#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/53/2215343.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215343_Fobs loop_ _publ_author_name 'Xia, Hai-Tao' 'Liu, Yu-Fen' 'Wang, Da-Qi' 'Yang, Shu-Ping' _publ_section_title ; Hexakis(\m-naphthalene-1-acetato)bis[(1,10-phenanthroline)terbium(III)] N,N-dimethylformamide disolvate ; _journal_coeditor_code AT2407 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2624 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.584 _cell_angle_gamma 90.000 _cell_length_a 13.4619 _cell_length_b 15.0860 _cell_length_c 22.1656 _exptl_crystal_F_000 1960.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file at2407Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070531h in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 427.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 38851.83 44675.09 678.66 o 2 0 0 15.97 58.15 44.46 o 3 0 0 44063.37 49281.46 837.52 o 4 0 0 35807.39 42884.07 468.84 o 5 0 0 103623.93 119816.31 1044.75 o 6 0 0 23121.63 27236.00 471.43 o 7 0 0 5475.32 6670.85 278.02 o 9 0 0 18208.00 22920.58 583.68 o 10 0 0 875.40 1060.29 271.12 o 11 0 0 48.73 184.77 303.93 o 12 0 0 10524.68 13239.82 623.40 o 14 0 0 2667.18 3540.06 473.16 o 15 0 0 2.21 86.34 357.46 o 4 1 0 12915.66 15966.41 481.07 o 5 1 0 2345.53 2358.99 96.92 o 6 1 0 9705.05 10417.20 171.03 o 7 1 0 10375.21 13462.54 402.54 o 8 1 0 406.09 607.02 152.41 o 9 1 0 425.45 512.52 154.97 o 10 1 0 65.50 -12.88 160.29 o 11 1 0 6964.15 8613.19 340.70 o 12 1 0 1678.43 1964.90 266.24 o 13 1 0 10.33 206.51 199.96 o 14 1 0 221.83 -136.35 213.66 o 15 1 0 488.41 152.34 244.78 o 2 2 0 171.68 189.00 93.69 o 3 2 0 569.17 484.58 86.34 o 5 2 0 4121.65 4864.56 253.85 o 6 2 0 41.99 80.11 76.68 o 7 2 0 1741.37 2184.03 117.81 o 8 2 0 6673.85 8163.37 776.72 o 10 2 0 207.90 180.83 167.24 o 11 2 0 1372.10 1779.51 223.94 o 12 2 0 4060.91 4568.35 538.78 o 13 2 0 4896.75 5332.98 318.00 o 14 2 0 476.28 408.77 265.94 o 15 2 0 23.06 0.12 245.62 o 8 3 0 1722.86 1855.58 190.30 o 9 3 0 5786.19 7160.70 366.46 o 10 3 0 12175.28 15943.82 448.12 o 11 3 0 12737.67 16506.72 420.26 o 12 3 0 7339.92 8908.89 359.65 o 13 3 0 78.57 199.97 217.74 o 14 3 0 3288.84 3652.37 301.42 o 15 3 0 4411.71 4710.25 377.59 o 0 4 0 7827.91 9270.94 548.13 o 1 4 0 873.76 759.09 117.13 o 3 4 0 2743.02 2499.45 238.93 o 4 4 0 1659.02 1591.44 247.80 o 5 4 0 793.63 837.93 98.32 o 6 4 0 450.40 327.19 92.56 o 7 4 0 2139.09 2173.23 604.40 o 8 4 0 523.20 447.36 103.16 o 9 4 0 5.71 -78.99 105.56 o 10 4 0 31.85 -18.41 130.98 o 11 4 0 15.90 -178.00 181.43 o 12 4 0 959.28 1316.78 223.92 o 13 4 0 9.66 0.62 205.38 o 14 4 0 35.18 2.18 268.53 o 15 4 0 51.04 143.33 352.28 o 3 5 0 23662.58 22432.31 625.60 o 4 5 0 36.34 34.69 132.35 o 8 5 0 1678.65 1771.76 303.93 o 9 5 0 1606.40 1579.09 132.29 o 