#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/53/2215323.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215323_Fobs loop_ _publ_author_name 'Diao, Yun-Peng' 'Huang, Shan-Shan' 'Zhang, Bao-Jing' 'Li, Kun' _publ_section_title ; Azido{1-[(2-diethylaminoethylimino-\k^2^N,N')methyl]naphthalen-2-olato-\kO}nickel(II) ; _journal_coeditor_code AT2384 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2495 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.2200 _cell_length_b 13.8730 _cell_length_c 33.6300 _exptl_crystal_F_000 1552.00 _reflns_d_resolution_high 0.7507 _[local]_cod_data_source_file at2384Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 402.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 1059.70 1159.96 62.34 o 4 1 0 13166.21 13174.70 258.06 o 6 1 0 154.69 82.74 19.06 o 8 1 0 38.41 147.94 44.25 o 0 2 0 150101.67 105779.84 3253.76 o 2 2 0 11361.77 13259.47 359.93 o 4 2 0 35729.77 37991.23 876.22 o 2 3 0 2409.46 2395.57 52.33 o 4 3 0 6948.45 7206.22 148.36 o 6 3 0 0.66 22.95 20.47 o 8 3 0 431.64 411.01 52.92 o 0 4 0 630.16 467.60 21.29 o 2 4 0 1744.89 1716.96 46.22 o 4 4 0 9010.96 8382.88 170.71 o 8 4 0 1234.69 1111.25 101.45 o 2 5 0 176.99 244.15 16.39 o 4 5 0 1521.69 1517.83 49.50 o 6 5 0 0.51 55.26 21.82 o 8 5 0 142.91 82.07 45.34 o 0 6 0 15716.62 13284.49 360.60 o 2 6 0 350.43 347.12 27.41 o 4 6 0 3182.37 2740.24 79.54 o 6 6 0 2085.35 1954.63 78.37 o 8 6 0 245.32 295.03 50.88 o 2 7 0 992.35 1066.62 57.98 o 4 7 0 3282.04 3455.83 92.72 o 6 7 0 71.86 175.13 29.69 o 8 7 0 42.89 41.19 36.60 o 0 8 0 10825.63 11003.58 305.95 o 2 8 0 1519.80 1381.95 45.33 o 4 8 0 3987.00 4117.77 122.66 o 6 8 0 305.82 326.00 46.05 o 8 8 0 19.59 17.82 40.14 o 2 9 0 4650.11 4625.07 160.98 o 4 9 0 376.25 416.54 36.55 o 6 9 0 348.29 370.53 49.91 o 8 9 0 92.02 7.99 51.51 o 0 10 0 4413.59 4839.07 158.89 o 2 10 0 54.73 58.81 17.93 o 4 10 0 172.32 283.15 43.04 o 6 10 0 232.60 143.66 44.09 o 2 11 0 4584.85 4629.42 130.21 o 4 11 0 6.45 15.74 21.21 o 6 11 0 44.00 6.90 31.91 o 0 12 0 26.61 54.28 28.98 o 2 12 0 743.79 662.35 66.59 o 4 12 0 237.07 250.39 42.23 o 6 12 0 344.66 506.82 116.32 o 2 13 0 962.89 858.04 48.61 o 4 13 0 1959.90 1885.15 