#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:34:26 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181070 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/50/2215077.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215077_Fobs loop_ _publ_author_name 'Li, Kao-Zhen' 'He, Qing-Peng' 'Li, Rong-Shan' 'Wang, Da-Qi' 'Lu, Ze-Hua' _publ_section_title ; 4-Amino-3,5-bis(1-hydroxyethyl)-4H-1,2,4-triazole ; _journal_coeditor_code CV2290 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3908 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.7936 _cell_length_b 8.8609 _cell_length_c 16.0583 _exptl_crystal_F_000 608.00 _reflns_d_resolution_high 0.8402 _cod_data_source_file cv2290Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070530c in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 177.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5414.97 5798.81 177.45 o 4 0 0 6.75 8.88 1.28 o 6 0 0 96.36 80.15 7.00 o 8 0 0 132.48 130.86 10.42 o 10 0 0 21.19 24.49 7.70 o 2 1 0 142.11 142.45 4.45 o 4 1 0 1642.89 1672.50 26.03 o 6 1 0 49.81 50.60 4.73 o 8 1 0 136.31 137.68 8.82 o 10 1 0 238.20 252.80 12.09 o 0 2 0 6500.63 6920.74 206.11 o 2 2 0 31645.58 34959.19 1006.37 o 4 2 0 1063.99 1012.45 30.18 o 6 2 0 160.77 142.97 6.86 o 8 2 0 153.13 155.06 8.23 o 10 2 0 0.18 -3.19 3.39 o 2 3 0 735.30 808.30 26.29 o 4 3 0 1862.21 1881.81 55.16 o 6 3 0 487.81 489.03 27.56 o 8 3 0 365.12 367.02 30.35 o 10 3 0 11.29 8.94 4.67 o 0 4 0 54.14 32.09 2.81 o 2 4 0 2240.86 2330.29 60.39 o 4 4 0 1089.08 1130.67 34.97 o 6 4 0 33.22 44.89 4.95 o 8 4 0 30.14 28.87 5.43 o 2 5 0 6.89 1.73 1.51 o 4 5 0 1572.40 1616.14 54.11 o 6 5 0 81.86 94.77 10.46 o 8 5 0 76.29 88.35 10.44 o 0 6 0 242.97 255.32 9.28 o 2 6 0 77.07 73.60 3.21 o 4 6 0 9.04 3.67 2.18 o 6 6 0 226.84 210.44 9.53 o 8 6 0 4.34 0.14 3.80 o 2 7 0 1373.02 1383.55 28.23 o 4 7 0 121.91 124.35 5.68 o 6 7 0 190.87 137.81 11.42 o 0 8 0 4.31 9.79 5.55 o 2 8 0 37.88 33.69 4.06 o 4 8 0 4.28 -1.99 2.46 o 6 8 0 3.41 3.54 4.43 o 2 9 0 248.70 225.30 10.71 o 4 9 0 16.44 11.25 4.16 o 0 10 0 7.84 4.66 6.33 o 2 10 0 1.92 -5.01 3.34 o 1 1 1 64.67 60.17 1.19 o 2 1 1 14086.33 15686.73 349.96 o 3 1 1 300.32 290.44 5.60 o 4 1 1 11.42 