#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/49/2214976.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214976_Fobs loop_ _publ_author_name 'Roy, Saikat' 'Nangia, Ashwini' _publ_section_title ; p-Tosylhydrazine: a redetermination from single-crystal data at 100 K ; _journal_coeditor_code BI2204 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3696 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.260 _cell_angle_gamma 90.000 _cell_length_a 8.4166 _cell_length_b 5.6056 _cell_length_c 17.9484 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.8100 _[local]_cod_data_source_file bi2204Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' an499_m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 138.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 70.17 47.16 3.03 o 2 0 0 19201.14 18506.91 177.59 o 3 0 0 76.49 100.88 3.95 o 4 0 0 115.99 123.06 4.86 o 5 0 0 685.24 642.90 11.98 o 6 0 0 936.59 926.86 22.55 o 7 0 0 1563.78 1566.48 29.78 o 8 0 0 529.98 495.72 21.12 o 9 0 0 629.41 618.30 25.12 o 10 0 0 381.28 418.77 21.13 o 1 1 0 4016.59 4097.10 26.55 o 2 1 0 645.60 681.22 6.58 o 3 1 0 1300.96 1362.40 11.44 o 4 1 0 2.00 2.57 1.71 o 5 1 0 571.47 631.25 8.59 o 6 1 0 530.22 575.44 11.30 o 7 1 0 3.52 8.65 3.72 o 8 1 0 497.22 517.42 13.68 o 9 1 0 34.04 47.58 4.54 o 10 1 0 250.58 269.55 12.05 o 0 2 0 177.59 160.96 4.40 o 1 2 0 7.07 7.73 1.64 o 2 2 0 2610.14 2928.91 19.84 o 3 2 0 261.76 269.93 5.55 o 4 2 0 2159.08 2387.91 20.75 o 5 2 0 0.69 2.73 1.73 o 6 2 0 31.78 42.83 4.21 o 7 2 0 1.32 9.73 2.82 o 8 2 0 3.67 16.41 3.46 o 9 2 0 214.88 207.90 16.69 o 1 3 0 68.15 49.81 2.87 o 2 3 0 46.30 41.96 3.02 o 3 3 0 26.86 48.49 3.05 o 4 3 0 11.22 21.20 4.18 o 5 3 0 341.34 303.76 8.41 o 6 3 0 191.77 193.82 8.03 o 7 3 0 17.29 20.88 4.33 o 8 3 0 4.45 13.03 3.77 o 9 3 0 40.35 54.49 7.26 o 0 4 0 117.14 103.57 8.45 o 1 4 0 110.93 100.31 4.87 o 2 4 0 759.64 709.19 12.36 o 3 4 0 510.31 462.08 10.43 o 4 4 0 876.11 786.85 14.14 o 5 4 0 255.22 223.28 9.06 o 6 4 0 133.32 116.12 6.31 o 7 4 0 145.87 148.37 8.40 o 8 4 0 4.79 18.23 3.27 o 1 5 0 788.38 780.51 15.89 o 2 5 0 16.56 25.52 3.94 o 3 5 0 1507.00 1389.75 22.71 o 4 5 0 291.41 273.49 9.74 o 5 5 0 289.32 281.01 11.49 o 6 5 0 216.94 210.41 8.73 o 7 