#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/52/2215249.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215249_Fobs loop_ _publ_author_name 'Vasiliev, Alexander D.' 'Chudin, Oleg S.' 'Antonova, Alla B.' _publ_section_title ; \m-Carbonyl-1:2\k^2^C-carbonyl-1\kC-(1{\h}^5^-cyclopentadienyl)(\m-phenylvinylidene)bis(triphenylphosphine-2\kP)rheniumplatinum(Re---Pt) diethyl ether hemisolvate ; _journal_coeditor_code RK2027 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2272 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.469 _cell_angle_gamma 90.000 _cell_length_a 22.5290 _cell_length_b 9.1786 _cell_length_c 21.9410 _exptl_crystal_F_000 2268.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file rk2027Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ant1_2 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 608.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 76275.87 73504.27 3221.76 o 4 0 0 2940.27 3078.79 255.19 o 5 0 0 193444.31 199262.83 4497.14 o 6 0 0 3697.97 3884.30 242.67 o 7 0 0 24180.98 21910.61 707.99 o 8 0 0 1145.32 1637.58 124.99 o 9 0 0 245.57 340.73 162.92 o 10 0 0 10034.78 12055.08 436.62 o 11 0 0 48157.36 51005.08 1148.96 o 12 0 0 57021.59 58309.69 893.70 o 13 0 0 47883.97 47179.55 750.37 o 14 0 0 112213.04 109081.77 2094.56 o 15 0 0 6577.58 6917.21 343.46 o 16 0 0 92307.91 89871.12 1796.18 o 17 0 0 8730.83 8762.25 404.24 o 18 0 0 28281.29 28986.87 781.86 o 19 0 0 22373.01 21244.30 990.72 o 20 0 0 9119.17 10086.89 1066.02 o 21 0 0 14029.23 14049.58 547.19 o 22 0 0 3008.60 3203.51 483.23 o 23 0 0 337.31 669.76 249.07 o 24 0 0 241.40 -214.73 214.73 o 25 0 0 1367.93 776.95 301.61 o 26 0 0 688.40 -8.54 259.75 o 27 0 0 2296.34 2677.36 546.98 o 28 0 0 3518.37 2979.36 396.57 o 29 0 0 179.39 160.35 316.63 o 1 1 0 9290.00 9552.57 132.43 o 2 1 0 883.92 1198.60 49.67 o 3 1 0 277.86 142.05 24.47 o 4 1 0 18105.98 17680.30 224.75 o 5 1 0 216.35 309.17 57.23 o 6 1 0 451.70 611.45 57.02 o 7 1 0 20310.97 21287.36 288.74 o 8 1 0 16394.10 17406.20 254.67 o 9 1 0 26910.94 27274.09 366.23 o 10 1 0 2952.05 2952.36 106.64 o 11 1 0 11883.97 11212.23 210.72 o 12 1 0 283.71 178.97 64.29 o 13 1 0 611.60 498.18 78.89 o 14 1 0 3772.27 3915.05 141.47 o 15 1 0 586.40 677.65 132.93 o 16 1 0 303.38 255.91 127.13 o 17 1 0 478.91 307.47 139.28 o 18 1 0 15.42 80.32 138.50 o 19 1 0 141.00 -74.94 140.38 o 20 1 0 95.27 57.93 143.70 o 21 1 0 2788.98 2550.92 218.40 o 22 1 0 48.87 -134.15 151.68 o 