#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2215005.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215005_Fobs loop_ _publ_author_name 'Habibi, Mohammad Hossein' 'Mikhak, Maryam' 'Harrington, Ross W.' 'Clegg, William' _publ_section_title ; Bis[chloridobis(triphenylphosphine)copper(I)-\m-chlorido]bis(1,2-diaminopropane)copper(II) acetonitrile disolvate ; _journal_coeditor_code BT2455 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2305 _journal_page_last m2306 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.957 _cell_angle_gamma 90.000 _cell_length_a 15.8960 _cell_length_b 9.4181 _cell_length_c 26.5330 _exptl_crystal_F_000 1670.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file bt2455Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mhh507 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 345.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 24839.78 27132.01 975.95 o 5 0 0 105.72 60.51 16.01 o 6 0 0 853.48 945.81 45.77 o 7 0 0 52.03 31.27 19.82 o 8 0 0 880.64 830.76 53.98 o 9 0 0 51246.70 59013.88 3066.34 o 10 0 0 29.91 -5.64 95.16 o 11 0 0 74.83 118.40 59.23 o 12 0 0 2488.90 2937.01 268.70 o 13 0 0 11340.52 12868.94 849.06 o 14 0 0 493.09 544.86 95.15 o 15 0 0 0.05 -98.82 67.55 o 16 0 0 3068.54 3303.63 274.34 o 17 0 0 125.36 246.58 99.23 o 18 0 0 4246.82 4400.51 576.59 o 3 1 0 20877.38 20240.71 564.07 o 4 1 0 3360.67 3497.79 93.46 o 5 1 0 183.89 153.86 23.86 o 6 1 0 10220.43 10893.14 318.75 o 7 1 0 977.01 1172.40 84.35 o 8 1 0 4790.84 5182.25 146.74 o 9 1 0 1669.48 1916.19 75.18 o 10 1 0 5480.03 5804.50 205.56 o 11 1 0 829.53 811.74 54.86 o 12 1 0 8767.23 9364.91 309.53 o 13 1 0 632.32 676.39 58.03 o 14 1 0 742.77 773.99 65.01 o 15 1 0 1408.09 1332.12 86.22 o 16 1 0 14.04 6.21 55.94 o 17 1 0 1331.64 1387.50 104.07 o 18 1 0 236.91 97.80 119.55 o 0 2 0 20059.31 9996.52 402.73 o 1 2 0 7705.47 6553.92 206.00 o 2 2 0 5005.20 4506.69 110.39 o 3 2 0 6935.70 6825.33 135.39 o 4 2 0 29782.73 31604.15 597.46 o 5 2 0 674.76 755.08 29.77 o 6 2 0 9452.54 9823.16 229.63 o 7 2 0 1502.35 1284.22 51.66 o 8 2 0 1261.59 1391.73 53.93 o 9 2 0 1877.91 1917.63 69.05 o 10 2 0 5600.78 6130.07 171.27 o 11 2 0 3168.85 3178.78 108.04 o 12 2 0 3696.29 3973.65 153.97 o 13 2 0 1954.93 2061.63 101.44 o 14 2 0 136.31 166.08 76.30 o 15 2 0 113.92 374.64 71.87 o 16 2 0 115.35 100.22 98.77 o 17 2 0 3.14 38.77 58.03 o 18 2 0 92.79 172.36 63.32 o 1 3 0 88.39 103.96 9.46 o 2 3 0 1694.63 1714.26 43.91 o 3 3 0 35.02 25.71 11.80 o 4 3 0 2683.67 2894.90 63.30 o 5 3 0 13755.90 13841.04 271.24 o 6 3 0 2770.92 2886.63 80.58 o 7 3 0 