103.09 o 6 13 0 93.11 80.68 34.68 o 0 14 0 1487.46 1318.66 92.76 o 2 14 0 239.76 305.13 39.28 o 4 14 0 169.29 224.45 47.82 o 2 15 0 875.01 746.08 99.75 o 4 15 0 738.38 608.58 65.41 o 0 16 0 731.81 624.97 73.65 o 2 16 0 48.17 9.86 42.95 o 4 16 0 63.48 20.09 41.00 o 2 17 0 223.98 142.95 65.42 o 0 18 0 27.77 25.97 73.48 o 1 1 1 43924.26 42131.92 552.32 o 2 1 1 162197.58 138610.52 1811.67 o 3 1 1 944.62 1151.22 23.41 o 4 1 1 34.52 29.65 7.24 o 5 1 1 3638.19 3745.40 64.67 o 6 1 1 1849.58 1870.56 41.02 o 7 1 1 23.79 -10.44 16.42 o 8 1 1 208.80 201.64 41.00 o 9 1 1 132.70 127.82 48.43 o 0 2 1 9224.48 9340.17 175.96 o 1 2 1 18945.47 19315.03 279.75 o 2 2 1 38995.54 38081.72 501.79 o 3 2 1 342.37 181.64 9.05 o 4 2 1 306.75 282.48 13.13 o 5 2 1 261.49 213.44 12.97 o 6 2 1 3047.61 2952.86 65.08 o 7 2 1 0.52 39.51 15.34 o 8 2 1 85.00 92.08 24.39 o 9 2 1 0.03 34.57 35.26 o 1 3 1 814.20 552.87 11.67 o 2 3 1 17329.29 17980.46 240.23 o 3 3 1 426.57 391.33 12.48 o 4 3 1 2598.21 2391.29 41.67 o 5 3 1 4193.89 4000.45 65.39 o 6 3 1 5389.80 4823.77 99.39 o 7 3 1 120.20 192.38 21.91 o 8 3 1 119.88 182.87 28.39 o 9 3 1 139.95 106.17 86.75 o 0 4 1 712.24 635.21 18.10 o 1 4 1 624.52 659.27 14.12 o 2 4 1 534.66 591.22 14.79 o 3 4 1 307.55 525.66 14.42 o 4 4 1 307.08 345.89 13.88 o 5 4 1 33.40 11.33 9.66 o 6 4 1 633.02 580.62 30.39 o 7 4 1 0.72 44.97 16.14 o 8 4 1 19.31 39.98 23.56 o 9 4 1 0.08 -4.43 34.61 o 1 5 1 787.79 901.90 17.42 o 2 5 1 1010.14 1117.09 24.69 o 3 5 1 539.84 428.19 14.37 o 4 5 1 1665.52 1689.78 37.60 o 5 5 1 2130.07 2125.71 49.91 o 6 5 1 1874.27 1885.59 53.06 o 7 5 1 130.00 75.91 18.30 o 8 5 1 138.14 132.28 28.13 o 9 5 1 145.87 192.29 57.60 o 0 6 1 162.89 197.70 21.15 o 1 6 1 1536.64 1511.89 26.73 o 2 6 1 1301.68 1316.44 42.51 o 3 6 1 22.53 20.49 7.29 o 4 6 1 212.54 204.21 14.56 o 5 6 1 427.96 385.36 24.41 o 6 6 1 320.63 327.11 25.29 o 7 6 1 125.08 107.89 22.04 o 8 6 1 2.72 25.70 24.51 o 1 7 1 1562.79 1554.64 33.58 o 2 7 1 3758.72 3789.39 66.12 o 3 7 1 573.23 662.51 27.54 o 4 7 1 192.41 226.22 15.89 o 5 7 1 2198.52 2156.36 56.33 o 6 7 1 3.43 -7.10 14.17 o 7 7 1 0.87 19.17 21.31 o 8 7 1 136.83 92.70 29.69 o 0 8 1 1948.18 1690.49 44.28 o 1 8 1 82.53 