12.70 1.29 o 5 1 1 182.96 169.43 2.99 o 6 1 1 38.84 44.41 4.08 o 7 1 1 4.52 3.43 1.91 o 8 1 1 34.69 28.84 3.32 o 9 1 1 0.08 -1.49 2.20 o 10 1 1 4.39 4.62 2.88 o 0 2 1 595.46 644.84 10.59 o 1 2 1 77.20 70.90 2.94 o 2 2 1 3134.49 3159.48 52.64 o 3 2 1 68.18 44.66 1.32 o 4 2 1 2.11 -0.84 0.62 o 5 2 1 1433.73 1478.44 17.96 o 6 2 1 258.53 254.42 6.79 o 7 2 1 19.22 15.40 2.55 o 8 2 1 61.77 67.56 4.64 o 9 2 1 43.03 45.82 4.22 o 10 2 1 0.96 -1.61 2.56 o 1 3 1 3586.74 3745.47 42.43 o 2 3 1 3811.50 4035.35 106.93 o 3 3 1 8.86 6.29 0.99 o 4 3 1 2078.89 2186.56 46.86 o 5 3 1 6.37 3.41 0.92 o 6 3 1 136.53 121.02 4.54 o 7 3 1 333.37 352.13 9.00 o 8 3 1 0.71 1.05 2.04 o 9 3 1 3.64 2.78 2.44 o 10 3 1 64.57 70.14 5.50 o 0 4 1 1.02 3.33 1.00 o 1 4 1 224.95 226.08 4.82 o 2 4 1 320.02 335.14 7.99 o 3 4 1 2147.07 2339.52 29.98 o 4 4 1 414.26 418.81 9.01 o 5 4 1 16.27 15.36 1.98 o 6 4 1 155.02 151.59 16.00 o 7 4 1 7.00 1.07 2.17 o 8 4 1 21.76 26.60 3.37 o 9 4 1 44.03 48.78 5.53 o 1 5 1 173.77 160.03 3.34 o 2 5 1 33.14 38.21 2.01 o 3 5 1 910.51 893.98 14.95 o 4 5 1 1352.90 1376.52 19.01 o 5 5 1 645.07 629.93 12.62 o 6 5 1 99.65 96.28 3.79 o 7 5 1 1.42 -0.13 1.98 o 8 5 1 6.23 4.19 2.53 o 9 5 1 33.50 52.22 5.93 o 0 6 1 326.65 346.50 8.01 o 1 6 1 57.78 56.87 2.30 o 2 6 1 512.99 566.76 7.92 o 3 6 1 0.04 -1.55 1.03 o 4 6 1 159.12 151.11 4.12 o 5 6 1 204.78 211.32 6.16 o 6 6 1 559.06 553.52 23.26 o 7 6 1 132.30 135.90 5.62 o 8 6 1 50.87 67.62 7.38 o 1 7 1 5.04 2.99 1.51 o 2 7 1 22.28 19.89 2.21 o 3 7 1 646.79 640.66 9.87 o 4 7 1 18.66 16.34 2.02 o 5 7 1 199.82 197.12 6.10 o 6 7 1 31.86 31.86 4.39 o 7 7 1 65.00 56.66 10.57 o 0 8 1 1559.89 1629.35 40.66 o 1 8 1 9.40 6.19 2.16 o 2 8 1 13.52 17.94 2.66 o 3 8 1 103.11 108.55 4.33 o 4 8 1 71.41 65.16 3.74 o 5 8 1 17.01 21.90 2.80 o 6 8 1 173.79 195.50 12.21 o 1 9 1 209.69 229.18 7.65 o 2 9 1 28.14 27.95 3.64 o 3 9 1 0.14 0.26 2.23 o 4 9 1 2.32 -0.28 2.14 o 5 9 1 21.54 21.12 3.47 o 0 10 1 2.24 -4.05 3.86 o 1 10 1 0.24 -2.08 2.43 o 2 10 1 34.20 26.23 3.81 o 3 10 1 7.75 5.53 2.84 o 0 0 2 2812.51 2419.02 51.72 o 1 0 2 280.17 259.95 4.59 o 2 0 2 385.14 446.35 8.43 o 3 0 2 298.34 302.13 6.72 o 4 0 2 418.40 467.31 9.95 o 5 0 2 125.39 123.58 4.03 o 6 0 2 