#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:34:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181071 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/51/2215111.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215111_Fobs loop_ _publ_author_name 'Feng, Yong-Lan' 'Xu, Jin-Sheng' 'Kuang, Dai-Zhi' 'Peng, Yun-Lin' _publ_section_title ; A two-dimensional holmium(III) coordination polymer: poly[aminotris(\m-4-aminobenzoato)holmium(III)] ; _journal_coeditor_code GW2020 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2338 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.020 _cell_angle_gamma 90.000 _cell_length_a 9.7720 _cell_length_b 22.7610 _cell_length_c 9.8321 _exptl_crystal_F_000 1160.00 _reflns_d_resolution_high 0.8255 _cod_data_source_file gw2020Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' b in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 394.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8107.17 7899.79 68.53 o 4 0 0 7335.68 6604.53 87.33 o 6 0 0 19760.78 19659.30 191.40 o 8 0 0 6075.55 5809.41 129.16 o 10 0 0 653.86 722.18 72.63 o 1 1 0 93108.14 96618.53 1922.40 o 2 1 0 3066.84 3124.68 46.84 o 3 1 0 10612.79 10082.79 95.19 o 4 1 0 625.42 651.02 36.79 o 5 1 0 37819.71 38387.43 243.83 o 6 1 0 1.67 35.49 38.86 o 7 1 0 10879.80 10518.68 155.64 o 8 1 0 146.63 182.98 53.42 o 9 1 0 4153.58 4097.56 118.23 o 10 1 0 17.31 9.40 50.75 o 11 1 0 387.19 414.32 67.99 o 0 2 0 93319.65 104540.91 1056.27 o 1 2 0 1299.43 1404.22 24.56 o 2 2 0 77990.31 79481.39 249.16 o 3 2 0 3249.07 3350.60 57.75 o 4 2 0 22233.42 21279.60 161.01 o 5 2 0 3.98 -6.39 36.91 o 6 2 0 12158.08 11600.08 149.46 o 7 2 0 208.35 223.83 50.59 o 8 2 0 5103.42 4835.04 122.56 o 9 2 0 37.03 39.04 47.02 o 10 2 0 682.35 738.90 72.45 o 11 2 0 0.03 -23.07 58.56 o 1 3 0 27032.60 27391.61 113.18 o 2 3 0 4713.17 5001.25 61.20 o 3 3 0 17468.37 17623.30 130.00 o 4 3 0 81.17 93.00 28.57 o 5 3 0 29333.80 29639.10 217.38 o 6 3 0 2599.32 2686.55 80.21 o 7 3 0 10685.78 10559.82 159.53 o 8 3 0 147.29 107.55 50.05 o 9 3 0 2299.73 2195.51 97.33 o 10 3 0 117.69 89.62 57.32 o 11 3 0 371.00 364.78 65.68 o 0 4 0 89903.27 94378.30 1892.99 o 1 4 0 2495.44 2545.66 38.29 o 2 4 0 27766.64 27990.07 148.12 o 3 4 0 2654.19 2760.64 56.88 o 4 4 0 13534.50 13320.72 130.38 o 5 4 0 102.37 116.60 37.09 o 6 4 0 11901.50 11739.38 153.48 o 7 4 0 357.34 317.44 52.02 o 8 4 0 4381.76 4376.17 116.36 o 9 4 0 