55.57 7.53 o 2 8 1 108.34 93.15 10.15 o 3 8 1 2561.95 2120.87 44.98 o 4 8 1 98.11 109.47 14.54 o 5 8 1 5.78 7.28 14.04 o 6 8 1 39.14 47.87 19.14 o 7 8 1 417.06 389.82 51.59 o 8 8 1 0.10 23.41 26.69 o 1 9 1 3582.41 3528.68 56.83 o 2 9 1 2688.64 2772.91 56.61 o 3 9 1 2228.96 2312.07 49.21 o 4 9 1 197.55 172.59 18.34 o 5 9 1 55.21 74.62 17.12 o 6 9 1 3.93 -5.47 20.39 o 7 9 1 6.65 1.01 22.62 o 8 9 1 77.05 -10.72 75.98 o 0 10 1 3031.48 3206.08 84.54 o 1 10 1 2255.87 2117.92 44.63 o 2 10 1 3.24 7.63 9.50 o 3 10 1 1639.67 1576.40 40.18 o 4 10 1 338.34 360.52 25.04 o 5 10 1 167.21 195.97 23.93 o 6 10 1 1.58 -20.19 20.19 o 7 10 1 116.74 75.25 27.89 o 1 11 1 881.66 882.25 29.19 o 2 11 1 57.89 92.17 13.68 o 3 11 1 150.94 103.63 15.82 o 4 11 1 294.23 277.93 26.02 o 5 11 1 304.96 346.57 33.99 o 6 11 1 130.19 102.52 26.56 o 7 11 1 3.86 -19.83 27.03 o 0 12 1 1857.13 1829.07 86.32 o 1 12 1 1769.62 1721.12 41.77 o 2 12 1 301.25 302.48 20.07 o 3 12 1 425.85 509.26 29.45 o 4 12 1 450.12 501.44 36.85 o 5 12 1 5.34 -23.40 23.40 o 6 12 1 345.38 352.68 36.82 o 1 13 1 515.57 474.44 27.49 o 2 13 1 3.54 17.36 13.20 o 3 13 1 4.44 5.17 17.13 o 4 13 1 163.11 169.83 27.61 o 5 13 1 699.12 641.78 45.85 o 6 13 1 11.69 50.29 23.55 o 0 14 1 342.26 422.01 40.09 o 1 14 1 105.34 97.25 18.48 o 2 14 1 442.59 419.18 31.41 o 3 14 1 1011.49 940.62 56.01 o 4 14 1 120.90 105.78 26.19 o 5 14 1 6.21 32.54 23.68 o 1 15 1 403.91 507.58 31.62 o 2 15 1 306.56 334.08 34.69 o 3 15 1 17.63 34.87 23.12 o 4 15 1 60.23 83.06 26.61 o 5 15 1 126.47 57.00 38.19 o 0 16 1 56.28 28.75 25.63 o 1 16 1 120.91 78.65 25.49 o 2 16 1 37.61 33.84 27.20 o 3 16 1 391.09 364.71 44.99 o 4 16 1 17.50 19.95 27.14 o 1 17 1 22.10 43.29 24.85 o 2 17 1 161.72 194.57 37.36 o 3 17 1 20.49 2.67 36.04 o 0 18 1 46.75 70.27 45.38 o 1 18 1 48.02 50.37 29.80 o 2 18 1 8.08 -45.94 45.94 o 0 0 2 15818.53 13804.45 518.15 o 1 0 2 43484.28 42214.43 782.83 o 2 0 2 6530.31 6622.84 129.79 o 3 0 2 20145.14 22401.74 424.27 o 4 0 2 7102.46 6652.31 137.63 o 5 0 2 0.13 -0.67 9.72 o 6 0 2 31.20 -7.45 12.79 o 7 0 2 1456.45 1477.21 72.14 o 8 0 2 28.88 -34.53 50.51 o 9 0 2 233.78 131.84 66.20 o 1 1 2 165.21 204.81 6.13 o 2 1 2 329.04 330.82 14.37 