5 0 186.48 178.93 9.25 o 0 6 0 306.26 301.12 16.89 o 1 6 0 18.47 33.69 4.66 o 2 6 0 148.26 169.12 7.63 o 3 6 0 173.02 173.39 7.99 o 4 6 0 1.92 17.16 3.28 o 5 6 0 100.91 107.70 6.93 o -10 1 1 1.09 4.51 3.40 o -9 1 1 0.05 15.66 3.52 o -8 1 1 340.61 325.62 10.74 o -7 1 1 493.80 477.83 12.57 o -6 1 1 805.44 770.09 13.17 o -5 1 1 47.56 53.17 2.90 o -4 1 1 278.96 313.67 5.96 o -3 1 1 808.03 716.17 7.46 o -2 1 1 71.86 91.58 2.48 o -1 1 1 961.12 1016.07 7.80 o 0 1 1 865.99 887.20 6.77 o 1 1 1 136.34 140.15 2.93 o 2 1 1 709.20 705.71 6.80 o 3 1 1 2.93 28.50 1.97 o 4 1 1 603.18 692.42 8.49 o 5 1 1 487.23 454.54 7.40 o 6 1 1 426.21 376.88 11.09 o 7 1 1 52.57 59.81 5.42 o 8 1 1 853.92 863.02 17.97 o 9 1 1 2.55 16.45 5.17 o 10 1 1 67.64 73.20 5.78 o -9 2 1 421.04 419.46 18.91 o -8 2 1 62.22 56.13 5.44 o -7 2 1 856.27 819.63 16.79 o -6 2 1 0.01 0.36 2.75 o -5 2 1 469.68 446.20 8.64 o -4 2 1 45.71 63.16 2.64 o -3 2 1 659.91 602.68 7.40 o -2 2 1 684.79 824.92 8.24 o -1 2 1 2311.21 2364.97 16.42 o 0 2 1 621.28 569.71 6.16 o 1 2 1 27.46 41.15 2.27 o 2 2 1 1661.25 1648.03 12.86 o 3 2 1 7.62 16.90 1.75 o 4 2 1 779.06 792.12 12.89 o 5 2 1 17.68 22.87 2.92 o 6 2 1 76.12 74.55 4.96 o 7 2 1 69.01 58.27 5.39 o 8 2 1 19.28 31.53 4.52 o 9 2 1 47.18 73.02 5.52 o -9 3 1 48.14 73.43 7.76 o -8 3 1 41.93 64.61 5.35 o -7 3 1 36.61 43.98 5.11 o -6 3 1 224.84 217.22 8.34 o -5 3 1 0.82 4.50 3.18 o -4 3 1 1211.40 1218.24 19.19 o -3 3 1 2.33 2.81 1.95 o -2 3 1 34.26 24.15 2.45 o -1 3 1 8.43 3.47 2.07 o 0 3 1 118.58 167.92 3.76 o 1 3 1 132.54 131.29 4.13 o 2 3 1 48.42 60.58 3.45 o 3 3 1 450.70 431.91 9.13 o 4 3 1 358.31 307.62 8.13 o 5 3 1 110.35 121.11 7.83 o 6 3 1 11.47 18.65 3.64 o 7 3 1 31.27 47.67 5.00 o 8 3 1 41.36 51.21 5.46 o 9 3 1 12.53 17.41 3.34 o -8 4 1 19.34 25.39 4.38 o -7 4 1 0.87 4.63 4.26 o -6 4 1 15.79 25.89 4.14 o -5 4 1 14.68 25.90 4.25 o -4 4 1 110.77 104.97 5.59 o -3 4 1 5.75 4.43 2.62 o -2 4 1 102.80 94.03 4.20 o -1 4 1 347.62 311.59 8.00 o 0 4 1 0.68 0.34 2.19 o 1 4 1 306.91 283.18 7.54 o 2 4 1 1.65 12.32 3.42 o 3 4 1 11.14 13.59 3.10 o 4 4 1 79.31 74.43 5.81 o 5 4 1 598.46 548.53 15.57 o 6 4 1 60.60 71.20 5.18 o 7 4 1 51.95 59.16 5.20 o 8 4 1 3.86 8.28 3.51 o -7 5 1 132.35 140.97 8.05 o -6 5 1 26.23 45.42 