23 1 0 3710.54 3558.03 250.62 o 24 1 0 78.06 -162.72 162.72 o 25 1 0 1741.17 1642.67 223.60 o 26 1 0 14.53 -179.69 179.69 o 27 1 0 569.21 318.98 205.20 o 28 1 0 344.58 -88.28 207.15 o 29 1 0 110.67 -189.38 215.97 o 0 2 0 98222.80 103374.68 2082.16 o 1 2 0 26127.48 27642.85 424.97 o 2 2 0 169518.22 179954.56 2643.01 o 3 2 0 50690.59 55682.88 942.87 o 4 2 0 73634.13 75265.71 747.34 o 5 2 0 24940.09 24953.32 329.95 o 6 2 0 19038.50 19685.97 233.54 o 7 2 0 1239.63 1028.14 82.20 o 8 2 0 2152.75 2299.82 77.72 o 9 2 0 4961.35 6087.66 183.93 o 10 2 0 9518.39 10320.39 276.25 o 11 2 0 6795.45 6560.70 219.26 o 12 2 0 26368.61 26012.85 579.88 o 13 2 0 6293.25 5189.04 283.77 o 14 2 0 44399.70 42961.21 577.85 o 15 2 0 145.05 106.62 82.34 o 16 2 0 36605.68 34793.65 608.94 o 17 2 0 2187.83 2073.29 179.83 o 18 2 0 17219.00 16967.62 407.37 o 19 2 0 7358.97 6945.00 283.14 o 20 2 0 6914.83 7139.03 286.01 o 21 2 0 2154.94 2572.19 209.94 o 22 2 0 958.19 960.49 190.86 o 23 2 0 784.54 983.58 274.38 o 24 2 0 470.03 165.48 178.30 o 25 2 0 14.36 -177.80 177.80 o 26 2 0 1513.14 1059.00 231.23 o 27 2 0 503.98 292.47 206.34 o 28 2 0 2420.78 2268.31 271.35 o 1 3 0 586.57 518.43 40.99 o 2 3 0 38831.09 38940.40 447.59 o 3 3 0 7190.03 7534.88 168.78 o 4 3 0 50923.58 50416.29 570.78 o 5 3 0 80844.10 83142.75 835.38 o 6 3 0 7601.37 7388.85 124.74 o 7 3 0 115975.73 115502.43 1240.12 o 8 3 0 4283.84 5006.41 221.93 o 9 3 0 96599.46 95664.69 974.57 o 10 3 0 36932.12 37749.16 433.13 o 11 3 0 39037.43 38205.55 441.66 o 12 3 0 36565.02 34519.86 523.28 o 13 3 0 6030.79 6171.36 199.13 o 14 3 0 9377.00 8891.76 216.96 o 15 3 0 82.65 -88.61 88.61 o 16 3 0 67.31 10.29 92.91 o 17 3 0 28.29 -76.98 119.05 o 18 3 0 1953.75 1858.27 257.64 o 19 3 0 2968.04 3008.02 212.45 o 20 3 0 4940.56 4679.17 256.08 o 21 3 0 14652.56 13638.39 408.31 o 22 3 0 691.43 1187.95 193.80 o 23 3 0 20242.22 20484.22 508.41 o 24 3 0 19.16 -167.60 167.60 o 25 3 0 10765.58 11961.97 412.98 o 26 3 0 2179.17 2522.14 309.63 o 27 3 0 2840.42 3098.53 334.72 o 28 3 0 2428.49 2826.04 331.68 o 0 4 0 5543.95 5615.89 191.01 o 1 4 0 470.46 516.83 46.76 o 2 4 0 45.08 74.43 39.00 o 3 4 0 221.02 148.38 48.46 o 4 4 0 5455.09 5390.73 137.36 o 5 4 0 54.28 70.39 47.32 o 6 4 0 5698.76 5910.11 115.90 o 7 4 0 4148.72 4427.21 127.48 o 8 4 0 427.08 278.88 55.15 o 9 4 0 298.78 370.00 59.32 o 10 4 0 205.16 105.09 55.33 o 11 4 0 560.83 670.82 67.59 o 12 4 0 287.55 213.31 78.34 o 13 4 0 428.35 303.19 93.33 o 14 4 0 