o 3 1 2 13.61 -3.50 4.34 o 4 1 2 4602.85 4532.74 69.65 o 5 1 2 20.18 32.40 8.48 o 6 1 2 89.67 122.31 14.16 o 7 1 2 42.51 88.85 21.04 o 8 1 2 50.00 30.58 25.50 o 9 1 2 15.93 6.83 42.43 o 0 2 2 11249.57 10999.98 226.47 o 1 2 2 15556.30 16388.53 238.11 o 2 2 2 2.28 25.56 4.16 o 3 2 2 23703.13 25045.62 334.69 o 4 2 2 2952.92 2868.61 50.76 o 5 2 2 14.78 0.66 7.65 o 6 2 2 181.82 225.02 18.53 o 7 2 2 1820.72 1837.18 55.40 o 8 2 2 148.56 102.52 24.73 o 9 2 2 200.78 166.71 44.59 o 1 3 2 289.40 485.15 10.91 o 2 3 2 687.42 689.71 18.65 o 3 3 2 1581.21 1845.82 31.90 o 4 3 2 5563.59 5715.74 85.39 o 5 3 2 12.47 21.78 8.31 o 6 3 2 103.81 129.10 16.51 o 7 3 2 12.94 -14.33 14.33 o 8 3 2 282.16 296.57 33.10 o 9 3 2 7.04 42.61 55.72 o 0 4 2 6115.14 4907.11 97.63 o 1 4 2 5608.51 5470.70 76.52 o 2 4 2 138.52 106.02 8.23 o 3 4 2 15003.15 14562.76 198.56 o 4 4 2 340.71 448.47 17.17 o 5 4 2 355.03 336.62 19.91 o 6 4 2 338.15 334.55 24.20 o 7 4 2 2043.90 1741.42 63.22 o 8 4 2 546.19 602.07 45.64 o 9 4 2 78.37 71.86 39.57 o 1 5 2 734.37 842.29 16.68 o 2 5 2 359.38 365.14 11.95 o 3 5 2 483.62 472.62 15.91 o 4 5 2 13.80 21.58 8.13 o 5 5 2 1109.33 1016.85 33.93 o 6 5 2 16.01 20.36 14.44 o 7 5 2 29.17 0.29 17.53 o 8 5 2 238.60 232.60 31.91 o 9 5 2 47.47 73.73 47.64 o 0 6 2 96.00 28.10 7.12 o 1 6 2 893.48 784.81 16.91 o 2 6 2 423.42 420.75 13.72 o 3 6 2 5174.59 4707.44 80.09 o 4 6 2 182.80 109.44 12.03 o 5 6 2 70.57 66.12 13.30 o 6 6 2 155.61 171.92 19.70 o 7 6 2 624.24 669.01 39.92 o 8 6 2 1.91 -2.53 24.70 o 1 7 2 1916.21 2122.91 36.02 o 2 7 2 17.35 9.77 5.26 o 3 7 2 246.41 302.45 16.04 o 4 7 2 88.78 76.85 12.99 o 5 7 2 2279.08 2325.67 59.02 o 6 7 2 17.49 59.56 18.86 o 7 7 2 4.92 11.93 19.43 o 8 7 2 94.49 66.40 29.06 o 0 8 2 148.68 131.10 19.16 o 1 8 2 3599.70 3403.34 54.05 o 2 8 2 169.99 156.99 12.15 o 3 8 2 3541.90 3305.95 62.29 o 4 8 2 447.58 529.17 26.67 o 5 8 2 79.23 57.69 18.83 o 6 8 2 0.49 2.02 16.22 o 7 8 2 85.30 127.70 27.82 o 8 8 2 105.92 78.29 34.68 o 1 9 2 6123.49 6204.70 96.72 o 2 9 2 12.63 21.07 9.09 o 3 9 2 61.22 94.66 12.58 o 4 9 2 1008.60 1011.17 40.67 o 5 9 2 1239.39 1097.03 47.03 o 6 9 2 47.26 38.56 19.73 o 7 9 2 7.67 -7.76 22.82 o 8 9 2 45.37 48.03 37.05 