4.96 o -5 5 1 54.12 68.98 5.82 o -4 5 1 65.07 80.10 5.31 o -3 5 1 0.01 6.49 2.73 o -2 5 1 36.74 38.48 4.32 o -1 5 1 43.45 48.45 4.37 o 0 5 1 0.37 5.15 2.57 o 1 5 1 381.21 349.74 10.54 o 2 5 1 43.00 48.97 4.64 o 3 5 1 511.05 435.93 12.19 o 4 5 1 41.25 40.90 4.38 o 5 5 1 181.85 163.68 8.63 o 6 5 1 0.99 11.26 2.85 o -5 6 1 481.64 519.06 16.85 o -4 6 1 0.48 14.27 3.61 o -3 6 1 98.29 99.72 5.87 o -2 6 1 378.18 367.04 11.62 o -1 6 1 2.50 13.27 3.13 o 0 6 1 465.93 450.52 14.97 o 1 6 1 331.88 307.41 10.37 o 2 6 1 419.83 404.64 12.28 o 3 6 1 52.26 69.50 4.75 o 4 6 1 274.08 278.37 10.25 o -10 0 2 303.98 288.34 17.59 o -9 0 2 0.07 10.06 4.82 o -8 0 2 183.99 180.12 16.30 o -7 0 2 919.85 945.77 39.93 o -6 0 2 78.29 79.39 7.13 o -5 0 2 769.65 810.83 12.58 o -4 0 2 105.90 93.91 3.56 o -3 0 2 263.40 332.93 11.55 o -2 0 2 1659.22 1935.12 22.06 o -1 0 2 6755.52 6965.54 53.75 o 0 0 2 876.51 922.05 10.52 o 1 0 2 6997.13 7222.79 55.23 o 2 0 2 127.91 69.65 3.58 o 3 0 2 85.15 86.58 4.09 o 4 0 2 559.36 597.47 11.16 o 5 0 2 784.83 784.10 14.09 o 6 0 2 3304.61 3478.89 45.62 o 7 0 2 232.81 200.81 10.18 o 8 0 2 499.24 476.17 20.54 o 9 0 2 173.74 210.11 14.15 o 10 0 2 115.72 116.65 10.15 o -10 1 2 28.29 46.76 4.85 o -9 1 2 27.44 43.79 4.24 o -8 1 2 77.43 88.51 5.67 o -7 1 2 0.19 3.79 3.15 o -6 1 2 1239.83 1320.42 19.44 o -5 1 2 101.20 122.45 4.26 o -4 1 2 5046.05 5470.07 33.93 o -3 1 2 136.43 148.22 3.69 o -2 1 2 12467.80 13022.53 93.28 o -1 1 2 1674.87 1677.69 11.55 o 0 1 2 5015.45 5132.62 28.82 o 1 1 2 2642.92 2662.67 20.03 o 2 1 2 137.88 118.83 3.34 o 3 1 2 1315.76 1392.61 11.94 o 4 1 2 300.60 290.28 5.48 o 5 1 2 2511.52 2689.89 21.56 o 6 1 2 152.13 156.03 6.28 o 7 1 2 1874.49 1891.74 26.33 o 8 1 2 30.95 46.45 4.35 o 9 1 2 713.60 704.53 19.47 o -9 2 2 5.37 10.04 3.48 o -8 2 2 5.15 19.01 4.00 o -7 2 2 99.97 82.02 5.46 o -6 2 2 39.07 35.82 4.82 o -5 2 2 128.47 146.68 6.98 o -4 2 2 281.06 262.43 5.22 o -3 2 2 2545.61 2827.62 20.40 o -2 2 2 177.46 196.47 3.87 o -1 2 2 120.21 131.48 3.69 o 0 2 2 1945.33 1959.08 14.25 o 1 2 2 857.54 865.08 9.23 o 2 2 2 564.52 566.91 7.47 o 3 2 2 4.65 22.91 2.34 o 4 2 2 1356.30 1407.42 15.26 o 5 2 2 83.82 97.83 4.44 o 6 2 2 9.12 17.19 4.09 o 7 2 2 8.90 18.68 4.00 o 8 2 2 137.44 172.91 11.31 