#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/52/2215262.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215262_Fobs loop_ _publ_author_name 'Grigoriev, Mikhail S.' 'Krot, Nikolai N.' _publ_section_title ; Reinvestigation of trisodium dihydroxidotetraoxidoneptunate(VII) ; _journal_coeditor_code SG2188 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i176 _journal_volume 63 _journal_year 2007 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 20.0791 _cell_length_b 5.9534 _cell_length_c 10.2062 _exptl_crystal_F_000 1408.00 _reflns_d_resolution_high 0.5026 _[local]_cod_data_source_file sg2188Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' n in Fdd2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 615.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -20 14425.93 14547.54 936.38 o 4 0 -20 21634.15 22218.79 809.04 o 1 1 -19 9984.61 11116.84 402.71 o 3 1 -19 10265.23 10265.39 370.72 o 5 1 -19 8980.07 8745.76 235.01 o 7 1 -19 10638.75 9962.22 314.64 o 9 1 -19 13768.34 13455.29 411.69 o 11 1 -19 11632.42 11811.88 311.18 o 13 1 -19 10271.56 9962.92 268.39 o 1 3 -19 13393.71 13115.17 534.47 o 3 3 -19 12037.49 12496.92 283.67 o 5 3 -19 7516.35 7696.86 235.42 o 7 3 -19 6911.30 6985.94 231.39 o 9 3 -19 7524.06 7692.02 243.52 o 2 0 -18 29163.25 29001.56 770.10 o 6 0 -18 29157.67 28155.54 588.80 o 10 0 -18 35092.56 33913.19 673.86 o 14 0 -18 28232.38 27750.19 609.87 o 18 0 -18 17388.31 17625.71 492.70 o 0 2 -18 32991.29 33102.84 1294.17 o 2 2 -18 107.42 497.16 189.06 o 4 2 -18 29095.72 28721.24 415.95 o 6 2 -18 265.16 232.14 124.15 o 8 2 -18 27499.18 27120.37 409.82 o 10 2 -18 58.63 76.71 130.94 o 12 2 -18 25920.14 25814.98 457.73 o 14 2 -18 171.52 249.78 139.86 o 16 2 -18 20460.10 21088.81 395.59 o 2 4 -18 29943.11 29920.04 375.96 o 4 4 -18 154.50 192.81 158.42 o 6 4 -18 21351.43 21904.44 406.42 o 8 4 -18 21.11 168.53 146.71 o 10 4 -18 19513.09 19435.26 520.32 o 12 4 -18 60.62 115.14 214.04 o 1 1 -17 14732.75 13868.53 505.54 o 3 1 -17 15342.01 15287.42 287.48 o 5 1 -17 21660.67 20938.00 398.91 o 7 1 -17 18143.99 17825.90 299.08 o 9 1 -17 12762.21 13037.41 274.18 o 11 1 -17 13322.41 12512.73 273.61 o 13 1 -17 11852.59 11401.93 269.85 o 15 1 -17 13944.11 13906.79 339.62 o 17 1 -17 15925.76 15729.93 322.20 o 19 1 -17 10468.57 11013.54 296.86 o 21 1 -17 8764.49 8767.46 338.46 o 1 3 -17 12999.70 12549.63 259.52 o 3 3 -17 14519.71 14851.54 294.03 o 5 3 -17 18117.74 18141.61 316.52 o 7 3 -17 16007.32 16066.74 301.84 o 9 3 -17 12226.43 12249.10 270.07 o 11 3 -17 11311.73 11294.62 267.50 o 13 3 -17 11168.30 11211.75 409.06 o 15 3 -17 12284.36 13056.43 377.26 o 17 3 -17 12395.78 12789.98 336.00 o 19 3 -17 9031.20 9962.51 436.49 o 1 5 -17 9517.48 9686.06 233.25 o 3 5 -17 12325.54 12928.21 251.04 o 5 5 -17 13866.54 14100.89 263.04 o 7 5 -17 13277.27 13898.23 261.12 o 9 5 -17 10480.15 11028.43 248.14 o 11 5 -17 7983.13 8448.76 253.17 o 13 5 -17 8376.02 8740.60 260.23 o 0 0 -16 56067.14 53613.36 1375.28 o 4 0 -16 35136.57 34566.59 585.78 o 8 0 -16 25005.39 25277.59 486.80 o 12 0 -16 30101.77 29361.06 519.89 o 16 0 -16 29344.13 28710.92 496.03 o 20 0 -16 28160.41 28607.08 591.16 o 24 0 -16 17056.43 17366.24 463.79 o 2 2 -16 33448.24 32912.74 388.67 o 4 2 -16 659.19 663.38 110.74 o 6 2 -16 31844.88 30896.96 433.50 o 8 2 -16 89.47 174.14 109.78 o 10 2 -16 36566.73 35671.24 440.56 o 12 2 -16 408.64 545.56 112.16 o 14 2 -16 25038.58 25392.99 361.03 o 16 2 -16 291.51 409.59 100.66 o 18 2 -16 20804.16 20629.51 324.59 o 20 2 -16 59.73 394.76 129.66 o 22 2 -16 21712.24 22258.84 390.28 o 0 4 -16 26801.27 27500.31 446.54 o 2 4 -16 139.94 195.25 88.86 o 4 4 -16 24728.78 25108.98 307.16 o 6 4 -16 204.30 224.67 97.16 o 8 4 -16 31561.77 32230.75 506.45 o 10 4 -16 111.53 393.14 138.53 o 12 4 -16 30067.43 29492.70 436.71 o 14 4 -16 54.56 154.79 157.30 o 16 4 -16 16610.58 16840.34 317.81 o 18 4 -16 169.10 246.70 141.35 o 20 4 -16 15233.02 15342.55 408.44 o 2 6 -16 25586.16 25949.27 412.98 o 4 6 -16 227.99 147.33 127.97 o 6 6 -16 17078.71 17222.65 334.43 o 8 6 -16 118.99 296.22 134.44 o 10 6 -16 17567.04 18352.01 343.76 o 12 6 -16 56.44 53.85 136.70 o 1 1 -15 32854.77 32006.15 426.42 o 3 1 -15 33180.79 31837.38 368.25 o 5 1 -15 19959.13 20013.15 286.84 o 7 1 -15 22166.09 21816.46 304.48 o 9 1 -15 22865.98 22499.93 305.45 o 11 1 -15 18824.28 19161.22 262.88 o 13 1 -15 22205.20 21525.99 254.22 o 15 1 -15 18741.02 18102.15 229.23 o 17 1 -15 17246.66 17168.86 227.32 o 19 1 -15 20186.99 20004.00 274.91 o 21 1 -15 17522.24 17881.05 275.22 o 23 1 -15 14939.90 15305.29 300.83 o 25 1 -15 12132.60 12088.92 352.10 o 1 3 -15 21236.53 21275.17 271.17 o 3 3 -15 20450.59 20177.87 284.86 o 5 3 -15 19815.89 20235.54 295.78 o 7 3 -15 22236.94 22101.71 308.76 o 9 3 -15 27215.48 26874.82 342.03 o 11 3 -15 25874.26 25728.50 296.28 o 13 3 -15 23315.24 23354.37 285.15 o 15 3 -15 17877.61 17585.73 266.40 o 17 3 -15 11033.05 11297.89 231.37 o 19 3 -15 10897.26 11082.28 255.49 o 21 3 -15 10553.14 10533.62 289.42 o 23 3 -15 10157.63 10703.34 235.16 o 1 5 -15 17747.98 18091.17 300.15 o 3 5 -15 15801.32 16434.23 263.55 o 5 5 -15 19082.87 19223.59 286.13 o 7 5 -15 16519.95 17119.84 270.98 o 9 5 -15 18597.85 18787.23 270.02 o 11 5 -15 18898.90 19328.11 290.59 o 13 5 -15 13897.03 14384.02 251.68 o 15 5 -15 12602.66 13030.96 244.51 o 17 5 -15 10427.19 10505.32 239.28 o 19 5 -15 10019.28 10554.40 236.04 o 21 5 -15 11519.32 11907.40 248.89 o 1 7 -15 18669.93 19452.06 412.47 o 3 7 -15 12757.14 13185.44 599.04 o 5 7 -15 11578.62 11384.83 318.41 o 7 7 -15 8787.45 9332.22 308.50 o 9 7 -15 7493.04 7533.15 210.16 o 11 7 -15 10091.87 10368.66 239.22 o 2 0 -14 61283.31 57685.86 894.14 o 6 0 -14 60633.16 59407.40 855.31 o 10 0 -14 31552.93 30961.76 415.42 o 14 0 -14 45166.93 43797.99 553.57 o 18 0 -14 45523.80 44484.70 579.26 o 22 0 -14 25644.42 26597.17 499.34 o 26 0 -14 25467.50 25938.27 618.68 o 0 2 -14 35884.63 34460.83 612.03 o 2 2 -14 206.98 185.75 84.14 o 4 2 -14 60679.87 59067.59 553.60 o 6 2 -14 417.03 602.55 87.57 o 8 2 -14 54385.64 53748.17 480.11 o 10 2 -14 83.98 204.56 75.32 o 12 2 -14 34487.46 33367.16 319.06 o 