#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214913.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214913_Fobs loop_ _publ_author_name 'Zhang, Yu-Zhen' 'Chen, Zi-Lu' 'Ng, Seik Weng' _publ_section_title ; Diaquabis[(1R,2R)-(+)--1,2-diphenylethylenediamine-\k^2^N,N']nickel(II) dichloride--dichloridobis(1,10-phenanthroline-\k^2^N,N')nickel(II) (1/2) ; _journal_coeditor_code XU2291 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2123 _journal_volume 63 _journal_year 2007 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.348 _cell_angle_gamma 90.000 _cell_length_a 12.3896 _cell_length_b 13.8185 _cell_length_c 21.2613 _exptl_crystal_F_000 1620.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file xu2291Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 492.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 9 -14 0 4.92 120.40 128.45 o 7 -13 0 125.41 54.97 107.80 o 8 -13 0 563.47 262.52 138.37 o 9 -13 0 591.94 656.99 178.85 o 10 -13 0 241.34 282.36 156.87 o 6 -12 0 5.76 -86.61 82.59 o 7 -12 0 1335.94 1540.80 194.14 o 8 -12 0 186.13 450.49 131.93 o 9 -12 0 846.62 650.28 170.54 o 10 -12 0 45.09 13.68 120.13 o 11 -12 0 94.85 -18.50 119.06 o 5 -11 0 111.85 41.83 75.62 o 6 -11 0 319.79 465.77 121.20 o 7 -11 0 20.38 31.37 89.03 o 8 -11 0 914.20 1289.55 183.95 o 9 -11 0 57.31 72.67 102.70 o 10 -11 0 136.75 170.55 127.64 o 11 -11 0 93.69 65.70 118.52 o 12 -11 0 4.64 56.85 134.88 o 4 -10 0 1623.23 1580.75 135.95 o 5 -10 0 2185.70 2169.63 159.55 o 6 -10 0 266.21 295.23 100.56 o 7 -10 0 811.27 999.41 144.80 o 8 -10 0 492.97 658.06 136.22 o 9 -10 0 1523.31 1807.10 201.91 o 10 -10 0 3.86 -46.66 92.78 o 11 -10 0 47.51 -127.37 93.05 o 12 -10 0 14.92 -4.83 104.31 o 13 -10 0 4.07 20.38 133.27 o 4 -9 0 3094.41 3148.05 173.49 o 5 -9 0 165.65 115.57 89.97 o 6 -9 0 2233.49 2254.74 111.54 o 7 -9 0 253.05 277.80 93.05 o 8 -9 0 815.27 991.90 152.84 o 9 -9 0 730.66 650.02 134.88 o 10 -9 0 106.40 176.98 115.04 o 11 -9 0 89.81 47.19 110.48 o 12 -9 0 56.30 119.33 120.40 o 13 -9 0 73.68 16.36 134.61 o 3 -8 0 186.99 71.33 56.31 o 4 -8 0 412.69 490.35 72.28 o 5 -8 0 1169.36 1108.15 82.19 o 6 -8 0 103.88 27.46 44.28 o 7 -8 0 803.76 937.47 128.98 o 8 -8 0 9.97 -16.89 73.21 o 9 -8 0 18.84 -55.77 79.37 o 10 -8 0 56.36 61.68 100.83 o 11 -8 0 209.17 66.50 106.19 o 12 -8 0 17.61 18.77 107.26 o 13 -8 0 140.77 164.92 143.46 o 14 -8 0 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