10351.67 11116.82 277.90 o 8 3 0 11.55 -12.88 35.45 o 9 3 0 444.71 474.21 45.66 o 10 3 0 0.75 5.60 22.38 o 11 3 0 1126.84 1180.35 52.62 o 12 3 0 33.09 129.20 33.72 o 13 3 0 1446.94 1528.48 76.96 o 14 3 0 1.81 22.63 45.81 o 15 3 0 0.15 42.01 42.54 o 16 3 0 395.69 366.56 83.69 o 17 3 0 262.75 205.83 75.57 o 18 3 0 109.92 152.67 65.39 o 0 4 0 1924.78 1890.18 79.47 o 1 4 0 2818.74 2634.34 69.21 o 2 4 0 9266.82 9125.63 222.11 o 3 4 0 595.79 497.84 21.74 o 4 4 0 4369.86 4359.85 128.29 o 5 4 0 1183.72 1286.27 41.36 o 6 4 0 3424.08 3750.58 100.64 o 7 4 0 412.89 478.75 28.74 o 8 4 0 6174.59 6247.03 169.74 o 9 4 0 991.62 962.73 44.86 o 10 4 0 1767.08 1822.55 67.23 o 11 4 0 3054.07 3077.72 99.40 o 12 4 0 4.73 -6.13 28.50 o 13 4 0 76.77 43.23 32.15 o 14 4 0 571.91 517.14 52.82 o 15 4 0 25.85 45.15 49.62 o 16 4 0 190.05 215.07 49.23 o 17 4 0 1036.02 903.87 87.97 o 1 5 0 112.28 80.73 18.30 o 2 5 0 1909.50 1981.16 57.64 o 3 5 0 2817.33 2653.68 105.92 o 4 5 0 1596.42 1645.73 63.10 o 5 5 0 491.53 681.78 40.73 o 6 5 0 742.92 668.25 30.48 o 7 5 0 32.68 17.99 17.54 o 8 5 0 6.10 11.94 18.21 o 9 5 0 10.75 -20.12 42.81 o 10 5 0 339.07 376.97 34.67 o 11 5 0 102.82 96.92 32.55 o 12 5 0 381.60 454.47 49.00 o 13 5 0 1025.68 1037.56 99.29 o 14 5 0 26.85 -65.82 56.91 o 15 5 0 441.01 363.40 78.80 o 16 5 0 0.60 8.70 88.10 o 0 6 0 6487.56 6532.46 232.64 o 1 6 0 2617.34 2398.20 71.09 o 2 6 0 241.94 257.28 22.27 o 3 6 0 50.92 51.44 23.08 o 4 6 0 1945.09 2093.29 87.78 o 5 6 0 1877.22 2219.00 93.47 o 6 6 0 1075.78 1271.68 67.78 o 7 6 0 45.40 -3.73 20.01 o 8 6 0 89.20 132.27 28.59 o 9 6 0 7907.53 8492.65 278.55 o 10 6 0 4443.29 4212.80 226.04 o 11 6 0 90.74 22.18 42.36 o 12 6 0 158.63 112.71 49.32 o 13 6 0 317.18 285.86 50.66 o 14 6 0 721.67 900.67 97.25 o 15 6 0 173.22 304.09 81.88 o 1 7 0 355.81 334.16 23.00 o 2 7 0 751.05 639.28 68.67 o 3 7 0 700.33 728.31 51.15 o 4 7 0 2201.70 2220.51 96.65 o 5 7 0 3875.69 4268.50 158.52 o 6 7 0 3142.18 3663.94 141.92 o 7 7 0 2364.39 2388.68 156.67 o 8 7 0 5416.09 5761.48 321.09 o 9 7 0 29.64 -42.51 52.62 o 10 7 0 1242.28 1423.40 133.31 o 11 7 0 1101.70 1229.74 155.12 o 12 7 0 83.29 -54.61 62.15 o 13 7 0 972.73 847.04 104.61 o 14 7 0 126.51 113.44 77.18 o 0 8 0 8.02 93.15 53.93 o 1 8 0 133.30 69.81 85.16 o 2 8 0 5016.00 5427.16 247.45 o 3 8 0 69.05 33.06 47.15 o 4 8 0 2962.42 3716.88 172.78 o 5 8 0 953.13 1211.92 109.62 o 6 8 0 1174.89 1207.04 89.56 o 7 8 0 3237.21 3427.59 188.82 o 8 8 0 50.81 16.62 58.97 o 9 8 0 231.21 158.06 58.67 o 10 8 0 73.37 -26.95 79.09 o 11 8 0 1288.34 168.14 219.94 o 12 8 0 690.45 177.60 327.30 o 13 8 0 101.14 -66.77 93.60 o 1 9 0 47.87 58.23 102.48 o 2 9 0 42.95 19.83 62.61 o 3 9 0 1.57 -17.96 75.83 o 4 9 0 688.15 787.14 151.45 o 5 9 0 15.53 39.24 61.08 o 6 9 0 498.66 495.55 159.45 o 7 9 0 30.23 18.30 61.38 o 8 9 0 70.22 27.97 66.13 o 9 9 0 42.14 65.11 81.84 o 10 9 0 1431.03 1767.27 174.15 o 11 9 0 107.18 82.17 87.71 o 0 10 0 3602.17 3314.96 508.26 o 1 10 0 279.06 155.72 122.65 o 2 10 0 201.59 21.57 124.41 o 3 10 0 78.93 129.57 90.16 o 4 10 0 70.51 52.15 140.70 o 5 10 0 20.17 -31.67 81.46 o 6 10 0 344.86 336.26 97.47 o 7 10 0 151.90 294.82 127.35 o 8 10 0 34.99 40.12 111.83 o 1 11 0 740.20 -40.13 112.89 o 2 11 0 75.58 26.21 118.54 o 3 11 0 109.08 -102.10 112.13 o -18 1 1 778.11 949.90 213.96 o -17 1 1 72.11 118.80 62.91 o -16 1 1 91.33 71.02 53.21 o -15 1 1 2.92 8.67 47.44 o -14 1 1 5.50 106.67 73.10 o -13 1 1 264.39 239.60 58.15 o -12 1 1 204.55 299.63 53.92 o -11 1 1 2274.26 2156.54 95.43 o -10 1 1 12235.45 13318.75 413.62 o -9 1 1 20182.68 21753.34 571.65 o -8 1 1 381.82 425.47 27.89 o -7 1 1 7431.75 8524.85 205.93 o -6 1 1 8800.44 9514.54 223.67 o -5 1 1 928.67 813.28 57.47 o -4 1 1 10.77 62.44 17.81 o -3 1 1 50.21 62.88 29.85 o 3 1 1 74768.07 83546.09 1630.25 o 4 1 1 2330.47 2498.58 62.70 o 5 1 1 22819.81 26226.03 517.31 o 6 1 1 803.09 863.33 129.58 o 7 1 1 1016.80 965.57 39.29 o 8 1 1 11615.69 12394.56 335.64 o 9 1 1 18383.42 19399.86 458.45 o 10 1 1 512.87 497.73 45.75 o 11 1 1 38.78 33.01 48.45 o 12 1 1 221.99 283.90 52.95 o 13 1 1 301.13 142.76 66.79 o 14 1 1 36.32 49.41 50.46 o 15 1 1 133.91 147.92 54.83 o 16 1 1 373.50 276.15 61.94 o 17 1 1 253.64 234.47 71.33 o 18 1 1 1187.89 1040.83 73.65 o -18 2 1 108.55 162.96 57.29 o -17 2 1 593.73 539.71 75.02 o -16 2 1 780.20 698.19 69.95 o -15 2 1 308.75 339.35 57.83 o -14 2 1 20.49 6.28 52.16 o -13 2 1 19.63 -62.99 53.10 o -12 2 1 102.64 243.66 56.58 o -11 2 1 6602.31 6834.43 234.22 o -10 2 1 2674.48 2650.76 103.48 o -9 2 1 12022.73 12333.01 309.02 o -8 2 1 6651.91 7327.25 216.88 o -7 2 1 14692.27 16339.42 432.61 o -6 2 1 10943.55 11791.90 249.46 o -5 2 1 2159.31 2283.67 58.79 o -4 2 1 774.96 852.13 28.96 o -3 2 1 788.85 946.03 42.44 o -2 2 1 3447.61 3794.36 80.43 o -1 2 1 10827.95 9529.27 220.86 o 0 2 1 5648.33 3642.12 120.94 o 1 2 1 21216.93 17735.93 690.66 o 2 2 1 20851.61 20582.98 532.22 o 3 2 1 2902.25 2779.51 74.31 o 4 2 1 871.02 886.23 37.26 o 5 2 1 13900.37 14427.92 294.05 o 6 2 1 1171.78 1530.81 85.45 o 7 2 1 9462.45 9725.05 229.52 o 8 2 1 6984.46 7185.51 213.08 o 9 2 1 323.80 357.34 28.27 o 10 2 1 15881.82 17257.38 504.65 o 11 2 1 1412.07 1683.90 73.37 o 12 2 1 1614.61 1717.99 114.78 