10 5 0 6917.65 8305.63 233.89 o 11 5 0 2287.26 2903.36 187.10 o 12 5 0 5136.04 5238.08 508.56 o 13 5 0 2.35 18.13 180.72 o 14 5 0 1444.62 1270.97 336.74 o 2 6 0 3574.12 2975.37 153.43 o 5 6 0 15752.34 14944.71 509.30 o 6 6 0 2894.43 2794.52 445.39 o 7 6 0 254.18 170.28 103.79 o 10 6 0 1635.25 1693.93 146.59 o 11 6 0 29.72 -174.44 116.29 o 12 6 0 3793.08 4985.44 462.80 o 13 6 0 3525.55 3622.95 404.08 o 14 6 0 1244.04 1010.21 385.09 o 1 7 0 31.15 70.22 63.36 o 2 7 0 187.53 -24.67 63.50 o 3 7 0 1228.51 1250.72 78.20 o 4 7 0 95.44 136.76 63.89 o 5 7 0 328.19 290.76 94.22 o 6 7 0 1975.59 1828.87 110.86 o 7 7 0 0.69 -61.26 101.16 o 8 7 0 355.33 535.94 161.44 o 9 7 0 3.99 9.26 202.85 o 10 7 0 389.93 297.43 118.68 o 11 7 0 158.22 242.56 211.07 o 12 7 0 116.81 299.32 337.60 o 13 7 0 3.10 342.59 346.24 o 14 7 0 138.16 119.10 644.12 o 1 8 0 11778.93 13306.31 617.69 o 2 8 0 171.24 9.62 66.61 o 4 8 0 17844.32 15700.23 363.61 o 5 8 0 12052.16 11164.00 441.20 o 6 8 0 2103.27 1959.91 118.98 o 7 8 0 5052.85 4437.48 408.12 o 8 8 0 14278.84 14576.60 1353.72 o 10 8 0 1586.51 2006.17 482.66 o 11 8 0 414.48 544.74 416.17 o 12 8 0 3924.77 4637.99 364.21 o 13 8 0 3830.56 4870.37 835.80 o 1 9 0 5261.71 5676.04 350.63 o 2 9 0 7973.57 8379.71 635.84 o 4 9 0 7.56 -97.28 64.85 o 5 9 0 1711.46 1544.53 122.63 o 6 9 0 5356.67 5004.50 178.39 o 7 9 0 4603.48 3705.01 259.88 o 8 9 0 3180.37 3108.54 441.21 o 9 9 0 98.14 -35.05 280.61 o 10 9 0 4804.30 5162.70 442.08 o 11 9 0 3350.23 3825.04 406.67 o 12 9 0 1391.15 1522.85 298.81 o 13 9 0 3.38 -119.21 268.73 o 0 10 0 4340.70 4769.80 167.03 o 1 10 0 1824.43 1621.37 119.29 o 2 10 0 196.08 418.72 115.45 o 3 10 0 723.04 666.70 85.63 o 4 10 0 408.10 231.02 78.11 o 5 10 0 1113.38 1180.18 127.52 o 6 10 0 641.68 650.26 130.67 o 7 10 0 249.93 139.39 147.46 o 8 10 0 358.59 197.82 181.69 o 9 10 0 979.57 1416.02 312.56 o 10 10 0 264.13 141.60 286.66 o 11 10 0 46.95 -448.98 316.02 o 12 10 0 355.37 -278.02 328.10 o 1 11 0 4372.31 4247.31 192.45 o 2 11 0 11703.72 12421.72 461.49 o 3 11 0 10550.91 10370.87 535.64 o 4 11 0 943.79 863.89 120.66 o 5 11 0 2812.24 2649.60 174.50 o 6 11 0 11715.69 12829.23 690.00 o 7 11 0 6643.19 5877.21 284.93 o 8 11 0 922.21 428.65 151.32 o 9 11 0 749.96 1026.80 457.62 o 10 11 0 4028.89 3911.41 252.12 o 11 11 0 4444.02 3767.21 243.96 o 12 11 0 1341.42 697.65 379.91 o 0 12 0 7014.27 7084.64 334.15 o 1 12 0 2586.92 2303.84 170.41 o 2 12 0 119.39 58.19 162.01 o 3 12 0 957.28 857.71 226.59 o 4 12 0 3209.24 3136.79 230.57 o 5 12 0 2343.78 2573.84 293.66 o 6 12 0 160.98 164.36 153.12 o 7 12 0 34.67 -216.39 198.59 o 8 12 0 477.87 337.89 176.88 o 9 12 0 1171.43 818.01 287.52 o 10 12 0 116.40 -191.53 163.20 o 11 12 0 1.76 111.36 318.61 o 1 13 0 994.21 760.91 158.71 o 2 13 0 3859.74 4050.93 312.53 o 3 13 0 2366.30 2384.88 264.55 