1477.28 1572.35 38.44 o 7 0 2 137.17 146.22 7.36 o 8 0 2 325.85 321.16 19.34 o 9 0 2 114.73 114.96 7.95 o 10 0 2 3.88 2.29 3.82 o 1 1 2 9084.71 9082.73 292.46 o 2 1 2 482.57 473.11 5.95 o 3 1 2 3706.47 4064.94 64.17 o 4 1 2 739.40 744.40 9.54 o 5 1 2 5.54 1.21 0.87 o 6 1 2 167.40 151.06 4.91 o 7 1 2 212.91 210.81 8.95 o 8 1 2 27.57 33.65 3.53 o 9 1 2 179.39 175.00 6.58 o 10 1 2 0.51 -0.05 2.67 o 0 2 2 794.69 928.65 15.24 o 1 2 2 25.90 16.88 0.84 o 2 2 2 82.00 87.37 1.81 o 3 2 2 713.19 684.10 8.70 o 4 2 2 927.87 1030.01 14.06 o 5 2 2 289.70 279.98 6.49 o 6 2 2 412.05 433.20 9.73 o 7 2 2 119.69 106.11 4.47 o 8 2 2 132.27 136.01 5.42 o 9 2 2 125.90 126.38 5.63 o 10 2 2 12.15 12.12 3.34 o 1 3 2 5916.00 6220.86 154.87 o 2 3 2 1623.66 1688.77 35.00 o 3 3 2 0.04 -0.73 0.59 o 4 3 2 1197.97 1266.90 24.71 o 5 3 2 14.24 14.95 1.22 o 6 3 2 366.17 370.14 7.63 o 7 3 2 551.23 539.31 12.05 o 8 3 2 1.77 -0.55 2.00 o 9 3 2 50.92 56.13 4.75 o 0 4 2 118.37 114.03 3.33 o 1 4 2 373.36 350.65 5.92 o 2 4 2 303.01 332.42 5.29 o 3 4 2 2069.85 2163.16 40.72 o 4 4 2 3.83 2.85 1.01 o 5 4 2 690.60 694.08 14.57 o 6 4 2 20.39 23.44 2.47 o 7 4 2 47.48 39.89 4.83 o 8 4 2 31.75 26.92 3.58 o 9 4 2 8.58 7.39 2.94 o 1 5 2 19.63 21.93 1.77 o 2 5 2 1516.18 1606.75 19.85 o 3 5 2 219.23 222.69 4.40 o 4 5 2 1024.11 1049.17 16.73 o 5 5 2 753.74 729.39 13.05 o 6 5 2 117.51 123.21 4.23 o 7 5 2 28.41 27.72 3.73 o 8 5 2 4.85 2.58 2.32 o 9 5 2 0.42 2.72 3.29 o 0 6 2 169.47 184.56 7.22 o 1 6 2 204.74 207.23 4.79 o 2 6 2 24.00 21.37 2.00 o 3 6 2 6.84 5.70 1.46 o 4 6 2 0.34 -1.11 1.13 o 5 6 2 35.43 38.26 3.01 o 6 6 2 0.00 -2.84 1.89 o 7 6 2 3.91 10.20 3.28 o 8 6 2 0.10 -0.25 3.06 o 1 7 2 1.50 -0.75 1.41 o 2 7 2 19.31 15.00 2.11 o 3 7 2 7.39 3.59 1.45 o 4 7 2 201.08 200.45 4.70 o 5 7 2 17.95 14.87 2.45 o 6 7 2 124.55 107.43 5.56 o 7 7 2 15.74 12.12 3.28 o 0 8 2 38.74 32.68 5.83 o 1 8 2 394.94 372.25 8.69 o 2 8 2 11.47 7.81 2.25 o 3 8 2 165.36 173.05 5.49 o 4 8 2 2.15 -2.04 1.69 o 5 8 2 103.61 94.31 6.00 o 6 8 2 1.65 2.71 3.17 o 1 9 2 30.80 34.36 3.53 o 2 9 2 5.39 0.76 2.12 o 3 9 2 0.51 -2.33 2.03 o 4 9 2 3.56 2.75 2.23 o 5 9 2 3.08 1.29 3.01 o 0 10 2 65.83 70.86 9.21 o 1 10 2 2.66 2.54 2.79 o 2 10 2 38.04 31.72 4.10 o 3 