o 9 2 2 131.05 152.94 8.20 o -9 3 2 0.59 22.21 9.29 o -8 3 2 0.25 8.84 2.86 o -7 3 2 4.70 14.82 3.70 o -6 3 2 443.16 391.90 13.00 o -5 3 2 13.28 14.44 3.83 o -4 3 2 191.41 190.40 5.48 o -3 3 2 98.63 88.88 3.83 o -2 3 2 22.24 23.67 3.09 o -1 3 2 184.07 201.99 4.51 o 0 3 2 14.67 37.85 2.28 o 1 3 2 1096.03 1024.03 11.79 o 2 3 2 221.19 263.04 5.99 o 3 3 2 73.15 61.90 4.89 o 4 3 2 38.41 41.17 3.99 o 5 3 2 426.81 411.10 9.95 o 6 3 2 0.34 6.65 3.17 o 7 3 2 128.03 104.85 6.74 o 8 3 2 44.13 55.33 8.06 o 9 3 2 1.53 17.22 4.07 o -8 4 2 83.79 87.82 6.24 o -7 4 2 231.03 213.62 10.22 o -6 4 2 38.09 52.22 4.42 o -5 4 2 811.24 730.63 15.59 o -4 4 2 2.70 6.88 2.92 o -3 4 2 1348.09 1227.44 18.04 o -2 4 2 9.52 9.71 2.30 o -1 4 2 190.13 166.87 6.10 o 0 4 2 4.32 1.82 2.36 o 1 4 2 9.41 19.59 3.19 o 2 4 2 929.99 918.51 14.56 o 3 4 2 324.02 321.61 8.92 o 4 4 2 1315.86 1282.01 18.84 o 5 4 2 363.15 309.67 9.10 o 6 4 2 256.33 237.34 9.18 o 7 4 2 13.37 18.54 4.50 o 8 4 2 79.15 91.27 7.15 o -7 5 2 149.35 125.79 7.65 o -6 5 2 16.12 41.31 4.68 o -5 5 2 211.94 185.68 9.38 o -4 5 2 271.14 263.84 9.47 o -3 5 2 133.57 144.65 6.89 o -2 5 2 498.79 461.38 12.20 o -1 5 2 292.74 267.08 7.85 o 0 5 2 215.57 189.43 7.65 o 1 5 2 293.05 303.23 9.84 o 2 5 2 194.17 165.05 7.35 o 3 5 2 953.96 953.45 18.64 o 4 5 2 2.12 15.15 3.05 o 5 5 2 154.39 148.39 7.21 o 6 5 2 1.43 11.30 2.57 o -5 6 2 73.59 100.09 6.65 o -4 6 2 9.61 16.84 4.62 o -3 6 2 32.63 42.24 3.92 o -2 6 2 139.62 136.65 6.65 o -1 6 2 218.95 206.19 12.18 o 0 6 2 273.59 244.43 10.67 o 1 6 2 799.14 785.61 17.46 o 2 6 2 524.39 507.22 14.02 o 3 6 2 315.73 282.18 10.24 o 4 6 2 427.61 414.89 12.84 o -10 1 3 193.22 190.57 10.17 o -9 1 3 154.09 154.94 10.17 o -8 1 3 26.07 39.84 4.80 o -7 1 3 1334.93 1290.73 19.00 o -6 1 3 0.03 3.42 2.72 o -5 1 3 53.64 59.46 3.16 o -4 1 3 33.03 30.05 2.12 o -3 1 3 19.46 25.01 1.71 o -2 1 3 9951.06 10474.69 56.80 o -1 1 3 196.79 171.03 3.21 o 0 1 3 7376.34 7826.48 42.70 o 1 1 3 27.67 35.39 1.75 o 2 1 3 477.80 526.18 6.96 o 3 1 3 303.75 346.39 5.24 o 4 1 3 197.31 217.45 4.85 o 5 1 3 33.91 34.58 3.16 o 6 1 3 55.53 64.67 4.62 o 7 1 3 449.61 464.27 12.16 o 8 1 3 2.73 8.32 2.74 o 9 1 3 264.51 265.28 11.36 o -9 2 3 3.59 14.10 4.24 o -8 2 3 556.14 515.55 16.12 o -7 