14 2 -14 362.91 409.83 80.71 o 16 2 -14 42363.70 41634.11 395.93 o 18 2 -14 112.83 419.01 93.07 o 20 2 -14 29370.94 29467.91 331.62 o 22 2 -14 35.62 -38.40 87.61 o 24 2 -14 22798.49 23092.22 390.81 o 26 2 -14 94.64 181.32 99.89 o 28 2 -14 20875.16 21063.30 321.68 o 2 4 -14 34275.04 34084.20 350.68 o 4 4 -14 366.87 280.56 88.64 o 6 4 -14 51564.51 51403.18 438.32 o 8 4 -14 39.34 136.68 72.05 o 10 4 -14 36218.45 36081.75 352.25 o 12 4 -14 67.18 149.86 79.01 o 14 4 -14 36225.31 36629.46 381.43 o 16 4 -14 94.27 204.05 91.65 o 18 4 -14 28121.74 28188.57 315.97 o 20 4 -14 37.21 177.86 90.45 o 22 4 -14 16262.03 16137.31 264.95 o 24 4 -14 103.84 5.90 110.55 o 0 6 -14 28280.43 28109.11 585.39 o 2 6 -14 85.97 130.98 107.00 o 4 6 -14 35379.54 36112.55 443.73 o 6 6 -14 125.03 249.23 104.87 o 8 6 -14 27053.71 27337.72 388.44 o 10 6 -14 127.31 136.95 151.86 o 12 6 -14 20770.78 21204.93 325.94 o 14 6 -14 25.62 17.08 112.94 o 16 6 -14 27474.63 27948.11 384.97 o 18 6 -14 126.94 30.85 116.91 o 20 6 -14 18864.51 19754.66 291.74 o 2 8 -14 19852.96 19800.47 430.87 o 4 8 -14 28.83 310.98 137.34 o 6 8 -14 24129.96 24359.57 444.20 o 8 8 -14 33.20 204.46 156.58 o 10 8 -14 14268.94 13901.83 321.02 o 1 1 -13 31268.94 30468.38 349.80 o 3 1 -13 24957.36 24739.12 251.67 o 5 1 -13 30728.67 29956.68 299.36 o 7 1 -13 28167.75 27703.96 255.43 o 9 1 -13 27510.52 26662.94 253.73 o 11 1 -13 31259.81 30667.04 285.02 o 13 1 -13 21568.12 21031.66 230.97 o 15 1 -13 17894.23 17308.42 200.54 o 17 1 -13 19764.86 19247.04 211.70 o 19 1 -13 15506.60 15656.38 199.52 o 21 1 -13 17789.54 18063.35 233.35 o 23 1 -13 17140.56 17183.55 207.91 o 25 1 -13 11600.63 11622.00 181.09 o 27 1 -13 11803.51 11917.30 221.87 o 29 1 -13 10087.45 10351.79 197.95 o 1 3 -13 33625.30 33208.13 315.10 o 3 3 -13 24332.68 24334.72 244.98 o 5 3 -13 23110.45 22790.37 238.21 o 7 3 -13 20278.47 20072.45 230.80 o 9 3 -13 19366.53 19239.72 235.09 o 11 3 -13 23797.23 23277.43 251.65 o 13 3 -13 21847.31 21842.85 233.16 o 15 3 -13 19628.27 19877.81 227.83 o 17 3 -13 19021.40 19056.66 216.67 o 19 3 -13 16210.80 16366.02 210.93 o 21 3 -13 14650.16 14884.31 211.88 o 23 3 -13 12242.34 12185.15 193.70 o 25 3 -13 9546.87 9719.98 202.69 o 27 3 -13 9343.68 9394.12 204.19 o 1 5 -13 18460.61 19102.78 236.16 o 3 5 -13 19869.67 19956.72 246.12 o 5 5 -13 17783.38 18308.71 250.41 o 7 5 -13 18623.98 19042.47 251.50 o 9 5 -13 20726.56 20923.22 268.45 o 11 5 -13 17659.29 17670.66 259.24 o 13 5 -13 14820.89 15097.73 210.33 o 15 5 -13 12847.56 13103.71 195.28 o 17 5 -13 12368.90 12592.42 193.92 o 19 5 -13 13048.21 13089.77 221.06 o 21 5 -13 12952.95 13112.90 244.77 o 23 5 -13 11291.89 11859.54 236.51 o 25 5 -13 8697.56 8841.88 217.13 o 1 7 -13 13779.33 13745.42 267.47 o 3 7 -13 13800.57 14127.38 270.70 o 5 7 -13 10683.06 11123.33 259.77 o 7 7 -13 12928.35 13037.30 279.42 o 9 7 -13 13777.82 14148.34 290.38 o 11 7 -13 11828.02 11897.77 231.31 o 13 7 -13 13043.11 12808.84 229.25 o 15 7 -13 9784.31 9379.04 209.10 o 17 7 -13 7057.95 7299.84 211.39 o 19 7 -13 9132.40 9061.12 203.60 o 1 9 -13 8724.82 