#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/52/2215248.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215248_Fobs loop_ _publ_author_name 'Begum, Noor Shahina' 'Vasundhara, D. E.' 'Hegde, V. S.' 'Khazi, I. M.' _publ_section_title ; 7-(4-Methylphenyl)-5-(methylsulfanyl)-2-phenyl-1,3-benzothiazole-4-carbonitrile ; _journal_coeditor_code PV2025 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3902 _journal_volume 63 _journal_year 2007 _chemical_formula_sum 'C22 H16 N2 S2' _chemical_formula_weight 372.49 _space_group_IT_number 14 _symmetry_cell_setting monoclinic _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _cell_angle_alpha 90.000 _cell_angle_beta 94.869 _cell_angle_gamma 90.000 _cell_formula_units_Z 4 _cell_length_a 11.4142 _cell_length_b 7.9101 _cell_length_c 20.5530 _cell_measurement_reflns_used 15 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 8.02 _cell_measurement_theta_min 6.9 _cell_volume 1849.0(3) _computing_cell_refinement 'SAINTPLUS (Bruker, 1998)' _computing_data_collection 'SMART (Bruker, 1998)' _computing_data_reduction SAINTPLUS _computing_molecular_graphics 'ORTEP-3 for Windows (Farrugia, 1997)' _computing_publication_material SHELXL-97 _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1997)' _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker SMART CCD area detector' _diffrn_measurement_method '\f and \w' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0258 _diffrn_reflns_av_sigmaI/netI 0.0259 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 12852 _diffrn_reflns_reduction_process ; ; _diffrn_reflns_theta_full 25.00 _diffrn_reflns_theta_max 25.00 _diffrn_reflns_theta_min 1.79 _exptl_absorpt_coefficient_mu 0.296 _exptl_absorpt_correction_type none _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.338 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description rectangular _exptl_crystal_F_000 776 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.257 _refine_diff_density_min -0.192 _refine_diff_density_rms 0.043 _refine_ls_extinction_coef ? _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.154 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 237 _refine_ls_number_reflns 3260 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.154 _refine_ls_R_factor_all 0.0698 _refine_ls_R_factor_gt 0.0563 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0511P)^2^+0.8652P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1229 _refine_ls_wR_factor_ref 0.1289 _reflns_d_resolution_high 0.8008 _reflns_number_gt 2730 _reflns_number_total 3260 _reflns_threshold_expression >2sigma(I) _[local]_cod_data_source_file pv2025Isup2.hkl _[local]_cod_data_source_block I _[local]_cod_cif_authors_sg_H-M 'P 1 2~1~/c 1' #BEGIN Tags that were not found in dictionaries: _shelx_title ' v1nsb_m in space group P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 114.