o 13 2 1 129.92 102.24 47.81 o 14 2 1 140.77 69.22 42.92 o 15 2 1 19.89 99.56 42.47 o 16 2 1 2.63 10.66 52.91 o 17 2 1 131.86 137.37 65.19 o 18 2 1 90.07 74.29 72.85 o -18 3 1 255.03 233.49 64.15 o -17 3 1 439.90 367.97 67.86 o -16 3 1 802.38 911.74 93.84 o -15 3 1 3.45 36.54 44.39 o -14 3 1 1263.53 1254.00 84.87 o -13 3 1 211.72 78.60 50.75 o -12 3 1 7613.17 7920.55 269.30 o -11 3 1 5350.39 5574.86 178.10 o -10 3 1 864.84 850.39 64.04 o -9 3 1 227.23 236.44 40.51 o -8 3 1 8316.35 8801.60 254.16 o -7 3 1 6009.16 6227.02 188.56 o -6 3 1 2.28 2.11 13.79 o -5 3 1 20516.65 21864.67 402.40 o -4 3 1 277.93 411.93 22.52 o -3 3 1 10875.74 10273.90 223.94 o -2 3 1 46628.26 49531.42 787.86 o -1 3 1 949.33 1002.62 32.25 o 0 3 1 7792.42 7795.89 156.21 o 1 3 1 22726.01 21645.26 365.56 o 2 3 1 9774.10 9344.26 191.88 o 3 3 1 947.90 825.35 21.68 o 4 3 1 22271.82 22663.65 421.79 o 5 3 1 3547.18 4085.50 114.10 o 6 3 1 14264.15 14614.17 323.05 o 7 3 1 5239.04 4805.42 123.40 o 8 3 1 203.41 238.91 23.48 o 9 3 1 11.53 26.54 19.87 o 10 3 1 3724.75 3597.31 104.90 o 11 3 1 5174.94 5331.29 152.94 o 12 3 1 1022.69 1080.91 53.53 o 13 3 1 475.37 550.68 54.95 o 14 3 1 431.65 439.24 53.84 o 15 3 1 1569.43 1465.56 90.04 o 16 3 1 89.78 31.09 48.69 o 17 3 1 18.57 18.19 60.25 o 18 3 1 263.52 302.12 110.16 o -17 4 1 794.32 792.22 70.95 o -16 4 1 217.37 226.07 51.70 o -15 4 1 2015.61 2064.01 135.69 o -14 4 1 3.00 26.90 36.55 o -13 4 1 3180.66 3074.60 103.21 o -12 4 1 0.52 55.82 49.98 o -11 4 1 1097.69 1166.85 55.37 o -10 4 1 510.93 431.39 33.10 o -9 4 1 787.37 845.97 42.46 o -8 4 1 2361.72 2522.03 82.31 o -7 4 1 3054.80 3022.91 93.29 o -6 4 1 4170.30 4238.78 121.23 o -5 4 1 267.88 250.65 18.33 o -4 4 1 18329.77 19337.34 413.37 o -3 4 1 59.76 67.55 15.05 o -2 4 1 3040.86 2659.01 115.81 o -1 4 1 2294.59 2034.15 51.02 o 0 4 1 4757.03 4608.00 103.21 o 1 4 1 12362.11 11441.91 228.33 o 2 4 1 467.15 516.75 20.22 o 3 4 1 2777.22 2358.13 62.93 o 4 4 1 1688.88 1974.90 52.68 o 5 4 1 13797.16 14531.82 301.70 o 6 4 1 796.39 964.26 33.43 o 7 4 1 5873.52 6303.97 169.83 o 8 4 1 266.66 258.40 24.54 o 9 4 1 4623.16 4559.34 132.35 o 10 4 1 913.73 936.80 46.09 o 11 4 1 38.99 18.03 44.81 o 12 4 1 412.12 472.59 38.95 o 13 4 1 29.45 103.48 33.09 o 14 4 1 2546.16 2521.49 132.37 o 15 4 1 10.32 55.62 43.88 o 16 4 1 1456.41 1430.02 86.19 o 17 4 1 18.32 71.16 54.42 o -16 5 1 2642.50 2320.40 255.47 o -15 5 1 180.13 120.81 59.41 o -14 5 1 4412.32 3515.73 241.39 o -13 5 1 288.16 281.74 39.62 o -12 5 1 21.68 32.05 30.59 o -11 5 1 209.94 229.20 40.82 o -10 5 1 4131.89 4304.02 128.52 o -9 5 1 3635.08 