o 0 10 2 2467.78 2425.96 61.70 o 1 10 2 4912.87 4925.27 85.44 o 2 10 2 10.13 7.68 9.52 o 3 10 2 2392.70 2358.45 54.34 o 4 10 2 181.40 254.72 21.95 o 5 10 2 59.75 65.44 19.74 o 6 10 2 14.83 11.10 21.44 o 7 10 2 174.89 116.07 29.92 o 1 11 2 8428.67 8129.72 132.71 o 2 11 2 159.43 201.25 17.03 o 3 11 2 1957.93 1912.95 48.88 o 4 11 2 3.61 15.87 16.89 o 5 11 2 726.05 728.40 41.99 o 6 11 2 1.78 -21.35 21.35 o 7 11 2 40.77 11.63 25.30 o 0 12 2 1532.16 1369.59 60.12 o 1 12 2 352.57 331.64 21.31 o 2 12 2 4.72 6.81 11.56 o 3 12 2 1855.69 1896.73 50.50 o 4 12 2 323.95 400.49 33.15 o 5 12 2 2.27 14.55 21.35 o 6 12 2 3.69 19.88 23.76 o 1 13 2 2773.89 2444.41 60.81 o 2 13 2 74.69 70.65 15.78 o 3 13 2 550.15 548.77 35.35 o 4 13 2 271.04 264.57 30.91 o 5 13 2 1128.23 1138.27 59.84 o 6 13 2 8.91 47.84 23.32 o 0 14 2 37.99 -19.27 19.27 o 1 14 2 2.93 19.24 15.37 o 2 14 2 34.23 41.66 18.87 o 3 14 2 861.90 910.12 52.23 o 4 14 2 89.82 69.03 25.20 o 5 14 2 19.65 51.15 25.42 o 1 15 2 422.70 431.50 30.82 o 2 15 2 137.14 148.17 27.48 o 3 15 2 2.01 -13.41 23.74 o 4 15 2 48.52 59.44 25.78 o 5 15 2 736.87 486.75 67.65 o 0 16 2 52.84 77.59 28.32 o 1 16 2 245.31 266.77 39.52 o 2 16 2 3.31 13.16 26.78 o 3 16 2 188.02 155.33 50.11 o 4 16 2 1.06 42.86 30.03 o 1 17 2 310.36 252.37 39.45 o 2 17 2 106.25 110.42 38.24 o 3 17 2 14.36 12.12 32.79 o 0 18 2 0.16 65.58 87.53 o 1 18 2 155.38 217.99 49.76 o 2 18 2 0.19 5.71 51.22 o 1 1 3 15750.43 16399.26 226.59 o 2 1 3 3064.60 2992.75 44.45 o 3 1 3 1220.25 1188.80 23.08 o 4 1 3 698.85 779.62 21.78 o 5 1 3 4787.69 4613.10 76.19 o 6 1 3 515.77 551.70 25.73 o 7 1 3 230.12 298.69 26.17 o 8 1 3 467.88 390.78 46.67 o 9 1 3 67.65 90.31 48.87 o 0 2 3 7163.84 7711.99 146.23 o 1 2 3 77.04 77.04 4.66 o 2 2 3 1993.36 2235.53 36.07 o 3 2 3 6.13 26.60 5.94 o 4 2 3 18.17 53.73 9.15 o 5 2 3 183.92 228.37 15.08 o 6 2 3 503.42 574.42 25.43 o 7 2 3 13.26 49.77 17.39 o 8 2 3 23.84 -21.13 21.13 o 9 2 3 12.65 41.26 37.34 o 1 3 3 13286.09 13842.23 185.02 o 2 3 3 17811.29 17270.18 241.49 o 3 3 3 273.54 230.45 9.79 o 4 3 3 3143.74 3171.39 52.10 o 5 3 3 1876.38 1794.66 35.95 o 6 3 3 23.56 31.40 14.69 o 7 3 3 187.41 225.93 22.77 o 8 3 3 922.65 1087.71 56.55 o 