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_group _atom_site_disorder_assembly C1 C 0.9027(2) 0.7127(4) -0.02928(14) 0.0446(7) Uani 1 d . . . C2 C 0.8276(3) 0.6166(4) 0.05881(15) 0.0467(7) Uani 1 d . . . C3 C 1.0029(3) 0.7342(4) 0.01428(14) 0.0452(7) Uani 1 d . . . C4 C 0.9041(3) 0.7583(4) -0.09522(15) 0.0483(7) Uani 1 d . . . C5 C 1.0078(3) 0.8232(4) -0.11692(15) 0.0531(8) Uani 1 d . . . C6 C 1.1065(3) 0.8403(4) -0.07267(16) 0.0520(8) Uani 1 d . . . H6 H 1.175(3) 0.877(4) -0.0863(17) 0.058(10) Uiso 1 d . . . C7 C 1.1080(3) 0.8004(4) -0.00666(15) 0.0455(7) Uani 1 d . . . C8 C 1.2178(3) 0.8258(4) 0.03667(15) 0.0466(7) Uani 1 d . . . C9 C 1.2497(3) 0.7210(5) 0.08930(17) 0.0526(8) Uani 1 d . . . H9 H 1.205(3) 0.630(4) 0.0988(15) 0.055(9) Uiso 1 d . . . C10 C 1.3538(3) 0.7431(5) 0.12779(19) 0.0594(9) Uani 1 d . . . H10 H 1.374(4) 0.662(5) 0.165(2) 0.082(12) Uiso 1 d . . . C11 C 1.4303(3) 0.8725(5) 0.11495(17) 0.0589(9) Uani 1 d . . . C12 C 1.5458(4) 0.8981(9) 0.1561(3) 0.0849(14) Uani 1 d . . . H12A H 1.535(4) 0.999(7) 0.185(3) 0.117(17) Uiso 1 d . . . H12B H 1.598(5) 0.901(8) 0.131(3) 0.13(2) Uiso 1 d . . . H12C H 1.561(5) 0.810(7) 0.191(3) 0.13(2) Uiso 1 d . . . C13 C 1.3986(3) 0.9782(5) 0.06248(19) 0.0616(10) Uani 1 d . . . H13 H 1.445(3) 1.068(5) 0.0526(17) 0.055(9) Uiso 1 d . . . C14 C 1.2947(3) 0.9560(4) 0.02381(18) 0.0547(8) Uani 1 d . . . H14 H 1.276(3) 1.041(5) -0.0146(16) 0.045(9) Uiso 1 d . . . C15 C 0.7422(3) 0.5403(4) 0.09969(15) 0.0481(7) Uani 1 d . . . C16 C 0.7639(3) 0.5262(5) 0.16663(18) 0.0615(9) Uani 1 d . . . H16 H 0.832(3) 0.560(4) 0.1869(17) 0.064(11) Uiso 1 d . . . C17 C 0.6819(4) 0.4536(6) 0.2037(2) 0.0732(12) Uani 1 d . . . H17 H 0.699(3) 0.449(5) 0.248(2) 0.075(13) Uiso 1 d . . . C18 C 0.5773(4) 0.3960(6) 0.1740(2) 0.0717(11) Uani 1 d . . . H18 H 0.522(3) 0.346(4) 0.1975(16) 0.065(10) Uiso 1 d . . . C19 C 0.5544(3) 0.4091(5) 0.1075(2) 0.0662(10) Uani 1 d . . . H19 H 0.479(3) 0.366(5) 0.0883(19) 0.082(12) Uiso 1 d . . . C20 C 0.6359(3) 0.4809(5) 0.07039(19) 0.0587(9) Uani 1 d . . . H20 H 0.621(3) 0.491(4) 0.0263(18) 0.059(10) Uiso 1 d . . . C21 C 0.8001(3) 0.7345(5) -0.13869(16) 0.0536(8) Uani 1 d . . . C22 C 1.1479(5) 0.9563(8) -0.2095(3) 0.0882(15) Uani 1 d . . . H22A H 1.171(5) 1.083(8) -0.183(3) 0.15(2) Uiso 1 d . . . H22B H 1.145(3) 0.976(5) -0.249(2) 0.077(13) Uiso 1 d . . . H22C H 1.204(5) 0.870(7) -0.201(3) 0.13(2) Uiso 1 d . . . N1 N 0.8054(2) 0.6455(4) -0.00331(13) 0.0476(6) Uani 1 d . . . N2 N 0.7190(3) 0.7147(5) -0.17417(16) 0.0748(10) Uani 1 d . . . S1 S 0.96953(7) 0.67111(11) 0.09166(4) 0.0508(3) Uani 1 d . . . S2 S 1.00579(9) 0.87246(18) -0.20032(5) 0.0879(4) Uani 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0435(16) 0.0431(17) 0.0476(18) 0.0010(13) 0.0067(14) 0.0030(13) C2 0.0461(17) 0.0455(18) 0.0485(18) -0.0013(14) 0.0035(14) 0.0039(14) C3 0.0469(16) 0.0458(18) 0.0431(17) 0.0016(13) 0.0044(14) 0.0071(13) C4 0.0467(18) 0.0505(19) 0.0475(17) 0.0045(15) 0.0033(14) 0.0046(14) C5 0.0530(19) 0.059(2) 0.0469(18) 0.0078(15) 0.0044(15) 0.0035(15) C6 0.0445(18) 0.057(2) 0.054(2) 0.0068(16) 0.0057(15) -0.0019(15) C7 0.0450(16) 0.0420(17) 0.0497(18) 0.0010(14) 0.0049(14) 0.0039(13) C8 0.0453(16) 0.0473(18) 0.0476(18) -0.0036(14) 0.0071(14) 0.0040(14) C9 0.0471(18) 0.054(2) 0.057(2) 0.0005(16) 0.0040(16) -0.0050(16) C10 0.054(2) 0.067(2) 0.056(2) -0.002(2) 0.0008(17) 0.0049(18) C11 0.0469(18) 0.073(2) 0.057(2) -0.0173(18) 0.0042(16) 0.0010(17) C12 0.057(3) 0.114(4) 0.082(3) -0.018(3) -0.006(2) -0.009(3) C13 0.054(2) 0.063(2) 0.069(2) -0.0110(19) 0.0139(19) -0.0132(18) C14 0.053(2) 0.051(2) 0.061(2) -0.0004(17) 0.0084(16) 