#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:34:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181071 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/51/2215191.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215191_Fobs loop_ _publ_author_name 'Jiang, Gang-Biao' 'Zhang, Shu-Hua' 'Zeng, Ming-Hua' _publ_section_title ; Aqua{6,6'-dimethoxy-2,2'-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato-\k^4^O,N,N',O'}cobalt(II) ; _journal_coeditor_code KP2129 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2383 _journal_volume 63 _journal_year 2007 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.9827 _cell_length_b 24.8632 _cell_length_c 7.5784 _exptl_crystal_F_000 836.00 _reflns_d_resolution_high 0.8108 _cod_data_source_file kp2129Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' co1 in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 307.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4372.01 4383.50 47.12 o 4 0 0 366.20 395.10 19.15 o 6 0 0 6497.03 6975.64 104.20 o 8 0 0 14065.28 14424.37 396.25 o 10 0 0 334.91 356.22 33.32 o 2 1 0 543.04 657.81 20.44 o 4 1 0 48.08 23.87 3.73 o 6 1 0 1379.99 1256.06 33.42 o 8 1 0 708.39 673.14 27.40 o 10 1 0 121.27 123.56 20.58 o 2 2 0 4154.31 4114.60 48.10 o 4 2 0 2557.86 2956.63 27.97 o 6 2 0 4036.83 4091.94 54.82 o 8 2 0 1481.41 1624.69 26.86 o 10 2 0 512.02 557.76 27.48 o 2 3 0 10.48 3.70 1.65 o 4 3 0 13.52 25.56 4.61 o 6 3 0 1418.16 1479.47 22.71 o 8 3 0 1028.85 1128.02 21.42 o 10 3 0 149.89 194.96 31.89 o 0 4 0 326.13 343.82 8.26 o 2 4 0 86.42 137.73 8.98 o 4 4 0 1420.65 1863.57 23.69 o 6 4 0 260.56 241.04 9.98 o 8 4 0 139.24 151.45 19.78 o 10 4 0 282.29 351.63 33.99 o 2 5 0 4314.20 4393.25 62.87 o 4 5 0 21261.29 23538.65 221.54 o 6 5 0 1575.69 1488.58 24.28 o 8 5 0 255.89 238.37 11.31 o 10 5 0 678.09 724.70 45.10 o 0 6 0 14707.60 15016.36 279.04 o 2 6 0 9957.85 10092.06 148.92 o 4 6 0 222.29 218.58 13.35 o 6 6 0 963.95 950.00 17.38 o 8 6 0 1521.92 1447.70 25.46 o 10 6 0 868.91 934.60 50.56 o 2 7 0 2860.48 2810.50 75.17 o 4 7 0 19779.33 22597.50 213.24 o 6 7 0 9.78 7.93 5.10 o 8 7 0 56.28 44.50 10.55 o 10 7 0 984.64 1126.89 55.54 o 0 8 0 15429.30 15476.96 289.96 o 2 8 0 14759.69 14907.04 162.39 o 4 8 0 57.11 53.70 6.28 o 6 8 0 681.12 661.51 14.38 o 8 8 0 2516.33 2387.32 51.79 o 10 8 0 1329.06 1313.14 60.52 o 2 9 0 689.55 668.18 16.87 o 4 9 0 298.99 214.33 10.53 o 6 9 0 5.54 4.09 5.58 o 8 9 0 63.06 37.10 12.07 o 10 9 0 726.00 749.02 46.25 o 0 10 0 9603.15 10361.06 