 1 307.05 314.94 3.72 o 2 10 1 101.28 99.43 1.44 o 3 10 1 193.87 200.97 2.92 o 4 10 1 149.48 167.97 2.58 o 5 10 1 4.66 5.49 0.45 o 6 10 1 6.77 8.26 0.57 o 7 10 1 10.07 15.08 0.73 o 8 10 1 21.97 25.54 0.95 o -8 11 1 110.02 102.57 2.07 o -7 11 1 34.37 33.42 1.04 o -6 11 1 398.04 411.59 5.63 o -5 11 1 91.97 89.67 1.68 o -4 11 1 181.69 188.78 2.83 o -3 11 1 27.70 27.13 0.79 o -2 11 1 0.61 0.74 0.18 o -1 11 1 9.74 10.90 0.36 o 0 11 1 200.93 191.09 2.44 o 1 11 1 4.58 3.59 0.41 o 2 11 1 558.55 557.74 6.35 o 3 11 1 112.72 113.23 1.90 o 4 11 1 34.23 35.63 0.93 o 5 11 1 154.15 155.32 2.54 o 6 11 1 29.97 37.76 1.07 o 7 11 1 65.91 64.79 1.52 o 8 11 1 219.54 241.05 5.53 o -8 12 1 0.36 0.85 0.36 o -7 12 1 135.56 137.56 2.48 o -6 12 1 181.82 176.26 2.88 o -5 12 1 330.75 315.29 4.45 o -4 12 1 213.37 189.76 2.89 o -3 12 1 725.68 715.78 9.00 o -2 12 1 297.97 285.94 3.49 o -1 12 1 30.05 28.11 0.58 o 0 12 1 50.80 45.80 0.89 o 1 12 1 0.82 0.51 0.23 o 2 12 1 8.90 12.08 0.55 o 3 12 1 195.91 194.64 2.92 o 4 12 1 176.85 163.31 2.60 o 5 12 1 32.74 35.17 1.01 o 6 12 1 0.16 1.47 0.36 o 7 12 1 3.40 6.14 0.96 o 8 12 1 4.61 7.27 1.09 o -8 13 1 2.48 2.73 0.64 o -7 13 1 165.55 179.85 3.04 o -6 13 1 0.04 0.76 0.35 o -5 13 1 136.81 137.04 2.36 o -4 13 1 322.62 312.44 4.39 o -3 13 1 69.10 63.81 1.33 o -2 13 1 5.55 4.80 0.41 o -1 13 1 35.96 32.68 0.88 o 0 13 1 0.06 0.45 0.23 o 1 13 1 9.13 6.90 0.47 o 2 13 1 274.21 257.26 3.66 o 3 13 1 427.36 406.29 5.47 o 4 13 1 8.07 8.22 0.54 o 5 13 1 278.19 277.58 4.09 o 6 13 1 284.08 284.98 4.26 o 7 13 1 17.17 19.43 0.85 o -7 14 1 1.21 0.80 0.36 o -6 14 1 4.20 5.63 0.54 o -5 14 1 99.59 98.51 1.91 o -4 14 1 0.05 0.35 0.31 o -3 14 1 130.27 123.66 2.12 o -2 14 1 842.54 815.71 10.27 o -1 14 1 0.06 0.92 0.29 o 0 14 1 315.84 293.98 3.66 o 2 14 1 58.76 51.29 1.18 o 3 14 1 47.60 44.50 1.11 o 4 14 1 1.53 1.85 0.38 o 5 14 1 0.00 0.06 0.29 o 6 14 1 4.99 4.25 0.51 o -7 15 1 3.08 4.09 1.02 o -6 15 1 105.60 108.98 2.15 o -5 15 1 77.67 74.10 1.62 o -4 15 1 4.93 6.03 0.55 o -3 15 1 75.96 73.12 3.18 o -2 15 1 126.60 124.86 2.63 o -1 15 1 32.43 29.25 0.89 o 0 15 1 127.09 126.10 2.20 o 1 15 1 5.12 4.67 0.55 o 2 15 1 34.64 33.25 0.95 o 3 15 1 55.38 52.54 1.26 o 4 15 1 99.82 100.00 1.94 o 5 15 1 43.18 45.94 1.23 o 6 15 1 73.85 79.06 1.78 o -6 16 1 1.71 2.19 0.48 o -5 16 1 7.61 10.17 0.66 o -4 16 1 8.47 9.38 0.60 o -3 16 1 81.42 80.45 1.98 o -2 16 