2 3 299.00 275.72 9.56 o -6 2 3 80.12 87.63 5.71 o -5 2 3 982.18 881.46 11.95 o -4 2 3 420.93 431.95 6.72 o -3 2 3 731.11 604.26 7.67 o -2 2 3 123.63 104.00 3.09 o -1 2 3 1761.12 1713.82 14.50 o 0 2 3 118.82 111.90 2.88 o 1 2 3 200.92 144.18 3.04 o 2 2 3 224.67 182.78 4.41 o 3 2 3 265.89 222.93 5.37 o 4 2 3 525.84 461.77 8.33 o 5 2 3 166.68 151.62 5.40 o 6 2 3 864.56 844.86 14.49 o 7 2 3 297.63 270.98 10.72 o 8 2 3 265.36 279.01 11.32 o 9 2 3 163.06 159.18 8.36 o -9 3 3 303.73 338.27 18.19 o -8 3 3 120.04 104.89 6.98 o -7 3 3 0.48 1.74 2.61 o -6 3 3 387.02 352.49 12.38 o -5 3 3 336.73 323.77 9.71 o -4 3 3 1158.10 1125.36 23.33 o -3 3 3 757.91 746.30 9.36 o -2 3 3 503.67 479.84 7.04 o -1 3 3 63.59 79.48 3.01 o 0 3 3 525.65 495.45 6.70 o 1 3 3 85.44 82.32 3.93 o 2 3 3 1229.56 1280.73 17.75 o 3 3 3 794.60 773.18 20.97 o 4 3 3 0.55 5.42 2.57 o 5 3 3 204.65 210.53 7.38 o 6 3 3 9.11 16.33 3.41 o 7 3 3 42.41 58.11 5.40 o 8 3 3 1.81 15.64 3.01 o -8 4 3 56.20 88.11 6.28 o -7 4 3 95.71 95.94 6.63 o -6 4 3 179.18 169.66 8.79 o -5 4 3 174.49 173.55 7.55 o -4 4 3 274.69 239.16 7.65 o -3 4 3 343.91 324.02 8.62 o -2 4 3 217.51 217.03 6.90 o -1 4 3 8.67 11.44 3.09 o 0 4 3 0.00 1.81 2.57 o 1 4 3 395.27 392.07 10.96 o 2 4 3 132.83 130.06 5.95 o 3 4 3 111.05 115.61 7.51 o 4 4 3 28.96 41.37 4.08 o 5 4 3 37.48 42.57 3.88 o 6 4 3 79.41 93.62 7.36 o 7 4 3 41.92 47.65 4.46 o -7 5 3 0.56 19.14 4.27 o -6 5 3 72.38 74.20 5.57 o -5 5 3 1.77 10.12 4.29 o -4 5 3 108.41 112.23 6.15 o -3 5 3 35.25 46.33 4.26 o -2 5 3 32.99 41.39 4.48 o -1 5 3 71.62 71.12 4.23 o 0 5 3 104.34 100.99 5.70 o 1 5 3 3.71 12.05 3.00 o 2 5 3 307.55 301.35 10.09 o 3 5 3 24.76 36.55 4.60 o 4 5 3 175.29 164.19 7.67 o 5 5 3 57.82 70.15 4.96 o 6 5 3 27.15 32.10 3.83 o -5 6 3 61.76 52.35 5.03 o -4 6 3 84.16 99.08 6.30 o -3 6 3 299.92 330.57 11.02 o -2 6 3 154.10 141.92 7.94 o -1 6 3 225.63 242.05 10.69 o 0 6 3 23.15 28.24 3.38 o 1 6 3 524.05 494.72 13.67 o 2 6 3 22.71 45.40 4.14 o 3 6 3 93.60 94.08 5.74 o 4 6 3 35.04 43.44 3.77 o -10 0 4 79.78 80.04 9.17 o -9 0 4 72.73 84.71 7.24 o -8 0 4 1203.53 1155.42 26.73 o -7 0 4 43.16 58.45 7.28 o -6 0 4 2086.60 2034.47 32.38 o -5 0 4 706.77 788.24 29.65 o -4 0 4 14.83 5.90 3.14 o -3 0 4 32.03 42.98 3.76 o -2 0 4 