200.61 o 2 10 0 9359.52 9980.92 111.94 o 4 10 0 649.74 769.74 26.67 o 6 10 0 48.05 65.50 13.36 o 8 10 0 2563.28 2577.02 55.11 o 10 10 0 1117.81 1204.16 57.65 o 2 11 0 1056.43 987.85 19.05 o 4 11 0 4477.83 4484.45 118.60 o 6 11 0 176.41 167.43 10.12 o 8 11 0 33.53 56.00 14.01 o 10 11 0 518.64 469.41 38.78 o 0 12 0 1234.33 1579.92 43.86 o 2 12 0 5571.90 5552.23 66.66 o 4 12 0 52.48 47.80 8.15 o 6 12 0 228.19 237.08 11.49 o 8 12 0 215.65 296.18 19.29 o 2 13 0 4359.40 4137.52 52.19 o 4 13 0 5264.99 5141.45 66.18 o 6 13 0 1511.52 1488.01 37.35 o 8 13 0 18.82 23.33 13.06 o 0 14 0 3999.80 4066.09 92.50 o 2 14 0 852.03 803.30 15.80 o 4 14 0 109.57 103.87 29.49 o 6 14 0 110.26 99.87 24.22 o 8 14 0 753.07 800.94 29.04 o 2 15 0 1821.11 1754.83 27.07 o 4 15 0 6970.78 7011.90 95.00 o 6 15 0 1248.25 1173.39 25.02 o 8 15 0 226.14 186.82 36.91 o 0 16 0 11272.87 12553.26 248.40 o 2 16 0 3954.18 3928.90 66.25 o 4 16 0 5.08 7.86 11.36 o 6 16 0 1063.98 1001.46 23.23 o 8 16 0 1516.32 1477.44 41.42 o 2 17 0 1433.43 1339.83 32.11 o 4 17 0 140.42 113.14 13.55 o 6 17 0 1595.98 981.43 37.92 o 8 17 0 52.37 75.17 25.76 o 0 18 0 7094.34 7473.08 159.92 o 2 18 0 1595.43 1661.60 37.66 o 4 18 0 897.30 875.31 27.05 o 8 18 0 1204.05 1294.37 57.84 o 2 19 0 573.16 545.60 33.23 o 4 19 0 999.50 1010.95 29.72 o 8 19 0 31.12 39.84 26.53 o 0 20 0 6498.93 6814.27 150.92 o 2 20 0 895.15 940.89 53.05 o 4 20 0 24.56 11.76 13.60 o 6 20 0 328.05 280.86 28.82 o 8 20 0 1166.60 1254.34 60.14 o 2 21 0 360.24 356.27 18.11 o 4 21 0 3169.23 3178.14 62.80 o 6 21 0 420.26 267.17 26.91 o 8 21 0 91.18 165.76 34.47 o 0 22 0 2506.85 2367.53 70.86 o 2 22 0 1741.79 1824.04 43.20 o 4 22 0 83.10 93.04 17.00 o 6 22 0 615.38 583.37 25.90 o 2 23 0 1118.30 1190.37 34.67 o 4 23 0 862.63 871.61 30.30 o 6 23 0 408.14 378.44 34.66 o 0 24 0 26.89 30.45 16.09 o 2 24 0 1981.15 1946.68 46.44 o 4 24 0 18.08 8.34 14.38 o 6 24 0 325.56 342.53 35.05 o 2 25 0 23.06 59.00 14.64 o 4 25 0 905.03 952.53 33.08 o 6 25 0 10.34 12.26 27.77 o 0 26 0 736.25 788.76 41.37 o 2 26 0 1555.78 1560.19 50.08 o 4 26 0 12.49 -10.47 17.00 o 2 27 0 395.47 512.39 25.93 o 4 27 0 347.88 343.93 34.71 o 0 28 0 1319.28 1330.66 56.98 o 2 28 0 467.48 476.90 35.10 o 4 28 0 22.02 23.85 17.89 o 2 29 0 216.35 212.84 26.67 o 0 30 0 353.51 377.29 34.76 o 2 30 0 291.55 305.78 58.51 o 1 0 1 16980.31 17476.12 283.83 o 2 0 1 702.46 676.66 10.53 o 3 0 1 33.08 69.71 7.72 o 4 0 1 9.09 10.83 3.79 o 5 0 1 37.26 35.53 11.53 o 6 0 1 50.37 25.64 4.60 o 7 0 1 10115.83 10738.83 