#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:35:19 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181073 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/53/2215316.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215316_Fobs loop_ _publ_author_name 'Grapperhaus, Craig A.' 'O'Toole, Martin G.' 'Mashuta, Mark S.' _publ_section_title ; {3,3'-[Ethane-1,2-diylbis(methylimino)]bis(propane-1-thiolato)}nickel(II) ; _journal_coeditor_code ZL2056 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2281 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.931 _cell_angle_gamma 90.000 _cell_length_a 8.2290 _cell_length_b 13.3037 _cell_length_c 11.6910 _exptl_crystal_F_000 624.00 _reflns_d_resolution_high 0.7552 _cod_data_source_file zl2056Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' data_1 ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 244.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1063.58 -0.96 0.96 o 2 0 0 1296.45 1291.45 22.06 o 3 0 0 1418.07 1446.68 25.07 o 4 0 0 4567.83 4703.31 77.72 o 5 0 0 1428.23 1414.01 25.20 o 6 0 0 567.11 493.10 12.88 o 7 0 0 3717.76 3759.02 80.05 o 8 0 0 288.45 305.69 11.02 o 9 0 0 2314.52 2298.72 43.75 o 10 0 0 284.33 289.97 28.10 o 1 1 0 32138.57 26855.70 4660.24 o 2 1 0 3.92 -0.81 0.81 o 3 1 0 2422.78 2480.02 26.12 o 4 1 0 4.18 5.38 1.35 o 5 1 0 1772.74 1664.25 20.16 o 6 1 0 4988.81 4881.81 58.00 o 7 1 0 7.59 6.66 3.17 o 8 1 0 1155.41 1117.09 18.63 o 9 1 0 1.89 2.12 5.24 o 10 1 0 2434.93 2452.41 33.77 o 1 2 0 4.85 10.83 2.50 o 2 2 0 27.20 17.94 1.20 o 3 2 0 957.73 998.76 10.20 o 4 2 0 6573.21 6671.48 62.65 o 5 2 0 4054.91 4009.61 42.36 o 6 2 0 592.69 535.90 8.98 o 7 2 0 1833.05 1776.08 23.50 o 8 2 0 4.18 8.56 4.20 o 9 2 0 504.97 513.21 16.31 o 10 2 0 22.52 28.52 7.53 o 1 3 0 693.39 701.68 9.81 o 2 3 0 7145.92 7481.02 69.77 o 3 3 0 2087.27 2179.82 21.13 o 4 3 0 2244.91 2321.83 22.70 o 5 3 0 8758.92 9079.66 93.72 o 6 3 0 5343.11 5377.74 63.57 o 7 3 0 47.06 54.26 3.98 o 8 3 0 356.31 365.95 8.72 o 9 3 0 363.04 379.54 10.14 o 10 3 0 54.33 64.56 8.07 o 0 4 0 127.82 127.88 2.64 o 1 4 0 4269.99 4558.21 42.83 o 2 4 0 3416.56 3624.91 34.37 o 3 4 0 3774.15 3843.63 36.61 o 4 4 0 7309.72 7462.21 70.21 o 5 4 0 3576.70 3586.33 38.25 o 6 4 0 2529.57 2507.86 31.26 o 7 4 0 1965.10 1848.77 24.39 o 8 4 0 363.18 347.74 