3904.84 118.27 o -8 5 1 1504.56 1478.25 50.91 o -7 5 1 390.83 396.66 24.98 o -6 5 1 10.59 -13.88 12.36 o -5 5 1 12988.39 13954.48 346.45 o -4 5 1 783.69 737.57 34.10 o -3 5 1 7767.35 8345.83 305.83 o -2 5 1 3094.67 2907.54 79.94 o -1 5 1 25455.48 24925.93 547.47 o 0 5 1 11693.41 11106.12 212.95 o 1 5 1 1972.51 2142.10 63.72 o 2 5 1 3918.19 3697.67 87.90 o 3 5 1 216.53 220.17 15.41 o 4 5 1 8591.78 8633.59 268.90 o 5 5 1 472.93 382.45 23.57 o 6 5 1 1388.26 1380.91 48.31 o 7 5 1 3437.65 3429.45 95.92 o 8 5 1 6009.32 6204.21 157.68 o 9 5 1 498.77 472.59 33.94 o 10 5 1 447.58 474.24 43.79 o 11 5 1 0.71 84.73 35.40 o 12 5 1 415.53 343.67 65.72 o 13 5 1 1203.00 1293.28 69.57 o 14 5 1 2.14 -24.92 40.18 o 15 5 1 1749.06 1720.18 98.69 o 16 5 1 60.43 -94.89 63.26 o -14 6 1 177.49 224.14 63.19 o -13 6 1 1012.57 1178.66 103.54 o -12 6 1 1.56 -22.68 48.86 o -11 6 1 74.34 15.00 46.69 o -10 6 1 44.44 83.43 36.87 o -9 6 1 7.20 23.87 26.22 o -8 6 1 220.65 197.58 23.01 o -7 6 1 24.75 9.30 30.37 o -6 6 1 1429.21 1535.73 67.26 o -5 6 1 461.10 633.52 71.74 o -4 6 1 8052.53 8982.05 489.92 o -3 6 1 3140.41 3336.10 145.96 o -2 6 1 5460.53 5810.55 208.65 o -1 6 1 468.69 534.03 42.60 o 0 6 1 415.68 416.72 24.61 o 1 6 1 1104.38 1056.33 36.11 o 2 6 1 477.25 457.00 22.30 o 3 6 1 3719.65 3595.71 132.38 o 4 6 1 610.57 553.98 44.57 o 5 6 1 4775.22 5033.20 161.70 o 6 6 1 557.00 376.91 73.70 o 7 6 1 32.86 17.02 24.93 o 8 6 1 121.72 121.90 27.58 o 9 6 1 2848.03 3001.91 110.51 o 10 6 1 95.76 103.73 40.36 o 11 6 1 1137.57 1265.53 71.08 o 12 6 1 76.32 29.48 59.99 o 13 6 1 128.63 56.84 51.12 o 14 6 1 1225.05 1121.47 101.72 o 15 6 1 640.05 713.07 110.76 o -14 7 1 110.73 68.66 70.63 o -13 7 1 0.48 4.44 59.23 o -12 7 1 55.09 33.37 71.44 o -11 7 1 1112.25 1131.69 149.13 o -10 7 1 306.69 306.29 63.31 o -9 7 1 182.17 167.09 62.48 o -8 7 1 229.64 220.62 62.07 o -7 7 1 138.72 152.30 48.36 o -6 7 1 292.82 281.09 56.60 o -5 7 1 2581.32 3109.71 115.61 o -4 7 1 1671.54 1612.82 81.01 o -3 7 1 2547.33 2874.77 122.49 o -2 7 1 1386.22 1313.94 73.02 o -1 7 1 3.80 42.79 19.17 o 0 7 1 393.57 432.86 23.35 o 1 7 1 3998.48 3842.81 99.63 o 2 7 1 26.44 20.17 25.35 o 3 7 1 1250.18 1328.19 82.92 o 4 7 1 126.64 159.59 37.42 o 5 7 1 818.39 888.15 57.25 o 6 7 1 273.74 217.37 67.04 o 7 7 1 116.58 -102.22 107.25 o 8 7 1 132.38 105.69 60.50 o 9 7 1 1981.66 1326.84 436.00 o 10 7 1 987.93 845.28 184.32 o 11 7 1 66.84 10.80 58.98 o 12 7 1 330.41 151.01 71.72 o 13 7 1 4.32 31.25 67.18 o 14 7 1 43.43 137.41 78.06 o -13 8 1 109.43 115.13 90.38 o -12 8 1 49.18 17.03 88.09 o -11 8 1 69.95 -4.17 70.49 o -10 8 1 171.35 