249.63 o 8 0 1 363.64 367.94 18.59 o 9 0 1 88.89 85.52 14.55 o 10 0 1 39.11 -1.63 21.83 o 11 0 1 209.04 215.17 33.80 o 0 1 1 2095.68 2168.16 30.47 o 1 1 1 10278.68 11570.93 120.88 o 2 1 1 2124.17 2269.65 19.70 o 3 1 1 1045.07 927.05 10.45 o 4 1 1 297.58 246.20 4.90 o 5 1 1 3825.26 3752.40 30.48 o 6 1 1 33.62 9.77 2.90 o 7 1 1 3718.63 3980.77 44.65 o 8 1 1 189.91 201.75 11.04 o 9 1 1 120.65 109.63 12.33 o 10 1 1 123.20 78.56 23.46 o 11 1 1 77.72 78.65 20.82 o 1 2 1 12976.56 13883.87 116.20 o 2 2 1 3164.81 3230.01 27.00 o 3 2 1 248.77 222.65 4.51 o 4 2 1 8.24 13.84 2.63 o 5 2 1 82.79 82.47 8.83 o 6 2 1 705.22 728.06 10.25 o 7 2 1 3610.22 3725.99 36.46 o 8 2 1 249.02 248.47 11.59 o 9 2 1 444.01 452.85 15.22 o 10 2 1 128.92 100.57 15.39 o 0 3 1 2004.80 2082.14 64.25 o 1 3 1 6157.55 6731.82 52.72 o 2 3 1 2702.86 2878.47 34.11 o 3 3 1 3229.33 3064.87 29.70 o 4 3 1 158.58 112.86 3.83 o 5 3 1 2701.57 2466.24 20.96 o 6 3 1 107.46 81.21 5.46 o 7 3 1 3.65 13.25 14.03 o 8 3 1 243.07 254.76 11.12 o 9 3 1 32.71 26.79 9.23 o 10 3 1 160.46 141.70 15.56 o 1 4 1 11004.65 11852.59 80.01 o 2 4 1 205.09 184.38 4.32 o 3 4 1 72.28 50.61 4.70 o 4 4 1 470.73 468.28 6.59 o 5 4 1 71.46 39.94 4.77 o 6 4 1 378.91 440.33 8.61 o 7 4 1 1137.10 1183.52 19.32 o 8 4 1 0.76 -1.84 6.95 o 9 4 1 995.69 1022.05 26.63 o 10 4 1 78.67 50.53 12.79 o 0 5 1 5.30 5.80 2.44 o 1 5 1 1074.32 1103.45 17.21 o 2 5 1 3610.40 3889.27 32.54 o 3 5 1 9746.58 10056.55 71.51 o 4 5 1 0.04 -0.78 2.19 o 5 5 1 1384.39 1215.28 14.10 o 6 5 1 203.42 196.63 6.22 o 7 5 1 388.14 412.03 11.34 o 8 5 1 95.42 92.67 13.80 o 9 5 1 108.96 71.80 16.77 o 10 5 1 222.03 241.89 18.38 o 1 6 1 649.05 635.06 6.93 o 2 6 1 87.43 70.26 3.02 o 3 6 1 7795.34 8787.73 65.97 o 4 6 1 24.81 10.96 3.53 o 5 6 1 1607.07 1614.75 17.20 o 6 6 1 15.04 18.41 3.98 o 7 6 1 459.70 454.34 11.89 o 8 6 1 6.71 7.83 7.09 o 9 6 1 953.73 1010.68 26.69 o 10 6 1 50.37 17.44 17.11 o 0 7 1 8844.06 9137.05 87.73 o 1 7 1 329.62 357.32 5.33 o 2 7 1 4623.76 5065.17 39.68 o 3 7 1 14694.26 16018.38 123.70 o 4 7 1 0.21 0.54 2.85 o 5 7 1 3849.12 3999.93 34.36 o 6 7 1 274.63 256.41 6.93 o 7 7 1 692.47 667.10 14.21 o 8 7 1 534.20 505.42 13.58 o 9 7 1 0.36 1.93 8.95 o 10 7 1 189.93 199.88 20.24 o 1 8 1 192.83 141.21 4.78 o 2 8 1 11.50 3.43 2.17 o 3 8 1 231.70 185.42 5.56 o 4 8 1 39.90 6.98 3.08 o 5 8 1 116.79 69.72 5.70 o 6 8 1 56.63 35.99 4.85 o 7 8 1 334.03 355.60 10.93 o 8 8 1 29.12 25.62 7.74 o 9 8 1 1121.90 1134.89 29.70 o 10 8 1 99.92 88.41 20.93 o 0 9 1 1320.19 1276.71 