9 3 3 136.18 212.19 48.20 o 0 4 3 437.49 521.98 16.65 o 1 4 3 1927.80 1760.79 28.21 o 2 4 3 1465.56 1385.01 25.82 o 3 4 3 149.33 125.20 7.79 o 4 4 3 878.82 984.57 23.48 o 5 4 3 36.00 42.33 11.19 o 6 4 3 524.99 612.87 29.35 o 7 4 3 0.34 11.64 17.21 o 8 4 3 0.15 13.23 22.75 o 9 4 3 4.92 40.31 37.78 o 1 5 3 647.50 823.28 16.61 o 2 5 3 5626.00 6304.43 94.35 o 3 5 3 20.95 48.00 7.69 o 4 5 3 4473.42 4564.66 79.55 o 5 5 3 886.51 941.33 40.72 o 6 5 3 336.79 408.79 26.99 o 7 5 3 75.59 126.14 23.74 o 8 5 3 491.19 418.22 37.75 o 9 5 3 59.69 70.89 46.73 o 0 6 3 237.97 176.06 14.80 o 1 6 3 237.08 352.94 11.48 o 2 6 3 286.34 301.10 11.95 o 3 6 3 433.04 491.08 27.62 o 4 6 3 264.61 239.29 16.82 o 5 6 3 24.06 14.07 11.62 o 6 6 3 492.31 454.65 31.51 o 7 6 3 145.64 113.34 22.58 o 8 6 3 76.21 69.28 30.16 o 1 7 3 1106.54 949.69 20.45 o 2 7 3 1571.55 1619.80 31.78 o 3 7 3 33.71 19.52 7.91 o 4 7 3 586.48 540.89 25.01 o 5 7 3 612.41 643.50 32.42 o 6 7 3 741.73 713.30 38.87 o 7 7 3 1.28 -11.37 19.08 o 8 7 3 110.76 135.64 30.60 o 0 8 3 664.25 376.63 23.76 o 1 8 3 167.44 244.28 12.63 o 2 8 3 1667.48 1495.20 33.91 o 3 8 3 3651.50 3752.48 72.57 o 4 8 3 48.32 30.84 12.84 o 5 8 3 55.07 45.12 16.63 o 6 8 3 606.50 694.70 40.19 o 7 8 3 284.08 263.36 32.09 o 8 8 3 17.95 91.79 29.50 o 1 9 3 1327.83 1311.97 29.40 o 2 9 3 7696.67 7150.95 117.50 o 3 9 3 1100.20 1058.67 43.77 o 4 9 3 12.02 21.15 12.22 o 5 9 3 15.32 2.32 16.35 o 6 9 3 558.02 517.19 39.08 o 7 9 3 18.79 -21.85 21.85 o 8 9 3 62.31 196.42 46.02 o 0 10 3 4080.50 3836.09 87.83 o 1 10 3 4373.82 4128.56 73.97 o 2 10 3 1956.41 1781.93 55.42 o 3 10 3 2233.91 2274.98 53.42 o 4 10 3 305.75 335.82 27.12 o 5 10 3 231.22 199.26 24.40 o 6 10 3 528.65 427.38 38.31 o 7 10 3 79.23 59.48 26.53 o 8 10 3 0.36 -42.09 44.66 o 1 11 3 536.22 544.36 25.03 o 2 11 3 7919.71 7332.75 123.35 o 3 11 3 7.91 17.16 12.80 o 4 11 3 103.38 156.31 22.40 o 5 11 3 269.44 371.03 31.93 o 6 11 3 327.85 326.13 36.04 o 7 11 3 19.69 56.86 25.11 o 0 12 3 4796.60 4656.31 134.82 o 1 12 3 2798.48 2697.62 59.22 o 2 12 3 1.08 4.03 11.97 o 3 12 3 1100.12 1026.26 49.42 o 4 12 3 787.69 808.17 42.55 o 5 12 3 11.99 4.77 21.08 o 6 12 3 71.37 53.03 24.51 o 1 13 3 358.70 406.59 