10 2 0.23 -2.05 2.61 o 1 1 3 25.70 22.56 0.72 o 2 1 3 5633.66 5763.92 107.84 o 3 1 3 88.89 79.57 1.63 o 4 1 3 2323.24 2566.53 30.00 o 5 1 3 2.49 3.12 1.08 o 6 1 3 58.20 51.53 2.50 o 7 1 3 6.40 5.26 2.10 o 8 1 3 0.95 -0.89 1.93 o 9 1 3 22.65 22.81 3.44 o 10 1 3 25.58 23.37 3.84 o 0 2 3 1471.36 1401.53 25.33 o 1 2 3 858.88 802.87 14.54 o 2 2 3 645.96 609.97 11.89 o 3 2 3 154.63 164.58 2.87 o 4 2 3 34.24 38.67 1.39 o 5 2 3 537.11 549.14 7.77 o 6 2 3 4.26 2.38 1.34 o 7 2 3 211.55 190.34 6.11 o 8 2 3 281.88 277.54 12.53 o 9 2 3 146.17 142.38 6.01 o 10 2 3 4.18 -0.18 2.79 o 1 3 3 48.44 40.55 1.45 o 2 3 3 574.93 618.49 7.63 o 3 3 3 237.96 230.77 3.65 o 4 3 3 373.21 415.19 6.14 o 5 3 3 84.56 72.12 2.21 o 6 3 3 14.23 15.03 1.98 o 7 3 3 188.28 187.90 7.83 o 8 3 3 16.40 19.48 3.08 o 9 3 3 0.80 -0.10 2.39 o 0 4 3 105.81 97.55 3.64 o 1 4 3 8.17 3.54 1.06 o 2 4 3 178.29 218.34 3.96 o 3 4 3 1697.14 1718.48 18.13 o 4 4 3 624.61 633.78 13.77 o 5 4 3 46.13 48.37 2.28 o 6 4 3 231.30 222.44 6.83 o 7 4 3 59.30 67.92 4.53 o 8 4 3 1.60 3.82 2.38 o 9 4 3 16.41 17.58 3.33 o 1 5 3 771.27 812.72 14.16 o 2 5 3 506.46 524.39 8.56 o 3 5 3 4.06 2.16 1.01 o 4 5 3 99.66 86.23 2.78 o 5 5 3 378.22 354.60 7.77 o 6 5 3 14.65 11.85 2.17 o 7 5 3 0.02 -3.37 2.28 o 8 5 3 0.24 -0.10 2.69 o 9 5 3 22.64 39.14 5.24 o 0 6 3 4878.00 5300.78 125.09 o 1 6 3 99.86 93.78 3.10 o 2 6 3 32.22 32.32 2.95 o 3 6 3 66.74 67.62 2.51 o 4 6 3 6.35 5.96 1.46 o 5 6 3 17.25 13.86 2.26 o 6 6 3 166.51 142.39 5.91 o 7 6 3 0.82 0.22 2.42 o 8 6 3 4.98 6.26 2.92 o 1 7 3 712.90 734.29 13.75 o 2 7 3 53.72 45.83 4.38 o 3 7 3 56.64 52.93 3.55 o 4 7 3 11.37 15.38 2.30 o 5 7 3 154.53 140.26 6.03 o 6 7 3 11.74 11.37 2.87 o 7 7 3 99.26 106.43 5.64 o 0 8 3 15.39 10.10 3.87 o 1 8 3 7.84 5.27 2.09 o 2 8 3 965.02 1051.13 18.15 o 3 8 3 6.49 2.43 2.06 o 4 8 3 185.16 169.97 5.50 o 5 8 3 6.98 10.84 3.29 o 6 8 3 9.77 4.98 3.26 o 1 9 3 6.43 4.54 2.36 o 2 9 3 18.03 13.16 2.73 o 3 9 3 33.21 28.59 3.31 o 4 9 3 1.00 -1.97 2.17 o 5 9 3 3.04 1.80 4.18 o 0 10 3 268.42 316.05 13.88 o 1 10 3 8.74 7.49 2.99 o 2 10 3 126.89 127.46 6.06 o 0 0 4 19172.89 13949.23 433.26 o 1 0 4 325.27 312.51 6.47 o 2 0 4 14346.91 15833.50 229.50 o 3 0 4 133.29 127.78 2.78 o 4 0 