30.71 o 1 9 1 3447.06 3535.13 33.44 o 2 9 1 4534.47 5040.13 43.54 o 3 9 1 10952.39 11754.86 114.43 o 4 9 1 33.27 18.99 3.42 o 5 9 1 4380.33 4556.52 41.52 o 6 9 1 218.50 197.08 6.91 o 7 9 1 884.51 827.92 16.26 o 8 9 1 181.38 180.49 16.84 o 9 9 1 196.74 215.37 17.07 o 10 9 1 288.55 338.20 21.03 o 1 10 1 3377.37 3255.59 42.27 o 2 10 1 26.84 22.90 2.87 o 3 10 1 350.74 297.21 6.59 o 4 10 1 2.15 4.32 3.42 o 5 10 1 537.22 485.18 9.55 o 6 10 1 1.97 1.07 4.57 o 7 10 1 832.04 807.36 16.13 o 8 10 1 39.61 20.41 7.67 o 9 10 1 1236.23 1186.73 30.32 o 10 10 1 71.33 86.23 16.70 o 0 11 1 529.20 452.55 10.20 o 1 11 1 88.51 40.33 2.81 o 2 11 1 746.10 769.62 13.93 o 3 11 1 6198.30 6536.87 54.83 o 4 11 1 98.71 79.39 9.41 o 5 11 1 2613.51 2529.35 26.60 o 6 11 1 31.79 20.78 5.05 o 7 11 1 13.49 16.77 6.61 o 8 11 1 82.60 77.59 11.86 o 9 11 1 22.47 27.91 12.62 o 10 11 1 101.01 92.59 20.97 o 1 12 1 2150.16 2010.56 22.65 o 2 12 1 434.91 437.97 9.02 o 3 12 1 892.17 871.03 11.99 o 4 12 1 549.72 504.58 9.46 o 5 12 1 202.29 158.56 9.53 o 6 12 1 216.77 207.56 8.87 o 7 12 1 168.50 222.05 10.14 o 8 12 1 0.85 -9.91 7.63 o 9 12 1 1199.60 1234.62 31.71 o 10 12 1 127.13 100.32 21.61 o 0 13 1 2902.95 3152.11 41.08 o 1 13 1 29.64 7.64 4.28 o 2 13 1 988.42 1007.39 13.68 o 3 13 1 781.02 751.20 11.26 o 4 13 1 0.11 0.55 3.78 o 5 13 1 1077.08 1022.46 16.37 o 6 13 1 372.13 365.90 10.96 o 7 13 1 37.82 51.07 11.27 o 8 13 1 250.56 229.57 18.25 o 9 13 1 6.91 -0.18 15.91 o 1 14 1 1298.95 1235.57 14.48 o 2 14 1 136.27 132.69 6.96 o 3 14 1 1341.41 1246.74 15.80 o 4 14 1 731.37 667.92 11.43 o 5 14 1 113.75 105.71 10.68 o 6 14 1 21.59 32.19 6.55 o 7 14 1 375.82 436.95 12.89 o 8 14 1 18.50 14.15 9.36 o 9 14 1 458.82 497.65 26.51 o 0 15 1 2232.71 2216.82 31.62 o 1 15 1 3623.87 3877.36 45.89 o 2 15 1 299.64 273.88 7.87 o 3 15 1 2466.71 2342.57 43.16 o 4 15 1 110.29 94.77 9.97 o 5 15 1 2869.41 2951.42 38.68 o 6 15 1 123.11 114.61 9.84 o 7 15 1 733.93 643.97 21.20 o 8 15 1 222.31 226.00 13.86 o 9 15 1 103.96 67.99 18.97 o 1 16 1 2809.97 3080.40 58.87 o 2 16 1 2.45 -3.75 4.88 o 3 16 1 563.08 520.04 12.77 o 4 16 1 364.64 358.74 10.08 o 5 16 1 897.56 932.77 17.01 o 6 16 1 1.28 -2.16 7.81 o 7 16 1 1529.09 1558.75 32.68 o 8 16 1 14.75 -3.46 10.28 o 9 16 1 191.37 213.02 76.27 o 0 17 1 2084.71 2087.10 42.11 o 1 17 1 1565.98 1603.21 30.42 o 2 17 1 222.48 188.42 9.16 o 3 17 1 1512.53 1477.96 28.70 o 4 17 1 414.12 380.75 12.24 o 5 17 1 4908.87 4963.46 58.79 o 6 17 1 21.38 22.66 18.88 o 7 17 1 265.13 273.12 23.99 o 8 17 1 