13.31 -13.49 50.22 o 10 4 0 401.67 438.65 66.22 o 11 4 0 195.32 186.53 64.60 o 1 5 0 21819.01 21595.37 114.72 o 2 5 0 101.08 142.36 23.79 o 3 5 0 25465.69 24884.57 164.18 o 4 5 0 386.67 423.58 36.76 o 5 5 0 19868.29 20270.33 183.59 o 6 5 0 641.09 657.24 53.11 o 7 5 0 5461.39 5439.84 119.65 o 8 5 0 1.56 7.98 48.80 o 9 5 0 3228.13 3148.09 112.39 o 10 5 0 20.43 48.09 50.39 o 11 5 0 610.30 653.39 73.51 o 0 6 0 19955.90 19854.36 107.71 o 1 6 0 596.76 630.28 28.28 o 2 6 0 15570.99 15241.78 117.05 o 3 6 0 0.16 37.97 25.20 o 4 6 0 30339.69 30353.53 208.03 o 5 6 0 0.14 4.44 35.31 o 6 6 0 12173.57 12101.67 158.49 o 7 6 0 4.10 -28.92 47.02 o 8 6 0 2555.07 2621.80 94.89 o 9 6 0 182.72 148.02 53.95 o 10 6 0 1285.56 1330.36 88.31 o 11 6 0 183.26 134.53 67.62 o 1 7 0 29799.13 29162.64 152.05 o 2 7 0 873.44 871.85 35.58 o 3 7 0 23908.25 22663.46 165.50 o 4 7 0 344.44 349.11 37.82 o 5 7 0 22249.46 22469.07 201.25 o 6 7 0 2102.18 2086.56 77.98 o 7 7 0 12592.43 12519.84 178.40 o 8 7 0 72.10 64.60 50.93 o 9 7 0 1244.71 1314.62 82.99 o 10 7 0 201.36 135.77 58.21 o 11 7 0 374.25 340.28 64.97 o 0 8 0 21953.28 21871.91 130.79 o 1 8 0 4029.98 4139.34 61.22 o 2 8 0 33987.00 33597.91 190.43 o 3 8 0 790.14 927.76 43.73 o 4 8 0 33679.89 33475.12 229.48 o 5 8 0 413.77 501.46 47.77 o 6 8 0 8602.38 8418.99 137.54 o 7 8 0 136.77 126.72 52.89 o 8 8 0 4711.75 4889.97 129.58 o 9 8 0 0.47 -21.83 53.77 o 10 8 0 1341.76 1271.76 86.18 o 11 8 0 304.31 285.24 70.82 o 1 9 0 44909.29 43532.74 209.42 o 2 9 0 258.42 317.82 30.72 o 3 9 0 46306.99 47282.68 258.90 o 4 9 0 28.56 11.36 31.59 o 5 9 0 14271.10 14170.28 165.31 o 6 9 0 1388.93 1408.81 69.88 o 7 9 0 5470.31 5349.09 126.55 o 8 9 0 307.87 329.99 59.47 o 9 9 0 4271.74 4414.27 133.19 o 10 9 0 40.80 27.86 56.07 o 11 9 0 390.74 427.27 70.47 o 0 10 0 43386.50 41973.35 208.59 o 1 10 0 5662.42 6201.32 81.83 o 2 10 0 47194.95 45849.63 243.87 o 3 10 0 3940.88 4205.86 81.02 o 4 10 0 20689.46 20445.68 189.30 o 5 10 0 142.32 123.00 42.24 o 6 10 0 6514.76 6674.14 130.94 o 7 10 0 119.89 105.06 52.18 o 8 10 0 4390.32 4271.14 123.08 o 9 10 0 25.85 67.08 55.72 o 10 10 0 1404.12 1607.30 94.00 o 1 11 0 43250.91 41195.33 223.57 o 2 11 0 1180.84 1263.81 49.98 o 3 11 0 17510.55 17025.99 162.36 o 4 11 0 645.69 685.51 48.50 o 5 11 0 15730.87 15834.78 184.28 o 6 11 0 3916.02 3878.17 104.73 o 7 11 0 10009.07 10061.39 173.43 o 8 11 0 4.29 -14.20 48.80 o 9 11 0 1142.56 1395.20 83.68 o 10 11 