9415.15 244.94 o 3 9 -13 9842.05 10244.66 250.52 o 0 0 -12 93958.73 92861.32 1524.36 o 4 0 -12 72698.09 72260.02 757.74 o 8 0 -12 91782.45 89361.36 971.43 o 12 0 -12 101710.09 98702.41 968.84 o 16 0 -12 48321.97 47195.49 533.37 o 20 0 -12 35090.61 34636.93 472.40 o 24 0 -12 39485.28 39297.35 507.50 o 28 0 -12 35789.32 36258.46 599.57 o 32 0 -12 24334.19 24862.45 695.66 o 2 2 -12 91915.63 90721.77 750.02 o 4 2 -12 997.80 1196.76 69.99 o 6 2 -12 70454.08 69065.67 497.60 o 8 2 -12 513.85 623.03 61.91 o 10 2 -12 78648.55 76446.33 578.80 o 12 2 -12 456.79 749.36 67.79 o 14 2 -12 55770.83 54404.75 412.11 o 16 2 -12 763.93 959.14 75.00 o 18 2 -12 47871.41 47000.82 378.93 o 20 2 -12 100.54 215.10 74.97 o 22 2 -12 49132.35 49042.04 407.69 o 24 2 -12 906.94 1135.52 99.48 o 26 2 -12 26945.90 27301.27 296.00 o 28 2 -12 46.91 333.66 115.24 o 30 2 -12 19694.94 20027.18 320.70 o 0 4 -12 98677.56 98040.59 1027.95 o 2 4 -12 195.45 275.96 64.80 o 4 4 -12 61943.68 61864.19 477.75 o 6 4 -12 74.22 143.09 64.14 o 8 4 -12 45560.22 46268.75 404.45 o 10 4 -12 181.37 219.77 62.93 o 12 4 -12 52758.27 52868.78 433.05 o 14 4 -12 167.12 328.53 73.77 o 16 4 -12 46078.70 46000.57 422.75 o 18 4 -12 458.23 540.50 87.54 o 20 4 -12 45344.90 44741.70 436.74 o 22 4 -12 51.86 236.14 113.47 o 24 4 -12 29983.63 29548.23 329.40 o 26 4 -12 137.39 294.88 122.38 o 28 4 -12 16358.63 16502.88 301.84 o 2 6 -12 44337.48 44920.13 503.77 o 4 6 -12 923.12 1121.97 95.83 o 6 6 -12 39407.66 39089.75 405.11 o 8 6 -12 10.09 179.04 81.55 o 10 6 -12 51251.36 51647.55 587.45 o 12 6 -12 588.29 784.06 95.65 o 14 6 -12 37523.40 37223.38 402.49 o 16 6 -12 254.56 440.97 97.55 o 18 6 -12 22991.59 23754.52 321.49 o 20 6 -12 17.10 162.79 108.59 o 22 6 -12 23449.04 23651.17 359.55 o 24 6 -12 116.68 147.23 117.25 o 0 8 -12 26379.86 27245.18 877.15 o 2 8 -12 134.52 81.31 112.57 o 4 8 -12 26519.43 26629.84 404.92 o 6 8 -12 426.77 385.20 102.56 o 8 8 -12 32806.56 32310.40 501.42 o 10 8 -12 3.83 160.44 114.60 o 12 8 -12 28464.81 28012.40 401.09 o 14 8 -12 180.09 310.84 121.24 o 16 8 -12 16419.33 16757.41 283.64 o 1 1 -11 24099.58 24026.74 240.04 o 3 1 -11 43367.63 43402.38 317.42 o 5 1 -11 59461.76 58906.50 413.36 o 7 1 -11 55584.27 54919.88 418.79 o 9 1 -11 46566.55 45757.76 348.48 o 11 1 -11 30252.24 30264.99 246.58 o 13 1 -11 32164.68 31265.89 262.67 o 15 1 -11 36691.68 36028.05 300.17 o 17 1 -11 26454.94 26166.07 247.55 o 19 1 -11 23500.52 23158.80 218.47 o 21 1 -11 17036.64 17210.49 192.71 o 23 1 -11 13923.36 14264.24 185.22 o 25 1 -11 20904.52 20854.93 291.98 o 27 1 -11 18017.79 18268.45 254.06 o 29 1 -11 15764.37 15928.10 254.80 o 31 1 -11 13454.36 13521.78 262.39 o 33 1 -11 7892.05 7862.28 247.47 o 1 3 -11 41340.99 41532.42 315.22 o 3 3 -11 48856.09 48538.82 378.24 o 5 3 -11 41162.67 41720.73 343.45 o 7 3 -11 32652.41 32375.43 265.95 o 9 3 -11 20312.54 20455.83 193.06 o 11 3 -11 16441.65 16735.07 169.69 o 13 3 -11 26304.79 26403.21 224.90 o 15 3 -11 33998.76 34020.52 274.94 o 17 3 -11 34911.66 34926.70 302.89 o 19 3 -11 28107.58 28236.43 267.32 o 21 