26.15 o 2 13 3 1281.79 1344.14 45.91 o 3 13 3 172.85 219.26 25.46 o 4 13 3 156.18 124.28 23.73 o 5 13 3 822.91 769.19 60.09 o 6 13 3 240.32 248.31 41.93 o 0 14 3 700.31 629.79 81.39 o 1 14 3 55.40 40.62 15.48 o 2 14 3 27.70 66.37 18.66 o 3 14 3 902.16 862.11 52.87 o 4 14 3 615.59 596.24 44.51 o 5 14 3 2.34 -11.87 21.73 o 1 15 3 285.24 321.82 34.88 o 2 15 3 101.69 127.19 23.86 o 3 15 3 22.45 59.94 21.45 o 4 15 3 0.78 25.32 26.59 o 5 15 3 200.43 326.08 62.83 o 0 16 3 398.32 364.56 51.98 o 1 16 3 25.15 41.94 21.47 o 2 16 3 68.86 78.58 25.80 o 3 16 3 183.78 206.50 37.22 o 4 16 3 267.49 290.09 39.64 o 1 17 3 101.76 154.47 28.72 o 2 17 3 79.59 91.49 31.33 o 3 17 3 89.45 97.01 37.64 o 0 18 3 687.27 654.47 90.46 o 1 18 3 85.01 89.48 75.23 o 2 18 3 68.69 152.24 57.50 o 0 0 4 37102.38 37475.26 982.64 o 1 0 4 10511.03 10317.43 212.52 o 2 0 4 2534.53 2291.60 49.94 o 3 0 4 2081.77 1395.11 36.64 o 4 0 4 7343.42 6636.72 137.50 o 5 0 4 62.57 50.74 13.10 o 6 0 4 1900.77 1944.80 63.45 o 7 0 4 4.06 -18.11 18.57 o 8 0 4 102.69 -3.45 35.84 o 9 0 4 0.05 49.80 49.80 o 1 1 4 1770.96 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13 27 3.06 -4.48 28.50 o 2 13 27 396.72 454.81 53.75 o 3 13 27 61.76 77.17 35.85 o 2 14 27 53.06 47.23 76.76 o 0 0 28 1997.44 1900.79 99.87 o 1 0 28 3037.73 2908.68 115.36 o 2 0 28 611.50 630.66 44.25 o 3 0 28 3459.94 2827.78 97.00 o 4 0 28 20.95 38.38 22.99 o 5 0 28 56.03 33.36 27.91 o 6 0 28 340.54 303.06 52.38 o 7 0 28 165.78 212.44 56.00 o 1 1 28 0.44 33.36 13.04 o 2 1 28 45.39 85.33 15.77 o 3 1 28 93.00 98.34 17.73 o 4 1 28 10.92 38.59 16.90 o 5 1 28 22.08 20.56 17.73 o 6 1 28 0.26 -0.65 21.24 o 7 1 28 32.92 59.70 38.23 o 0 2 28 7.09 5.44 14.83 o 1 2 28 1972.42 1860.03 51.45 o 2 2 28 230.32 203.75 20.06 o 3 2 28 1770.65 1597.94 50.61 o 4 2 28 49.89 23.54 16.81 o 5 2 28 45.12 25.87 19.58 o 6 2 28 133.69 91.62 26.32 o 7 2 28 239.55 230.81 70.38 o 1 3 28 64.60 94.06 14.53 o 2 3 28 484.04 444.76 27.00 o 3 3 28 320.89 364.63 26.48 o 4 3 28 17.37 45.18 17.34 o 5 3 28 86.62 108.56 23.74 o 6 3 28 1.35 -2.91 23.27 o 7 3 28 17.42 -8.47 39.86 o 0 4 28 65.19 22.03 19.83 o 1 4 28 874.44 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