0 85.00 104.70 59.80 o 0 12 0 44361.49 43471.29 234.89 o 1 12 0 119.80 195.23 43.66 o 2 12 0 21890.22 21428.03 176.46 o 3 12 0 25.69 4.08 33.54 o 4 12 0 14851.66 14843.23 172.08 o 5 12 0 64.03 124.40 41.17 o 6 12 0 11430.12 11369.16 172.63 o 7 12 0 84.92 21.83 53.06 o 8 12 0 1540.45 1605.70 89.41 o 9 12 0 0.72 -2.84 50.75 o 10 12 0 359.07 432.05 67.99 o 1 13 0 23245.01 22143.65 177.46 o 2 13 0 169.71 201.28 32.30 o 3 13 0 14262.52 14062.62 158.59 o 4 13 0 0.15 22.00 39.04 o 5 13 0 11708.32 11782.74 169.04 o 6 13 0 151.76 192.56 50.76 o 7 13 0 4175.11 4066.50 120.38 o 8 13 0 73.47 130.61 53.06 o 9 13 0 839.85 883.56 78.50 o 10 13 0 14.70 16.68 58.91 o 0 14 0 28520.82 27974.85 204.12 o 1 14 0 299.81 241.98 49.36 o 2 14 0 17224.85 16366.69 167.76 o 3 14 0 59.99 88.37 35.31 o 4 14 0 12530.10 12645.82 168.44 o 5 14 0 126.83 137.36 51.11 o 6 14 0 4416.14 4477.05 119.74 o 7 14 0 25.63 7.28 48.98 o 8 14 0 2841.67 2786.63 110.90 o 9 14 0 36.32 54.65 53.77 o 10 14 0 494.78 476.84 75.09 o 1 15 0 17627.23 16442.56 165.92 o 2 15 0 44.66 24.84 40.46 o 3 15 0 9910.10 9702.32 142.99 o 4 15 0 49.04 74.35 43.83 o 5 15 0 8228.43 8258.70 148.89 o 6 15 0 1.93 31.05 50.39 o 7 15 0 3964.54 3965.90 124.07 o 8 15 0 1.41 -51.28 51.28 o 9 15 0 2019.37 2153.80 106.51 o 0 16 0 14474.80 13813.30 155.85 o 1 16 0 108.00 17.39 47.92 o 2 16 0 11799.41 11428.76 150.24 o 3 16 0 133.42 154.40 44.37 o 4 16 0 13190.64 13034.36 182.60 o 5 16 0 367.50 332.33 54.32 o 6 16 0 8172.99 8032.32 162.70 o 7 16 0 14.91 17.21 52.52 o 8 16 0 2396.80 2477.37 109.23 o 9 16 0 6.68 -11.53 65.30 o 1 17 0 12497.68 12096.47 153.21 o 2 17 0 107.07 -1.77 52.71 o 3 17 0 16470.54 15541.19 191.59 o 4 17 0 504.98 505.69 61.79 o 5 17 0 5852.31 5835.64 135.48 o 6 17 0 2.24 35.31 50.22 o 7 17 0 4035.55 3967.44 126.90 o 8 17 0 131.39 141.80 58.92 o 9 17 0 1451.31 1405.40 94.53 o 0 18 0 10570.33 10369.24 148.91 o 1 18 0 356.59 338.55 53.61 o 2 18 0 16382.86 15994.23 194.07 o 3 18 0 18.49 17.39 62.28 o 4 18 0 7419.52 7734.10 149.19 o 5 18 0 1534.74 1537.70 84.26 o 6 18 0 7822.11 7797.85 168.09 o 7 18 0 1.91 -8.16 55.18 o 8 18 0 2739.94 2673.34 118.68 o 1 19 0 18200.07 17593.65 201.32 o 2 19 0 472.45 325.99 70.13 o 3 19 0 9498.18 9032.32 156.40 o 4 19 0 1.08 34.96 50.04 o 5 19 0 5049.93 4905.69 134.22 o 6 19 0 126.84 38.33 58.92 o 7 19 0 3980.38 4005.91 138.09 o 8 19 0 2.39 6.74 59.09 o 0 20 0 4376.76 4228.36 104.56 o 1 20 0 1441.98 1658.93 