4 876.91 886.07 14.56 o 5 0 4 363.03 371.30 8.95 o 6 0 4 837.24 851.86 17.84 o 7 0 4 249.18 232.39 22.77 o 8 0 4 456.16 447.93 23.04 o 9 0 4 0.25 -2.00 2.93 o 10 0 4 387.68 398.57 27.90 o 1 1 4 705.69 660.39 8.84 o 2 1 4 929.73 890.74 12.33 o 3 1 4 932.35 908.47 10.13 o 4 1 4 127.73 122.57 2.23 o 5 1 4 1029.67 1091.59 15.30 o 6 1 4 128.96 123.77 3.41 o 7 1 4 190.16 200.76 6.27 o 8 1 4 3.76 4.38 2.34 o 9 1 4 0.35 -2.91 2.11 o 10 1 4 36.17 37.64 4.39 o 0 2 4 13395.22 12837.22 809.39 o 1 2 4 1182.33 1190.57 14.24 o 2 2 4 187.00 190.06 3.17 o 3 2 4 866.11 902.97 9.89 o 4 2 4 16.33 21.08 2.40 o 5 2 4 124.49 131.35 2.87 o 6 2 4 134.67 125.06 3.39 o 7 2 4 2.44 2.50 2.01 o 8 2 4 179.60 163.05 6.03 o 9 2 4 1.81 -0.18 2.32 o 10 2 4 123.59 132.25 6.19 o 1 3 4 593.34 609.89 7.98 o 2 3 4 58.89 62.93 1.66 o 3 3 4 25.67 15.06 1.54 o 4 3 4 279.07 250.51 4.03 o 5 3 4 63.91 63.88 2.15 o 6 3 4 401.33 391.99 8.09 o 7 3 4 141.75 140.96 5.32 o 8 3 4 66.15 62.11 4.55 o 9 3 4 23.74 17.20 3.37 o 0 4 4 1183.44 1207.17 35.36 o 1 4 4 7.22 3.14 0.87 o 2 4 4 92.87 114.52 3.83 o 3 4 4 796.20 805.94 15.00 o 4 4 4 321.04 342.26 6.27 o 5 4 4 254.83 251.94 6.24 o 6 4 4 11.92 18.25 2.29 o 7 4 4 6.89 3.76 2.14 o 8 4 4 141.94 133.95 5.64 o 9 4 4 14.84 15.19 4.05 o 1 5 4 47.45 47.58 3.53 o 2 5 4 1544.65 1588.39 25.52 o 3 5 4 95.55 98.95 2.78 o 4 5 4 23.46 17.41 1.66 o 5 5 4 0.07 -1.85 1.24 o 6 5 4 86.37 67.21 4.15 o 7 5 4 0.07 -3.10 2.07 o 8 5 4 23.03 24.49 3.64 o 0 6 4 418.01 420.50 11.14 o 1 6 4 114.05 118.60 4.01 o 2 6 4 21.81 20.68 1.95 o 3 6 4 45.54 46.08 2.95 o 4 6 4 2.98 1.27 1.36 o 5 6 4 44.53 57.36 4.85 o 6 6 4 119.70 101.64 4.74 o 7 6 4 0.91 -1.20 2.32 o 8 6 4 14.40 11.60 3.27 o 1 7 4 16.66 12.37 2.17 o 2 7 4 124.43 116.61 4.32 o 3 7 4 1.79 -1.74 1.66 o 4 7 4 1242.82 1254.64 78.56 o 5 7 4 1.65 -1.67 1.81 o 6 7 4 1.38 1.64 2.96 o 7 7 4 0.56 1.78 3.40 o 0 8 4 3.17 3.63 3.18 o 1 8 4 2.50 -2.14 1.70 o 2 8 4 19.65 18.65 2.78 o 3 8 4 18.23 14.85 2.66 o 4 8 4 0.43 -2.35 1.97 o 5 8 4 9.01 14.71 3.12 o 6 8 4 18.08 13.63 3.81 o 1 9 4 40.07 35.13 3.99 o 2 9 4 270.25 260.91 8.37 o 3 9 4 1.83 0.88 2.15 o 4 9 4 1.41 -3.38 3.38 o 0 10 4 110.17 111.19 8.79 o 1 10 4 67.24 65.95 5.46 o 2 10 4 6.57 3.22 2.58 o 1 