8.69 o 9 4 0 44.49 47.55 6.24 o 10 4 0 79.57 79.09 8.41 o 1 5 0 4747.40 5061.71 49.79 o 2 5 0 1740.14 1719.11 20.80 o 3 5 0 656.05 673.13 7.61 o 4 5 0 2099.91 1967.80 23.72 o 5 5 0 4904.65 4910.23 51.68 o 6 5 0 826.32 816.40 12.30 o 7 5 0 23.05 17.59 3.66 o 8 5 0 1307.20 1275.67 18.95 o 9 5 0 451.76 424.09 11.06 o 10 5 0 104.02 118.56 9.22 o 0 6 0 4626.90 4815.99 81.17 o 1 6 0 1882.95 2162.60 21.00 o 2 6 0 2227.94 2319.02 22.66 o 3 6 0 33.47 30.93 2.45 o 4 6 0 202.59 187.32 3.74 o 5 6 0 119.17 119.12 4.13 o 6 6 0 66.29 65.35 3.72 o 7 6 0 698.80 668.48 11.58 o 8 6 0 4.00 3.49 4.97 o 9 6 0 705.34 667.83 13.77 o 10 6 0 14.26 21.39 12.50 o 1 7 0 3050.51 3112.80 33.29 o 2 7 0 725.01 692.68 9.74 o 3 7 0 1254.60 1174.09 17.43 o 4 7 0 535.66 519.15 6.84 o 5 7 0 85.51 88.67 3.80 o 6 7 0 234.92 222.49 5.61 o 7 7 0 113.02 118.49 6.08 o 8 7 0 1309.36 1302.16 23.31 o 9 7 0 0.59 2.94 7.60 o 0 8 0 513.10 465.66 15.64 o 1 8 0 904.32 882.68 11.24 o 2 8 0 4176.87 4127.46 67.99 o 3 8 0 19.00 24.40 2.47 o 4 8 0 127.93 125.68 4.16 o 5 8 0 62.15 58.30 3.89 o 6 8 0 109.34 98.45 5.18 o 7 8 0 252.13 272.55 9.33 o 8 8 0 2.67 2.80 6.74 o 9 8 0 834.12 822.91 19.02 o 1 9 0 385.22 357.99 11.76 o 2 9 0 112.44 113.38 4.25 o 3 9 0 1059.16 1068.63 15.32 o 4 9 0 0.34 1.79 2.74 o 5 9 0 0.21 1.42 3.38 o 6 9 0 60.54 64.64 5.14 o 7 9 0 1.04 0.40 5.91 o 8 9 0 284.34 287.32 12.56 o 9 9 0 14.82 11.94 11.54 o 0 10 0 2103.83 2012.00 37.26 o 1 10 0 1717.52 1731.18 23.16 o 2 10 0 672.65 669.78 10.98 o 3 10 0 987.18 994.31 16.97 o 4 10 0 57.83 61.21 7.51 o 5 10 0 29.22 39.16 5.01 o 6 10 0 0.02 0.28 5.00 o 7 10 0 34.57 34.81 7.75 o 8 10 0 27.35 19.93 9.65 o 1 11 0 916.70 945.41 24.16 o 2 11 0 0.54 2.20 3.06 o 3 11 0 10.77 12.76 3.61 o 4 11 0 448.24 418.83 9.15 o 5 11 0 510.50 485.79 15.23 o 6 11 0 26.07 34.44 6.60 o 7 11 0 704.41 676.12 88.14 o 8 11 0 69.98 79.33 15.58 o 0 12 0 1846.65 1814.11 42.54 o 1 12 0 716.39 683.46 15.88 o 2 12 0 18.13 19.31 4.07 o 3 12 0 1077.52 1038.16 19.41 o 4 12 0 462.57 436.46 10.10 o 5 12 0 27.10 17.53 5.87 o 6 12 0 236.31 251.58 12.61 o 7 12 0 542.60 560.58 19.56 o 1 13 0 617.54 635.63 14.86 o 2 13 0 147.85 146.46 6.88 o 3 13 0 2.85 0.60 4.61 o 4 13 0 933.18 892.21 18.79 o 5 13 0 559.55 517.16 20.12 o 6 13 0 731.44 717.90 17.87 o 7 13 0 1263.80 1305.71 45.06 o 0 14 0 593.55 623.21 