77.68 o 2 20 0 13324.31 13287.97 188.13 o 3 20 0 1.09 42.76 66.19 o 4 20 0 8488.23 8373.80 165.76 o 5 20 0 1289.00 1226.66 80.68 o 6 20 0 4493.48 4663.54 139.61 o 7 20 0 140.93 142.33 61.76 o 8 20 0 2225.02 2377.22 120.21 o 1 21 0 8455.86 8244.15 150.40 o 2 21 0 437.17 366.61 67.11 o 3 21 0 14481.12 14049.45 205.14 o 4 21 0 49.39 -7.28 63.71 o 5 21 0 3154.62 3137.98 118.58 o 6 21 0 22.92 63.70 56.78 o 7 21 0 2577.49 2553.58 115.46 o 0 22 0 7957.35 7881.20 149.55 o 1 22 0 9.98 143.73 50.22 o 2 22 0 7639.42 7729.46 152.87 o 3 22 0 45.36 -29.81 68.85 o 4 22 0 5307.93 5655.95 143.13 o 5 22 0 973.46 913.53 83.31 o 6 22 0 2535.68 2639.15 112.08 o 7 22 0 46.82 53.59 65.66 o 1 23 0 10227.41 10061.77 176.97 o 2 23 0 17.51 -20.23 57.67 o 3 23 0 5724.96 5839.22 146.77 o 4 23 0 3.80 -45.60 61.40 o 5 23 0 2976.02 3006.70 122.99 o 6 23 0 98.73 75.07 65.84 o 0 24 0 5787.23 5637.74 141.24 o 1 24 0 0.03 73.82 53.59 o 2 24 0 7763.19 7883.90 166.57 o 3 24 0 10.46 -60.69 60.69 o 4 24 0 2833.00 2873.17 116.21 o 5 24 0 300.66 284.17 71.00 o 1 25 0 7386.15 7387.15 161.11 o 2 25 0 48.48 32.83 63.35 o 3 25 0 4335.53 4324.02 134.92 o 4 25 0 7.62 18.28 59.44 o 0 26 0 6437.80 6318.82 156.82 o 1 26 0 29.45 122.62 61.40 o 2 26 0 6306.15 6490.85 161.25 o 3 26 0 40.14 10.47 67.96 o 1 27 0 5438.70 5737.05 159.66 o 2 27 0 145.35 274.54 67.97 o -11 0 1 5820.11 6131.00 171.19 o -9 0 1 10093.28 9797.90 181.24 o -7 0 1 17025.60 16982.62 196.24 o -5 0 1 3773.92 3855.33 78.16 o -3 0 1 882.90 865.00 34.71 o -1 0 1 6484.73 6717.43 45.68 o 1 0 1 65.14 53.08 12.43 o 3 0 1 743.68 686.52 32.19 o 5 0 1 26961.68 27987.69 208.96 o 7 0 1 5751.82 5732.06 119.18 o 9 0 1 4568.95 4475.93 128.45 o 11 0 1 5188.57 5499.46 165.70 o -11 1 1 14.07 17.92 70.62 o -10 1 1 8517.20 8446.81 183.24 o -9 1 1 0.01 -17.03 57.49 o -8 1 1 8081.97 7809.19 150.15 o -7 1 1 1029.91 1027.25 68.60 o -6 1 1 15862.31 15910.76 173.27 o -5 1 1 2144.47 2314.00 63.81 o -4 1 1 4368.15 4175.17 72.50 o -3 1 1 2535.94 2686.11 52.08 o -2 1 1 457.88 675.25 26.50 o -1 1 1 2259.76 2219.35 27.97 o 0 1 1 0.57 54.83 6.34 o 1 1 1 103.54 114.35 13.85 o 2 1 1 524.73 483.37 27.92 o 3 1 1 309.60 341.90 27.53 o 4 1 1 13642.35 13824.72 129.71 o 5 1 1 277.69 298.27 38.35 o 6 1 1 11862.77 11662.32 150.38 o 7 1 1 11.83 14.37 44.54 o 8 1 1 4360.86 4205.27 113.68 o 9 1 1 0.11 9.58 51.28 o 10 1 1 6570.75 6619.60 167.09 o 11 1 1 79.23 85.89 70.98 o -11 2 1 5989.58 5730.98 168.18 o -10 2 1 59.14 94.58 69.21 o -9 2 1 8179.72 8108.06 163.08 o -8 2 1 1.13 21.12 49.15 o -7 2 1 14828.37 14453.45 182.16 o -6 2 1 823.28 927.07 54.73 o -5 2 1 11723.86 11606.17 133.22 o -4 2 1 225.17 206.31 29.65 o -3 2 1 112.02 163.13 24.67 o -2 2 1 2268.68 2458.61 42.49 o -1 2 1 5631.95 5681.00 45.27 o 0 2 1 129.52 199.89 8.53 o 1 2 1 1027.44 1164.82 26.24 o 2 2 1 29.47 66.02 23.78 o 3 2 1 5816.24 5973.91 76.01 o 4 2 1 2829.76 3061.49 65.38 o 5 2 1 13553.22 13540.49 147.15 o 6 2 1 1414.44 1628.16 64.03 o 7 2 1 5649.73 5439.48 116.47 o 8 2 1 127.47 121.39 53.06 o 9 2 1 5261.41 5358.79 138.19 o 10 2 1 406.39 386.11 75.27 o 11 2 1 6568.72 6258.00 174.50 o -11 3 1 46.79 14.20 75.95 o -10 3 1 6359.19 6583.75 161.36 o -9 3 1 123.32 122.10 57.15 o -8 3 1 8016.46 7834.02 149.94 o -7 3 1 1986.56 1897.24 80.09 o -6 3 1 12723.92 12633.17 154.87 o -5 3 1 310.31 369.32 36.75 o -4 3 1 2371.34 2319.02 57.65 o -3 3 1 8481.34 9028.68 91.09 o -2 3 1 26379.21 28006.26 136.65 o -1 3 1 3697.21 3736.71 40.22 o 0 3 1 4900.52 5231.80 52.68 o 1 3 1 7875.75 8122.39 67.73 o 2 3 1 37.53 80.22 23.96 o 3 3 1 1261.93 1350.14 41.67 o 4 3 1 7703.13 7695.96 100.96 o 5 3 1 93.11 115.54 33.90 o 6 3 1 8484.42 8234.46 130.99 o 7 3 1 306.81 261.49 50.06 o 8 3 1 5716.09 5543.02 130.13 o 9 3 1 3.36 38.33 51.99 o 10 3 1 7324.72 7347.71 175.09 o 11 3 1 0.75 2.13 75.06 o -11 4 1 7700.40 7667.77 191.71 o -10 4 1 2.04 18.10 62.81 o -9 4 1 7108.53 6976.92 157.13 o -8 4 1 161.90 146.78 56.26 o -7 4 1 15509.25 15201.95 189.52 o -6 4 1 1310.92 1207.37 59.40 o -5 4 1 4098.77 4051.04 82.83 o -4 4 1 1331.99 1322.47 47.35 o -3 4 1 24411.79 25176.72 155.48 o -2 4 1 947.06 1155.10 34.73 o -1 4 1 241.51 275.89 20.25 o 0 4 1 6513.73 6740.49 50.81 o 1 4 1 246.83 338.94 26.29 o 2 4 1 2196.30 2258.83 47.57 o 3 4 1 205.62 169.56 26.63 o 4 4 1 3050.15 3352.30 71.29 o 5 4 1 8889.44 9022.82 125.03 o 6 4 1 8.31 41.17 36.73 o 7 4 1 6908.54 6817.62 132.25 o 8 4 1 1136.25 1218.33 74.99 o 9 4 1 7978.41 8136.29 167.81 o 10 4 1 43.42 126.70 62.64 o 11 4 1 4873.09 5020.17 158.69 o -11 5 1 2.86 21.65 74.35 o -10 5 1 8183.33 7999.79 185.48 o -9 5 1 1.85 50.39 55.54 o -8 5 1 4802.37 4828.95 120.17 o -7 5 1 136.46 118.73 50.23 o -6 5 1 3689.12 3652.45 90.70 o -5 5 1 480.72 459.83 41.03 o -4 5 1 20270.53 20729.41 163.36 o -3 5 1 2903.14 3233.03 58.86 o -2 5 1 29262.63 29928.98 152.69 o -1 5 1 3697.26 3898.93 49.36 o 0 5 1 212.58 283.84 23.53 o 1 5 1 