319.74 348.05 6.07 o -1 0 4 4360.70 4461.41 36.27 o 0 0 4 1050.94 1099.22 14.48 o 1 0 4 9480.19 9554.73 72.97 o 2 0 4 967.49 998.62 12.76 o 3 0 4 1694.41 1736.80 20.12 o 4 0 4 69.84 62.16 4.44 o 5 0 4 1757.10 1838.37 24.20 o 6 0 4 2207.24 2175.89 33.55 o 7 0 4 427.98 392.57 17.62 o 8 0 4 374.44 365.81 18.13 o 9 0 4 89.10 104.79 9.34 o -10 1 4 34.10 47.49 6.34 o -9 1 4 32.35 53.55 5.02 o -8 1 4 9.18 12.76 3.20 o -7 1 4 113.69 122.92 6.28 o -6 1 4 2.32 -0.28 2.64 o -5 1 4 120.30 136.16 4.29 o -4 1 4 324.20 384.77 6.57 o -3 1 4 222.91 212.81 3.88 o -2 1 4 538.95 652.89 6.84 o -1 1 4 78.88 83.91 2.48 o 0 1 4 833.76 818.77 7.35 o 1 1 4 2205.98 2263.99 15.38 o 2 1 4 996.62 932.82 8.68 o 3 1 4 459.16 454.08 6.22 o 4 1 4 502.88 503.68 7.37 o 5 1 4 118.89 115.93 5.46 o 6 1 4 135.38 139.84 5.53 o 7 1 4 59.02 59.26 4.68 o 8 1 4 13.24 17.87 3.78 o 9 1 4 53.88 69.51 5.55 o -9 2 4 16.93 31.27 4.77 o -8 2 4 8.63 11.76 2.84 o -7 2 4 6.73 15.43 3.35 o -6 2 4 86.29 91.67 5.09 o -5 2 4 67.79 63.65 3.56 o -4 2 4 1519.88 1512.94 14.10 o -3 2 4 493.97 459.76 6.73 o -2 2 4 266.46 281.96 4.99 o -1 2 4 377.40 451.88 6.09 o 0 2 4 0.61 1.00 1.17 o 1 2 4 698.58 760.90 8.49 o 2 2 4 552.99 568.97 8.16 o 3 2 4 756.98 776.65 10.45 o 4 2 4 50.62 61.37 4.39 o 5 2 4 443.71 457.54 9.20 o 6 2 4 727.15 670.25 14.33 o 7 2 4 139.45 148.73 7.86 o 8 2 4 4.64 8.67 6.15 o 9 2 4 1.19 17.62 6.76 o -9 3 4 100.66 89.23 9.39 o -8 3 4 104.34 102.59 6.98 o -7 3 4 173.48 165.18 8.88 o -6 3 4 63.76 68.97 6.13 o -5 3 4 147.36 137.21 6.72 o -4 3 4 19.55 15.18 2.92 o -3 3 4 633.56 619.62 8.72 o -2 3 4 88.44 76.77 3.39 o -1 3 4 207.08 226.09 4.80 o 0 3 4 1276.51 1336.11 18.52 o 1 3 4 6.15 6.74 2.67 o 2 3 4 189.00 174.43 6.07 o 3 3 4 685.46 632.73 17.74 o 4 3 4 85.87 79.84 4.88 o 5 3 4 65.61 65.60 4.62 o 6 3 4 17.86 32.12 3.95 o 7 3 4 29.55 37.12 5.15 o 8 3 4 0.60 8.64 3.82 o -8 4 4 69.36 85.97 11.06 o -7 4 4 9.24 16.14 4.11 o -6 4 4 134.69 124.75 7.76 o -5 4 4 74.42 73.13 5.35 o -4 4 4 197.10 157.24 6.33 o -3 4 4 989.37 967.26 14.79 o -2 4 4 1.07 0.95 2.36 o -1 4 4 737.33 698.04 12.18 o 0 4 4 94.90 112.12 5.20 o 1 4 4 400.60 386.90 10.03 o 2 4 4 209.68 200.69 7.21 o 3 4 4 628.63 604.14 15.48 o 4 4 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