202.73 189.26 21.83 o 9 17 1 19.83 21.83 26.43 o 1 18 1 2659.20 2779.06 37.22 o 2 18 1 106.45 117.45 10.53 o 3 18 1 1499.16 1368.38 44.38 o 4 18 1 75.69 57.09 7.92 o 5 18 1 253.29 241.50 11.50 o 6 18 1 13.59 19.67 9.89 o 7 18 1 1300.53 1281.34 30.49 o 8 18 1 59.34 44.78 18.60 o 0 19 1 1464.65 1353.49 33.28 o 1 19 1 1157.77 1234.20 22.37 o 2 19 1 346.27 295.60 11.24 o 3 19 1 136.62 140.13 10.49 o 4 19 1 113.21 93.97 9.52 o 5 19 1 876.08 894.57 20.24 o 6 19 1 115.93 119.53 13.61 o 7 19 1 368.99 360.61 17.98 o 8 19 1 192.92 219.58 24.24 o 1 20 1 1383.11 1499.78 25.72 o 2 20 1 514.53 513.26 14.82 o 3 20 1 517.40 496.55 14.62 o 4 20 1 616.02 641.84 20.28 o 5 20 1 208.06 229.94 12.89 o 6 20 1 148.91 144.47 20.69 o 7 20 1 975.94 968.55 27.66 o 8 20 1 48.12 80.84 21.52 o 0 21 1 377.73 321.62 17.60 o 1 21 1 522.87 541.92 15.47 o 2 21 1 1.37 -1.23 7.19 o 3 21 1 215.22 241.74 11.84 o 4 21 1 27.67 13.12 8.33 o 5 21 1 220.50 244.65 16.23 o 6 21 1 2.41 -3.15 11.52 o 7 21 1 316.77 345.30 19.25 o 1 22 1 2309.13 2258.04 34.67 o 2 22 1 36.59 17.38 8.61 o 3 22 1 961.42 941.09 21.29 o 4 22 1 258.14 243.70 18.04 o 5 22 1 411.78 372.47 18.07 o 6 22 1 7.71 -5.78 15.11 o 7 22 1 919.43 959.66 28.92 o 0 23 1 46.43 57.41 12.86 o 1 23 1 9.76 57.15 17.93 o 2 23 1 166.28 168.16 12.35 o 3 23 1 1576.39 1669.68 30.12 o 4 23 1 5.19 -3.62 9.10 o 5 23 1 897.08 906.03 26.82 o 6 23 1 3.51 -12.37 13.22 o 7 23 1 22.94 -19.26 14.34 o 1 24 1 635.36 626.10 18.01 o 2 24 1 0.50 -1.32 8.51 o 3 24 1 161.28 179.70 27.33 o 4 24 1 97.93 74.74 11.20 o 5 24 1 247.28 253.95 19.35 o 6 24 1 7.14 -4.70 14.18 o 0 25 1 596.80 587.92 25.11 o 1 25 1 25.13 19.39 9.36 o 2 25 1 399.83 374.81 17.10 o 3 25 1 1948.46 2013.57 34.78 o 4 25 1 17.93 14.36 10.14 o 5 25 1 755.57 757.99 25.85 o 6 25 1 42.95 50.68 16.09 o 1 26 1 51.97 53.48 10.36 o 2 26 1 2.39 -1.48 10.00 o 3 26 1 186.92 187.51 14.38 o 4 26 1 18.03 14.45 11.80 o 5 26 1 209.63 221.87 19.83 o 0 27 1 290.57 286.01 21.92 o 1 27 1 162.47 167.27 13.85 o 2 27 1 327.56 316.50 15.14 o 3 27 1 773.01 756.27 21.75 o 4 27 1 2.02 -2.98 11.56 o 5 27 1 287.24 263.03 21.83 o 1 28 1 288.47 307.15 15.66 o 2 28 1 2.08 10.03 11.41 o 3 28 1 17.15 12.20 13.77 o 4 28 1 173.13 179.97 19.43 o 0 29 1 184.61 228.56 22.84 o 1 29 1 24.65 36.47 11.89 o 2 29 1 59.85 37.88 12.34 o 3 29 1 325.75 339.32 17.08 o 1 30 1 445.74 468.36 19.10 o 0 0 2 94616.31 95757.67 1747.59 o 1 0 2 5564.75 5805.27 77.98 o 2 0 2 407.17 338.20 10.39 o 3 0 2 1573.23 1320.90 19.11 o 4 0 2 14.59 23.08 4.25 o 5 0 2 