17.79 o 1 14 0 212.95 217.93 9.80 o 2 14 0 111.14 105.62 6.61 o 3 14 0 33.81 39.83 5.97 o 4 14 0 685.04 656.94 19.80 o 5 14 0 118.29 114.16 9.52 o 6 14 0 1.03 -4.94 11.17 o 1 15 0 438.13 414.52 11.42 o 2 15 0 777.15 759.86 14.98 o 3 15 0 151.97 144.01 8.58 o 4 15 0 448.03 454.38 18.39 o 5 15 0 1101.11 1033.69 39.67 o 0 16 0 1534.15 1557.44 35.61 o 1 16 0 552.00 551.37 14.03 o 2 16 0 31.78 36.90 7.77 o 3 16 0 822.85 805.83 19.04 o 4 16 0 719.11 666.64 32.36 o 1 17 0 325.51 341.29 36.79 o 2 17 0 222.13 205.04 32.36 o -10 1 1 20.88 13.25 7.16 o -9 1 1 77.08 77.47 6.35 o -8 1 1 12.56 13.24 4.00 o -7 1 1 1442.71 1446.47 26.17 o -6 1 1 150.56 155.91 5.59 o -5 1 1 265.39 239.84 3.96 o -4 1 1 565.61 551.69 10.61 o -3 1 1 113.88 119.71 2.20 o -2 1 1 359.39 380.37 4.52 o -1 1 1 241.97 210.31 7.11 o 0 1 1 56.12 -0.63 0.63 o 1 1 1 350.85 328.72 3.55 o 2 1 1 4236.21 4581.57 57.35 o 3 1 1 1138.61 1188.70 13.16 o 4 1 1 1636.49 1506.98 16.70 o 5 1 1 6.91 6.49 1.98 o 6 1 1 3.54 6.90 2.57 o 7 1 1 1172.34 1131.62 16.24 o 8 1 1 222.51 220.79 7.09 o 9 1 1 0.42 2.93 5.43 o 10 1 1 0.81 4.75 7.51 o -10 2 1 123.38 133.46 8.52 o -9 2 1 16.55 14.46 5.48 o -8 2 1 1202.48 1211.83 17.87 o -7 2 1 178.61 193.29 5.79 o -6 2 1 1812.16 1727.93 26.78 o -5 2 1 138.20 119.32 3.03 o -4 2 1 124.61 105.79 2.53 o -3 2 1 7014.81 7327.69 68.51 o -2 2 1 343.51 334.19 4.85 o -1 2 1 120.19 111.35 2.04 o 0 2 1 3363.11 3309.25 73.80 o 1 2 1 5112.48 5566.00 51.90 o 2 2 1 523.98 527.70 6.95 o 3 2 1 1994.32 1959.39 19.04 o 4 2 1 595.02 604.02 10.90 o 5 2 1 1339.84 1337.71 15.42 o 6 2 1 773.96 748.31 11.38 o 7 2 1 14.33 14.80 3.34 o 8 2 1 608.96 569.06 10.80 o 9 2 1 88.13 86.87 6.66 o 10 2 1 35.26 37.77 7.87 o -10 3 1 3.56 11.19 7.40 o -9 3 1 385.90 388.38 10.21 o -8 3 1 245.54 245.40 7.47 o -7 3 1 2821.64 2875.41 35.88 o -6 3 1 1.17 3.59 2.57 o -5 3 1 26.74 22.43 2.00 o -4 3 1 5453.42 5785.33 54.63 o -3 3 1 1647.69 1674.50 16.51 o -2 3 1 249.97 240.28 3.17 o -1 3 1 80.61 72.73 1.73 o 0 3 1 31.52 38.96 1.35 o 1 3 1 886.03 971.76 9.62 o 2 3 1 68.53 68.36 1.78 o 3 3 1 1664.47 1670.04 16.48 o 4 3 1 4681.06 4549.41 43.18 o 5 3 1 22.51 32.16 2.44 o 6 3 1 218.30 211.51 7.09 o 7 3 1 1288.13 1260.72 17.82 o 8 3 1 84.68 87.23 5.44 o 9 3 1 26.01 34.10 5.97 o 10 3 1 6.23 6.02 7.73 o -10 4 1 211.43 198.57 10.27 o -9 4 1 316.87 321.77 9.73 