2138.08 2160.45 128.64 o 15 4 0 862.36 756.42 108.66 o 16 4 0 3238.88 3447.52 161.07 o 17 4 0 13.66 -15.93 99.76 o 18 4 0 1592.37 1614.45 176.32 o 19 4 0 4.89 -70.40 160.82 o 20 4 0 256.18 224.51 183.99 o 21 4 0 0.10 46.89 183.77 o 22 4 0 6.71 134.28 192.30 o 23 4 0 19.28 -66.95 202.20 o 24 4 0 10.47 44.77 293.69 o 25 4 0 119.83 325.73 236.20 o 26 4 0 302.38 222.50 292.74 o 27 4 0 8.92 -235.75 235.75 o 1 5 0 1276.46 1358.83 78.75 o 2 5 0 13667.12 13900.08 218.68 o 3 5 0 13596.37 14640.70 361.22 o 4 5 0 21899.38 21473.17 303.90 o 5 5 0 68282.81 69002.22 795.23 o 6 5 0 11411.53 10942.87 203.77 o 7 5 0 125730.40 126957.84 1392.74 o 8 5 0 71.15 292.51 105.33 o 9 5 0 87667.91 84736.04 971.59 o 10 5 0 12547.33 12761.42 237.61 o 11 5 0 33129.88 32521.79 447.83 o 12 5 0 19303.05 18691.23 652.05 o 13 5 0 3121.63 3352.94 231.57 o 14 5 0 9805.51 9509.33 283.99 o 15 5 0 228.40 158.84 114.97 o 16 5 0 906.67 897.82 196.59 o 17 5 0 1689.25 1696.92 159.13 o 18 5 0 3471.40 3132.90 194.03 o 19 5 0 5565.65 5176.60 363.72 o 20 5 0 4393.55 4622.65 302.12 o 21 5 0 12005.33 11517.67 443.39 o 22 5 0 888.43 1021.39 232.26 o 23 5 0 12880.86 12934.57 494.15 o 24 5 0 707.47 438.88 231.79 o 25 5 0 7892.72 8962.38 443.68 o 26 5 0 1881.92 2496.77 312.15 o 0 6 0 25068.14 23772.50 536.71 o 1 6 0 735.87 685.42 82.22 o 2 6 0 20975.73 20332.30 343.56 o 3 6 0 5283.90 5282.15 161.33 o 4 6 0 8354.66 8197.96 176.68 o 5 6 0 7074.08 6813.80 166.85 o 6 6 0 705.78 721.70 80.50 o 7 6 0 1834.70 1640.96 100.76 o 8 6 0 133.09 60.62 72.70 o 9 6 0 108.69 -10.81 71.30 o 10 6 0 53.62 -74.20 74.20 o 11 6 0 1451.30 1375.64 128.68 o 12 6 0 3839.26 3646.03 176.94 o 13 6 0 2332.23 2546.42 160.88 o 14 6 0 5797.30 6012.15 232.51 o 15 6 0 184.84 151.42 117.43 o 16 6 0 6667.64 6781.69 256.03 o 17 6 0 766.61 897.40 145.69 o 18 6 0 4403.87 4597.96 238.63 o 19 6 0 880.82 862.99 201.43 o 20 6 0 1510.12 1604.89 237.49 o 21 6 0 1309.98 1465.94 240.63 o 22 6 0 327.66 403.50 211.56 o 23 6 0 407.32 275.64 213.35 o 24 6 0 0.44 -11.76 223.01 o 25 6 0 1.33 64.66 238.70 o 1 7 0 1721.23 1552.94 110.72 o 2 7 0 32.39 -22.73 79.04 o 3 7 0 10365.12 9920.14 243.14 o 4 7 0 295.58 293.19 91.45 o 5 7 0 14240.80 14458.19 552.70 o 6 7 0 367.52 345.10 91.76 o 7 7 0 11013.26 10475.20 251.78 o 8 7 0 2.87 -26.68 84.21 o 9 7 0 10067.49 10171.09 257.42 o 10 7 0 232.97 225.16 94.16 o 11 7 0 5136.87 5132.18 208.81 o 12 7 0 1341.66 977.84 168.02 o 13 7 0 3749.54 3837.22 194.76 o 14 7 0 692.35 820.77 