3 -11 18350.52 18318.39 216.12 o 23 3 -11 15041.56 14791.94 220.48 o 25 3 -11 15066.78 15092.93 237.41 o 27 3 -11 14294.04 14581.69 254.77 o 29 3 -11 10979.13 11491.23 255.31 o 31 3 -11 8394.69 8959.89 233.31 o 1 5 -11 21142.94 21005.71 226.62 o 3 5 -11 30305.84 30549.20 274.33 o 5 5 -11 34093.73 34400.93 296.93 o 7 5 -11 34229.89 34136.03 302.82 o 9 5 -11 22110.40 22089.93 230.67 o 11 5 -11 16656.21 16726.14 211.14 o 13 5 -11 18152.28 18456.11 238.69 o 15 5 -11 20097.08 20302.82 267.94 o 17 5 -11 24348.60 24761.91 295.10 o 19 5 -11 18860.43 19238.38 261.45 o 21 5 -11 15131.75 15399.25 244.63 o 23 5 -11 14212.12 14671.87 243.30 o 25 5 -11 10681.62 10867.84 249.89 o 27 5 -11 10858.43 11470.10 259.49 o 29 5 -11 8733.24 8888.13 285.94 o 1 7 -11 12773.29 12673.47 211.27 o 3 7 -11 14807.58 14914.79 224.61 o 5 7 -11 22244.35 21659.87 285.56 o 7 7 -11 21833.85 21870.39 278.49 o 9 7 -11 17607.39 18422.36 274.72 o 11 7 -11 18347.69 18588.25 338.24 o 13 7 -11 16169.80 15861.78 254.15 o 15 7 -11 15557.46 16011.87 254.43 o 17 7 -11 13470.92 13740.54 263.17 o 19 7 -11 8253.60 8690.81 233.18 o 21 7 -11 6265.26 6533.16 212.08 o 23 7 -11 7415.09 7949.12 222.61 o 1 9 -11 10678.91 10474.20 207.35 o 3 9 -11 10237.93 10765.74 217.15 o 5 9 -11 14968.72 14874.11 266.41 o 7 9 -11 10933.58 11397.08 288.82 o 9 9 -11 8919.66 8988.00 207.48 o 11 9 -11 8897.05 8802.61 209.90 o 13 9 -11 7242.29 7402.17 209.29 o 2 0 -10 94625.22 94556.85 828.97 o 6 0 -10 85509.69 85397.34 814.44 o 10 0 -10 93485.27 91981.84 858.08 o 14 0 -10 80193.28 77922.22 780.42 o 18 0 -10 49749.03 49663.00 514.32 o 22 0 -10 35885.78 35626.55 465.54 o 26 0 -10 35667.89 36095.22 517.40 o 30 0 -10 32474.22 32424.86 609.56 o 34 0 -10 18457.72 19327.90 916.42 o 0 2 -10 86182.63 85766.83 907.03 o 2 2 -10 221.63 349.48 54.72 o 4 2 -10 86154.57 84924.94 615.27 o 8 2 -10 86014.47 84808.35 591.07 o 10 2 -10 356.12 458.64 48.18 o 12 2 -10 65878.88 65297.89 462.43 o 14 2 -10 154.95 368.92 58.46 o 16 2 -10 52955.92 52060.11 382.43 o 18 2 -10 319.93 487.35 63.40 o 20 2 -10 53614.05 53202.09 420.17 o 22 2 -10 136.29 288.08 83.60 o 24 2 -10 38286.80 37728.00 398.46 o 26 2 -10 474.93 685.35 94.64 o 28 2 -10 24740.69 24752.37 298.64 o 30 2 -10 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4 8 4 49775.67 49096.79 606.16 o 6 8 4 890.79 1225.03 129.48 o 8 8 4 60567.29 59095.41 717.67 o 10 8 4 8.89 361.90 113.73 o 12 8 4 38841.91 38547.54 522.50 o 14 8 4 227.55 363.00 116.50 o 16 8 4 30246.34 30268.92 434.01 o 18 8 4 23.95 -70.05 112.34 o 20 8 4 25992.81 25112.07 545.17 o 22 8 4 492.28 455.75 170.40 o 24 8 4 23420.62 23805.77 537.68 o 26 8 4 427.50 11.14 171.65 o 28 8 4 19907.48 20798.75 459.67 o 2 10 4 34780.39 33761.64 529.43 o 4 10 4 389.18 502.00 147.48 o 6 10 4 22626.77 23036.05 405.20 o 8 10 4 45.05 110.78 138.03 o 10 10 4 15918.36 16242.75 315.15 o 12 10 4 58.18 147.34 154.61 o 14 10 4 23445.11 22931.77 452.97 o 16 10 4 7.79 156.79 177.88 o 18 10 4 23756.78 23767.30 536.06 o 1 1 5 60233.40 60135.25 682.15 o 3 1 5 89846.15 92535.54 1229.29 o 5 1 5 147711.09 