o 4 13 0 91.63 -153.84 276.30 o 5 13 0 552.28 369.87 148.69 o 6 13 0 1425.87 1217.98 308.25 o 7 13 0 631.34 190.32 143.25 o 8 13 0 11.26 73.08 145.43 o 9 13 0 561.50 749.42 492.15 o 10 13 0 362.14 234.66 280.61 o 0 14 0 7850.41 7898.65 445.53 o 1 14 0 3140.34 4002.56 235.50 o 2 14 0 398.85 136.29 147.59 o 3 14 0 1003.84 586.74 174.91 o 4 14 0 4746.44 4708.52 244.67 o 5 14 0 3510.60 3269.27 230.71 o 6 14 0 614.64 325.30 169.98 o 7 14 0 182.09 -41.75 191.23 o 8 14 0 2523.26 2163.19 373.00 o 9 14 0 3200.00 2751.58 258.06 o 1 15 0 308.21 494.62 210.61 o 2 15 0 226.40 -56.01 160.68 o 3 15 0 44.55 -261.38 174.25 o 4 15 0 15.77 -68.66 178.11 o 5 15 0 276.83 171.23 212.00 o 6 15 0 399.71 45.42 290.49 o 7 15 0 428.59 248.18 156.82 o 8 15 0 481.64 528.42 245.21 o 0 16 0 2467.82 3013.37 397.18 o 1 16 0 1388.68 1430.60 226.61 o 2 16 0 32.37 24.76 172.59 o 3 16 0 197.62 92.16 194.98 o 4 16 0 1110.31 1110.23 201.31 o 5 16 0 1084.45 1001.02 206.47 o 6 16 0 89.39 -116.20 179.21 o 7 16 0 184.39 126.73 225.33 o 1 17 0 1183.19 1333.68 250.93 o 2 17 0 1664.93 2279.55 486.11 o 3 17 0 1321.55 1770.46 254.38 o 4 17 0 29.80 -250.81 204.77 o -15 1 1 174.88 -334.21 222.81 o -14 1 1 983.37 452.84 258.32 o -13 1 1 5357.86 5333.93 527.56 o -11 1 1 14.09 173.88 195.14 o -10 1 1 506.24 475.81 162.39 o -8 1 1 15715.29 18207.56 263.86 o -7 1 1 4275.66 4510.65 135.96 o -6 1 1 12582.26 12913.46 734.28 o -5 1 1 21109.43 26130.04 261.49 o -2 1 1 24.39 38.76 30.87 o 3 1 1 1312.92 1375.54 176.47 o 7 1 1 1671.20 1810.70 385.09 o 10 1 1 815.50 988.14 188.73 o 11 1 1 300.92 556.97 189.08 o 12 1 1 7020.07 7982.87 924.73 o 13 1 1 7825.41 7974.68 367.24 o 14 1 1 2415.73 2724.36 308.30 o 15 1 1 113.80 -75.98 262.53 o -15 2 1 1892.66 2380.00 296.60 o -14 2 1 1662.71 1653.39 253.00 o -13 2 1 167.89 166.78 208.71 o -12 2 1 4552.65 5148.75 573.32 o -10 2 1 3642.40 4695.91 712.33 o -9 2 1 3934.35 4320.76 198.26 o -8 2 1 1531.77 1824.96 120.12 o -3 2 1 1827.80 1800.18 125.55 o -1 2 1 2072.13 2225.74 149.18 o 4 2 1 6274.67 6999.49 527.22 o 5 2 1 5046.99 6110.09 393.30 o 8 2 1 6008.91 7538.13 1023.16 o 9 2 1 538.17 771.70 167.34 o 10 2 1 8424.04 9253.58 436.03 o 11 2 1 13849.76 16524.18 1327.95 o 12 2 1 4056.87 4836.58 678.66 o 13 2 1 8.91 -101.29 225.27 o 14 2 1 1910.48 2111.10 562.09 o 15 2 1 2898.85 3451.75 361.38 o -15 3 1 49.00 -26.81 209.20 o -14 3 1 8.27 -155.08 207.02 o -13 3 1 1081.63 1275.83 217.34 o -12 3 1 40.54 106.28 198.32 o -11 3 1 1010.55 941.61 216.72 o -10 3 1 178.66 392.04 129.69 o -9 3 1 125.69 196.38 105.13 o -8 3 1 1056.66 1038.13 101.51 o -7 3 1 78.93 17.45 99.09 o -6 3 1 505.96 433.26 95.14 o -5 3 1 1554.90 1438.52 97.09 o -4 3 1 574.67 315.86 126.96 o -3 3 1 1004.73 1156.61 102.19 o -1 3 1 975.82 1306.72 86.44 o 0 3 1 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