138.27 o 15 7 0 929.94 1100.41 148.23 o 16 7 0 89.97 130.44 123.92 o 17 7 0 3380.06 3530.81 208.21 o 18 7 0 203.55 80.55 138.31 o 19 7 0 4239.60 4280.37 456.07 o 20 7 0 401.52 383.76 199.37 o 21 7 0 1718.95 1647.73 247.25 o 22 7 0 2.87 -236.12 236.12 o 23 7 0 1515.74 1205.18 264.40 o 0 8 0 34398.07 33137.69 752.66 o 1 8 0 1726.26 1921.38 135.83 o 2 8 0 29149.73 27417.79 469.93 o 3 8 0 9084.23 8769.49 246.74 o 4 8 0 8639.15 8078.46 246.30 o 5 8 0 9133.61 8497.22 240.95 o 6 8 0 1346.81 1358.49 138.66 o 7 8 0 687.58 689.81 109.37 o 8 8 0 29.57 -50.93 114.39 o 9 8 0 1740.59 1556.66 135.30 o 10 8 0 681.53 594.43 139.88 o 11 8 0 4849.90 4760.96 268.02 o 12 8 0 6279.19 5752.46 256.36 o 13 8 0 2196.69 2425.45 201.12 o 14 8 0 16128.29 15638.16 430.22 o 15 8 0 9.55 137.73 185.91 o 16 8 0 17237.51 17049.70 473.53 o 17 8 0 987.17 1395.77 192.45 o 18 8 0 8980.01 9229.97 475.73 o 19 8 0 3166.09 3462.52 267.77 o 20 8 0 1456.67 1305.34 501.91 o 21 8 0 2234.20 2693.69 349.60 o 1 9 0 139.37 238.28 109.42 o 2 9 0 7.64 79.26 98.91 o 3 9 0 271.55 147.50 102.51 o 4 9 0 30.75 54.18 102.20 o 5 9 0 80.24 -68.70 100.10 o 6 9 0 223.32 278.53 113.82 o 7 9 0 1.37 117.03 104.94 o 8 9 0 59.25 -101.45 101.45 o 9 9 0 68.49 -126.59 126.59 o 10 9 0 73.68 42.78 134.42 o 11 9 0 0.42 -10.47 133.78 o 12 9 0 17.69 -72.41 136.85 o 13 9 0 5.79 171.69 150.08 o 14 9 0 31.30 86.81 148.82 o 15 9 0 242.03 220.13 167.30 o 16 9 0 148.51 289.65 174.33 o 17 9 0 225.10 139.32 178.07 o 18 9 0 58.66 -16.97 180.11 o 19 9 0 47.63 262.74 337.48 o 0 10 0 9949.40 10794.16 438.65 o 1 10 0 319.55 268.01 126.83 o 2 10 0 9111.88 8871.30 279.44 o 3 10 0 1312.61 1195.71 147.56 o 4 10 0 5578.60 5334.68 230.44 o 5 10 0 1020.80 1283.09 203.05 o 6 10 0 1973.02 1765.37 164.06 o 7 10 0 117.70 -75.03 111.92 o 8 10 0 1298.10 1185.68 175.53 o 9 10 0 435.89 523.66 158.20 o 10 10 0 1018.35 1131.40 180.99 o 11 10 0 658.69 750.08 173.49 o 12 10 0 2468.43 2600.50 231.13 o 13 10 0 186.12 178.29 172.86 o 14 10 0 5287.72 5440.68 376.92 o 15 10 0 6.66 -14.75 171.70 o 1 11 0 9.57 -41.14 131.16 o 2 11 0 363.51 488.32 148.12 o 3 11 0 165.41 -129.00 129.00 o 4 11 0 324.67 308.32 144.04 o 5 11 0 2567.41 2698.72 194.54 o 6 11 0 506.02 410.62 146.14 o 7 11 0 4198.08 4784.81 278.49 o 8 11 0 137.28 343.15 174.06 o 9 11 0 2407.20 2463.44 228.93 o 10 11 0 329.30 492.31 185.01 o 11 11 0 799.74 1070.60 244.10 o -29 1 1 2476.77 2082.63 269.81 o -28 1 1 124.41 -203.08 203.08 o -27 1 1 946.77 -29.60 197.00 