151212.17 1751.72 o 7 1 5 140866.97 144354.86 1812.52 o 9 1 5 80260.90 81765.80 937.31 o 11 1 5 70450.91 70695.16 823.83 o 13 1 5 54781.30 55089.00 713.90 o 15 1 5 58849.10 59391.74 639.27 o 17 1 5 58305.84 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1 5 5 35002.11 34564.15 457.37 o 3 5 5 49683.08 49112.69 615.70 o 5 5 5 67688.93 66871.52 839.61 o 7 5 5 62888.39 62929.59 703.23 o 9 5 5 41618.78 41116.96 464.27 o 11 5 5 28053.60 28087.87 343.97 o 13 5 5 31993.60 31540.67 372.06 o 15 5 5 33467.27 33344.38 385.85 o 17 5 5 33512.96 33535.74 433.80 o 19 5 5 33137.47 32635.78 448.03 o 21 5 5 24081.80 24297.54 406.83 o 23 5 5 21053.69 21040.88 371.01 o 25 5 5 18595.59 18132.69 353.92 o 27 5 5 15413.01 15280.66 482.09 o 29 5 5 12522.11 12971.74 327.34 o 31 5 5 10638.66 10299.04 284.18 o 33 5 5 10649.74 10892.57 309.32 o 1 7 5 21589.04 22253.24 460.27 o 3 7 5 31928.54 30962.64 579.78 o 5 7 5 31895.01 31056.97 600.14 o 7 7 5 31864.55 31849.95 606.85 o 9 7 5 30574.97 30198.71 456.90 o 11 7 5 23443.54 23283.93 385.59 o 13 7 5 26035.42 26885.69 503.81 o 15 7 5 25136.60 24993.73 413.62 o 17 7 5 20067.70 20054.44 370.70 o 19 7 5 14992.10 14937.64 420.00 o 21 7 5 10883.92 11472.02 338.08 o 23 7 5 11767.28 11607.57 292.98 o 25 7 5 14639.70 14223.48 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7695.46 325.56 o 4 0 12 71608.77 72051.84 2645.42 o 8 0 12 93881.83 91413.26 2084.61 o 12 0 12 103110.36 100361.02 2995.99 o 16 0 12 45957.10 46007.33 1619.33 o 20 0 12 36921.32 37338.91 1364.67 o 24 0 12 40304.86 39472.69 1108.36 o 28 0 12 34507.56 34287.70 1465.13 o 32 0 12 24982.66 25433.54 1015.75 o 2 2 12 94340.70 96046.20 2340.36 o 4 2 12 1001.19 1025.77 164.70 o 6 2 12 67490.84 65748.65 1828.65 o 8 2 12 512.57 767.76 124.80 o 10 2 12 80573.97 80514.09 1687.60 o 12 2 12 448.81 833.87 299.10 o 14 2 12 56781.24 55402.22 1286.37 o 16 2 12 769.12 725.97 226.34 o 18 2 12 47188.91 46766.81 1176.58 o 20 2 12 105.99 53.66 346.23 o 22 2 12 49686.78 48707.77 1293.81 o 24 2 12 899.09 539.32 222.41 o 26 2 12 26908.75 27468.42 715.69 o 28 2 12 46.58 31.16 219.82 o 30 2 12 20231.67 21404.31 618.78 o 0 4 12 101197.14 103891.20 2590.56 o 2 4 12 192.75 324.79 117.31 o 4 4 12 61114.13 61537.94 1385.61 o 6 4 12 69.66 331.64 218.28 o 8 4 12 45673.90 45328.73 1107.89 o 10 4 12 197.24 76.29 194.94 o 12 4 12 54098.46 53245.78 1274.69 o 14 4 12 167.18 43.15 309.23 o 16 4 12 45109.71 45304.20 1169.14 o 18 4 12 437.26 478.29 244.33 o 20 4 12 46266.96 46695.25 1690.85 o 22 4 12 58.34 286.28 254.54 o 24 4 12 30397.94 29101.54 900.80 o 26 4 12 159.01 285.87 230.39 o 28 4 12 15843.84 15950.30 394.66 o 2 6 12 44696.04 45857.45 790.21 o 4 6 12 926.54 1102.00 190.34 o 6 6 12 39041.93 38953.40 707.18 o 8 6 12 6.11 150.85 143.17 o 10 6 12 52718.15 52720.39 896.08 o 12 6 12 573.60 928.50 162.89 o 14 6 12 36998.01 37584.47 703.03 o 16 6 12 275.18 320.34 157.15 o 18 6 12 22748.20 23293.10 522.77 o 20 6 12 29.55 220.68 242.20 o 22 6 12 24676.53 25617.88 642.12 o 24 6 12 85.39 377.27 171.07 o 0 8 12 28214.82 29231.95 907.64 o 2 8 