o -8 4 1 1.36 -0.48 4.34 o -7 4 1 587.21 582.89 10.93 o -6 4 1 901.09 908.98 13.23 o -5 4 1 32.04 35.02 2.25 o -4 4 1 1328.10 1422.20 14.57 o -3 4 1 5854.53 6210.47 58.40 o -2 4 1 4134.14 4100.97 50.91 o -1 4 1 7966.71 8416.27 157.08 o 0 4 1 61.61 67.51 1.88 o 1 4 1 3085.03 3329.79 38.16 o 2 4 1 5486.81 5936.48 55.69 o 3 4 1 28.47 24.66 1.59 o 4 4 1 247.53 202.20 3.51 o 5 4 1 5428.95 5541.02 58.02 o 6 4 1 20.35 18.53 2.89 o 7 4 1 20.67 16.70 3.76 o 8 4 1 734.63 734.96 16.04 o 9 4 1 1165.43 1177.71 18.76 o 10 4 1 529.09 532.11 14.12 o -10 5 1 350.09 382.43 14.96 o -9 5 1 628.12 630.84 13.14 o -8 5 1 3133.08 3055.45 44.12 o -7 5 1 701.48 702.29 19.96 o -6 5 1 32.19 34.52 3.02 o -5 5 1 248.02 262.08 4.63 o -4 5 1 1307.49 1386.53 21.11 o -3 5 1 5521.90 5837.65 63.05 o -2 5 1 1720.43 1831.67 21.47 o -1 5 1 6578.53 6844.44 134.44 o 0 5 1 1021.23 1084.04 15.29 o 1 5 1 11344.43 12241.62 113.71 o 2 5 1 1547.07 1670.18 16.52 o 3 5 1 3081.73 3065.63 29.61 o 4 5 1 1194.26 1179.04 12.51 o 5 5 1 53.70 54.79 2.90 o 6 5 1 1711.99 1704.22 22.41 o 7 5 1 9.14 9.63 3.56 o 8 5 1 998.76 990.29 16.41 o 9 5 1 2.80 0.39 5.98 o 10 5 1 740.74 746.46 17.02 o -10 6 1 9.77 0.16 12.41 o -9 6 1 1384.44 1380.63 22.61 o -8 6 1 1.82 5.26 4.94 o -7 6 1 2575.28 2513.01 32.07 o -6 6 1 355.86 335.13 6.46 o -5 6 1 55.85 56.52 3.48 o -4 6 1 218.72 235.79 4.16 o -3 6 1 223.21 217.12 5.01 o -2 6 1 11000.08 10752.47 127.11 o -1 6 1 3815.85 4101.86 38.85 o 0 6 1 5780.96 6154.65 55.56 o 1 6 1 48.49 54.01 2.21 o 2 6 1 14502.52 15067.07 187.72 o 3 6 1 57.69 72.91 2.60 o 4 6 1 486.84 432.40 5.89 o 5 6 1 1564.83 1551.64 18.02 o 6 6 1 80.46 74.85 4.32 o 7 6 1 277.51 254.84 7.11 o 8 6 1 11.94 8.42 5.09 o 9 6 1 3975.44 3983.18 50.37 o 10 6 1 462.79 511.69 29.96 o -9 7 1 0.49 -0.25 7.80 o -8 7 1 4720.64 4798.02 62.21 o -7 7 1 583.96 565.45 10.63 o -6 7 1 55.48 55.03 3.72 o -5 7 1 136.57 131.24 4.15 o -4 7 1 655.47 628.65 7.25 o -3 7 1 3657.78 3650.63 35.23 o -2 7 1 9.35 11.68 1.72 o -1 7 1 5791.63 5682.99 53.56 o 0 7 1 923.33 923.97 9.31 o 1 7 1 5873.01 6169.75 64.45 o 2 7 1 73.67 63.21 2.46 o 3 7 1 4726.65 4723.30 45.12 o 4 7 1 2398.85 2301.10 26.55 o 5 7 1 23.84 21.24 2.87 o 6 7 1 86.90 75.71 4.50 o 7 7 1 0.75 1.17 4.90 o 8 7 1 3085.74 2950.48 44.55 o 9 7 1 52.70 53.07 8.78 o -9 8 1 1395.54 1457.39 26.60 o -8 8 1 1046.20 