o -26 1 1 8.22 -174.05 174.05 o -25 1 1 101.80 -167.27 167.27 o -24 1 1 2196.73 2257.00 230.53 o -23 1 1 313.03 582.07 226.23 o -22 1 1 12426.11 12390.12 380.31 o -21 1 1 4320.29 5307.20 368.11 o -20 1 1 26547.64 26815.83 562.43 o -19 1 1 10219.34 10351.53 322.78 o -18 1 1 20786.37 19150.89 436.65 o -17 1 1 41215.48 39450.20 676.33 o -16 1 1 3482.42 3450.98 195.03 o -15 1 1 81290.20 78027.92 1119.70 o -14 1 1 4316.19 3974.54 333.76 o -13 1 1 52325.88 51828.70 1268.02 o -12 1 1 7136.08 6342.70 159.94 o -11 1 1 11911.41 12998.86 374.09 o -10 1 1 664.51 757.12 66.83 o -9 1 1 443.11 252.66 51.37 o -8 1 1 4213.55 3568.30 102.41 o -7 1 1 42.05 115.45 41.35 o -6 1 1 13975.49 13633.24 635.06 o -5 1 1 15067.22 14212.11 198.22 o -4 1 1 49209.71 50412.72 635.36 o -3 1 1 65082.70 66795.69 828.06 o -2 1 1 55352.12 64229.15 891.59 o -1 1 1 369908.31 383572.47 5131.40 o 0 1 1 4417.11 3371.44 68.05 o 1 1 1 278839.84 277793.38 3491.61 o 2 1 1 21363.13 20038.81 253.44 o 3 1 1 85204.70 92747.22 901.73 o 4 1 1 59087.59 63089.59 627.00 o 5 1 1 4431.13 4940.55 137.70 o 6 1 1 14993.98 13825.46 199.88 o 7 1 1 2119.24 2184.77 87.05 o 8 1 1 4890.75 5447.27 104.11 o 9 1 1 2045.79 2445.27 146.37 o 10 1 1 71235.92 71554.47 811.07 o 11 1 1 29007.72 29481.61 352.67 o 12 1 1 65353.61 61959.16 666.69 o 13 1 1 69515.84 68166.78 788.97 o 14 1 1 21629.75 21273.81 345.09 o 15 1 1 68859.50 68804.45 857.28 o 16 1 1 399.01 610.35 131.03 o 17 1 1 45570.61 44493.27 735.56 o 18 1 1 8173.36 7599.94 318.47 o 19 1 1 16605.89 16646.84 410.28 o 20 1 1 4048.45 4614.86 245.25 o 21 1 1 5463.27 5838.10 281.88 o 22 1 1 70.92 71.33 160.87 o 23 1 1 238.49 -132.44 153.65 o 24 1 1 1088.85 579.27 194.32 o 25 1 1 635.85 110.05 182.18 o 26 1 1 3932.72 4084.04 285.07 o 27 1 1 2543.42 1668.23 245.49 o 28 1 1 1877.75 2215.44 268.14 o 29 1 1 5943.79 6616.57 357.78 o -28 2 1 994.62 1214.61 242.59 o -27 2 1 1836.58 1581.53 274.60 o -26 2 1 4515.96 4609.44 298.80 o -25 2 1 515.96 313.27 181.52 o -24 2 1 8710.66 8390.26 339.20 o -23 2 1 59.99 -154.17 154.17 o -22 2 1 8422.34 7908.32 330.81 o -21 2 1 175.55 323.37 159.40 o -20 2 1 3345.70 2898.31 217.85 o -19 2 1 4.15 -115.98 138.66 o -18 2 1 656.84 464.08 144.69 o -17 2 1 1639.59 1788.63 173.39 o -16 2 1 84.30 128.72 122.32 o -15 2 1 5725.82 5601.51 175.27 o -14 2 1 9597.73 9862.41 287.29 o -13 2 1 28690.12 26531.75 466.74 o -12 2 1 48281.79 46694.47 597.78 o -11 2 1 46378.12 47439.99 597.69 o -10 2 1 38816.21 37076.82 