12 134.05 309.49 171.73 o 4 8 12 25959.33 25271.62 564.41 o 6 8 12 426.88 876.56 189.52 o 8 8 12 32232.24 30826.50 749.42 o 10 8 12 8.55 181.33 205.78 o 12 8 12 29686.88 30456.64 621.97 o 14 8 12 175.40 322.97 223.17 o 16 8 12 16398.83 16275.38 446.34 o 5 1 13 33551.19 33753.93 907.22 o 7 1 13 29212.45 28634.97 858.41 o 9 1 13 26955.32 26590.00 702.00 o 11 1 13 31291.72 30472.50 797.60 o 13 1 13 21085.90 20950.89 1087.89 o 15 1 13 19418.46 19476.49 597.06 o 17 1 13 21502.13 21069.49 651.15 o 19 1 13 15444.79 15161.31 1054.41 o 21 1 13 17693.74 17888.71 537.89 o 23 1 13 16578.11 16624.64 529.35 o 25 1 13 11746.10 12785.64 466.11 o 27 1 13 12761.95 13141.92 476.09 o 29 1 13 10536.77 10126.18 440.48 o 3 3 13 24785.23 25244.56 1109.60 o 7 3 13 22440.69 22393.33 1048.00 o 9 3 13 19694.70 19886.09 597.22 o 11 3 13 23122.54 23481.60 690.70 o 13 3 13 21283.92 21473.37 684.82 o 15 3 13 19874.48 19945.52 658.29 o 17 3 13 20121.29 19384.52 653.77 o 19 3 13 16866.01 16774.36 741.66 o 21 3 13 14744.65 14582.67 591.70 o 23 3 13 12541.92 13323.88 574.21 o 25 3 13 9628.82 9620.97 432.25 o 27 3 13 9785.25 10644.72 454.20 o 1 5 13 18430.78 18755.48 416.09 o 3 5 13 21010.58 20670.69 626.47 o 5 5 13 18357.30 18637.77 596.19 o 7 5 13 19266.03 19170.01 619.00 o 9 5 13 20408.87 19964.94 660.19 o 11 5 13 16914.80 16267.17 604.17 o 13 5 13 15670.96 15540.59 582.12 o 15 5 13 13758.77 13626.60 561.34 o 17 5 13 13580.27 13701.36 563.15 o 19 5 13 13431.92 12601.03 567.32 o 21 5 13 12021.88 12396.46 570.39 o 23 5 13 11112.15 10439.29 641.20 o 25 5 13 8772.23 9646.49 791.48 o 1 7 13 13179.48 13071.77 375.69 o 3 7 13 14446.05 14583.50 398.11 o 5 7 13 11444.53 11931.27 356.88 o 7 7 13 13994.13 14342.32 440.38 o 9 7 13 14056.35 13629.22 391.74 o 11 7 13 11195.48 11650.34 361.45 o 13 7 13 13053.41 12462.92 378.07 o 15 7 13 10135.05 10562.39 351.00 o 17 7 13 7574.09 7981.22 319.26 o 19 7 13 9737.89 9853.39 343.64 o 1 9 13 8427.05 8945.88 345.45 o 3 9 13 10116.76 10363.22 502.38 o 10 0 14 30709.33 31323.78 1145.15 o 14 0 14 42976.76 43554.14 1551.53 o 18 0 14 44606.18 43080.37 1611.06 o 22 0 14 26098.25 25445.89 1155.90 o 26 0 14 24297.10 24325.96 1163.34 o 8 2 14 52002.45 51901.78 1231.28 o 10 2 14 79.40 290.40 198.52 o 12 2 14 34361.80 34247.11 891.56 o 14 2 14 363.98 417.20 215.17 o 16 2 14 41646.38 42208.81 1082.77 o 18 2 14 120.97 55.38 221.90 o 20 2 14 27789.72 28462.04 725.49 o 22 2 14 30.42 125.43 229.71 o 24 2 14 22297.61 22545.44 641.73 o 26 2 14 85.69 -215.94 215.94 o 28 2 14 20813.75 20911.77 738.85 o 4 4 14 361.01 414.67 207.08 o 6 4 14 50238.60 49702.18 1214.17 o 8 4 14 44.87 342.21 204.74 o 10 4 14 35590.45 34848.78 1303.49 o 12 4 14 78.34 36.65 321.63 o 14 4 14 35341.29 35722.48 993.59 o 16 4 14 78.41 483.25 339.41 o 18 4 14 26961.74 26733.74 848.46 o 20 4 14 31.10 80.84 246.33 o 22 4 14 15852.62 16275.95 640.48 o 24 4 14 127.85 -118.30 261.58 o 0 6 14 27255.80 27015.18 790.01 o 2 6 14 88.94 307.54 149.12 o 4 6 14 34496.07 34672.89 774.45 o 6 6 14 130.36 126.98 165.93 o 8 6 14 26444.38 26383.30 812.58 o 10 6 