1 19.57 18.70 0.95 o -1 16 1 19.11 17.66 0.92 o 0 16 1 38.25 35.76 1.02 o 1 16 1 112.48 104.38 2.35 o 2 16 1 30.86 29.28 0.92 o 3 16 1 1.42 1.81 0.38 o 4 16 1 2.15 2.67 0.42 o 5 16 1 46.99 48.98 1.31 o 6 16 1 0.99 2.20 0.82 o -6 17 1 13.26 15.19 1.52 o -5 17 1 10.43 12.93 0.83 o -4 17 1 10.51 11.95 0.83 o -3 17 1 59.97 54.10 1.62 o -2 17 1 38.53 35.98 1.33 o -1 17 1 0.45 1.01 0.45 o 0 17 1 15.13 16.49 0.76 o 1 17 1 42.42 43.84 1.44 o 2 17 1 91.81 92.41 2.19 o 3 17 1 72.54 70.33 1.58 o 4 17 1 77.71 80.05 1.74 o 5 17 1 0.77 1.15 0.44 o -4 18 1 0.39 -0.15 0.45 o -3 18 1 200.61 189.28 3.72 o -2 18 1 94.89 96.12 2.38 o -1 18 1 25.10 25.79 1.17 o 0 18 1 16.11 18.17 0.98 o 1 18 1 0.32 0.50 0.44 o 2 18 1 1.48 1.69 0.45 o 3 18 1 1.30 1.26 0.44 o 4 18 1 33.96 32.40 1.07 o -3 19 1 6.97 6.25 0.85 o -2 19 1 13.97 14.81 0.98 o -1 19 1 14.38 14.58 0.96 o 0 19 1 0.61 1.01 0.69 o 1 19 1 7.18 9.06 0.93 o 2 19 1 54.54 59.78 1.77 o 3 19 1 9.31 11.70 0.86 o -2 20 1 8.93 9.68 1.05 o -1 20 1 9.16 9.47 1.69 o 0 20 1 23.58 22.13 1.50 o 1 20 1 18.88 21.48 1.07 o 2 20 1 0.71 1.42 0.45 o -10 0 2 137.22 151.11 3.88 o -9 0 2 37.08 35.06 1.55 o -8 0 2 156.19 146.49 3.44 o -7 0 2 2.65 6.12 0.66 o -6 0 2 549.80 543.05 9.65 o -5 0 2 459.20 508.89 7.34 o -4 0 2 296.74 380.53 5.53 o -3 0 2 57.11 71.05 1.27 o -1 0 2 4405.13 4380.93 59.90 o 0 0 2 8002.41 7247.58 98.88 o 1 0 2 1877.86 1825.19 30.53 o 2 0 2 15078.89 13205.87 187.38 o 3 0 2 1259.00 1422.72 19.57 o 4 0 2 110.66 98.97 1.74 o 5 0 2 78.62 76.05 1.49 o 6 0 2 27.76 24.87 1.07 o 7 0 2 188.12 174.77 5.76 o 8 0 2 256.33 215.62 7.08 o 9 0 2 49.90 54.73 3.05 o -10 1 2 64.75 68.70 1.93 o -9 1 2 221.37 212.43 3.36 o -8 1 2 164.87 188.10 2.95 o -7 1 2 133.87 114.70 1.96 o -6 1 2 331.66 346.25 4.07 o -5 1 2 150.73 140.99 1.68 o -4 1 2 30.87 39.79 0.64 o -3 1 2 390.59 372.12 4.12 o -2 1 2 294.80 301.75 3.34 o -1 1 2 173.51 167.04 2.19 o 0 1 2 361.57 378.94 3.78 o 1 1 2 2752.74 2754.30 29.00 o 2 1 2 2149.85 2211.22 21.29 o 3 1 2 34.86 25.88 0.54 o 4 1 2 913.03 948.16 9.36 o 5 1 2 373.29 363.93 4.22 o 6 1 2 227.37 221.29 3.15 o 7 1 2 165.98 161.10 3.02 o 8 1 2 1.51 2.03 0.57 o 9 1 2 3.42 2.76 0.61 o -10 2 2 14.71 17.98 0.99 o -9 2 2 0.05 0.19 0.35 o -8 2 2 28.97 28.27 0.90 o -7 2 2 875.07 832.41 10.30 o -6 2 2 89.05 96.94 1.58 o -5 2 2 4.57 5.05 0.28 o -4 2 2 1081.25 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