1037.60 24.73 o -7 8 1 1716.95 1703.54 29.79 o -6 8 1 537.42 542.09 11.12 o -5 8 1 120.66 125.43 4.95 o -4 8 1 85.66 93.95 3.92 o -3 8 1 2436.96 2397.91 61.00 o -2 8 1 10336.58 10503.34 108.74 o -1 8 1 0.21 2.04 1.99 o 0 8 1 1406.61 1388.12 15.90 o 1 8 1 703.67 736.31 9.44 o 2 8 1 1642.15 1532.39 37.15 o 3 8 1 1489.84 1482.29 17.33 o 4 8 1 2609.37 2574.48 28.62 o 5 8 1 1714.52 1792.19 23.73 o 6 8 1 2.45 5.18 4.00 o 7 8 1 145.25 144.84 7.88 o 8 8 1 167.78 159.73 9.71 o 9 8 1 2413.86 2410.98 71.95 o -9 9 1 125.57 159.98 20.73 o -8 9 1 1632.66 1642.22 58.89 o -7 9 1 2553.26 2449.64 41.72 o -6 9 1 297.12 284.15 7.96 o -5 9 1 874.91 920.30 16.72 o -4 9 1 1832.28 1815.92 47.25 o -3 9 1 7549.72 7650.61 104.95 o -2 9 1 2492.43 2365.08 70.90 o -1 9 1 1797.93 1755.41 30.63 o 0 9 1 468.85 411.70 7.47 o 1 9 1 176.61 155.53 4.57 o 2 9 1 624.59 620.03 13.63 o 3 9 1 4596.72 4628.26 67.38 o 4 9 1 9478.85 9840.43 102.81 o 5 9 1 729.83 696.43 11.62 o 6 9 1 237.97 260.45 8.00 o 7 9 1 1132.45 1136.10 20.61 o 8 9 1 1605.34 1535.38 26.85 o 9 9 1 31.97 27.18 12.26 o -8 10 1 486.11 465.93 17.22 o -7 10 1 945.48 937.21 40.44 o -6 10 1 2934.27 2999.65 51.14 o -5 10 1 802.26 792.50 15.54 o -4 10 1 3864.99 3938.20 48.92 o -3 10 1 3291.47 3208.56 88.65 o -2 10 1 4246.80 4245.76 52.14 o -1 10 1 39.74 39.71 3.25 o 0 10 1 290.53 262.56 10.31 o 1 10 1 92.51 88.34 4.21 o 2 10 1 1185.37 1203.10 35.89 o 3 10 1 5852.83 5772.85 78.75 o 4 10 1 2729.76 2770.84 43.29 o 5 10 1 3581.67 3640.18 97.30 o 6 10 1 1260.27 1234.65 43.50 o 7 10 1 1061.55 1021.04 24.95 o 8 10 1 405.57 395.38 16.48 o -8 11 1 626.21 618.52 21.96 o -7 11 1 612.51 598.08 31.28 o -6 11 1 1449.30 1403.76 24.67 o -5 11 1 2077.63 2057.22 32.70 o -4 11 1 481.86 516.45 10.16 o -3 11 1 2933.55 2859.08 65.38 o -2 11 1 1538.58 1443.10 21.12 o -1 11 1 752.97 769.56 20.03 o 0 11 1 376.41 363.81 9.27 o 1 11 1 1527.64 1519.77 21.04 o 2 11 1 457.88 465.22 8.94 o 3 11 1 1146.93 1123.21 16.81 o 4 11 1 2213.39 2162.35 33.87 o 5 11 1 1415.52 1321.28 28.36 o 6 11 1 2270.97 2301.93 36.89 o 7 11 1 244.66 252.07 20.07 o 8 11 1 254.21 267.11 22.89 o -7 12 1 964.28 955.65 20.95 o -6 12 1 172.80 176.99 9.94 o -5 12 1 479.74 466.50 15.17 o -4 12 1 1252.39 1203.72 18.42 o -3 12 1 417.02 391.29 8.98 o -2 12 1 1218.47 1180.41 17.69 o -1 12 1 534.78 488.11 9.83 o 0 12 