154.09 105.08 o -9 8 1 39.87 27.10 73.24 o -8 8 1 92.66 112.11 81.47 o -7 8 1 49.58 50.60 54.42 o -6 8 1 154.67 111.21 65.51 o -5 8 1 240.68 381.13 73.67 o -4 8 1 38.25 33.92 45.00 o -3 8 1 331.44 381.83 51.16 o -2 8 1 1724.16 1863.81 99.58 o -1 8 1 36.12 20.08 46.38 o 0 8 1 386.43 253.44 59.37 o 1 8 1 1032.48 1086.75 94.67 o 2 8 1 14.69 -23.93 64.09 o 3 8 1 42.95 13.58 46.51 o 4 8 1 659.48 835.82 163.84 o 5 8 1 116.49 263.35 62.13 o 6 8 1 1.73 86.01 66.43 o 7 8 1 591.50 225.08 239.86 o 8 8 1 3.55 -67.14 56.16 o 9 8 1 521.64 135.55 155.54 o 10 8 1 2.40 0.95 80.00 o 11 8 1 35.28 101.59 74.46 o 12 8 1 30.86 -62.47 89.47 o 13 8 1 84.68 110.17 87.04 o -11 9 1 96.73 40.06 95.50 o -10 9 1 293.62 65.65 111.74 o -9 9 1 1591.05 2003.99 445.62 o -8 9 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199.25 o -2 0 28 272.44 212.05 65.33 o -1 0 28 757.68 823.69 101.14 o 0 0 28 1752.66 1900.51 139.27 o 1 0 28 497.88 526.16 78.09 o 2 0 28 253.41 280.05 125.41 o 3 0 28 418.81 818.33 132.47 o 4 0 28 2690.60 2947.37 175.43 o 5 0 28 219.35 472.99 150.92 o 6 0 28 543.76 584.01 80.87 o 7 0 28 2.36 5.45 90.94 o -9 1 28 207.16 122.34 77.34 o -8 1 28 407.03 453.55 57.12 o -7 1 28 457.21 597.93 77.68 o -6 1 28 7.24 3.33 45.79 o -5 1 28 715.94 767.91 67.84 o -4 1 28 230.60 200.16 50.79 o -3 1 28 289.07 280.67 51.61 o -2 1 28 407.36 458.43 51.83 o -1 1 28 14.28 72.32 47.04 o 0 1 28 196.42 308.25 58.06 o 1 1 28 1127.61 1271.70 77.69 o 2 1 28 133.00 93.67 49.31 o 3 1 28 617.07 702.62 63.91 o 4 1 28 2.26 43.24 52.52 o 5 1 28 156.55 151.55 67.39 o 6 1 28 1.59 -8.23 83.56 o 7 1 28 186.41 269.57 70.36 o -9 2 28 96.80 9.99 59.31 o -8 2 28 649.53 558.08 137.88 o -7 2 28 124.41 60.46 60.71 o -6 2 28 87.58 81.12 57.50 o -5 2 28 28.63 97.54 47.32 o -4 2 28 84.07 14.80 62.73 o -3 2 28 317.20 350.18 53.14 o 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537.28 423.83 76.61 o 4 1 30 335.87 427.28 65.19 o -6 2 30 290.60 363.28 95.49 o -5 2 30 20.45 6.60 49.27 o -4 2 30 8.97 -18.54 60.04 o -3 2 30 96.92 89.35 57.20 o -2 2 30 46.31 39.18 47.21 o -1 2 30 3.69 -63.31 59.11 o 0 2 30 96.42 166.92 58.78 o 1 2 30 83.33 78.90 56.63 o 2 2 30 238.38 240.60 61.02 o 3 2 30 84.79 165.54 58.24 o -4 3 30 363.80 493.02 67.61 o -3 3 30 0.16 -21.23 52.02 o -2 3 30 43.82 55.91 55.19 o -1 3 30 6.74 32.32 51.10 o 0 3 30 6.42 -45.30 55.48 o 1 3 30 409.69 590.00 84.81 o -4 1 31 75.90 170.18 63.58 o -3 1 31 129.15 129.36 85.26 o -2 1 31 73.03 2.55 62.16 o -1 1 31 142.24 142.80 70.22 o 0 1 31 184.94 208.00 67.62 o 1 1 31 22.27 -5.86 58.87 o -2 2 31 0.05 29.06 67.30 o -1 2 31 10.82 5.98 54.39 o