1 5 580.69 563.11 7.80 o 2 1 5 1597.10 1537.97 18.77 o 3 1 5 121.89 118.77 2.08 o 4 1 5 805.33 855.22 9.15 o 5 1 5 233.08 235.97 4.73 o 6 1 5 0.70 0.33 1.11 o 7 1 5 0.03 -1.66 1.74 o 8 1 5 187.37 181.65 6.98 o 9 1 5 9.92 10.01 2.86 o 10 1 5 12.91 15.47 4.10 o 0 2 5 1681.75 1614.51 29.30 o 1 2 5 1217.59 1218.44 14.64 o 2 2 5 17.91 19.28 1.04 o 3 2 5 1581.66 1674.20 31.24 o 4 2 5 15.71 21.14 1.18 o 5 2 5 395.88 350.45 5.89 o 6 2 5 39.53 47.27 2.75 o 7 2 5 0.20 -2.25 1.75 o 8 2 5 202.04 194.83 6.72 o 9 2 5 12.42 7.24 2.92 o 1 3 5 242.76 249.80 5.36 o 2 3 5 74.36 82.56 7.95 o 3 3 5 247.89 207.76 3.48 o 4 3 5 96.79 84.31 1.97 o 5 3 5 0.15 -0.11 0.88 o 6 3 5 613.08 651.75 9.83 o 7 3 5 265.14 267.55 7.71 o 8 3 5 70.37 63.54 5.37 o 9 3 5 0.92 -1.52 2.67 o 0 4 5 860.94 918.68 19.80 o 1 4 5 52.98 45.47 2.59 o 2 4 5 249.24 222.53 4.08 o 3 4 5 55.46 45.45 1.76 o 4 4 5 1.31 0.29 0.92 o 5 4 5 489.26 491.67 8.40 o 6 4 5 186.50 160.68 4.22 o 7 4 5 3.28 1.65 2.26 o 8 4 5 7.03 1.23 2.68 o 9 4 5 74.92 85.59 6.01 o 1 5 5 12.75 7.80 1.70 o 2 5 5 300.62 295.62 5.68 o 3 5 5 144.28 156.79 3.86 o 4 5 5 0.89 0.08 1.12 o 5 5 5 47.59 52.80 2.89 o 6 5 5 79.90 73.73 3.70 o 7 5 5 43.10 44.37 4.30 o 8 5 5 59.50 65.13 7.19 o 0 6 5 16.07 8.91 2.47 o 1 6 5 0.80 -0.92 1.38 o 2 6 5 312.25 358.55 11.00 o 3 6 5 88.59 90.24 3.55 o 4 6 5 208.62 185.45 7.13 o 5 6 5 1.50 0.49 1.58 o 6 6 5 134.67 116.46 5.06 o 7 6 5 8.78 6.23 2.79 o 8 6 5 4.69 2.91 2.75 o 1 7 5 55.21 59.16 6.79 o 2 7 5 7.90 5.94 2.01 o 3 7 5 235.77 244.69 10.67 o 4 7 5 5.08 4.82 2.10 o 5 7 5 8.54 2.82 2.23 o 6 7 5 1.59 -1.16 2.71 o 7 7 5 0.01 -2.63 3.08 o 0 8 5 137.28 141.39 8.04 o 1 8 5 7.16 3.56 2.14 o 2 8 5 248.39 238.29 7.11 o 3 8 5 4.19 0.28 2.24 o 4 8 5 1.63 -2.16 2.06 o 5 8 5 6.76 5.46 2.70 o 6 8 5 6.12 8.55 4.05 o 1 9 5 241.53 255.95 7.42 o 2 9 5 40.84 35.20 3.64 o 3 9 5 14.24 20.30 15.05 o 4 9 5 0.72 -2.63 2.35 o 0 10 5 190.79 195.02 10.73 o 1 10 5 31.33 40.91 6.07 o 0 0 6 905.64 998.95 31.97 o 1 0 6 25.98 26.79 1.78 o 2 0 6 203.02 237.10 9.05 o 3 0 6 490.62 485.20 10.08 o 4 0 6 2.51 8.08 1.13 o 5 0 6 5.47 2.55 1.39 o 6 0 6 427.20 408.50 8.98 o 7 0 6 1.41 2.53 2.35 o 8 0 6 43.38 57.90 7.32 o 9 0 6 17.00 17.33 4.97 o 1 1 6 736.68 