0.0006(16) C15 0.0475(17) 0.0498(18) 0.0475(18) -0.0012(14) 0.0071(14) 0.0017(14) C16 0.055(2) 0.077(3) 0.052(2) 0.0034(18) 0.0001(17) -0.0065(19) C17 0.078(3) 0.091(3) 0.053(2) 0.012(2) 0.015(2) -0.008(2) C18 0.066(2) 0.080(3) 0.072(3) 0.008(2) 0.024(2) -0.009(2) C19 0.056(2) 0.074(3) 0.070(3) -0.004(2) 0.0108(19) -0.0126(19) C20 0.056(2) 0.069(2) 0.051(2) -0.0007(18) 0.0042(17) -0.0031(17) C21 0.0526(19) 0.064(2) 0.0448(19) 0.0060(16) 0.0080(16) 0.0011(16) C22 0.077(3) 0.116(5) 0.074(3) 0.033(3) 0.022(3) -0.010(3) N1 0.0458(14) 0.0511(17) 0.0459(16) 0.0006(13) 0.0037(12) 0.0019(12) N2 0.0580(19) 0.106(3) 0.058(2) 0.0010(18) -0.0041(16) -0.0108(18) S1 0.0471(5) 0.0616(5) 0.0436(5) 0.0013(4) 0.0030(3) -0.0010(4) S2 0.0671(6) 0.1441(12) 0.0514(6) 0.0296(6) -0.0009(5) -0.0234(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 C1 C3 116.1(3) . . ? N1 C1 C4 123.2(3) . . ? C3 C1 C4 120.7(3) . . ? N1 C2 C15 123.3(3) . . ? N1 C2 S1 115.6(2) . . ? C15 C2 S1 121.1(2) . . ? C1 C3 C7 121.3(3) . . ? C1 C3 S1 108.6(2) . . ? C7 C3 S1 130.1(2) . . ? C5 C4 C1 118.8(3) . . ? C5 C4 C21 121.8(3) . . ? C1 C4 C21 119.4(3) . . ? C6 C5 C4 119.2(3) . . ? C6 C5 S2 123.9(2) . . ? C4 C5 S2 116.9(2) . . ? C7 C6 C5 123.8(3) . . ? C7 C6 H6 116(2) . . ? C5 C6 H6 120(2) . . ? C6 C7 C3 116.2(3) . . ? C6 C7 C8 119.5(3) . . ? C3 C7 C8 124.2(3) . . ? C9 C8 C14 117.5(3) . . ? C9 C8 C7 122.6(3) . . ? C14 C8 C7 119.9(3) . . ? C10 C9 C8 121.8(3) . . ? C10 C9 H9 116(2) . . ? C8 C9 H9 122(2) . . ? C9 C10 C11 120.7(4) . . ? C9 C10 H10 119(2) . . ? C11 C10 H10 120(2) . . ? C10 C11 C13 117.8(3) . . ? C10 C11 C12 121.6(4) . . ? C13 C11 C12 120.6(4) . . ? C11 C12 H12A 107(3) . . ? C11 C12 H12B 108(4) . . ? H12A C12 H12B 118(5) . . ? C11 C12 H12C 113(3) . . ? H12A C12 H12C 98(4) . . ? H12B C12 H12C 112(5) . . ? C14 C13 C11 121.7(3) . . ? C14 C13 H13 117(2) . . ? C11 C13 H13 121(2) . . ? C13 C14 C8 120.6(4) . . ? C13 C14 H14 117.5(19) . . ? C8 C14 H14 121.9(19) . . ? C16 C15 C20 118.7(3) . . ? C16 C15 C2 122.0(3) . . ? C20 C15 C2 119.2(3) . . ? C17 C16 C15 120.7(4) . . ? C17 C16 H16 118(2) . . ? C15 C16 H16 121(2) . . ? C18 C17 C16 119.8(4) . . ? C18 C17 H17 122(2) . . ? C16 C17 H17 118(2) . . ? C17 C18 C19 120.2(4) . . ? C17 C18 H18 121(2) . . ? C19 C18 H18 118(2) . . ? C18 C19 C20 120.2(4) . . ? C18 C19 H19 117(2) . . ? C20 C19 H19 122(2) . . ? C19 C20 C15 120.4(3) . . ? C19 C20 H20 121(2) . . ? C15 C20 H20 119(2) . . ? N2 C21 C4 178.6(3) . . ? S2 C22 H22A 116(3) . . ? S2 C22 H22B 102(3) . . ? H22A C22 H22B 107(4) . . ? S2 C22 H22C 109(4) . . ? H22A C22 H22C 114(5) . . ? H22B C22 H22C 107(4) . . ? C2 N1 C1 110.5(3) . . ? C3 S1 C2 89.17(15) . . ? C5 S2 C22 104.5(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 N1 1.379(4) . ? C1 C3 1.402(4) . ? C1 C4 1.404(4) . ? C2 N1 1.301(4) . ? C2 C15 1.470(4) . ? C2 S1 1.755(3) . ? C3 C7 1.409(4) . ? C3 S1 1.740(3) . ? C4 C5 1.397(4) . ? C4 C21 1.436(5) . ? C5 C6 1.394(4) . ? C5 S2 1.756(3) . ? C6 C7 1.392(4) . ? C6 H6 0.90(4) . ? C7 C8 1.487(4) . ? C8 C9 1.387(4) . ? C8 C14 1.393(4) . ? C9 C10 1.382(5) . ? C9 H9 0.91(3) . ? C10 C11 1.385(5) . ? C10 H10 1.01(4) . ? C11 C13 1.388(5) . ? C11 C12 1.518(5) . ? C12 H12A 1.01(6) . ? C12 H12B 0.82(6) . ? C12 H12C 1.01(6) . ? C13 C14 1.381(5) . ? C13 H13 0.92(4) . ? C14 H14 1.05(3) . ? C15 C16 1.382(5) . ? C15 C20 1.389(5) . ? C16 C17 1.380(5) . ? C16 H16 0.89(4) . ? C17 C18 1.372(6) . ? C17 H17 0.91(4) . ? C18 C19 1.373(5) . ? C18 H18 0.92(4) . ? C19 C20 1.374(5) . ? C19 H19 0.98(4) . ? C20 H20 0.91(3) . ? C21 N2 1.140(4) . ? C22 S2 1.778(5) . ? C22 H22A 1.16(7) . ? C22 H22B 0.83(4) . ? C22 H22C 0.94(6) . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag C14 H14 N1 1.045(5) 2.685(6) 3.367(5) 123 3_775 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C1 C3 C7 179.5(3) . . . . ? C4 C1 C3 C7 -0.6(5) . . . . ? N1 C1 C3 S1 -1.6(3) . . . . ? C4 C1 C3 S1 178.3(2) . . . . ? N1 C1 C4 C5 -179.1(3) . . . . ? C3 C1 C4 C5 1.0(5) . . . . ? N1 C1 C4 C21 -0.2(5) . . . . ? C3 C1 C4 C21 179.9(3) . . . . ? C1 C4 C5 C6 0.2(5) . . . . ? C21 C4 C5 C6 -178.7(3) . . . . ? C1 C4 C5 S2 178.2(2) . . . . ? C21 C4 C5 S2 -0.7(4) . . . . ? C4 C5 C6 C7 -1.8(5) . . . . ? S2 C5 C6 C7 -179.7(3) . . . . ? C5 C6 C7 C3 2.1(5) . . . . ? C5 C6 C7 C8 -179.1(3) . . . . ? C1 C3 C7 C6 -0.8(4) . . . . ? S1 C3 C7 C6 -179.5(2) . . . . ? C1 C3 C7 C8 -179.6(3) . . . . ? S1 C3 C7 C8 1.6(5) . . . . ? C6 C7 C8 C9 -146.5(3) . . . . ? C3 C7 C8 C9 32.3(5) . . . . ? C6 C7 C8 C14 31.5(4) . . . . ? C3 C7 C8 C14 -149.7(3) . . . . ? C14 C8 C9 C10 -0.2(5) . . . . ? C7 C8 C9 C10 177.9(3) . . . . ? C8 C9 C10 C11 0.2(5) . . . . ? C9 C10 C11 C13 0.1(5) . . . . ? C9 C10 C11 C12 -179.3(4) . . . . ? C10 C11 C13 C14 -0.3(5) . . . . ? C12 C11 C13 C14 179.1(4) . . . . ? C11 C13 C14 C8 0.3(5) . . . . ? C9 C8 C14 C13 0.0(5) . . . . ? C7 C8 C14 C13 -178.1(3) . . . . ? N1 C2 C15 C16 -173.5(3) . . . . ? S1 C2 C15 C16 7.7(4) . . . . ? N1 C2 C15 C20 6.3(5) . . . . ? S1 C2 C15 C20 -172.5(3) . . . . ? C20 C15 C16 C17 0.4(6) . . . . ? C2 C15 C16 C17 -179.8(4) . . . . ? C15 C16 C17 C18 -0.6(6) . . . . ? C16 C17 C18 C19 0.6(7) . . . . ? C17 C18 C19 C20 -0.4(7) . . . . ? C18 C19 C20 C15 0.2(6) . . . . ? C16 C15 C20 C19 -0.2(5) . . . . ? C2 C15 C20 C19 -180.0(3) . . . . ? C5 C4 C21 N2 37(17) . . . . ? C1 C4 C21 N2 -142(17) . . . . ? C15 C2 N1 C1 -178.1(3) . . . . ? S1 C2 N1 C1 0.7(4) . . . . ? C3 C1 N1 C2 0.6(4) . . . . ? C4 C1 N1 C2 -179.3(3) . . . . ? C1 C3 S1 C2 1.6(2) . . . . ? C7 C3 S1 C2 -179.6(3) . . . . ? N1 C2 S1 C3 -1.4(3) . . . . ? C15 C2 S1 C3 177.5(3) . . . . ? C6 C5 S2 C22 -3.8(4) . . . . ? C4 C5 S2 C22 178.2(3) . . . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1635.14 1651.75 17.49 o 4 0 0 5404.88 5459.32 31.54 o 6 0 0 173.97 150.54 6.94 o 8 0 0 480.22 501.89 11.01 o 10 0 0 388.19 408.36 11.52 o 12 0 0 9.19 12.40 6.18 o 14 0 0 11.54 11.22 9.03 o 1 1 0 3.41 2.16 0.75 o 3 1 0 233.75 235.91 3.50 o 5 1 0 363.86 355.83 5.32 o 7 1 0 869.53 864.65 9.64 o 9 1 0 18.35 20.41 2.86 o 11 1 0 126.43 138.01 6.11 o 13 1 0 13.83 13.04 5.26 o 0 2 0 3207.76 3363.03 19.31 o 2 2 0 2271.22 2323.61 14.64 o 4 2 0 611.13 614.83 6.39 o 6 2 0 9.72 8.10 1.73 o 8 2 0 77.87 82.16 3.68 o 10 2 0 240.70 240.37 11.14 o 12 2 0 0.33 4.07 3.67 o 1 3 0 335.77 347.99 4.54 o 3 3 0 1418.18 1494.05 10.14 o 5 3 0 19.94 20.95 1.96 o 7 3 0 5.41 4.98 3.29 o 9 3 0 438.07 396.39 10.53 o 11 3 0 42.14 43.70 4.99 o 13 3 0 13.13 24.02 5.10 o 0 4 0 0.18 -0.17 2.79 o 2 4 0 2765.61 2782.98 15.76 o 4 4 0 523.75 510.22 7.73 o 6 4 0 379.05 380.24 8.37 