1 2366.35 2398.37 34.11 o 1 12 1 43.30 41.53 4.23 o 2 12 1 2540.90 2536.31 37.19 o 3 12 1 587.67 595.68 11.46 o 4 12 1 514.40 503.51 15.38 o 5 12 1 408.53 382.64 11.43 o 6 12 1 92.07 94.34 8.12 o 7 12 1 657.31 658.76 21.61 o -7 13 1 13.36 3.36 15.22 o -6 13 1 765.56 755.65 26.18 o -5 13 1 93.26 104.29 8.39 o -4 13 1 12.81 12.93 5.41 o -3 13 1 1089.01 1025.71 16.70 o -2 13 1 6.48 8.69 4.38 o -1 13 1 3572.71 3521.69 63.01 o 0 13 1 553.70 527.78 10.89 o 1 13 1 4556.55 4437.06 55.56 o 2 13 1 3.95 2.50 4.58 o 3 13 1 1319.61 1290.77 22.75 o 4 13 1 47.51 51.63 6.57 o 5 13 1 35.30 30.02 7.36 o 6 13 1 460.95 444.42 14.43 o -6 14 1 2.38 10.37 11.43 o -5 14 1 59.20 56.29 8.67 o -4 14 1 725.13 727.38 14.73 o -3 14 1 114.46 106.76 7.00 o -2 14 1 1384.29 1384.18 32.67 o -1 14 1 12.93 17.82 5.24 o 0 14 1 6302.64 6071.16 88.82 o 1 14 1 320.29 319.83 9.34 o 2 14 1 1748.40 1747.32 52.03 o 3 14 1 2.88 1.90 5.32 o 4 14 1 148.15 159.10 9.66 o 5 14 1 97.25 101.45 9.23 o 6 14 1 102.24 123.79 22.77 o -5 15 1 849.02 877.64 25.98 o -4 15 1 14.99 25.24 8.32 o -3 15 1 266.09 263.24 11.90 o -2 15 1 3.43 2.94 6.14 o -1 15 1 1740.39 1727.46 28.85 o 0 15 1 9.96 16.03 6.25 o 1 15 1 1981.86 1903.72 35.80 o 2 15 1 246.72 220.89 9.36 o 3 15 1 103.45 116.72 8.07 o 4 15 1 78.29 71.43 8.91 o 5 15 1 121.98 126.78 21.33 o -4 16 1 1129.29 1121.53 41.10 o -3 16 1 5.19 8.01 8.65 o -2 16 1 14.80 12.25 7.78 o -1 16 1 653.07 623.84 14.75 o 0 16 1 717.17 702.25 19.18 o 1 16 1 423.96 436.57 16.67 o 2 16 1 101.86 114.38 8.60 o 3 16 1 31.00 24.32 8.85 o -1 17 1 2.26 -9.11 16.54 o 0 17 1 21.45 13.30 17.14 o 1 17 1 189.26 191.38 29.24 o 2 17 1 456.85 441.35 35.83 o -10 0 2 383.19 389.46 23.97 o -9 0 2 3783.70 3903.17 69.11 o -8 0 2 500.60 497.47 14.10 o -7 0 2 385.34 376.53 13.42 o -6 0 2 104.30 116.72 5.80 o -5 0 2 2015.99 1942.71 27.49 o -4 0 2 8081.95 8031.29 106.28 o -3 0 2 1190.14 1051.24 18.06 o -2 0 2 4367.39 4532.90 124.30 o -1 0 2 1235.26 1233.93 17.02 o 0 0 2 31661.20 31173.90 413.96 o 1 0 2 16420.61 17100.03 226.92 o 2 0 2 28091.74 28273.26 375.13 o 3 0 2 1584.06 1648.90 28.56 o 4 0 2 8.71 16.18 4.43 o 5 0 2 14.92 16.49 3.33 o 6 0 2 506.33 498.54 12.18 o 7 0 2 8802.99 8815.78 146.04 o 8 0 2 761.05 768.32 18.80 o 9 0 2 680.70 699.55 20.19 o 10 0 2 104.75 103.74 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