1792.44 1801.11 41.28 o 2 5 1 58.21 82.88 24.67 o 3 5 1 50.00 31.94 25.02 o 4 5 1 5162.47 5202.38 87.92 o 5 5 1 1221.51 1452.10 57.80 o 6 5 1 4510.86 4468.49 100.26 o 7 5 1 128.90 124.94 51.82 o 8 5 1 7741.79 7437.31 150.52 o 9 5 1 75.90 79.15 60.87 o 10 5 1 6155.19 6367.49 165.21 o 11 5 1 35.06 51.28 70.98 o -11 6 1 5769.33 5506.69 169.73 o -10 6 1 14.63 82.69 67.96 o -9 6 1 8785.49 8853.08 173.90 o -8 6 1 724.97 715.59 68.74 o -7 6 1 6272.21 6171.66 126.77 o -6 6 1 3568.44 3585.19 88.88 o -5 6 1 10583.54 11077.08 137.36 o -4 6 1 712.02 791.23 43.72 o -3 6 1 21866.44 22280.07 153.52 o -2 6 1 3423.08 3880.69 58.29 o -1 6 1 2280.27 2407.41 42.94 o 0 6 1 4517.54 4603.83 43.67 o 1 6 1 883.86 938.54 35.06 o 2 6 1 827.97 846.53 35.75 o 3 6 1 153.18 128.34 27.34 o 4 6 1 159.03 204.30 34.44 o 5 6 1 4956.80 4825.18 97.39 o 6 6 1 30.61 20.58 39.04 o 7 6 1 6793.34 6434.03 134.34 o 8 6 1 39.67 59.80 50.40 o 9 6 1 6683.95 6812.15 158.42 o 10 6 1 25.65 93.16 62.46 o 11 6 1 6674.01 6580.51 181.47 o -11 7 1 5.86 -18.45 75.59 o -10 7 1 5499.76 5585.77 159.22 o -9 7 1 491.13 584.66 76.34 o -8 7 1 6330.51 6646.49 141.49 o -7 7 1 260.67 222.42 55.38 o -6 7 1 2532.78 2404.67 78.57 o -5 7 1 269.90 311.39 41.01 o -4 7 1 17387.32 17625.41 157.94 o -3 7 1 1501.85 1620.90 47.91 o -2 7 1 15007.07 15036.02 116.32 o -1 7 1 7377.52 7715.10 76.27 o 0 7 1 962.53 1211.98 86.42 o 1 7 1 1224.95 1318.79 40.25 o 2 7 1 6.72 37.62 22.89 o 3 7 1 139.06 151.94 30.89 o 4 7 1 1139.42 1077.23 50.33 o 5 7 1 83.12 61.94 38.33 o 6 7 1 7317.62 7168.42 129.55 o 7 7 1 374.86 384.01 53.97 o 8 7 1 7598.21 7246.65 151.89 o 9 7 1 16.64 38.15 58.56 o 10 7 1 3508.98 3521.50 127.70 o 11 7 1 38.29 9.05 75.42 o -11 8 1 6139.59 6172.49 175.85 o -10 8 1 0.21 -12.60 60.69 o -9 8 1 6166.63 6238.90 152.61 o -8 8 1 388.26 494.42 64.98 o -7 8 1 8899.49 9064.22 153.59 o -6 8 1 350.98 309.63 47.76 o -5 8 1 6734.30 6696.68 112.21 o -4 8 1 30.25 47.03 28.92 o -3 8 1 6894.83 6884.21 91.21 o -2 8 1 645.11 746.34 33.06 o -1 8 1 2044.06 2214.95 46.40 o 0 8 1 2075.87 2146.89 31.81 o 1 8 1 2751.60 3155.17 59.54 o 2 8 1 1879.96 2214.06 54.91 o 3 8 1 1143.38 1483.78 52.83 o 4 8 1 27.89 64.42 31.05 o 5 8 1 7772.91 7931.14 128.53 o 6 8 1 15.39 7.45 42.23 o 7 8 1 9849.91 10039.45 167.56 o 8 8 1 240.99 265.89 60.70 o 9 8 1 4762.43 4671.50 138.61 o 10 8 1 119.67 60.16 62.82 o -11 9 1 8.49 22.18 75.24 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