6932.30 6929.43 117.64 o 6 0 2 1335.15 1327.79 32.46 o 7 0 2 1515.51 1432.97 34.86 o 8 0 2 3473.83 3797.30 202.86 o 9 0 2 9.56 -12.72 20.21 o 10 0 2 23.73 15.16 14.67 o 1 1 2 7131.37 7975.07 62.37 o 2 1 2 2224.23 2291.91 22.81 o 3 1 2 231.01 286.16 5.99 o 4 1 2 740.41 615.08 8.59 o 5 1 2 348.07 383.28 15.46 o 6 1 2 3030.64 3011.15 34.72 o 7 1 2 4.33 -4.11 6.15 o 8 1 2 50.68 57.86 11.54 o 9 1 2 3.13 -2.88 8.73 o 10 1 2 4.05 1.64 10.18 o 0 2 2 1904.88 2098.65 31.25 o 1 2 2 18215.67 18862.66 143.52 o 2 2 2 965.07 1133.58 13.40 o 3 2 2 4485.97 4356.25 41.12 o 4 2 2 223.57 226.69 6.64 o 5 2 2 6535.76 6702.85 56.20 o 6 2 2 2453.55 2433.29 25.17 o 7 2 2 645.86 598.95 12.63 o 8 2 2 296.98 340.62 13.53 o 9 2 2 364.07 339.83 14.48 o 10 2 2 132.47 125.22 13.55 o 1 3 2 18198.24 19340.48 173.38 o 2 3 2 3150.30 3296.23 31.65 o 3 3 2 314.13 261.58 7.21 o 4 3 2 273.16 140.33 5.60 o 5 3 2 682.78 780.22 10.12 o 6 3 2 2026.65 2149.05 23.15 o 7 3 2 2565.81 2484.35 54.62 o 8 3 2 592.03 610.64 16.59 o 9 3 2 1075.96 1233.32 25.61 o 10 3 2 99.10 64.61 12.33 o 0 4 2 1319.42 1401.06 34.52 o 1 4 2 495.38 468.76 8.65 o 2 4 2 192.09 248.29 5.04 o 3 4 2 2826.74 2776.22 28.46 o 4 4 2 11.21 5.26 2.40 o 5 4 2 1954.11 1785.84 19.38 o 6 4 2 714.05 693.52 11.77 o 7 4 2 36.45 33.17 5.74 o 8 4 2 33.29 28.10 8.64 o 9 4 2 125.65 95.17 15.05 o 10 4 2 241.63 299.14 16.00 o 1 5 2 5188.04 5676.67 45.99 o 2 5 2 1125.93 1087.09 11.83 o 3 5 2 2284.22 2438.12 22.88 o 4 5 2 7815.65 8009.01 59.15 o 5 5 2 1337.03 1354.69 24.02 o 6 5 2 916.21 942.91 13.98 o 7 5 2 603.07 564.22 12.69 o 8 5 2 297.60 276.47 11.83 o 9 5 2 1331.40 1375.48 27.19 o 10 5 2 88.85 98.89 19.10 o 0 6 2 226.90 196.90 18.25 o 1 6 2 7.49 12.24 2.12 o 2 6 2 1362.84 1398.50 13.29 o 3 6 2 5.96 30.39 3.79 o 4 6 2 332.88 374.60 7.68 o 5 6 2 128.04 89.52 10.26 o 6 6 2 254.30 247.78 8.64 o 7 6 2 365.73 342.53 12.31 o 8 6 2 397.96 412.15 16.40 o 9 6 2 39.16 27.29 9.51 o 10 6 2 486.84 586.28 19.25 o 1 7 2 66.22 50.62 4.37 o 2 7 2 3033.61 3327.84 24.45 o 3 7 2 726.49 764.80 8.30 o 4 7 2 8523.07 9235.34 67.86 o 5 7 2 355.59 347.56 8.01 o 6 7 2 361.54 371.52 10.20 o 7 7 2 121.17 104.44 9.40 o 8 7 2 0.87 -7.47 7.97 o 9 7 2 447.25 493.54 16.55 o 10 7 2 217.86 259.65 25.58 o 0 8 2 1138.48 1059.95 14.06 o 1 8 2 109.69 80.90 3.10 o 2 8 2 3059.20 3225.05 25.43 o 3 8 2 5834.01 5789.22 44.27 o 4 8 2 19.66 3.91 2.97 o 5 8 2 2623.53 2591.40 26.58 o 6 8 2 430.20 387.18 10.55 o 7 8 2 1422.29 1239.76 23.35 o 8 8 2 816.93 797.56 25.90 o 9 8 2 33.99 35.52 10.83 