678.75 9.68 o 2 1 6 43.49 44.81 1.40 o 3 1 6 105.99 94.41 2.12 o 4 1 6 15.49 16.59 1.29 o 5 1 6 146.36 128.77 2.94 o 6 1 6 10.22 6.56 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13 89.91 82.66 3.44 o 3 2 13 354.31 368.16 7.88 o 4 2 13 6.56 5.15 2.66 o 5 2 13 10.71 11.86 3.51 o 6 2 13 0.55 0.39 2.36 o 7 2 13 12.63 9.03 2.96 o 1 3 13 109.22 103.46 3.91 o 2 3 13 102.66 77.01 3.54 o 3 3 13 4.70 1.27 1.78 o 4 3 13 157.03 149.07 6.55 o 5 3 13 29.03 28.89 4.06 o 6 3 13 130.98 132.86 6.57 o 7 3 13 26.80 33.34 4.00 o 0 4 13 63.24 49.56 5.50 o 1 4 13 5.15 2.08 1.85 o 2 4 13 113.22 104.35 4.09 o 3 4 13 85.29 82.79 3.92 o 4 4 13 182.76 197.82 7.87 o 5 4 13 80.37 92.22 6.70 o 6 4 13 0.81 -1.81 2.82 o 1 5 13 243.50 225.22 6.95 o 2 5 13 51.69 50.11 3.99 o 3 5 13 123.75 127.76 6.16 o 4 5 13 61.68 79.02 6.24 o 5 5 13 0.82 3.00 3.27 o 0 6 13 9.56 11.22 3.91 o 1 6 13 0.01 -1.35 1.92 o 2 6 13 103.04 108.31 5.50 o 3 6 13 2.75 0.73 2.09 o 4 6 13 0.06 -1.16 2.76 o 1 7 13 354.95 350.07 9.68 o 2 7 13 2.16 -1.80 2.17 o 3 7 13 154.40 158.69 5.78 o 0 0 14 1757.57 1696.79 57.04 o 1 0 14 18.35 19.92 4.00 o 2 0 14 416.58 404.69 13.79 o 3 0 14 1.94 1.58 2.57 o 4 0 14 23.55 25.26 6.43 o 5 0 14 34.16 32.61 9.12 o 6 0 14 235.13 249.89 10.74 o 7 0 14 11.12 13.42 4.58 o 1 1 14 1256.54 1237.84 31.02 o 2 1 14 35.53 35.85 5.50 o 3 1 14 80.50 75.92 4.04 o 4 1 14 211.98 215.62 7.83 o 5 1 14 202.00 203.65 12.10 o 6 1 14 15.82 13.73 4.90 o 7 1 14 91.67 99.09 5.73 o 0 2 14 159.08 143.32 7.32 o 1 2 14 0.56 -0.38 1.85 o 2 2 14 179.79 159.74 4.92 o 3 2 14 19.54 15.38 2.42 o 4 2 14 458.58 484.96 13.25 o 5 2 14 5.75 2.97 2.93 o 6 2 14 0.07 -2.16 2.40 o 1 3 14 237.71 237.63 6.92 o 2 3 14 7.44 5.76 2.07 o 3 3 14 13.81 12.19 2.41 o 4 3 14 7.36 6.18 3.16 o 5 3 14 3.58 0.13 2.66 o 6 3 14 62.68 85.39 6.59 o 0 4 14 5.34 3.92 3.07 o 1 4 14 142.12 132.59 5.19 o 2 4 14 173.05 171.13 5.42 o 3 4 14 156.74 145.20 4.98 o 4 4 14 36.70 27.31 4.67 o 5 4 14 82.54 96.80 7.71 o 1 5 14 30.56 23.90 3.29 o 2 5 14 13.73 15.83 2.68 o 3 5 14 77.76 92.44 4.58 o 4 5 14 20.66 18.82 5.73 o 5 5 14 4.06 -2.28 3.00 o 0 6 14 49.60 54.18 6.68 o 1 6 14 0.02 -2.77 2.21 o 2 6 14 6.72 4.24 2.41 o 3 6 14 149.26 145.37 5.43 o 1 7 14 5.23 5.07 2.74 