o 8 4 0 262.81 251.98 8.46 o 10 4 0 0.00 -4.17 4.30 o 12 4 0 0.10 7.04 11.29 o 1 5 0 18.76 22.73 2.14 o 3 5 0 12.78 9.78 1.97 o 5 5 0 119.63 120.28 7.20 o 7 5 0 563.68 518.08 11.65 o 9 5 0 58.79 51.49 6.35 o 11 5 0 2.21 2.59 4.59 o 0 6 0 212.64 201.74 7.75 o 2 6 0 72.79 65.69 3.63 o 4 6 0 67.51 69.41 4.49 o 6 6 0 13.33 17.33 4.76 o 8 6 0 40.94 36.71 8.04 o 10 6 0 1.97 9.76 4.75 o 1 7 0 61.66 63.93 4.53 o 3 7 0 0.22 2.65 4.20 o 5 7 0 234.30 236.23 10.67 o 7 7 0 20.35 25.31 5.24 o 9 7 0 118.30 111.02 8.76 o 0 8 0 0.19 -5.49 5.49 o 2 8 0 2.84 2.13 9.38 o 4 8 0 42.24 50.59 6.23 o 6 8 0 3.32 -2.55 4.56 o 8 8 0 2.87 8.20 5.27 o 1 9 0 8.24 -9.14 9.50 o 3 9 0 18.95 34.05 7.30 o 5 9 0 2.45 -0.76 7.88 o -13 1 1 53.23 48.75 6.47 o -11 1 1 46.17 71.69 8.57 o -9 1 1 13.81 9.77 3.77 o -7 1 1 283.95 259.95 5.37 o -5 1 1 18.83 16.28 2.11 o -3 1 1 0.74 3.81 2.24 o -1 1 1 1437.78 1415.21 8.67 o 1 1 1 2912.34 3040.33 12.93 o 3 1 1 104.86 112.29 2.82 o 5 1 1 1540.00 1628.15 11.45 o 7 1 1 384.85 386.31 6.50 o 9 1 1 97.07 91.78 4.19 o 11 1 1 1.59 -0.74 3.19 o 13 1 1 19.17 16.94 5.44 o -12 2 1 279.91 305.64 10.25 o -10 2 1 324.91 339.93 10.02 o -8 2 1 2047.40 2051.97 16.37 o -6 2 1 4214.91 4248.83 22.07 o -4 2 1 2278.17 2158.36 12.66 o -2 2 1 12467.92 12748.02 72.30 o 0 2 1 1147.71 1202.27 7.07 o 2 2 1 2467.39 2540.34 12.02 o 4 2 1 862.72 919.68 7.79 o 6 2 1 191.92 206.02 4.50 o 8 2 1 278.48 270.30 5.98 o 10 2 1 12.97 12.83 4.00 o 12 2 1 27.20 33.99 4.60 o -13 3 1 6.40 14.84 4.93 o -11 3 1 8.65 11.75 4.10 o -9 3 1 387.12 373.76 10.37 o -7 3 1 41.82 37.27 2.95 o -5 3 1 257.55 254.57 5.85 o -3 3 1 243.83 233.63 3.98 o -1 3 1 2265.35 2164.92 11.77 o 1 3 1 386.62 390.10 4.76 o 3 3 1 1183.58 1208.39 9.02 o 5 3 1 207.14 200.90 4.28 o 7 3 1 420.26 402.34 8.02 o 9 3 1 394.55 395.17 10.63 o 11 3 1 25.16 34.39 5.98 o 13 3 1 40.20 59.26 6.70 o -12 4 1 73.08 82.18 7.65 o -10 4 1 177.34 170.37 7.89 o -8 4 1 58.33 53.98 4.97 o -6 4 1 434.30 449.97 8.24 o -4 4 1 112.07 106.91 4.03 o -2 4 1 4265.60 4776.25 22.13 o 0 4 1 550.44 554.01 6.32 o 2 4 1 37.08 27.59 2.05 o 4 4 1 6.31 5.15 1.54 o 6 4 1 28.54 20.59 3.21 o 8 4 1 3.49 5.68 3.48 o 10 4 1 165.13 156.35 9.27 o 12 4 1 159.03 175.48 10.45 o -11 5 1 4.11 3.00 4.61 o -9 5 1 37.15 28.60 5.27 o -7 5 1 5.24 7.44 3.35 o -5 5 1 4.32 2.81 1.93 o -3 5 1 542.26 553.22 8.50 o -1 5 1 201.57 201.90 4.51 o 1 5 1 4.49 3.15 1.72 o 3 5 1 465.38 441.10 7.37 o 5 5 1 9.53 13.82 6.19 o 7 5 1 7.75 5.64 4.50 o 9 5 1 29.31 31.60 5.34 o 11 5 1 16.70 22.07 5.67 o -10 6 1 17.22 14.75 5.05 o -8 6 1 2.22 5.84 4.23 o -6 6 1 325.42 312.57 9.74 o -4 6 1 107.69 100.65 4.60 o -2 6 1 5.77 0.80 1.93 o 0 6 1 0.36 2.04 2.22 o 2 6 1 3.16 0.84 2.56 o 4 6 1 96.34 91.13 4.90 o 6 6 1 11.67 5.01 4.09 o 8 6 1 0.01 3.10 4.97 o 10 6 1 102.91 105.70 8.62 o -9 7 1 20.07 18.85 5.55 o -7 7 1 3.08 4.47 4.50 o -5 7 1 0.62 -0.77 4.09 o -3 7 1 0.03 0.48 2.02 o -1 7 1 8.79 3.31 5.40 o 1 7 1 56.31 61.46 4.36 o 3 7 1 22.79 26.69 4.12 o 5 7 1 7.59 5.92 3.83 o 7 7 1 15.83 8.42 6.30 o 9 7 1 7.82 5.96 4.57 o -8 8 1 21.33 15.39 7.95 o -6 8 1 5.49 -3.08 4.47 o -4 8 1 13.38 20.92 5.10 o -2 8 1 5.84 -2.42 4.11 o 0 8 1 51.03 51.17 5.56 o 2 8 1 23.99 22.52 5.44 o 4 8 1 24.68 29.55 5.98 o 6 8 1 20.12 23.34 5.63 o 8 8 1 17.55 28.66 6.35 o -5 9 1 6.68 -1.05 7.92 o -3 9 1 38.99 34.00 12.36 o 1 9 1 7.11 1.44 9.82 o 3 9 1 0.02 -2.29 9.81 o 5 9 1 12.22 8.20 8.61 o -14 0 2 223.40 243.55 20.89 o -12 0 2 213.72 209.67 9.34 o -10 0 2 37.16 31.48 4.63 o -8 0 2 819.23 801.65 14.02 o -6 0 2 1532.67 1542.53 17.10 o -4 0 2 957.07 893.93 10.70 o -2 0 2 2307.28 2307.69 14.74 o 0 0 2 10833.44 10276.74 225.91 o 2 0 2 0.40 -0.96 2.10 o 4 0 2 957.42 975.56 12.68 o 6 0 2 297.82 343.24 8.15 o 8 0 2 449.90 469.43 11.47 o 10 0 2 733.34 713.76 15.01 o 12 0 2 0.63 -6.51 6.51 o -13 1 2 1.73 13.18 3.89 o -11 1 2 151.03 150.24 6.06 o -9 1 2 120.34 114.50 5.09 o -7 1 2 202.01 197.88 4.76 o -5 1 2 464.43 483.87 6.24 o -3 1 2 2502.59 2539.18 12.56 o -1 1 2 2525.24 2600.80 19.88 o 1 1 2 940.46 982.90 6.78 o 3 1 2 84.23 81.57 2.26 o 5 1 2 913.23 999.69 8.87 o 7 1 2 1209.06 1207.18 11.42 o 9 1 2 161.87 160.14 6.30 o 11 1 2 227.11 236.52 7.73 o 13 1 2 124.61 150.08 9.37 o -12 2 2 54.18 54.85 6.01 o -10 2 2 42.31 48.09 4.91 o -8 2 2 368.67 358.96 6.81 o -6 2 2 67.68 68.60 3.39 o -4 2 2 143.93 152.06 3.25 o -2 2 2 127.02 142.65 3.39 o 0 2 2 3973.76 4118.52 18.08 o 2 2 2 1216.59 1292.15 7.80 o 4 2 2 209.75 217.29 3.78 o 6 2 2 196.01 174.68 4.17 o 8 2 2 1102.45 1109.86 13.85 o 10 2 2 255.13 254.16 8.93 o 12 2 2 6.74 18.32 4.84 o -13 3 2 0.25 6.73 4.35 o -11 3 2 0.21 7.09 7.19 o -9 3 2 39.27 44.49 4.91 o -7 3 2 8.22 5.08 2.14 o -5 3 2 357.75 353.69 5.29 o -3 3 2 2626.98 2930.98 18.09 o -1 3 2 1213.84 1244.62 8.51 o 1 3 2 162.30 145.69 3.09 o 3 3 2 215.70 210.02 3.75 o 5 3 2 73.05 77.53 2.83 o 7 3 2 79.82 77.54 4.32 o 9 3 2 60.00 56.84 5.33 o 11 3 2 11.99 1.12 7.53 o 13 3 2 5.98 8.70 4.50 o -12 4 2 179.73 188.69 10.53 o -10 4 2 73.22 78.86 5.99 o -8 4 2 454.93 430.11 12.99 o -6 4 2 1.47 1.28 1.76 o -4 4 2 86.27 96.67 3.87 o -2 4 2 2433.29 2505.14 14.71 o 0 4 2 256.93 274.45 5.14 o 2 4 2 560.30 581.48 6.90 o 4 4 2 1.67 1.38 1.32 o 6 4 2 40.54 47.11 4.04 o 8 4 2 195.34 192.71 9.52 o 10 4 2 39.67 39.47 6.12 o 12 4 2 3.91 13.88 5.24 o -11 5 2 6.59 24.98 8.84 o -9 5 2 1.40 -2.61 2.84 o -7 5 2 110.53 92.79 9.42 o -5 5 2 98.17 89.50 4.21 o -3 5 2 95.21 102.53 4.24 o -1 5 2 285.06 280.83 5.03 o 1 5 2 3.93 3.02 1.56 o 3 5 2 0.74 3.93 2.38 o 5 5 2 16.00 12.54 3.17 o 7 5 2 228.83 231.13 10.22 o 9 5 2 18.03 20.38 5.31 o 11 5 2 54.91 53.51 6.55 o -10 6 2 18.67 24.96 5.02 o -8 6 2 24.85 31.46 6.77 o -6 6 2 207.64 199.10 7.76 o -4 6 2 559.06 517.27 10.73 o -2 6 2 296.59 262.42 7.07 o 0 6 2 217.81 205.82 8.12 o 2 6 2 110.97 102.88 4.27 o 4 6 2 319.79 319.68 10.37 o 6 6 2 167.83 159.62 8.82 o 8 6 2 2.97 14.95 4.75 o 10 6 2 51.37 66.92 7.17 o -9 7 2 20.73 24.89 5.29 o -7 7 2 65.46 62.72 7.51 o -5 7 2 75.40 94.68 5.95 o -3 7 2 18.79 21.24 2.74 o -1 7 2 0.83 4.14 2.56 o 1 7 2 272.64 282.34 9.97 o 3 7 2 11.33 7.49 5.94 o 5 7 2 0.32 0.54 3.78 o 7 7 2 30.64 38.09 5.78 o 9 7 2 39.53 34.56 5.69 o -8 8 2 0.46 6.91 5.35 o -6 8 2 37.95 34.98 5.97 o -4 8 2 6.48 9.34 4.64 o -2 8 2 0.12 0.71 5.65 o 0 8 2 7.62 5.19 4.38 o 2 8 2 8.50 11.90 7.18 o 4 8 2 52.23 52.27 7.52 o 6 8 2 0.31 -1.09 4.43 o 8 8 2 3.85 -5.50 5.93 o -5 9 2 0.09 -11.01 11.01 o -3 9 2 0.30 -6.95 10.48 o 1 9 2 36.59 38.98 6.53 o 3 9 2 3.52 0.99 5.95 o 5 9 2 5.27 4.19 16.05 o -13 1 3 3.15 8.19 3.98 o -11 1 3 154.51 157.85 6.23 o -9 1 3 76.73 84.96 4.85 