14 114.74 109.43 291.25 o 12 6 14 19937.85 19438.69 812.15 o 14 6 14 19.88 417.26 265.47 o 16 6 14 26518.23 25920.40 851.23 o 18 6 14 148.66 443.97 273.10 o 20 6 14 18722.01 19331.01 1070.32 o 2 8 14 19836.82 19862.71 488.24 o 4 8 14 24.40 230.25 175.25 o 6 8 14 22680.16 23060.10 541.86 o 8 8 14 35.94 490.41 213.10 o 10 8 14 13545.72 13564.79 467.30 o 11 1 15 19946.96 21418.42 627.13 o 13 1 15 22014.48 22453.86 675.71 o 15 1 15 19678.34 19336.66 626.16 o 17 1 15 16060.69 15582.62 604.59 o 19 1 15 20546.79 20297.56 774.32 o 21 1 15 18312.12 18521.21 667.07 o 23 1 15 14426.25 13978.11 646.58 o 25 1 15 12968.48 11964.99 567.84 o 9 3 15 28218.64 27032.03 767.92 o 11 3 15 26360.50 26322.53 763.49 o 13 3 15 23799.71 23644.51 820.83 o 15 3 15 16672.46 16416.53 1396.71 o 17 3 15 10656.28 10344.03 505.93 o 19 3 15 11126.30 10940.25 521.78 o 21 3 15 11114.53 11061.23 541.23 o 23 3 15 11167.26 11957.55 477.33 o 3 5 15 16822.28 17943.57 583.29 o 5 5 15 17191.95 17635.87 615.92 o 7 5 15 16695.60 17019.86 1355.37 o 9 5 15 18380.77 18463.94 648.37 o 11 5 15 19192.83 18588.07 666.63 o 13 5 15 15577.86 15769.82 1044.07 o 15 5 15 11807.83 11577.08 548.33 o 17 5 15 10838.38 11234.41 529.68 o 19 5 15 9789.84 10243.51 529.11 o 21 5 15 11140.12 10770.23 547.50 o 1 7 15 19045.30 19260.98 547.14 o 3 7 15 12731.04 12949.80 516.12 o 5 7 15 11503.64 11324.76 360.95 o 7 7 15 8669.99 8501.63 322.50 o 9 7 15 7802.82 8305.04 432.61 o 11 7 15 10622.53 10581.10 410.13 o 12 0 16 28608.27 29963.24 1168.30 o 16 0 16 30383.07 30050.06 1202.20 o 20 0 16 29151.70 27619.61 1215.43 o 24 0 16 17251.74 17985.05 969.04 o 10 2 16 35742.98 35177.37 927.10 o 12 2 16 405.10 610.50 247.43 o 14 2 16 26437.75 26659.98 785.33 o 16 2 16 297.23 437.84 248.18 o 18 2 16 21974.78 22399.06 723.76 o 20 2 16 62.64 278.67 251.41 o 22 2 16 20657.38 20282.54 750.07 o 8 4 16 32592.86 32810.10 892.69 o 10 4 16 122.60 240.99 233.60 o 12 4 16 29549.64 29960.05 870.98 o 14 4 16 58.42 147.39 237.86 o 16 4 16 17868.23 16585.75 635.48 o 18 4 16 147.42 383.37 289.59 o 20 4 16 15370.18 16166.14 632.27 o 2 6 16 25294.91 24627.13 769.09 o 4 6 16 234.28 394.57 234.68 o 6 6 16 18960.80 19442.45 653.16 o 8 6 16 113.23 -120.20 223.33 o 10 6 16 17369.87 17589.15 654.03 o 12 6 16 46.78 190.05 252.25 o 13 1 17 11805.36 12456.16 512.43 o 15 1 17 13703.30 13955.57 559.66 o 17 1 17 15632.18 15354.92 606.72 o 19 1 17 10076.28 10274.40 517.24 o 21 1 17 8134.94 7936.63 481.27 o 11 3 17 11030.07 11808.27 502.29 o 13 3 17 10424.58 9970.64 500.29 o 15 3 17 11671.68 12718.87 990.95 o 17 3 17 12195.46 13224.77 667.66 o 19 3 17 8707.81 8149.92 496.56 o 5 5 17 13431.12 13688.47 747.86 o 7 5 17 12577.46 12955.90 549.83 o 9 5 17 9729.20 10072.88 500.30 o 11 5 17 7890.20 7091.64 455.59 o 13 5 17 8372.40 8799.38 482.32 o 14 0 18 27402.04 26970.55 1166.23 o 18 0 18 16955.32 16222.27 906.20 o 12 2 18 27369.77 28470.41 813.80 o 14 2 18 168.88 264.60 241.54 o 16 2 18 20265.04 20781.52 714.88 o 10 4 18 20391.09 19612.59 673.51 o 12 4 18 70.05 281.35 276.99 o 13 1 19 10998.93 10897.11 713.55 o