o 1 1 15 7.03 6.77 2.29 o 2 1 15 82.66 83.54 4.07 o 3 1 15 53.57 64.17 4.28 o 4 1 15 90.50 92.51 6.46 o 5 1 15 0.01 1.94 3.30 o 6 1 15 7.52 4.57 3.08 o 0 2 15 87.93 91.91 6.06 o 1 2 15 3.71 0.21 2.04 o 2 2 15 157.40 166.61 5.19 o 3 2 15 321.73 305.08 7.40 o 4 2 15 4.21 5.27 3.09 o 5 2 15 124.37 118.81 6.30 o 6 2 15 41.56 54.85 7.58 o 1 3 15 313.14 319.66 8.56 o 2 3 15 1.16 0.13 1.88 o 3 3 15 4.00 1.82 2.44 o 4 3 15 27.17 29.80 4.45 o 5 3 15 3.55 0.92 3.12 o 0 4 15 178.65 178.31 8.84 o 1 4 15 358.95 380.48 11.86 o 2 4 15 0.15 -0.60 1.89 o 3 4 15 208.83 206.35 6.92 o 4 4 15 2.10 -2.81 2.88 o 5 4 15 57.10 79.08 6.60 o 1 5 15 2.94 0.85 2.37 o 2 5 15 131.56 135.48 5.15 o 3 5 15 145.37 163.70 5.64 o 4 5 15 41.46 45.30 5.75 o 0 6 15 178.64 189.75 9.78 o 1 6 15 24.30 28.72 3.78 o 2 6 15 0.03 -0.17 2.24 o 0 0 16 37.59 24.88 6.47 o 1 0 16 11.79 6.51 3.24 o 2 0 16 217.38 182.64 11.69 o 3 0 16 9.71 1.94 3.24 o 4 0 16 117.01 123.72 10.59 o 5 0 16 24.38 40.39 8.29 o 1 1 16 227.46 203.55 6.53 o 2 1 16 15.27 14.18 2.80 o 3 1 16 186.46 187.74 6.24 o 4 1 16 37.79 31.89 5.38 o 5 1 16 10.75 5.84 3.88 o 0 2 16 68.31 60.44 6.32 o 1 2 16 37.63 36.68 3.77 o 2 2 16 2.03 0.26 2.62 o 3 2 16 43.47 41.19 7.38 o 4 2 16 13.04 9.01 4.01 o 5 2 16 14.97 18.90 4.65 o 1 3 16 182.40 189.45 8.73 o 2 3 16 164.13 181.16 5.76 o 3 3 16 15.30 16.68 2.67 o 4 3 16 25.76 40.86 4.86 o 0 4 16 104.20 92.26 6.59 o 1 4 16 246.66 273.51 8.19 o 2 4 16 0.45 1.11 2.40 o 3 4 16 108.89 117.20 5.45 o 4 4 16 1.33 -3.93 2.80 o 1 5 16 11.26 11.63 3.00 o 2 5 16 1.80 2.45 2.53 o 1 1 17 28.14 28.54 3.38 o 2 1 17 98.48 108.91 4.94 o 3 1 17 0.05 -0.76 2.18 o 4 1 17 12.21 13.16 4.41 o 0 2 17 13.84 12.10 5.64 o 1 2 17 3.47 3.67 2.44 o 2 2 17 2.08 -0.02 2.21 o 3 2 17 7.42 1.54 2.95 o 4 2 17 10.24 17.12 4.85 o 1 3 17 50.82 60.73 5.36 o 2 3 17 9.46 6.43 2.74 o 3 3 17 3.11 -0.41 2.51 o 0 4 17 72.06 90.72 9.15 o 1 4 17 2.30 -1.04 2.36 o 2 4 17 6.35 5.31 2.76 o 0 0 18 198.02 200.37 13.63 o 1 0 18 17.65 20.88 4.56 o 2 0 18 6.60 5.84 3.72 o 3 0 18 78.25 92.74 11.83 o 1 1 18 72.67 87.75 5.50 o 2 1 18 22.56 18.12 3.20 o 3 1 18 24.24 53.84 6.84 o 0 2 18 7.48 4.13 3.75 o 1 2 18 2.25 1.14 2.41 o 2 2 18 0.08 0.64 2.41 o 1 3 18 2.38 3.09 2.58 o