o 10 8 2 377.62 394.15 16.74 o 1 9 2 6.01 5.74 1.96 o 2 9 2 3303.38 3656.27 28.59 o 3 9 2 456.92 508.08 7.83 o 4 9 2 1503.75 1379.98 14.91 o 5 9 2 2001.38 2087.94 23.01 o 6 9 2 725.93 745.06 14.57 o 7 9 2 88.22 97.14 10.53 o 8 9 2 0.80 7.62 8.76 o 9 9 2 248.87 290.99 15.32 o 10 9 2 261.83 305.35 16.15 o 0 10 2 631.30 547.74 9.42 o 1 10 2 24.42 43.86 2.81 o 2 10 2 894.58 805.07 9.92 o 3 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50.13 o 7 2 3 363.49 353.20 10.57 o 8 2 3 156.30 137.19 22.02 o 9 2 3 113.73 126.09 12.18 o 10 2 3 194.26 207.02 29.87 o 0 3 3 4258.85 4516.54 90.49 o 1 3 3 903.96 964.19 11.95 o 2 3 3 1069.38 992.87 17.60 o 3 3 3 40.56 31.68 3.60 o 4 3 3 16.31 12.63 7.08 o 5 3 3 504.23 534.17 12.86 o 6 3 3 688.39 712.09 16.18 o 7 3 3 63.42 61.44 8.09 o 8 3 3 1409.24 1456.34 27.22 o 9 3 3 9.92 18.68 9.71 o 10 3 3 265.00 282.11 19.24 o 1 4 3 757.48 785.74 14.29 o 2 4 3 3308.48 3426.23 34.23 o 3 4 3 512.38 503.58 9.39 o 4 4 3 6410.77 6536.65 63.91 o 5 4 3 57.32 54.19 6.61 o 6 4 3 2647.74 2558.19 35.28 o 7 4 3 31.28 15.73 5.97 o 8 4 3 208.83 229.57 13.12 o 9 4 3 242.22 289.73 14.55 o 10 4 3 143.90 126.82 23.79 o 0 5 3 10.56 7.63 3.38 o 1 5 3 0.52 -3.34 2.23 o 2 5 3 2947.73 2932.32 26.92 o 3 5 3 337.34 327.51 7.85 o 4 5 3 151.64 174.52 12.11 o 5 5 3 10.10 12.30 4.58 o 6 5 3 1012.19 965.82 20.92 o 7 5 3 5.96 -0.78 5.57 o 8 5 3 635.12 655.68 17.87 o 9 5 3 32.32 32.12 9.76 o 10 5 3 348.51 342.85 16.89 o 1 6 3 756.52 721.03 10.58 o 2 6 3 755.58 655.47 9.37 o 3 6 3 3191.64 3470.72 35.64 o 4 6 3 3306.67 3080.29 33.28 o 5 6 3 509.91 514.02 11.86 o 6 6 3 636.16 576.12 12.71 o 7 6 3 38.02 19.79 6.91 o 8 6 3 181.03 190.03 21.85 o 9 6 3 243.20 298.28 14.30 o 10 6 3 55.30 48.29 19.60 o 0 7 3 9207.31 9596.95 136.05 o 1 7 3 105.76 122.90 5.36 o 2 7 3 3304.61 3402.01 31.02 o 3 7 3 767.07 853.72 11.18 o 4 7 3 391.92 354.91 7.36 o 5 7 3 38.95 38.71 5.45 o 6 7 3 629.68 597.14 13.07 o 7 7 3 2.02 -0.77 6.28 o 8 7 3 1579.55 1613.15 24.80 o 9 7 3 148.26 149.26 19.40 o 10 7 3 290.30 321.34 16.55 o 1 8 3 2770.69 3041.55 28.19 o 2 8 3 185.62 139.68 5.07 o 3 8 3 592.82 589.81 7.70 o 4 8 3 3496.42 3353.59 32.10 o 5 8 3 9.35 6.65 4.29 o 6 8 3 100.15 90.65 7.45 o 7 8 3 367.84 333.65 10.89 o 8 8 3 84.49 71.48 10.36 o 9 8 3 462.90 528.65 17.76 o 10 8 3 148.72 165.28 15.30 o 0 9 3 1807.84 1806.45 20.24 o 1 9 3 608.65 698.00 8.50 o 2 9 3 6283.19 6436.09 45.06 o 3 9 3 274.30 286.07 5.55 o 4 9 3 52.39 63.53 5.25 o 5 9 3 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