o -7 1 3 0.85 2.05 1.76 o -5 1 3 302.75 327.32 5.08 o -3 1 3 1966.28 1877.92 10.60 o -1 1 3 98.35 98.27 2.06 o 1 1 3 13021.69 13083.66 93.72 o 3 1 3 214.56 199.49 3.09 o 5 1 3 2499.85 2602.19 15.07 o 7 1 3 243.08 219.83 5.10 o 9 1 3 366.89 344.89 8.36 o 11 1 3 157.26 161.15 7.70 o 13 1 3 6.09 26.39 6.91 o -12 2 3 2.13 6.06 3.49 o -10 2 3 54.12 63.82 4.30 o -8 2 3 195.26 182.81 5.04 o -6 2 3 5.76 5.32 2.00 o -4 2 3 492.94 474.03 5.44 o -2 2 3 62.00 52.64 2.46 o 0 2 3 486.63 494.22 4.60 o 2 2 3 60.95 66.41 1.94 o 4 2 3 1436.01 1496.64 9.79 o 6 2 3 268.92 272.65 4.99 o 8 2 3 409.43 381.85 8.36 o 10 2 3 4.00 3.58 3.37 o 12 2 3 5.76 13.40 6.37 o -13 3 3 11.60 13.11 4.64 o -11 3 3 1.99 8.80 3.79 o -9 3 3 3.82 3.95 2.87 o -7 3 3 815.81 800.70 11.29 o -5 3 3 34.18 30.54 1.81 o -3 3 3 167.83 182.81 6.40 o -1 3 3 1292.27 1340.20 8.94 o 1 3 3 25.16 21.65 1.63 o 3 3 3 445.45 465.67 5.27 o 5 3 3 2129.21 2057.46 13.33 o 7 3 3 2310.08 2346.66 19.88 o 9 3 3 171.40 183.89 9.46 o 11 3 3 133.19 127.51 8.67 o 13 3 3 33.44 33.13 7.99 o -12 4 3 17.07 28.98 5.46 o -10 4 3 12.24 15.97 5.23 o -8 4 3 116.51 112.24 6.27 o -6 4 3 137.22 126.64 4.85 o -4 4 3 8.16 12.37 2.21 o -2 4 3 5008.72 5169.02 27.55 o 0 4 3 1922.62 1909.91 12.63 o 2 4 3 57.28 52.03 2.52 o 4 4 3 266.17 258.77 4.98 o 6 4 3 8.35 11.59 2.85 o 8 4 3 487.57 471.22 13.90 o 10 4 3 6.60 6.81 4.94 o 12 4 3 11.24 19.35 5.21 o -11 5 3 55.38 61.06 7.18 o -9 5 3 75.28 67.33 5.43 o -7 5 3 8.94 8.36 3.36 o -5 5 3 49.94 44.89 3.38 o -3 5 3 5.97 2.25 2.17 o -1 5 3 30.46 25.26 1.94 o 1 5 3 43.05 43.31 2.56 o 3 5 3 56.48 55.96 2.95 o 5 5 3 0.80 1.77 2.97 o 7 5 3 20.18 5.89 5.99 o 9 5 3 29.16 26.00 5.56 o 11 5 3 44.04 50.19 6.70 o -10 6 3 1.03 0.94 4.48 o -8 6 3 1.24 0.80 3.26 o -6 6 3 131.12 118.86 9.36 o -4 6 3 1092.56 1067.41 14.07 o -2 6 3 31.93 37.92 3.03 o 0 6 3 41.29 45.51 3.45 o 2 6 3 31.24 28.72 3.66 o 4 6 3 7.75 16.22 3.65 o 6 6 3 8.93 11.09 4.37 o 8 6 3 64.37 47.91 6.19 o 10 6 3 41.62 45.45 6.07 o -9 7 3 13.25 25.65 5.62 o -7 7 3 0.97 7.26 4.58 o -5 7 3 0.13 5.58 3.02 o -3 7 3 16.58 20.70 3.19 o -1 7 3 74.91 71.98 4.45 o 1 7 3 17.52 18.89 8.48 o 3 7 3 3.09 -0.81 2.97 o 5 7 3 12.92 23.78 4.58 o 7 7 3 3.87 1.10 8.30 o 9 7 3 5.67 12.88 4.80 o -8 8 3 0.52 -2.69 6.26 o -6 8 3 9.32 22.06 5.53 o -4 8 3 3.96 10.25 4.87 o -2 8 3 38.87 52.46 6.59 o 0 8 3 13.36 25.46 5.57 o 2 8 3 102.55 96.62 8.84 o 4 8 3 37.13 42.06 6.51 o 6 8 3 1.60 -2.22 4.22 o 8 8 3 1.84 25.40 7.24 o -5 9 3 32.24 14.49 12.77 o -3 9 3 0.97 -10.57 10.57 o -1 9 3 31.16 40.72 7.61 o 1 9 3 0.29 3.18 5.35 o 3 9 3 23.03 22.93 10.55 o 5 9 3 59.25 54.39 10.46 o -14 0 4 35.36 62.63 11.66 o -12 0 4 168.41 166.06 26.46 o -10 0 4 1289.54 1282.59 20.38 o -8 0 4 239.14 251.21 8.12 o -6 0 4 70.04 73.79 4.39 o -4 0 4 5649.90 5827.38 36.19 o -2 0 4 4709.47 4858.80 26.54 o 0 0 4 5744.36 5850.90 60.67 o 2 0 4 279.76 289.23 4.74 o 4 0 4 209.91 218.57 5.80 o 6 0 4 1761.59 1939.40 19.90 o 8 0 4 409.65 371.81 10.04 o 10 0 4 308.36 299.44 13.66 o 12 0 4 203.16 218.90 12.98 o -13 1 4 12.49 19.91 6.84 o -11 1 4 443.86 425.20 9.75 o -9 1 4 194.48 167.37 5.14 o -7 1 4 347.70 377.59 7.80 o -5 1 4 1684.99 1962.03 13.13 o -3 1 4 4077.45 4217.47 18.26 o -1 1 4 1343.95 1345.75 9.04 o 1 1 4 2559.28 2569.89 12.68 o 3 1 4 3201.42 3202.55 