#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/48/2214882.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214882_Fobs loop_ _publ_author_name 'Zhao, Wen-Na' _publ_section_title ; A dinuclear manganese(II) complex with a 4-aminoantipyrine-derived Schiff base ligand ; _journal_coeditor_code WK2058 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2095 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 72.678 _cell_angle_beta 77.661 _cell_angle_gamma 71.090 _cell_length_a 10.0525 _cell_length_b 12.3717 _cell_length_c 15.2573 _exptl_crystal_F_000 806.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file wk2058Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TREF in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 248.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2061.61 1967.39 26.40 o 3 0 0 153.53 166.80 16.48 o 4 0 0 975.45 954.68 37.13 o 5 0 0 778.41 865.59 24.40 o 6 0 0 2398.56 2445.61 42.65 o 7 0 0 2545.68 2601.22 65.77 o 8 0 0 1133.40 1214.42 46.64 o 9 0 0 89.56 118.74 27.05 o 10 0 0 5.96 -12.97 45.56 o 11 0 0 32.93 -5.91 28.82 o 12 0 0 41.87 97.32 42.90 o -11 1 0 4.14 -29.00 29.00 o -10 1 0 41.92 105.61 53.26 o -9 1 0 176.08 162.13 46.04 o -8 1 0 76.34 74.64 28.09 o -7 1 0 91.04 106.28 25.05 o -6 1 0 0.36 14.79 35.99 o -5 1 0 1077.92 1097.00 32.45 o -4 1 0 757.84 776.26 37.25 o -3 1 0 491.53 589.03 26.99 o -2 1 0 169.10 174.42 12.51 o -1 1 0 295.98 326.28 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