480.66 o -9 2 1 8582.37 8565.91 171.17 o -8 2 1 52733.03 51323.38 541.37 o -7 2 1 3263.47 3135.79 79.70 o -6 2 1 74276.24 77373.03 893.08 o -5 2 1 3221.60 3011.31 73.81 o -4 2 1 75502.10 82859.08 819.71 o -3 2 1 4475.95 4970.05 114.04 o -2 2 1 8285.04 8301.37 190.02 o -1 2 1 23757.42 26777.88 343.02 o 0 2 1 2221.37 2195.23 136.55 o 1 2 1 14232.50 15364.62 274.14 o 2 2 1 11437.13 12525.47 187.53 o 3 2 1 38536.88 39430.32 407.43 o 4 2 1 20768.74 21031.95 239.20 o 5 2 1 25625.13 26810.72 328.57 o 6 2 1 30441.43 30657.02 338.00 o 7 2 1 351.27 532.59 57.77 o 8 2 1 54882.23 54699.90 626.07 o 9 2 1 810.58 801.96 51.37 o 10 2 1 41603.49 41285.95 524.82 o 11 2 1 2683.97 3165.32 95.29 o 12 2 1 3555.56 3659.62 99.74 o 13 2 1 117.59 176.34 83.23 o 14 2 1 645.11 617.65 90.35 o 15 2 1 1568.81 1492.64 119.30 o 16 2 1 483.44 513.91 103.80 o 17 2 1 3313.95 2899.87 192.56 o 18 2 1 4420.63 4330.32 264.15 o 19 2 1 6549.06 6148.81 267.63 o 20 2 1 8995.15 7997.87 298.81 o 21 2 1 3547.88 3928.44 346.21 o 22 2 1 13995.38 12840.37 390.33 o 23 2 1 491.20 528.18 185.88 o 24 2 1 6799.54 7539.13 333.23 o 25 2 1 23.70 13.53 183.87 o 26 2 1 2496.45 3064.87 268.37 o 27 2 1 436.12 304.42 208.94 o 28 2 1 545.25 559.23 222.71 o -28 3 1 15.17 -247.07 247.07 o -27 3 1 403.98 88.48 244.22 o -26 3 1 178.59 153.58 239.47 o -25 3 1 84.26 246.80 185.09 o -24 3 1 718.94 985.92 260.09 o -23 3 1 234.04 305.01 179.77 o -22 3 1 1565.66 1513.41 207.32 o -21 3 1 1525.24 2027.16 204.14 o -20 3 1 3697.42 3255.50 224.86 o -19 3 1 8783.67 8841.93 396.02 o -18 3 1 2735.57 2841.41 226.46 o -17 3 1 11682.69 11437.89 326.73 o -16 3 1 140.75 37.03 98.20 o -15 3 1 8538.51 8341.30 216.00 o -14 3 1 333.41 148.06 85.79 o -13 3 1 4151.05 3879.55 178.82 o -12 3 1 2948.89 2827.87 140.15 o -11 3 1 1164.49 1315.06 111.60 o -10 3 1 24.46 -41.28 41.28 o -9 3 1 1122.48 1315.08 65.65 o -8 3 1 3627.00 3041.85 88.60 o -7 3 1 3507.48 3692.93 92.31 o -6 3 1 37886.36 38629.12 420.21 o -5 3 1 16473.89 16403.17 205.67 o -4 3 1 22329.47 23898.85 335.36 o -3 3 1 36481.76 36795.23 429.62 o -2 3 1 2282.77 2304.54 73.18 o -1 3 1 57771.80 59598.56 656.71 o 0 3 1 504.31 434.68 45.81 o 1 3 1 13844.63 13874.34 190.21 o 2 3 1 2307.90 2479.74 75.81 o 3 3 1 19376.71 20167.88 259.76 o 4 3 1 314.30 294.34 34.45 o 5 3 1 27868.62 29674.26 366.10 o 6 3 1 12234.84 13345.35 249.58 o 7 3 1 497.48 678.59 59.84 o 8 3 1 3700.77 3691.16 98.19 o 9 3 1 117.06 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