14.53 o 5 1 4 5572.99 6103.00 26.11 o 7 1 4 1345.10 1326.29 12.08 o 9 1 4 2.67 4.22 4.90 o 11 1 4 112.04 115.53 8.38 o 13 1 4 2.34 -1.42 6.07 o -12 2 4 74.45 78.26 5.90 o -10 2 4 31.13 31.43 3.43 o -8 2 4 195.10 180.29 5.83 o -6 2 4 96.78 98.08 3.28 o -4 2 4 3.41 8.63 1.70 o -2 2 4 946.25 980.75 8.84 o 0 2 4 980.53 959.12 6.87 o 2 2 4 45.49 43.59 1.90 o 4 2 4 34.86 36.74 2.62 o 6 2 4 408.66 438.69 6.09 o 8 2 4 647.70 610.77 10.50 o 10 2 4 76.94 85.75 5.98 o 12 2 4 0.07 3.08 6.36 o -13 3 4 0.20 4.84 8.45 o -11 3 4 58.90 52.60 5.31 o -9 3 4 92.97 90.85 4.79 o -7 3 4 403.55 378.22 8.01 o -5 3 4 166.50 159.00 4.84 o -3 3 4 947.27 1042.85 10.67 o -1 3 4 419.41 438.48 5.20 o 1 3 4 820.44 805.91 6.87 o 3 3 4 64.29 88.35 2.57 o 5 3 4 8.16 7.34 2.41 o 7 3 4 43.78 36.98 3.73 o 9 3 4 220.37 213.19 14.40 o 11 3 4 7.03 13.47 5.15 o 13 3 4 5.34 24.51 10.87 o -12 4 4 1.04 9.74 5.31 o -10 4 4 0.00 5.17 3.65 o -8 4 4 6.53 1.26 2.89 o -6 4 4 11.54 11.10 2.29 o -4 4 4 29.75 31.34 2.74 o -2 4 4 4987.66 5256.32 29.23 o 0 4 4 0.31 -0.24 1.28 o 2 4 4 217.35 230.38 4.35 o 4 4 4 63.07 52.11 3.07 o 6 4 4 8.82 4.78 3.94 o 8 4 4 29.64 30.19 5.61 o 10 4 4 3.66 15.64 6.84 o 12 4 4 0.24 -2.64 4.57 o -11 5 4 0.56 3.42 4.72 o -9 5 4 106.89 110.11 6.58 o -7 5 4 84.74 82.25 6.06 o -5 5 4 203.43 200.58 6.14 o -3 5 4 25.90 30.14 2.88 o -1 5 4 1490.85 1435.98 20.16 o 1 5 4 0.51 0.34 1.43 o 3 5 4 308.56 291.34 7.80 o 5 5 4 332.45 321.67 10.31 o 7 5 4 1.52 0.99 4.00 o 9 5 4 255.95 261.74 11.70 o 11 5 4 0.01 1.14 5.94 o -10 6 4 8.03 6.69 4.65 o -8 6 4 90.96 83.83 6.47 o -6 6 4 44.09 42.42 4.49 o -4 6 4 652.04 647.98 11.14 o -2 6 4 559.09 540.33 8.93 o 0 6 4 10.09 11.72 3.18 o 2 6 4 171.51 170.34 6.98 o 4 6 4 3.06 6.39 4.41 o 6 6 4 54.73 45.49 5.91 o 8 6 4 8.68 22.29 8.23 o 10 6 4 8.98 20.42 5.26 o -9 7 4 49.25 50.42 6.67 o -7 7 4 6.90 14.55 3.97 o -5 7 4 97.36 103.31 6.29 o -3 7 4 38.59 34.51 3.46 o -1 7 4 73.03 80.73 5.72 o 1 7 4 166.84 185.85 10.72 o 3 7 4 35.52 28.77 4.17 o 5 7 4 19.56 16.57 4.07 o 7 7 4 3.07 1.60 4.28 o 9 7 4 8.32 -2.01 4.64 o -8 8 4 17.59 31.38 12.81 o -6 8 4 56.60 65.25 7.00 o -4 8 4 190.79 180.70 9.51 o -2 8 4 52.82 51.21 5.70 o 0 8 4 4.79 7.65 4.71 o 2 8 4 42.73 48.31 7.03 o 4 8 4 29.12 30.69 11.40 o 6 8 4 21.19 26.32 8.76 o -5 9 4 4.79 -9.36 10.83 o -1 9 4 0.43 4.99 10.38 o 1 9 4 1.67 -8.54 8.54 o 3 9 4 3.61 10.81 5.13 o -13 1 5 0.81 6.19 4.17 o -11 1 5 194.18 194.66 6.96 o -9 1 5 3.37 5.64 2.08 o -7 1 5 1090.82 1041.20 10.85 o -5 1 5 1.36 -1.41 1.41 o -3 1 5 1099.52 1131.65 10.35 o -1 1 5 6281.80 6621.77 29.82 o 1 1 5 610.09 600.46 7.06 o 3 1 5 454.51 420.16 5.50 o 5 1 5 289.66 268.77 6.75 o 7 1 5 24.15 24.00 2.58 o 9 1 5 0.29 -3.47 3.47 o 11 1 5 0.25 12.38 5.56 o 13 1 5 5.59 16.36 6.58 o -12 2 5 2.60 5.11 5.40 o -10 2 5 310.41 312.18 8.30 o -8 2 5 857.55 834.90 12.08 o -6 2 5 81.42 75.95 2.97 o -4 2 5 746.22 790.48 7.59 o -2 2 5 2390.43 2525.64 13.16 o 0 2 5 1589.98 1560.55 9.23 o 2 2 5 56.35 46.76 3.11 o 4 2 5 115.31 89.86 3.44 o 6 2 5 51.11 46.07 3.41 o 8 2 5 91.12 72.94 4.79 o 10 2 5 22.34 24.45 4.56 o 12 2 5 6.24 9.16 6.15 o -13 3 5 4.02 10.72 5.58 o -11 3 5 126.48 110.40 6.59 o -9 3 5 185.82 177.26 6.35 o -7 3 5 332.94 335.01 7.70 o -5 3 5 1245.59 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